CN102775884A - Solvent-free colored floor coating - Google Patents
Solvent-free colored floor coating Download PDFInfo
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- CN102775884A CN102775884A CN2012103027948A CN201210302794A CN102775884A CN 102775884 A CN102775884 A CN 102775884A CN 2012103027948 A CN2012103027948 A CN 2012103027948A CN 201210302794 A CN201210302794 A CN 201210302794A CN 102775884 A CN102775884 A CN 102775884A
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Abstract
The invention discloses a solvent-free colored floor coating and belongs to the technical field of functional decoration materials. The solvent-free colored floor coating is divided into an A component and a B component; and during the use, the A and B components are mixed evenly. The floor coating prepared by the invention is stable in performance, good in self-flatting effect, beautiful in color, high in film gloss, high in fullness, simple in production process, environmentally-friendly and free of volatile organic compounds, can be applied to different climate areas, not only has excellent ornamental performance, but also does not cause environment pollution. The solvent-free colored floor coating can be applied to parking lots, gyms, workshops, public amenities and the like and is excellent in decoration effect.
Description
Technical field
The invention belongs to functional ornamentation material technology field, particularly relate to a kind of no-solvent type color floor coating.
Technical background
Epoxy flooring coating is also referred to as functional terrace finishing material, and being can be fast, economical and obtain smooth, firmly and one type of material of decorative ground function arranged effectively.Terrace paint is divided into inorganic and organic two big types usually.The mineral-type terrace paint is actually a kind of cement-based mortar class material; The powdery single component surface structures material that is normally mixed by inorganic coagulation material, superplasticizer, economization agent, skimmer, flow agent various additives and fine sand etc. is a kind of of functional building mortar; Organic type of epoxy flooring coating, main application is the epoxy resin terrace paint at present.
Traditional solvent epoxy varnish terrace paint can give off a large amount of organic volatile (VOC) in production, construction, solidification process, cause environmental pollution, and influences the health of human body.In the last few years, corresponding laws and regulations had been worked out to the production of coating in countries in the world, with the quantity discharged of restriction solvent (VOC).
Summary of the invention
The present invention seeks to overcome the problems referred to above and deficiency, provide a kind of manufacture craft simple, not only paint having no volatile substances discharging, and construction and safeguard all color floor coating eaily, and have aesthetic value.
The no-solvent type color floor coating of the present invention's preparation is divided into first component and component B two portions;
The proportioning of first component consists of: the epoxy resin E51 of 80-100 mass parts; The reactive thinner of 8-15 mass parts, the softening agent of 3-10 mass parts, the coupling agent of 3-5 mass parts; 1.5-3.5 the skimmer of mass parts; 0.5-1.0 the flow agent of mass parts, the filler of 120-160 mass parts, the pigment of 5-15 mass parts;
The proportioning of component B consists of: the solidifying agent of 15-30 mass parts, the curing catalyst of 5-14 mass parts.
Described reactive thinner is the low molecular weight epoxy reactive thinner, is specially butylglycidyl ether.
Described softening agent is DOP (DOP).
Described coupling agent is KH560.
Described skimmer is BYK-019.
Described flow agent is BYK-348.
Described filler is a talcum powder.
Described pigment is mineral dye, is specially a kind of in red iron oxide, fluorescent yellow, the chromoxide green.
Described solidifying agent is alicyclic modified amine hardener.
Described curing catalyst is DMP-30.
The preparation method of no-solvent type color floor coating of the present invention is:
(1) proportioning according to above-mentioned first component takes by weighing each component, and 80-100 ℃ of heating in water bath epoxy resin E51 added reactive thinner after 20-40 minute, and temperature 20-30 ℃ of following dispersing and mixing, stirring velocity is 500-1000r/min; Mix the back and add filler; Then stirring velocity is adjusted to 1000-1500r/min; Stir and add softening agent, coupling agent, skimmer, flow agent successively after 5-15 minute, mix fully with 1500-2000r/min high-speed stirring 10-20 minute to mixture; Add pigment at last and stirred 10-15 minute, filter and obtain the first component with the 200-600r/min rotating speed;
(2) proportioning according to component B takes by weighing each component, successively solidifying agent and curing catalyst is joined in the reaction kettle, stirs 15-20 minute with the rotating speed of 500-1500r/min, mixes after-filtration fully and obtains component B;
When (3) using, above-mentioned first component and the component B for preparing mixed, promptly get no-solvent type color floor coating.
