CN104030787B - A kind of treated starch ether coating long-acting slow-release compound fertilizers - Google Patents
A kind of treated starch ether coating long-acting slow-release compound fertilizers Download PDFInfo
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- CN104030787B CN104030787B CN201410199804.9A CN201410199804A CN104030787B CN 104030787 B CN104030787 B CN 104030787B CN 201410199804 A CN201410199804 A CN 201410199804A CN 104030787 B CN104030787 B CN 104030787B
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 38
- 239000011248 coating agent Substances 0.000 title claims abstract description 24
- 229920002472 Starch Polymers 0.000 title claims abstract description 21
- 235000019698 starch Nutrition 0.000 title claims abstract description 21
- 239000008107 starch Substances 0.000 title claims abstract description 21
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 238000000576 coating method Methods 0.000 title claims abstract description 15
- 150000001875 compounds Chemical class 0.000 title claims abstract description 15
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 16
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000463 material Substances 0.000 claims abstract description 16
- 150000002170 ethers Chemical class 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 9
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims abstract description 8
- 241000196324 Embryophyta Species 0.000 claims abstract description 8
- 239000004743 Polypropylene Substances 0.000 claims abstract description 8
- 229910052796 boron Inorganic materials 0.000 claims abstract description 8
- 239000000835 fiber Substances 0.000 claims abstract description 8
- -1 polypropylene Polymers 0.000 claims abstract description 8
- 229920001155 polypropylene Polymers 0.000 claims abstract description 8
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 8
- 244000061456 Solanum tuberosum Species 0.000 claims abstract description 7
- 235000002595 Solanum tuberosum Nutrition 0.000 claims abstract description 7
- 239000002253 acid Substances 0.000 claims abstract description 7
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 7
- 235000012343 cottonseed oil Nutrition 0.000 claims abstract description 7
- 235000012054 meals Nutrition 0.000 claims abstract description 7
- 238000004519 manufacturing process Methods 0.000 claims abstract description 5
- 238000000034 method Methods 0.000 claims abstract description 5
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims abstract description 4
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 4
- LWNCNSOPVUCKJL-UHFFFAOYSA-N [Mg].[P] Chemical compound [Mg].[P] LWNCNSOPVUCKJL-UHFFFAOYSA-N 0.000 claims abstract description 4
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004202 carbamide Substances 0.000 claims abstract description 4
- 239000010433 feldspar Substances 0.000 claims abstract description 4
- 239000002893 slag Substances 0.000 claims abstract description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 239000002002 slurry Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- OAVRWNUUOUXDFH-UHFFFAOYSA-H 2-hydroxypropane-1,2,3-tricarboxylate;manganese(2+) Chemical compound [Mn+2].[Mn+2].[Mn+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O OAVRWNUUOUXDFH-UHFFFAOYSA-H 0.000 claims description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 6
- FWBOFUGDKHMVPI-UHFFFAOYSA-K dicopper;2-oxidopropane-1,2,3-tricarboxylate Chemical compound [Cu+2].[Cu+2].[O-]C(=O)CC([O-])(C([O-])=O)CC([O-])=O FWBOFUGDKHMVPI-UHFFFAOYSA-K 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 6
- 210000003746 feather Anatomy 0.000 claims description 6
- 238000000855 fermentation Methods 0.000 claims description 6
- 230000004151 fermentation Effects 0.000 claims description 6
- 235000014872 manganese citrate Nutrition 0.000 claims description 6
- 239000011564 manganese citrate Substances 0.000 claims description 6
- 229940097206 manganese citrate Drugs 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 235000019353 potassium silicate Nutrition 0.000 claims description 6
- 244000144977 poultry Species 0.000 claims description 6
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 6
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 6
- 239000004575 stone Substances 0.000 claims description 6
- 239000001117 sulphuric acid Substances 0.000 claims description 6
- 235000011149 sulphuric acid Nutrition 0.000 claims description 6
- 150000003608 titanium Chemical class 0.000 claims description 6
