CN104921217B - A kind of black fruit fructus lycii, hawthorn, the preparation method of lemon composite beverage - Google Patents
A kind of black fruit fructus lycii, hawthorn, the preparation method of lemon composite beverage Download PDFInfo
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- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Natural products OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 2
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- 229910021529 ammonia Inorganic materials 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
- A23L2/74—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration using membranes, e.g. osmosis, ultrafiltration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Water Supply & Treatment (AREA)
- Non-Alcoholic Beverages (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to a kind of black fruit fructus lycii, hawthorn, lemon composite beverage preparation method, the method comprises the following steps：(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively obtains black fruit fructus lycii juice, haw juice and lemon juice；After black fruit fructus lycii juice, haw juice and lemon juice are fully mixed, obtain mixing juice；(2) mixing juice carries out heating water bath extraction with water, obtains leaching liquor；(3) after leaching liquor grinds 1 ~ 8 time through colloid mill, the compound extracting solution of colloidal is obtained；By the compound extracting solution homogeneous of colloidal after, through enzymolysis, centrifugation, respectively obtain supernatant A and filter residue；(5) supernatant is obtained into filtrate through ceramic membrane removal of impurities；(6) filtrate is allocated with haw juice, supernatant B is obtained after centrifugation, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.The present invention is with low cost, and products obtained therefrom activity substance content is high, natural health nutrition.
Description
Technical field
The present invention relates to the preparation method of beverage, more particularly to a kind of black fruit fructus lycii, hawthorn, the preparation of lemon composite beverage
Method.
Background technology
Black fruit fructus lycii（Lycium ruthenicum）It is Solanaceae（Solanaceae）Lycium（LyciumL.）It is China
The distinctive perennial shrub in the Northwest, its berry is spherical, is atropurpureus after maturation, rich in anthocyanidin, flavonoids, polysaccharide, ammonia
The effects such as base acid, mineral element composition, because containing the water colo(u)r for enriching --- there is good dietotherapeutic anthocyanidin
Function.Used as a kind of natural food colour in food additives, anthocyanidin is because of its unique anti-oxidation characteristics and good for health
Effect is increasingly subject to the favor of people.Hawthorn（Crataegus pinnatifida）And lemon（Citrus limon）Because being rich in
Organic acid, flavonoids, vitamin isoreactivity composition and extremely people's concern, with edible and medical value very high, extensively should
For industries such as medicine, chemical industry, food and cosmetics.
At present, the extraction to anthocyanidin, flavonoids, organic acid isoreactivity material is prepared generally using infusion process, flowing back carries
Follow the example of, ultrasonic extraction and microwave loss mechanisms.Wherein：First, infusion process is a kind of traditional natural product extraction method, the method
Refer to soak wherein chemical with dissolution during the raw material that will be crushed at ambient temperature is put into the closed container for fill appropriate solvent
The method of composition.The method operating process is fairly time consuming, and extraction efficiency is poor, and solvent-oil ratio is big and leaching liquor easily goes mouldy.Second,
Reflux extraction is the method with volatile organic solvent heating and refluxing extraction plant component.The method operation it is cumbersome, carry
Take that the time is long, solvent-oil ratio is larger, and be heated to reflux that the compound of thermally labile can be destroyed for a long time.3rd, ultrasound
Extraction method is the method extracted using ultrasonic assistant Extraction solvent.The main cavitation using ultrasonic wave, destruction is planted
Thing crude drug cell, easily penetrates solvent intracellular, simultaneously because the judder energy of ultrasonic wave, strengthens releasing for intracellular organic matter
Put, spread and dissolve, accelerate the leaching of active ingredient.The method Extracting temperature is difficult to control to, and is still at present the small rule in laboratory
Mould is used, and large-scale production needs to solve plant issue.4th, microwave loss mechanisms are that a kind of main utilization microwave is strong
The method that fuel factor is extracted to active ingredient in natural drug.The method is high to instrument and equipment requirement, and operating cost is high, and
Range of application is narrower.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of high black of with low cost, products obtained therefrom activity substance content
Fruit matrimony vine, hawthorn, the preparation method of lemon composite beverage.