The reactive thinner that the present invention uses can reduce the viscosity of coating, can not increase the volatile organic matter of coating again; The filler crystal structure that the present invention uses is to be lamellated, and special oilness is arranged, and also has resistivity against fire, resistance to acid, and opacifying power is good, soft smooth, good physics-chem characteristic such as adsorptive power is strong; The solidifying agent that the present invention uses has good characteristics such as Ginkgo Biloba Leaf Extract, anti-flavescence, anti-albefaction, has the advantage that viscosity is low, curing speed is fast again.
It is simple to the invention provides a kind of production technique, the organic terrace paint of environmental protection non-volatility.The coating products stable performance of the present invention's preparation, effective from levelling, beautiful in colour, coating film gloss is high, and fullness ratio is high.Applicable to the different climate area, not only have good ornamental performance but also can not cause environmental pollution.Be applied to the parking, the gymnasium, factory floor, place of public amusement etc., decorative effect is splendid.
Embodiment
Further specify characteristics of the present invention through instance below, and unrestricted the present invention; Outstanding feature of the present invention never is limited to following instance.
Embodiment 1
1. first component: get the 80g epoxy resin E51 of 100 ℃ of heating in water bath after 25 minutes, the 8g butylglycidyl ether drops in the reactor drum, and 25 ℃ of following dispersing and mixing, stirring velocity are 500r/min; After mixing the 120g talcum powder is added above-mentioned reactor drum, stirring velocity is adjusted into 1000r/min stirred 5 minutes; Add the 3g plasticizer DOP then successively, 3g coupling agent KH560,1.5g skimmer BYK-019; 0.5g flow agent BYK-348; With the stirring velocity high-speed stirring of 1500r/min 10 minutes, add the 5g ferric oxide red colorant at last and stirred 10 minutes with 500r/min, filter and obtain the first component;
2. component B: get the alicyclic modified amine hardener CDA-3080 of 15g, 5g curing catalyst DMP-30 is mixed in the whipping appts, stirs 15 minutes with 500r/min, filters and obtains component B;
3. when using, first component and component B are mixed, promptly get no-solvent type color floor coating.
Embodiment 2
1. first component: get the 95g epoxy resin E51 of 90 ℃ of heating in water bath after 30 minutes, the 10g butylglycidyl ether drops in the reactor drum, 25 ℃ of following dispersing and mixing of temperature, and stirring velocity is 500r/min; After mixing the 140g talcum powder is added above-mentioned reactor drum, stirring velocity is adjusted into 1100r/min stirred 10 minutes; Add the 6g plasticizer DOP then successively, 3.5g coupling agent KH560,2.5g skimmer BYK-019; 0.7g flow agent BYK-348; With the stirring velocity high-speed stirring of 1800r/min 20 minutes, add 7g fluorescent yellow pigment at last and stirred 12 minutes with 500r/min, filter and obtain the first component;
2. component B: get the alicyclic modified amine hardener CDA-3034 of 20g, 8g curing catalyst DMP-30 is mixed in the whipping appts, stirs 15 minutes with 500r/min, filters and obtains component B;
3. when using, first component and component B are mixed, promptly get no-solvent type color floor coating.
Embodiment 3
1. first component: get the 100g epoxy resin E51 of 100 ℃ of heating in water bath after 30 minutes, the 14g butylglycidyl ether drops in the reactor drum, 25 ℃ of following dispersing and mixing of temperature, and stirring velocity is 900r/min; After mixing the 150g talcum powder is added above-mentioned reactor drum, stirring velocity is adjusted into 1200r/min stirred 5 minutes; Add the 8g plasticizer DOP then successively, 3g coupling agent KH560,1.5g skimmer BYK-019; 1.0g flow agent BYK-348; With the stirring velocity high-speed stirring of 2000r/min 15 minutes, add 15g chromoxide green pigment at last and stirred 10 minutes with 500r/min, filter and obtain the first component;
2. component B: get the alicyclic modified amine hardener HY-32 of 25g, 12g curing catalyst DMP-30 is mixed in the whipping appts, stirs 20 minutes with 500r/min, filters and obtains component B;
3. when using, first component and component B are mixed, promptly get no-solvent type color floor coating.
