CN104087030A - 一种氟橡胶专用氧化镁及其制备方法 - Google Patents
一种氟橡胶专用氧化镁及其制备方法 Download PDFInfo
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- CN104087030A CN104087030A CN201410317135.0A CN201410317135A CN104087030A CN 104087030 A CN104087030 A CN 104087030A CN 201410317135 A CN201410317135 A CN 201410317135A CN 104087030 A CN104087030 A CN 104087030A
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- Prior art keywords
- magnesium oxide
- viton
- magnesium
- special
- agent
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- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 title claims abstract description 62
- 239000000395 magnesium oxide Substances 0.000 title claims abstract description 40
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 title claims abstract description 39
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 229920001973 fluoroelastomer Polymers 0.000 title abstract description 7
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 30
- 239000011777 magnesium Substances 0.000 claims abstract description 30
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000006087 Silane Coupling Agent Substances 0.000 claims abstract description 14
- 230000000694 effects Effects 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 12
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002253 acid Substances 0.000 claims abstract description 9
- 239000002245 particle Substances 0.000 claims abstract description 9
- 239000011248 coating agent Substances 0.000 claims abstract description 8
- 238000000576 coating method Methods 0.000 claims abstract description 8
- 229910052717 sulfur Inorganic materials 0.000 claims abstract description 8
- 239000011593 sulfur Substances 0.000 claims abstract description 8
- 238000004381 surface treatment Methods 0.000 claims abstract description 3
- 235000012245 magnesium oxide Nutrition 0.000 claims description 35
- 229920002449 FKM Polymers 0.000 claims description 33
- 230000003647 oxidation Effects 0.000 claims description 15
- 238000007254 oxidation reaction Methods 0.000 claims description 15
- 239000003795 chemical substances by application Substances 0.000 claims description 14
- 239000012756 surface treatment agent Substances 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 6
- 238000009775 high-speed stirring Methods 0.000 claims description 6
- -1 magnesium lipid Chemical class 0.000 claims description 6
- 238000012986 modification Methods 0.000 claims description 6
- 230000004048 modification Effects 0.000 claims description 6
- 125000000217 alkyl group Chemical group 0.000 claims description 4
- 239000007822 coupling agent Substances 0.000 claims description 4
- TXDNPSYEJHXKMK-UHFFFAOYSA-N sulfanylsilane Chemical compound S[SiH3] TXDNPSYEJHXKMK-UHFFFAOYSA-N 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 3
- 150000004671 saturated fatty acids Chemical class 0.000 claims description 3
- 239000000344 soap Substances 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 235000021122 unsaturated fatty acids Nutrition 0.000 claims description 3
- UUEWCQRISZBELL-UHFFFAOYSA-N 3-trimethoxysilylpropane-1-thiol Chemical compound CO[Si](OC)(OC)CCCS UUEWCQRISZBELL-UHFFFAOYSA-N 0.000 claims description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 2
- 229910052791 calcium Inorganic materials 0.000 claims description 2
- 239000011575 calcium Substances 0.000 claims description 2
- 239000012535 impurity Substances 0.000 claims description 2
- 238000012216 screening Methods 0.000 claims description 2
- 150000004670 unsaturated fatty acids Chemical class 0.000 claims description 2