- WGIWBXUNRXCYRA-UHFFFAOYSA-H trizinc;2-hydroxypropane-1,2,3-tricarboxylate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O WGIWBXUNRXCYRA-UHFFFAOYSA-H 0.000 claims description 6
- 235000006076 zinc citrate Nutrition 0.000 claims description 6
- 239000011746 zinc citrate Substances 0.000 claims description 6
- 229940068475 zinc citrate Drugs 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000008367 deionised water Substances 0.000 claims description 3
- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 238000005469 granulation Methods 0.000 claims description 3
- 230000003179 granulation Effects 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 238000009775 high-speed stirring Methods 0.000 claims description 3
- 230000007062 hydrolysis Effects 0.000 claims description 3
- 238000006460 hydrolysis reaction Methods 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 230000001954 sterilising effect Effects 0.000 claims description 3
- 238000004659 sterilization and disinfection Methods 0.000 claims description 3
- 238000007601 warm air drying Methods 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 235000015097 nutrients Nutrition 0.000 abstract description 10
- 239000002131 composite material Substances 0.000 abstract description 8
- 239000002689 soil Substances 0.000 abstract description 5
- 210000003608 fece Anatomy 0.000 abstract description 4
- 239000010871 livestock manure Substances 0.000 abstract description 4
- 230000002045 lasting effect Effects 0.000 abstract description 3
- 230000009977 dual effect Effects 0.000 abstract description 2
- 238000012986 modification Methods 0.000 abstract description 2
- 230000004048 modification Effects 0.000 abstract description 2
- 244000068988 Glycine max Species 0.000 description 4
- 235000010469 Glycine max Nutrition 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 230000012010 growth Effects 0.000 description 3
- 230000008635 plant growth Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000607479 Yersinia pestis Species 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 235000021049 nutrient content Nutrition 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Abstract
The present invention relates to compound manure field, be specifically related to a kind of treated starch ether coating long-acting slow-release compound fertilizers, this fertilizer is obtained by the raw material of following weight part: 1250-2000 order diatomite 10-15, boron fertilizer 6-8, primary ammonium phosphate 18-20, potato pulp 12-15, plant ash 10-12, phosphorus magnesium slag 4-6, Repone K 10-12, feldspar in powder 4-6, cottonseed meal 12-15, brewer's grains 8-10, polypropylene fibre 2-3, starch ethers 10-12, titanium dioxide 0.2-0.3, urea 18-20, Witco 1298 Soft Acid 4-6, auxiliary agent 4-5; Organic and inanimate matter compound in composite fertilizer material of the present invention, nutrient is comprehensively plentiful, low to soil fail degree, production technique utilize the starch ethers coating agent of diatomite and modification formed dual coated to nutrient, effectively prevent the too early loss of nutrient, make fertilizer efficiency more lasting, the seed output and quality of crop all can be improved.
Description
Technical field
The present invention relates to compound manure field, be specifically related to a kind of treated starch ether coating long-acting slow-release compound fertilizers.
Background technology
In modern agricultural production, the figure of the composite fertilizer that is seen everywhere, it has, and nutrient content is high, minor component is few, utilization rate of fertilizer is high, the advantages such as convenient are used in storage, in promotion higher yield of crops stable yields, play important role.Slow-release compound fertilizer is a kind of important classification in composite fertilizer, the research emphasis of Ye Shi China Growth of Chemical Fertilizer Industry, its slowly-releasing principle is the hydrophobic substance at fertiliser granulates Surface coating thin layer, thus the nutrient of inside is discharged in soil slowly, constantly to farm crop supply nutrient, effectively raise the utilization ratio of fertilizer.But existing slow-release compound fertilizer also exists certain shortcoming, be mainly manifested in nutrients ratio relatively fixing, be difficult to the different demands meeting all kinds of soil and all kinds of crop; Slow release effect is not fully up to expectations, does not mate, thus reduces fertilizer efficiency, affect plant growth with crop growth demand, causes the underproduction reduction of income.