Claims (10)
1. a no-solvent type color floor coating is characterized in that, this terrace paint is divided into first component and component B two portions;
The proportioning of first component consists of: the epoxy resin E51 of 80-100 mass parts; The reactive thinner of 8-15 mass parts, the softening agent of 3-10 mass parts, the coupling agent of 3-5 mass parts; 1.5-3.5 the skimmer of mass parts; 0.5-1.0 the flow agent of mass parts, the filler of 120-160 mass parts, the pigment of 5-15 mass parts;
The proportioning of component B consists of: the solidifying agent of 15-30 mass parts, the curing catalyst of 5-14 mass parts.
2. no-solvent type color floor coating according to claim 1 is characterized in that described reactive thinner is the low molecular weight epoxy reactive thinner, is specially butylglycidyl ether.
3. no-solvent type color floor coating according to claim 1 is characterized in that described softening agent is a DOP.
4. no-solvent type color floor coating according to claim 1 is characterized in that described coupling agent is KH560.
5. no-solvent type color floor coating according to claim 1 is characterized in that described skimmer is BYK-019.
6. no-solvent type color floor coating according to claim 1 is characterized in that described flow agent is BYK-348.
7. no-solvent type color floor coating according to claim 1 is characterized in that described filler is a talcum powder; Described pigment is mineral dye, is specially a kind of in red iron oxide, fluorescent yellow, the chromoxide green.
8. no-solvent type color floor coating according to claim 1 is characterized in that described solidifying agent is alicyclic modified amine hardener.
9. no-solvent type color floor coating according to claim 1 is characterized in that described curing catalyst is DMP-30.
10. according to the preparation method of the arbitrary described no-solvent type color floor coating of claim 1-9, it is characterized in that its concrete preparation process is:
1) proportioning according to first component in the claim 1 takes by weighing each component, and 80-100 ℃ of heating in water bath epoxy resin E51 added reactive thinner after 20-40 minute, and temperature 20-30 ℃ of following dispersing and mixing, stirring velocity is 500-1000r/min; Mix the back and add filler; Then stirring velocity is adjusted to 1000-1500r/min; Stir and add softening agent, coupling agent, skimmer, flow agent successively after 5-15 minute, mix fully with 1500-2000r/min high-speed stirring 10-20 minute to mixture; Add pigment at last and stirred 10-15 minute, filter and obtain the first component with the 200-600r/min rotating speed;
2) proportioning according to component B in the claim 1 takes by weighing each component, successively solidifying agent and curing catalyst is joined in the reaction kettle, stirs 15-20 minute with the rotating speed of 800-1500r/min, mixes after-filtration fully and obtains component B;
When 3) using, the first component and the component B that prepare are mixed, promptly get no-solvent type color floor coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103027948A CN102775884A (en) | 2012-08-22 | 2012-08-22 | Solvent-free colored floor coating |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012103027948A CN102775884A (en) | 2012-08-22 | 2012-08-22 | Solvent-free colored floor coating |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103305091A (en) * | 2013-05-23 | 2013-09-18 | 杭州宝力物资再生利用有限公司 | Epoxy floor coating |
| CN103555145A (en) * | 2013-11-08 | 2014-02-05 | 西北永新涂料有限公司 | Epoxy self-leveling floor coating and preparation method thereof |
| CN104250510A (en) * | 2014-09-30 | 2014-12-31 | 洛阳双瑞防腐工程技术有限公司 | Solvent-free epoxy self-leveling roller coating floor paint and preparation and use method thereof |