To solve the above problems, a kind of black fruit fructus lycii of the present invention, hawthorn, the preparation method of lemon composite beverage,
Comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；The black fruit fructus lycii juice, haw juice and lemon juice press 4 ~ 11：1~5：After 1 ~ 4 volume ratio is fully mixed,
Obtain mixing juice；
(2) the mixing juice and water are pressed 1：1 ~ 60 material liquid volume ratio carries out heating water bath at a temperature of 20 ~ 60 DEG C
Extract, leaching liquor is obtained after 0.2 ~ 72 h；
(3) after the leaching liquor grinds 1 ~ 8 time through colloid mill, the compound extracting solution of colloidal is obtained；
(4) after the compound extracting solution of the colloidal being carried out into homogeneous under the pressure of 1 ~ 200 MPa, through enzymolysis, centrifugation
Separate, respectively obtain supernatant A and filter residue；
By the supernatant A with the flow velocity via hole diameter of 0.1 ~ 9 t/h as 0.01 ~ 10 μm ceramic membrane temperature be 15 ~
60 DEG C, pressure be 0.005 ~ 3 MPa under conditions of removal of impurities, obtain filtrate；
By the filtrate with the haw juice with 5 ~ 12：1 ~ 5 volume ratio is allocated, and supernatant is obtained after centrifugation
B, supernatant B be sterilized according to a conventional method, it is filling after obtain final product.
Above-mentioned steps are replaced (2) to prepare leaching liquor with following preparation methods：The mixing juice and water are pressed 1：1 ~ 60 material
Liquid volume ratio temperature be 15 ~ 60 DEG C, power be 50 ~ 1000 W under conditions of carry out ultrasonic extraction, obtained final product after 0.2 ~ 36 h.
The step (3) in colloid mill rotor speed be 2000 ~ 20000 r/min.
(4) middle enzymatic hydrolysis condition refers to that hydrolysis temperature is 10 ~ 60 DEG C to the step, and enzymolysis time is 0.1 ~ 32 h, is used
Enzyme be the one kind in amylase, pectase, cellulase, hemicellulase, protease, two or more；Its consumption is institute
State the 0.01% ~ 1% of the compound extracting solution quality of colloidal.
The condition of the step (4) middle centrifugation refers to that centrifugal speed is 2000 ~ 20000 r/min, centrifugation time is 5 ~
50 min。
The condition of the step (6) middle centrifugation refers to that centrifugal speed is 2000 ~ 20000 r/min, centrifugation time is 5 ~
40 min。
The present invention has advantages below compared with prior art：
1st, the present invention is raw material from black fruit fructus lycii, hawthorn, lemon, make full use of anthocyanidin in lycium ruthenicum fruit,
The multiple efficacies material such as organic acid, flavonoids, vitamin in polysaccharide, amino acid, mineral element and hawthorn, lemon, by section
Compatibility is learned, is combined using active component extractive technique and zymotechnic, produced a kind of homogeneous figure, color stability, be naturally good for
Health, nutrition it is agreeable to the taste rich in anthocyanidin composite health care beverage.
2nd, the present invention is by colloid mill break-in technology, high pressure homogenization technique and membrane separation technique use in conjunction, not only effectively
Preparation time is shortened, operating efficiency, and gained beverage properties stabilization, anthocyanidin, flavonoids, organic acid, dimension life is improve
Element, amino acid isoreactivity component content are high.
3rd, because the present invention uses ceramic membrane separation, therefore, it is tannin not only effectively in removal leaching liquor, mucilaginous substance, thin
The impurity such as bacterium, and equipment investment is significantly reduced, energy consumption is reduced, while also making process simplification.
4th, because the present invention is with stock number abundant black fruit fructus lycii, hawthorn, lemon as raw material, therefore, significantly reduce
Production cost.
5th, product of the present invention highlights black fruit fructus lycii, hawthorn, distinctive coordination local flavor and hawthorn, the lemon of lemon mixing generation
Interact the stable color and luster and bioactivity for producing with black fruit fructus lycii anthocyanidin, while the present invention is using in hawthorn and lemon juice
Organic acid adjust the acidity of beverage, micromolecular polysaccharide and reduction that the material such as carbohydrate and pectin in black fruit fructus lycii enzymolysis is obtained
The sugariness of sugar regulation beverage, without extra addition acid and sweetener；Citric acid, malic acid in raw material hawthorn and lemon and
Vitamin C etc. is conducive to extracting and protect the natural anthocyanidin isoreactivity composition in black fruit fructus lycii, and through homogeneous and enzymolysis at
Nutritive effect composition is more easy to be absorbed and utilizes in beverage after reason, it is achieved thereby that modern pursues natural, healthy, nutrition
Diet theory, with food digesting stomach fortifying, the effect for promoting the production of body fluid to quench thirst, removing interior free yl, prevention cardiovascular and cerebrovascular disease.
6th, after testing, anthocyanidin content >=0.3 mg/mL, general flavone content >=0.5 mg/mL have products obtained therefrom of the present invention
Machine acid content >=0.3 mg/mL, pH value is 3.0 ~ 3.5.
7th, instrument and equipment of the present invention is easy to operate, and technical parameter is easily controllable, wide adaptation range, can be used for industrial metaplasia
Produce, form biological product industrial chain.
