CN104114533B - 制造甲基柠檬腈的新方法 - Google Patents

制造甲基柠檬腈的新方法 Download PDF

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Publication number
CN104114533B
CN104114533B CN201380009517.0A CN201380009517A CN104114533B CN 104114533 B CN104114533 B CN 104114533B CN 201380009517 A CN201380009517 A CN 201380009517A CN 104114533 B CN104114533 B CN 104114533B
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China
Prior art keywords
methyl
compound
ratio
dimethyl
nitrile
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CN201380009517.0A
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Chinese (zh)
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CN104114533A (zh
Inventor
拉斐尔·布玛
沃纳·邦拉蒂
西尔克·多恩
安吉拉·维尔德曼
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DSM IP Assets BV
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DSM IP Assets BV
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0007Aliphatic compounds
    • C11B9/0023Aliphatic compounds containing nitrogen as the only heteroatom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00Preparation of carboxylic acid nitriles
    • C07C253/30Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201380009517.0A 2012-02-15 2013-02-11 制造甲基柠檬腈的新方法 Active CN104114533B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12155593.2 2012-02-15
EP12155593.2A EP2628723B1 (en) 2012-02-15 2012-02-15 Novel process for the manufacture of methyl limonitrile
PCT/EP2013/052685 WO2013120805A1 (en) 2012-02-15 2013-02-11 Novel process for the manufacture of methyl limonitrile

Publications (2)

Publication Number Publication Date
CN104114533A CN104114533A (zh) 2014-10-22
CN104114533B true CN104114533B (zh) 2016-08-24

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ID=47884243

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CN201380009517.0A Active CN104114533B (zh) 2012-02-15 2013-02-11 制造甲基柠檬腈的新方法

Country Status (8)

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US (1) US9340750B2 (enExample)
EP (1) EP2628723B1 (enExample)
JP (1) JP5750748B2 (enExample)
CN (1) CN104114533B (enExample)
ES (1) ES2524405T3 (enExample)
IN (1) IN2014DN06143A (enExample)
MX (1) MX348784B (enExample)
WO (1) WO2013120805A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113999138B (zh) * 2021-11-26 2023-09-19 万华化学集团股份有限公司 一种甲基庚烯酮快速合成柠檬腈的方法
CN113999096B (zh) * 2021-11-29 2023-05-30 万华化学集团股份有限公司 一种缩合加氢合成6-甲基-5-辛烯-2-酮的方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3655722A (en) * 1967-02-02 1972-04-11 Int Flavors & Fragrances Inc 7-methyl-octadienenitriles
US3960923A (en) * 1973-12-03 1976-06-01 Rhodia, Inc. Process for the preparation of α,β-unsaturated nitriles
EP0074253B1 (en) * 1981-09-03 1986-06-18 Unilever Plc Aliphatic nitriles
WO2009013199A2 (de) * 2007-07-26 2009-01-29 Basf Se Verfahren zur herstellung von ethylgeranonitril

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2617154B1 (fr) * 1987-06-29 1990-11-30 Rhone Poulenc Chimie Procede d'obtention d'oxyde cerique et oxyde cerique a nouvelles caracteristiques morphologiques
FR2922888B1 (fr) * 2007-10-29 2010-02-12 Mane Fils V Octane(ene)nitriles substitues,leurs procedes de syntheses et leurs utilisations en parfumerie
EP2814809B1 (en) * 2012-02-15 2017-03-22 DSM IP Assets B.V. Novel process for the manufacture of methyl limonitrile

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3655722A (en) * 1967-02-02 1972-04-11 Int Flavors & Fragrances Inc 7-methyl-octadienenitriles
US3960923A (en) * 1973-12-03 1976-06-01 Rhodia, Inc. Process for the preparation of α,β-unsaturated nitriles
EP0074253B1 (en) * 1981-09-03 1986-06-18 Unilever Plc Aliphatic nitriles
WO2009013199A2 (de) * 2007-07-26 2009-01-29 Basf Se Verfahren zur herstellung von ethylgeranonitril

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Reaction of aliphatic ketones with α-cyano-α,β-unsaturated acid derivatives;Sato, Kikumasa et al;《Bulletin of the Chemical Society of Japan》;19671231;第40卷(第4期);第942-5页 *

Also Published As

Publication number Publication date
WO2013120805A1 (en) 2013-08-22
MX2014009885A (es) 2014-11-13
US9340750B2 (en) 2016-05-17
JP5750748B2 (ja) 2015-07-22
IN2014DN06143A (enExample) 2015-08-21
JP2015506996A (ja) 2015-03-05
EP2628723A1 (en) 2013-08-21
CN104114533A (zh) 2014-10-22
ES2524405T3 (es) 2014-12-09
MX348784B (es) 2017-06-28
US20150031597A1 (en) 2015-01-29
EP2628723B1 (en) 2014-09-10

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