Summary of the invention
The object of the invention is to provide the slow-release compound fertilizer of a kind of low cost, efficient, environmental protection, and to achieve these goals, the technical solution used in the present invention is as follows:
A kind of treated starch ether coating long-acting slow-release compound fertilizers, it is characterized in that, this fertilizer is made up of the raw material of following weight part: 1250-2000 order diatomite 10-15, boron fertilizer 6-8, primary ammonium phosphate 18-20, potato pulp 12-15, plant ash 10-12, phosphorus magnesium slag 4-6, Repone K 10-12, feldspar in powder 4-6, cottonseed meal 12-15, brewer's grains 8-10, polypropylene fibre 2-3, starch ethers 10-12, titanium dioxide 0.2-0.3, urea 18-20, Witco 1298 Soft Acid 4-6, auxiliary agent 4-5;
Auxiliary agent is made up of the raw material of following weight part: poultry feather 12-15, the sulphuric acid soln 30-35 of 30-40%, Sodium hydroxide q. s, M-Zyme 0.15-0.2, Cuprocitrol 1-2, manganese citrate 1-2, zinc citrate 1-2, medical stone fine powder 20-22, water glass 5-6, preparation method is: first poultry feather is passed through washing, pulverize after high-temperature sterilization, drop in sulphuric acid soln, hydrolysis 15-18h, appropriate sodium hydrate regulator solution pH value is added to 6.5-7.0 in the hydrolyzed solution obtained, and be heated to 50-60 DEG C, add M-Zyme, after enzymolysis 12-15h, add Cuprocitrol, manganese citrate, zinc citrate, after stirring reaction 2-3h, add water glass again, continue to stir 30-40min, finally add medical stone fine powder again, dry after stirring, and grind 40-50min, obtain.
Described a kind of treated starch ether coating long-acting slow-release compound fertilizers, its production stage is as follows:
(1) potato pulp, cottonseed meal, brewer's grains are mixed rear pulverizing, add appropriate water by fermentation to becoming thoroughly decomposed completely, fermentation material is for subsequent use;
(2) diatomite mix with waiting the water of weight part, grinding 20-30min, making diatomite slurry, add boron fertilizer, plant ash subsequently, stir rear mixture and to anhydrate drying, make diatomite coating material;
(3) first titanium dioxide and Witco 1298 Soft Acid mix and blend are disperseed 30-40min, obtained modified titanium slurry is for subsequent use, again starch ethers is mixed with appropriate deionized water, be stirred to after starch ethers dissolves dispersion completely, add modified titanium slurry, polypropylene fibre, high-speed stirring dispersion 1-2h, makes slow release coating agent for subsequent use;
(4) other leftover materials are mixed with step (1), (2) gained material; drop into granulation in tablets press; and at slow release coating agent prepared by obtained particle surface spraying process (3), the particle after coating, through warm air drying, room temperature cooling, gets product.
Beneficial effect of the present invention is: formula Raw wide material sources, take full advantage of raw material common in daily life production, the introducing of a large amount of organic matter material, not only reduces growth cost, improve the single fixing phenomenon of conventional composite fertilizer nutrient, also effectively protect soil; Production technique utilizes diatomite and boron fertilizer, plant ash etc. must the raw material of nutrient adsorb mutually containing plant growth, thus effectively prevent nutrient to run off too early; With slow release coating agent prepared by the starch ethers solution of the material modification such as polypropylene fibre, titanium dioxide, have excellent coated slow-release controllability, fertile amount is evenly lasting thoroughly; The slow release coating agent that composite fertilizer prepared by the present invention utilizes diatomite and treated starch ether to prepare is formed dual coated to nutrient, make the utilization ratio of fertilizer higher, fertilizer efficiency is more lasting, and not spoiled soil environment, directly improve Crop yield and quality efficiently.
Embodiment
Embodiment
The compound manure of the present embodiment is obtained by the raw material of following weight part (kilogram): 1250 order diatomite 15, boron fertilizer 8, primary ammonium phosphate 20, potato pulp 15, plant ash 10, phosphorus magnesium slag 6, Repone K 12, feldspar in powder 6, cottonseed meal 12, brewer's grains 10, polypropylene fibre 2, starch ethers 12, titanium dioxide 0.2, urea 20, Witco 1298 Soft Acid 6, auxiliary agent 5, auxiliary agent is made up of the raw material of following weight part: poultry feather 15, the sulphuric acid soln 35 of 40%, Sodium hydroxide q. s, M-Zyme 0.15, Cuprocitrol 2, manganese citrate 1, zinc citrate 2, medical stone fine powder 22, water glass 5, preparation method is: first poultry feather is passed through washing, pulverize after high-temperature sterilization, drop in sulphuric acid soln, hydrolysis 18h, appropriate sodium hydrate regulator solution pH value to 7.0 is added in the hydrolyzed solution obtained, and be heated to 50-60 DEG C, add M-Zyme, after enzymolysis 15h, add Cuprocitrol, manganese citrate, zinc citrate, stirring reaction 3h, add water glass again, continue to stir 40min, finally add medical stone fine powder again, dry after stirring, and grind 50min, obtain.
