CN103992905B - A kind of Gardenia Yellow gin preparation method rich in crocin and jasminoidin - Google Patents
A kind of Gardenia Yellow gin preparation method rich in crocin and jasminoidin Download PDFInfo
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- CN103992905B CN103992905B CN201410202005.2A CN201410202005A CN103992905B CN 103992905 B CN103992905 B CN 103992905B CN 201410202005 A CN201410202005 A CN 201410202005A CN 103992905 B CN103992905 B CN 103992905B
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Abstract
The preparation method that the present invention relates to a kind of Gardenia Yellow gin rich in crocin and jasminoidin, belongs to medicinal food and field of health care food. The preparation method that the present invention adopts includes extraction, precipitation and makes three steps. Liposoluble constituent more than 99.9% in material can be extracted (after defat in the dregs of rice oil content below 0.1%) by subcritical abstraction technology, take out the Fructus Gardeniae dregs of rice can directly brew rich in the Gardenia Yellow gin of crocin and jasminoidin; This Gardenia Yellow gin containing crocin and jasminoidin as health care while, be absent from again any abnormal flavour; Add the Fructus Gardeniae dregs of rice itself containing Gardenia Yellow, it is not necessary to add any industry pigment, wine still can being made to present golden yellow color and luster, so being called " Gardenia Yellow gin ", therefore there is very wide application prospect.
Description
Technical field
The present invention relates to a kind of Gardenia Yellow gin preparation method rich in crocin and jasminoidin, belong to medicinal food and field of health care food.
Technical background
As one of medicine-food two-purpose resource that country announces in the first batch, Fructus Gardeniae both as good to eat food consumption, can be used as again medical material and use. Fructus Gardeniae is the mature fruit of Maguireothamnus speciosus Fructus Gardeniae (GardeniajasminoidesEllis), it it is conventional Chinese medicine simply, all on the books from Compendium of Material Medica to successive dynasties medicine masterpieces such as " Chinese Pharmacopoeias ", there is the effect of pathogenic fire purging relieving restlessness, clearing away heat and promoting diuresis, removing pathogenic heat from blood and toxic substance from the body, also have external treatment bruise effect.
The effective ingredient of Fructus Gardeniae mainly has the oxygen-containing carotenoid such as the iridoids such as jasminoidin and Gardenia Yellow (one of main component is crocin). Raw material as Chinese Medicine Industry, mainly using the jasminoidin of about 3% content as quality standard, and content 0.12～0.25% crocin more Development volue (one of main component in Gardenia Yellow in Fructus Gardeniae, in the full fruit of SHANZHIZI, content is 0.20%, in seed 0.25%, in peel 0.12%. Yang Xiangyu. 2005. Shandong University's master's thesis). Crocin is the oxygen-containing carotenoid derivatives of water solublity that a class is rare, there is active anticancer and the hypotoxicity of wide spectrum, in dietetic therapy or prevention cardiovascular and cerebrovascular disease and cancer etc., there is clear and definite pharmacodynamics effect, after further basic research and clinical trial, it is expected to become following main flow PTS, or there is new drug (Deng Ying, the Guo Zhigang of the treatment cardiovascular and cerebrovascular disease of powerful blood circulation invigorating efficacies, Zeng Zhaolin, Wang Zhao. 2002. Croceous pharmacological research progress [J], CHINA JOURNAL OF CHINESE MATERIA MEDICA (27): 565-568). In recent years, from China conventional Chinese medicine Fructus Gardeniae, have also discovered crocin constituents (being called Gardenia Yellow), thus from Fructus Gardeniae, extract valuable crocin become study hotspot.