| CN104530913A (en) * | 2015-01-08 | 2015-04-22 | 武汉菲凡士建材有限公司 | Environment-friendly solvent-free epoxy ultrathin marking paint and preparing method thereof |
| CN105482618A (en) * | 2015-12-08 | 2016-04-13 | 中国海洋石油总公司 | Aqueous epoxy terrace paint and preparation method thereof |
| CN106398472A (en) * | 2016-09-12 | 2017-02-15 | 华南理工大学 | Nonmetal powder modified solvent-free epoxy floor coating for waste and old printed circuit boards, and preparation method thereof |
| CN108676460A (en) * | 2018-05-03 | 2018-10-19 | 广州挚业化工有限公司 | A kind of brilliant color terrace decorative paint and preparation method thereof |
| CN108929612A (en) * | 2018-05-29 | 2018-12-04 | 富思特新材料科技发展股份有限公司 | A kind of illusion-colour flash of light terrace finishing coat |
| CN114133829A (en) * | 2021-12-21 | 2022-03-04 | 胡庆龙 | Antibacterial waterproof epoxy floor paint and preparation method thereof |
| CN115820083A (en) * | 2022-11-29 | 2023-03-21 | 上海景江化工有限公司 | Solvent-free epoxy self-leveling coating and preparation method thereof |
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| CN101892002A (en) * | 2009-05-19 | 2010-11-24 | 江门市卡托化工有限公司 | Method for preparing epoxy thin coating floor |
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2012
- 2012-08-22 CN CN2012103027948A patent/CN102775884A/en active Pending
Patent Citations (4)
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| CN1394924A (en) * | 2001-07-11 | 2003-02-05 | 深圳市海川实业股份有限公司 | Preparation method of nuisance-free colour epoxy lawn paint |
| WO2008100608A2 (en) * | 2007-02-15 | 2008-08-21 | Dow Global Technologies, Inc | Aqueous coating composition having reduced plate out |
| CN101659828A (en) * | 2008-08-25 | 2010-03-03 | 武汉菲凡士建材有限公司 | High abrasion-resistant environmental protection floor coating and production and construction process thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103305091A (en) * | 2013-05-23 | 2013-09-18 | 杭州宝力物资再生利用有限公司 | Epoxy floor coating |
| CN103555145A (en) * | 2013-11-08 | 2014-02-05 | 西北永新涂料有限公司 | Epoxy self-leveling floor coating and preparation method thereof |
| CN103555145B (en) * | 2013-11-08 | 2016-01-13 | 西北永新涂料有限公司 | A kind of epoxy self-leveling floor coating and preparation method thereof |
| CN104250510B (en) * | 2014-09-30 | 2016-05-11 | 洛阳双瑞防腐工程技术有限公司 | A kind of solvent-free epoxy self-leveling roller coat floor coatings and preparation using method |
| CN104250510A (en) * | 2014-09-30 | 2014-12-31 | 洛阳双瑞防腐工程技术有限公司 | Solvent-free epoxy self-leveling roller coating floor paint and preparation and use method thereof |
| CN104530913A (en) * | 2015-01-08 | 2015-04-22 | 武汉菲凡士建材有限公司 | Environment-friendly solvent-free epoxy ultrathin marking paint and preparing method thereof |
| CN105482618A (en) * | 2015-12-08 | 2016-04-13 | 中国海洋石油总公司 | Aqueous epoxy terrace paint and preparation method thereof |
| CN106398472A (en) * | 2016-09-12 | 2017-02-15 | 华南理工大学 | Nonmetal powder modified solvent-free epoxy floor coating for waste and old printed circuit boards, and preparation method thereof |
| CN108676460A (en) * | 2018-05-03 | 2018-10-19 | 广州挚业化工有限公司 | A kind of brilliant color terrace decorative paint and preparation method thereof |
| CN108676460B (en) * | 2018-05-03 | 2020-06-30 | 广州挚业化工有限公司 | Crystal color floor decorative coating and preparation method thereof |
| CN108929612A (en) * | 2018-05-29 | 2018-12-04 | 富思特新材料科技发展股份有限公司 | A kind of illusion-colour flash of light terrace finishing coat |
| CN114133829A (en) * | 2021-12-21 | 2022-03-04 | 胡庆龙 | Antibacterial waterproof epoxy floor paint and preparation method thereof |
| CN115820083A (en) * | 2022-11-29 | 2023-03-21 | 上海景江化工有限公司 | Solvent-free epoxy self-leveling coating and preparation method thereof |
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Application publication date: 20121114 |