The composite heat transfer step of the present embodiment is as follows:
(1) potato pulp, cottonseed meal, brewer's grains are mixed rear pulverizing, add appropriate water by fermentation to becoming thoroughly decomposed completely, fermentation material is for subsequent use;
(2) diatomite mix with waiting the water of weight part, grinding 30min, making diatomite slurry, add boron fertilizer, plant ash subsequently, stir rear mixture and to anhydrate drying, make diatomite coating material;
(3) first titanium dioxide and Witco 1298 Soft Acid mix and blend are disperseed 40min, obtained modified titanium slurry is for subsequent use, again starch ethers is mixed with appropriate deionized water, be stirred to after starch ethers dissolves dispersion completely, add modified titanium slurry, polypropylene fibre, high-speed stirring dispersion 2h, makes slow release coating agent for subsequent use;
(4) other leftover materials are mixed with step (1), (2) gained material; drop into granulation in tablets press; and at slow release coating agent prepared by obtained particle surface spraying process (3), the particle after coating, through warm air drying, room temperature cooling, gets product.
The present embodiment is implemented at soybean planting, choose two pieces of areas respectively and be 3 mu experimental field, be labeled as test group and control group respectively, test group uses the present embodiment composite fertilizer, control group uses conventional composite fertilizer, all fertilizer is all as base manure applied once, the mu amount of executing is 60Kg, later stage no longer topdresses, two pieces of soybean varieties experimental field, daily administration is all identical, treat the harvest season, test group mu Yield of Soybean amount comparatively control group improves 20.4%, hundred counterpoises improve 7.4%, benefit per mu improves 18.7%, and test group soybean strain stem is sturdy, pod many satisfies, disease and pest incidence comparatively control group is low.
Claims (2)
1. a treated starch ether coating long-acting slow-release compound fertilizers, it is characterized in that, this fertilizer is made up of the raw material of following weight part: 1250-2000 order diatomite 10-15, boron fertilizer 6-8, primary ammonium phosphate 18-20, potato pulp 12-15, plant ash 10-12, phosphorus magnesium slag 4-6, Repone K 10-12, feldspar in powder 4-6, cottonseed meal 12-15, brewer's grains 8-10, polypropylene fibre 2-3, starch ethers 10-12, titanium dioxide 0.2-0.3, urea 18-20, Witco 1298 Soft Acid 4-6, auxiliary agent 4-5;
Described auxiliary agent is made up of the raw material of following weight part: poultry feather 12-15, the sulphuric acid soln 30-35 of 30-40%, Sodium hydroxide q. s, M-Zyme 0.15-0.2, Cuprocitrol 1-2, manganese citrate 1-2, zinc citrate 1-2, medical stone fine powder 20-22, water glass 5-6, preparation method is: first poultry feather is passed through washing, pulverize after high-temperature sterilization, drop in sulphuric acid soln, hydrolysis 15-18h, appropriate sodium hydrate regulator solution pH value is added to 6.5-7.0 in the hydrolyzed solution obtained, and be heated to 50-60 DEG C, add M-Zyme, after enzymolysis 12-15h, add Cuprocitrol, manganese citrate, zinc citrate, after stirring reaction 2-3h, add water glass again, continue to stir 30-40min, finally add medical stone fine powder again, dry after stirring, and grind 40-50min, obtain.