Subcritical abstraction technology can carry out under room temperature even cryogenic conditions, has both ensured the functional activity of effective ingredient in extract, extracts process natural environmental-protective, does not introduce any impurity foreign body. Utilize this technology to extract Gardenia Seed Oil aspect and can reach in the full defat dregs of rice residual oil content lower than 0.1%, it is ensured that after extracting oils and fats, " dregs of rice " Middle nutrition composition does not change;And effective ingredient (crocin and jasminoidin) free of losses in the dregs of rice, still there is very big Development volue; Additionally the Fructus Gardeniae dregs of rice after full defat are prone to storage, advantageously in exploitation. The present invention comprehensively utilizes the Fructus Gardeniae dregs of rice after the full defat of subcritical abstraction technology, prepares the Gardenia Yellow gin rich in crocin and jasminoidin both at home and abroad first, is a kind of method of abundant exploitation Fructus Gardeniae medicine-food two-purpose value.
Health promoting wine in the market does not all break away from the taste of Chinese medicine mostly, is difficult to meet the mouthfeel requirement of consumer, and this also becomes the key factor restricting many health promoting wine production developments. The present invention comprehensively utilizes the Fructus Gardeniae dregs of rice after the full defat of subcritical abstraction technology, prepares the Gardenia Yellow gin rich in crocin and jasminoidin both at home and abroad first, is a kind of method of abundant exploitation Fructus Gardeniae medicine-food two-purpose value.
Summary of the invention
The Fructus Gardeniae dregs of rice after utilizing the full defat of subcritical abstraction technology are used by the present invention, comprehensively prepare a kind of Gardenia Yellow gin rich in crocin and jasminoidin, specifically include following steps:
1) defat: by Fructus Gardeniae raw material drying, shelling, pulverizing, crosses 40 mesh sieves, is subsequently placed in and closes degreasing tank, evacuation, inject appropriate subcritical degreasing solvent to being totally submerged by sample, under certain degreasing condition, carry out repeatedly defat, until raw oil material content is lower than 0.1%;
2) the Fructus Gardeniae dregs of rice are carried out coarse vacuum and fine vacuum precipitation by precipitation: after defat terminates respectively, and in the Fructus Gardeniae dregs of rice obtained after precipitation, solvent is lower than 1ppm;
3) making of gold wine: by step 2) in the gained full defat Fructus Gardeniae dregs of rice add in appropriate wine, under certain condition brewed complete after, filter the impurity in feed liquid with fruit wine filter; The brew of gold wine can also add the Fructus Gardeniae dregs of rice in the initial period of brew base liquor, then carries out the brew of Gardenia Yellow gin together with brew base liquor raw material.
Described step 1) mass ratio of raw material and degreasing solvent is 1:1～10.
Described degreasing condition: pressure is 0.1～0.9MPa, temperature is 10～60 DEG C, and degreasing time is 10～40min, and defat number of times is 1～5 time.
Described subcritical fluids organic solvent is at least one in propane, butane, tetrafluoroethane.
Described step 3) in brewed Gardenia Yellow gin time the Fructus Gardeniae dregs of rice and wine mass volume ratio be 1:50～1000.
Described step 3) in gold wine brew can brew base liquor initial period add the Fructus Gardeniae dregs of rice, then carry out the brew of Gardenia Yellow gin together with brew base liquor raw material.
Described step 3) in the mass ratio of the Fructus Gardeniae dregs of rice and brew base liquor raw material be 1:50～1000.
Described step 3) in brewing conditions be temperature 20～50 DEG C, 1～30 day time.
Described step 3) in brew condition be original fermentation condition of selected base liquor.
Described step 3) described in brew base liquor raw material include: grain class, potato class, sugary raw material and some adjuvants (rice husk, bran coat, corn cob, sorghum husk, peanut skin etc.) etc.
This invention utilizes the Fructus Gardeniae dregs of rice to prepare Gardenia Yellow gin, because the medicine-food two-purpose of Fructus Gardeniae, while containing crocin and jasminoidin as health care, is absent from again any abnormal flavour; Add the Fructus Gardeniae dregs of rice itself containing Gardenia Yellow, it is not necessary to add any industry pigment, wine still can being made to present golden yellow color and luster, so being called " Gardenia Yellow gin ", and containing jasminoidin and crocin after testing. Additionally the present invention ensures to extract the comprehensive utilization of " dregs of rice " Middle nutrition composition after oils and fats, has very wide application prospect.