- 229920006395 saturated elastomer Polymers 0.000 claims 1
- 229920001971 elastomer Polymers 0.000 abstract description 8
- 239000000463 material Substances 0.000 abstract description 5
- 238000006116 polymerization reaction Methods 0.000 abstract description 2
- 230000002776 aggregation Effects 0.000 abstract 1
- 238000004220 aggregation Methods 0.000 abstract 1
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 238000003889 chemical engineering Methods 0.000 abstract 1
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 1
- 239000000194 fatty acid Substances 0.000 abstract 1
- 229930195729 fatty acid Natural products 0.000 abstract 1
- 150000004665 fatty acids Chemical class 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 230000000704 physical effect Effects 0.000 abstract 1
- 125000003396 thiol group Chemical group [H]S* 0.000 abstract 1
- 239000000370 acceptor Substances 0.000 description 6
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 4
- 239000000292 calcium oxide Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000004513 sizing Methods 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
- 241001441571 Hiodontidae Species 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000004073 vulcanization Methods 0.000 description 2
- 239000011787 zinc oxide Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 230000009916 joint effect Effects 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 229910001425 magnesium ion Inorganic materials 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000036314 physical performance Effects 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 238000005486 sulfidation Methods 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
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- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Description
Claims (11)
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CN201410317135.0A CN104087030B (zh) | 2014-07-07 | 2014-07-07 | 一种氟橡胶专用氧化镁及其制备方法 |
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CN104087030A true CN104087030A (zh) | 2014-10-08 |
CN104087030B CN104087030B (zh) | 2016-09-14 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113817401A (zh) * | 2021-10-23 | 2021-12-21 | 上海立投工贸有限公司 | 一种单组分聚氨酯防水涂料及其制备方法 |
Citations (10)
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JP2004189905A (ja) * | 2002-12-12 | 2004-07-08 | Nippon Unicar Co Ltd | 難燃性樹脂組成物及びそれから得られた押出成形品 |
CN1668710A (zh) * | 2002-07-19 | 2005-09-14 | 白石工业株式会社 | 改性碳酸钙及含改性碳酸钙的聚合物组合物及其制造方法 |
JP2007284702A (ja) * | 2007-08-09 | 2007-11-01 | Nippon Unicar Co Ltd | 難燃性樹脂組成物の可撓性改善方法及び可撓性が改善された押出成形品 |
CN101368009A (zh) * | 2007-12-12 | 2009-02-18 | 清华大学深圳研究生院 | 纳米氢氧化镁的改性方法 |
CN101402752A (zh) * | 2007-10-03 | 2009-04-08 | 日立电线株式会社 | 无卤素的阻燃性树脂组合物及使用该组合物的电线和电缆 |
JP2010059270A (ja) * | 2008-09-02 | 2010-03-18 | Toyo Tire & Rubber Co Ltd | 疎水性無機酸化物およびそれを用いたゴム組成物 |
CN102653599A (zh) * | 2012-05-08 | 2012-09-05 | 大连盖特科技发展有限公司 | 一种含高分子偶联剂的活性镁系阻燃剂及其制备方法 |
US20120277361A1 (en) * | 2011-04-29 | 2012-11-01 | Korea Institute Of Science And Technology | Functional reinforcing fillers modified with alkenylalkoxysilane and preparing method of the same |
CN102977383A (zh) * | 2012-07-30 | 2013-03-20 | 横店集团东磁股份有限公司 | 永磁铁氧体注塑母料的制备方法及制得的永磁铁氧体注塑母料 |
CN103881419A (zh) * | 2012-12-21 | 2014-06-25 | 中国科学院理化技术研究所 | 疏水性空心SiO2球形纳米粒子及其制备方法和应用 |
-
2014
- 2014-07-07 CN CN201410317135.0A patent/CN104087030B/zh active Active
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CN1668710A (zh) * | 2002-07-19 | 2005-09-14 | 白石工业株式会社 | 改性碳酸钙及含改性碳酸钙的聚合物组合物及其制造方法 |