2. a kind of treated starch ether coating long-acting slow-release compound fertilizers as claimed in claim 1, its production stage is as follows:
(1) potato pulp, cottonseed meal, brewer's grains are mixed rear pulverizing, add appropriate water by fermentation to becoming thoroughly decomposed completely, fermentation material is for subsequent use;
(2) diatomite mix with waiting the water of weight part, grinding 20-30min, making diatomite slurry, add boron fertilizer, plant ash subsequently, stir rear mixture and to anhydrate drying, make diatomite coating material;
(3) first titanium dioxide and Witco 1298 Soft Acid mix and blend are disperseed 30-40min, obtained modified titanium slurry is for subsequent use, again starch ethers is mixed with appropriate deionized water, be stirred to after starch ethers dissolves dispersion completely, add modified titanium slurry, polypropylene fibre, high-speed stirring dispersion 1-2h, makes slow release coating agent for subsequent use;
(4) other leftover materials are mixed with step (1), (2) gained material; drop into granulation in tablets press; and at slow release coating agent prepared by obtained particle surface spraying process (3), the particle after coating, through warm air drying, room temperature cooling, gets product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410199804.9A CN104030787B (en) | 2014-05-13 | 2014-05-13 | A kind of treated starch ether coating long-acting slow-release compound fertilizers |
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| CN201410199804.9A CN104030787B (en) | 2014-05-13 | 2014-05-13 | A kind of treated starch ether coating long-acting slow-release compound fertilizers |
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| CN104030787B true CN104030787B (en) | 2015-12-09 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105859414A (en) * | 2016-04-13 | 2016-08-17 | 吴申龙 | Modified coated long-acting slow release composite fertilizer and preparation method thereof |
| CN108633596A (en) * | 2018-05-16 | 2018-10-12 | 安徽梅兰园林景观工程有限公司 | A kind of implantation methods of deep gloomy Chinese scholartree fast-growth |
| CN115160069A (en) * | 2022-08-19 | 2022-10-11 | 山东联盟磷复肥有限公司 | Special fertilizer for lawn and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102219618A (en) * | 2011-04-04 | 2011-10-19 | 山东农业大学 | Rice seedling raising controlled-release nitrogenous fertilizer applied completely in one time and preparation method thereof |
| CN102718605A (en) * | 2012-07-19 | 2012-10-10 | 湖南省烟草公司郴州市公司 | Method for producing amino acid tobacco-specific foliar fertilizer by using abandoned fur |
| CN103497031A (en) * | 2013-08-29 | 2014-01-08 | 合肥市潜溪山庄农业生态园有限公司 | Agricultural fertilizer and its preparation method |
| CN103708950A (en) * | 2013-12-16 | 2014-04-09 | 天津丰润园精细化工科技有限公司 | Special soybean controlled-release organic fertilizer and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102219618A (en) * | 2011-04-04 | 2011-10-19 | 山东农业大学 | Rice seedling raising controlled-release nitrogenous fertilizer applied completely in one time and preparation method thereof |
| CN102718605A (en) * | 2012-07-19 | 2012-10-10 | 湖南省烟草公司郴州市公司 | Method for producing amino acid tobacco-specific foliar fertilizer by using abandoned fur |
| CN103497031A (en) * | 2013-08-29 | 2014-01-08 | 合肥市潜溪山庄农业生态园有限公司 | Agricultural fertilizer and its preparation method |
| CN103708950A (en) * | 2013-12-16 | 2014-04-09 | 天津丰润园精细化工科技有限公司 | Special soybean controlled-release organic fertilizer and preparation method thereof |
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Effective date of registration: 20170619 Address after: 510000 Guangdong city of Guangzhou province Zengcheng Licheng Street Garden Road No. 93, No. 101 first floor (not for plant use) Patentee after: Guangzhou vine Agriculture Development Co.,Ltd. Address before: 510000 unit 2414-2416, building, No. five, No. 371, Tianhe District, Guangdong, China Patentee before: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Effective date of registration: 20170619 Address after: 510000 unit 2414-2416, building, No. five, No. 371, Tianhe District, Guangdong, China Patentee after: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Address before: 243100 Anhui city of Ma'anshan province Dangtu County Rural River Village 25 villages spread Patentee before: MAANSHAN XINZHOU GRAPE SPECIALIZED COOPERATIVE |
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Effective date of registration: 20180125 Address after: 300000 Tianjin City Jizhou District Jizhou overpass west Patentee after: Jizhou District of Tianjin City Green Food Development Center Address before: 510000 Guangdong city of Guangzhou province Zengcheng Licheng Street Garden Road No. 93, No. 101 first floor (not for plant use) Patentee before: Guangzhou vine Agriculture Development Co.,Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151209 Termination date: 20200513 |