Detailed description of the invention
The present invention by the restriction of following embodiment, can not determine specific embodiment according to the technical scheme of the invention described above and practical situation.
Embodiment 1
Choose 200g SHANZHIZI raw material drying, shelling, pulverizing, cross 40 mesh sieves, load airtight degreasing tank, evacuation, inject subcritical butane degreasing solvent and sample is totally submerged, expect molten ratio 1:15, temperature 20 DEG C, time 20min, carry out three defats. After defat terminates, the liquid flux containing Fructus Gardeniae fruit oil is put into evaporator, degreasing tank and evaporator constant temperature are evaporated under reduced pressure, obtain Fructus Gardeniae dregs of rice 158g and Fructus Gardeniae fruit oil 42g respectively.
Take the Fructus Gardeniae dregs of rice (oil content≤0.1%) after the 6g full defat of subcritical butane, itself and the commercially available Maotai-flavor liquor of 300ml brand are brewageed under 37 DEG C of conditions. Chinese liquor to be not added with the Fructus Gardeniae dregs of rice compares. After 30 days, filter the solid particle in feed liquid, suspended material, colloidal particle and antibacterial, filtering and purification liquid with filter. Health promoting wine has been changed to transparent golden yellow; Suspend there are no particulate material under the microscope, find there is no obvious abnormal flavour compared with the control through tasting. Detect through HPLC, jasminoidin 0.0621% and crocin content respectively 0.0051% in gained health promoting wine.
Embodiment 2
Raw materials used sub for Fructus Gardeniae grandiflorae, subcritical degreasing solvent is that propane, degreasing method and desolventizing method are with embodiment 1.
Take the Fructus Gardeniae dregs of rice (oil content≤0.1%) after the full defat of 2.5g, be directly added into the commercially available fen-flavor type white spirit of 250ml brand, brewage under 30 DEG C of conditions. This brand Chinese liquor to be not added with the Fructus Gardeniae dregs of rice compares. After 30 days, filter the solid particle in feed liquid, suspended material, colloidal particle and antibacterial, filtering and purification liquid with filter. The wine adding the Fructus Gardeniae dregs of rice has been changed to transparent golden yellow; Suspend there are no particulate material under the microscope, find there is no obvious abnormal flavour compared with the control through tasting. Detect through HPLC, the content of jasminoidin and crocin respectively 0.0352% and 0.0025% in gained health promoting wine.
Embodiment 3
Raw materials used for SHANZHIZI, subcritical degreasing solvent is tetrafluoroethane, and defat number of times is 4 times, and degreasing method and desolventizing method are with embodiment 1.
Take the Fructus Gardeniae dregs of rice (oil content≤0.1%) after the full defat of 15g, in the ratio of 1:50 (w/w) in certain brand spirit brewing initial period, be directly added into the brew carrying out Gardenia Yellow gin in its liquor-making raw material together. Conventional brewing materials to be not added with the Fructus Gardeniae dregs of rice compares. After 30 days, filter the solid particle in feed liquid, suspended material, colloidal particle and antibacterial, filtering and purification liquid with filter. Compared with the control, the wine adding the Fructus Gardeniae dregs of rice becomes transparent golden yellow; Suspend there are no particulate material under the microscope, find there is no obvious abnormal flavour compared with the control through tasting. Detect through HPLC, containing jasminoidin and crocin in gained health promoting wine, its content respectively 0.0480% and 0.0042%.
It should be noted last that: above example is only in order to illustrate, and unrestricted technical scheme, although the present invention being described in detail with reference to above-described embodiment, it will be understood by those within the art that: still the present invention can be modified or equivalent replacement, without deviating from any modification or partial replacement of the spirit and scope of the present invention, it all should be encompassed in the middle of scope of the presently claimed invention.