JP2004189905A (ja) * | 2002-12-12 | 2004-07-08 | Nippon Unicar Co Ltd | 難燃性樹脂組成物及びそれから得られた押出成形品 |
JP2007284702A (ja) * | 2007-08-09 | 2007-11-01 | Nippon Unicar Co Ltd | 難燃性樹脂組成物の可撓性改善方法及び可撓性が改善された押出成形品 |
CN101402752A (zh) * | 2007-10-03 | 2009-04-08 | 日立电线株式会社 | 无卤素的阻燃性树脂组合物及使用该组合物的电线和电缆 |
CN101368009A (zh) * | 2007-12-12 | 2009-02-18 | 清华大学深圳研究生院 | 纳米氢氧化镁的改性方法 |
JP2010059270A (ja) * | 2008-09-02 | 2010-03-18 | Toyo Tire & Rubber Co Ltd | 疎水性無機酸化物およびそれを用いたゴム組成物 |
US20120277361A1 (en) * | 2011-04-29 | 2012-11-01 | Korea Institute Of Science And Technology | Functional reinforcing fillers modified with alkenylalkoxysilane and preparing method of the same |
CN102653599A (zh) * | 2012-05-08 | 2012-09-05 | 大连盖特科技发展有限公司 | 一种含高分子偶联剂的活性镁系阻燃剂及其制备方法 |
CN102977383A (zh) * | 2012-07-30 | 2013-03-20 | 横店集团东磁股份有限公司 | 永磁铁氧体注塑母料的制备方法及制得的永磁铁氧体注塑母料 |
CN103881419A (zh) * | 2012-12-21 | 2014-06-25 | 中国科学院理化技术研究所 | 疏水性空心SiO2球形纳米粒子及其制备方法和应用 |
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Title |
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N.M. AHMED ET AL.: "Utilization of new micronized and nano-CoO:MgO/kaolin mixed pigments in improving the properties of styrene-butadiene rubber composites", 《MATERIALS AND DESIGN》, vol. 32, no. 1, 12 June 2010 (2010-06-12) * |
张孟存等: "吸酸剂对氟橡胶性能影响的研究", 《邢台职业技术学院学报》, vol. 26, no. 3, 15 June 2009 (2009-06-15) * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113817401A (zh) * | 2021-10-23 | 2021-12-21 | 上海立投工贸有限公司 | 一种单组分聚氨酯防水涂料及其制备方法 |
CN113817401B (zh) * | 2021-10-23 | 2022-10-21 | 上海立投工贸有限公司 | 一种单组分聚氨酯防水涂料及其制备方法 |
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Effective date of registration: 20170602 Address after: 054600 Guangzong County, Hebei Province, west of the road west of the venture Patentee after: HEBEI MEITAI MEIZHI MATERIAL Co.,Ltd. Address before: 050018 No. 70 East Yuhua Road, Yuhua District, Hebei, Shijiazhuang Patentee before: Hebei University of Science and Technology |
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Denomination of invention: A special magnesium oxide for fluorine rubber and its preparation method Effective date of registration: 20230118 Granted publication date: 20160914 Pledgee: China Construction Bank Corporation Guangzong Sub-branch Pledgor: HEBEI MEISHEN TECHNOLOGY CO.,LTD. Registration number: Y2023980031570 |
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Effective date of registration: 20230517 Address after: No. 0018, West Side of Chuangye Avenue, Guangzong County, Xingtai City, Hebei Province, 054600 Patentee after: HEBEI MEISHEN TECHNOLOGY CO.,LTD. Patentee after: HEBEI MEITAI MEIZHI MATERIAL Co.,Ltd. Address before: 054000 west of Chuang Chuang Avenue, Guangzong County, Xingtai, Hebei Patentee before: HEBEI MEISHEN TECHNOLOGY CO.,LTD. |
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Date of cancellation: 20240102 Granted publication date: 20160914 Pledgee: China Construction Bank Corporation Guangzong Sub-branch Pledgor: HEBEI XINGTAI METALLURGICAL MAGNESIUM INDUSTRY Co.,Ltd.|HEBEI MEITAI MEIZHI MATERIAL Co.,Ltd.|HEBEI MEISHEN TECHNOLOGY CO.,LTD. Registration number: Y2023980031570 |
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Denomination of invention: A special magnesium oxide for fluororubber and its preparation method Granted publication date: 20160914 Pledgee: China Construction Bank Corporation Guangzong Sub-branch Pledgor: HEBEI MEISHEN TECHNOLOGY CO.,LTD.|HEBEI MEITAI MEIZHI MATERIAL Co.,Ltd.|HEBEI XINGTAI METALLURGICAL MAGNESIUM INDUSTRY Co.,Ltd. Registration number: Y2024990000026 |