Claims (9)
1. the preparation method rich in the Gardenia Yellow gin of crocin and jasminoidin, it is characterised in that comprise the steps:
1) defat: by Fructus Gardeniae raw material drying, shelling, pulverizing, crosses 40 mesh sieves, is placed in airtight degreasing tank, evacuation, inject appropriate subcritical degreasing solvent to being totally submerged by sample, under certain degreasing condition, carry out repeatedly defat, until feedstock fat content is lower than 0.1%;2) the Fructus Gardeniae dregs of rice are carried out coarse vacuum and fine vacuum precipitation by precipitation: after defat terminates respectively, it is thus achieved that precipitation after in the Fructus Gardeniae dregs of rice dissolvent residual content lower than 1ppm; 3) making of gold wine: by step 2) in the gained full defat Fructus Gardeniae dregs of rice add in appropriate wine, under certain condition brewed complete after, filter the impurity in feed liquid with fruit wine filter; Described degreasing condition: pressure is 0.1～0.9MPa, temperature is 10～60 DEG C, and degreasing time is 10～40min, and defat number of times is 1～5 time.
2. method according to claim 1, it is characterised in that described step 1) mass ratio of raw material and degreasing solvent is 1:1～10.
3. method according to claim 1, it is characterised in that described subcritical degreasing solvent is the mixing of one or more in propane, butane, tetrafluoroethane.
4. method according to claim 1, it is characterised in that described step 3) in the mass volume ratio of the Fructus Gardeniae dregs of rice and wine be 1:50～1000.
5. method according to claim 1, it is characterised in that described step 3) in brewing conditions be temperature 20～50 DEG C, 1～30 day time.
6. method according to claim 1, it is characterized in that, may be used without the method for brew and prepare gold wine, specifically: the 3) making of gold wine: by step 2) in produce the Fructus Gardeniae dregs of rice add in the initial period of brew base liquor, then carry out the brew of Gardenia Yellow gin together with brew base liquor raw material.
7. method according to claim 6, it is characterised in that described step 3) in brew condition be the fermentation condition of selected brew base liquor.
8. method according to claim 6, it is characterised in that described step 3) in the mass ratio of the Fructus Gardeniae dregs of rice and brew base liquor raw material be 1:50～1000.
9. method according to claim 6, it is characterised in that described step 3) described in brew base liquor raw material include: grain class, potato class and some adjuvant rice husk, bran coat, corn cob, sorghum husk, peanut skin.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410202005.2A CN103992905B (en) | 2014-05-13 | 2014-05-13 | A kind of Gardenia Yellow gin preparation method rich in crocin and jasminoidin |
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| CN201410202005.2A CN103992905B (en) | 2014-05-13 | 2014-05-13 | A kind of Gardenia Yellow gin preparation method rich in crocin and jasminoidin |
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| Publication Number | Publication Date |
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| CN103992905A CN103992905A (en) | 2014-08-20 |
| CN103992905B true CN103992905B (en) | 2016-06-15 |
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| CN106360181A (en) * | 2016-08-31 | 2017-02-01 | 四川百顺药业有限公司 | Cape jasmine fruit drink and preparation method thereof |
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| CN1670037A (en) * | 2005-02-24 | 2005-09-21 | 河南大学 | Complex utilization of Gardenia |
| CN101319183A (en) * | 2008-06-10 | 2008-12-10 | 罗建军 | Method for brewing fermentation of olive wine with fruit juice and residue of olive |
| CN103243007B (en) * | 2013-04-03 | 2018-02-13 | 天津华易科技发展有限公司 | A kind of Wine and preparation method thereof |
| CN103627591B (en) * | 2013-12-12 | 2015-07-29 | 重庆市柚神酒业有限责任公司 | Yellow Fructus Gardeniae Chinese medicinal liquor and preparation method thereof |
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Granted publication date: 20160615 Termination date: 20170513 |