Specific embodiment
A kind of black fruit fructus lycii of embodiment 1, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 5：1：1 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：1 material liquid volume ratio（kg/L）In the condition that temperature is 15 DEG C, power is 50 W
Under carry out ultrasonic extraction, obtain leaching liquor after 0.2 h.
(3) after leaching liquor grinds 1 time through the colloid mill that rotor speed is 2000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 1 MPa, then hydrolysis temperature be 10 DEG C,
Enzymolysis time obtains homogeneous enzymolysis liquid to use amylase, pectinase enzymatic hydrolysis under conditions of 32 h；Finally use centrifuge with
The centrifugal speed of 2000 r/min respectively obtains supernatant A and filter residue to the min of enzymolysis liquid centrifugation 5.Collect supernatant A,
Discard filter residue.
Wherein：The mass ratio of amylase, pectase（kg/kg）It is 1：8.
Enzyme dosage is the 1% of the compound extracting solution quality of colloidal.
(5) it is as 15 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 0.1 t/h is 0.01 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 0.005 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 5：1 volume ratio（L/L）Allocated, be centrifuged through the centrifugal speed of 2000 r/min
Supernatant B is obtained after 5 min, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 2, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 11：5：4 volume ratio（L/L）After fully mixing, obtain
Mixing juice.
(2) mixing juice is pressed 1 with water：60 material liquid volume ratio（kg/L）Heating water bath is carried out at a temperature of 60 DEG C to carry
Take, leaching liquor is obtained after 0.2h.
(3) after leaching liquor grinds 8 times through the colloid mill that rotor speed is 20000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 200 MPa, be then 60 in hydrolysis temperature
DEG C, enzymolysis time be 0.1 h under conditions of use amylase, pectase, cellulase, hemicellulase, protease hydrolyzed, obtain
To homogeneous enzymolysis liquid；Finally use centrifuge with the centrifugal speed of 20000 r/min to the min of enzymolysis liquid centrifugation 50, point
Supernatant A and filter residue are not obtained.Supernatant A is collected, filter residue is discarded.
Wherein：Amylase, pectase, cellulase, hemicellulase, the mass ratio of protease（kg/kg）It is 1：9：3：
1：3.
Enzyme dosage is the 0.01% of the compound extracting solution quality of colloidal.
By supernatant A with ceramic membrane that the flow velocity via hole diameter of 9 t/h is 10 μm temperature be 60 DEG C, pressure is for 3
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 12：5 volume ratio（L/L）Allocated, through 20000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 40, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 3, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 11：1：1 volume ratio（L/L）After fully mixing, obtain
Mixing juice.
(2) mixing juice is pressed 1 with water：60 material liquid volume ratio（kg/L）Temperature be 60 DEG C, power be 1000 W
Under the conditions of carry out ultrasonic extraction, obtain leaching liquor after 36 h.
(3) after leaching liquor grinds 8 times through the colloid mill that rotor speed is 20000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 200 MPa, be then 10 in hydrolysis temperature
DEG C, enzymolysis time be 32 h under conditions of use amylase, pectase, cellulase, hemicellulase, protease hydrolyzed, obtain
To homogeneous enzymolysis liquid；Finally use centrifuge with the centrifugal speed of 20000 r/min to the min of enzymolysis liquid centrifugation 50, point
Supernatant A and filter residue are not obtained.Supernatant A is collected, filter residue is discarded.
Wherein：Amylase, pectase, cellulase, hemicellulase, the mass ratio of protease（kg/kg）It is 1：8：2：
1：3.
Enzyme dosage is the 1% of the compound extracting solution quality of colloidal.
By supernatant A with ceramic membrane that the flow velocity via hole diameter of 9 t/h is 10 μm temperature be 60 DEG C, pressure is for 3
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 12：1 volume ratio（L/L）Allocated, through 20000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 40, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 4, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 4：5：4 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：1 material liquid volume ratio（kg/L）Heating water bath extraction is carried out at a temperature of 20 DEG C,
Leaching liquor is obtained after 72 h.
(3) after leaching liquor grinds 1 time through the colloid mill that rotor speed is 2000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 1 MPa, be then 60 in hydrolysis temperature
DEG C, enzymolysis time be 0.1 h under conditions of use amylase, pectinase enzymatic hydrolysis, obtain homogeneous enzymolysis liquid；Finally using centrifugation
Machine, to the min of enzymolysis liquid centrifugation 5, respectively obtains supernatant A and filter residue with the centrifugal speed of 2000 r/min.Collect supernatant
Liquid A, discards filter residue.
Wherein：The mass ratio of amylase, pectase（kg/kg）It is 1：5.
Enzyme dosage is the 0.01% of the compound extracting solution quality of colloidal.
(5) it is as 15 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 0.1 t/h is 0.01 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 0.005 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 1：1 volume ratio（L/L）Allocated, be centrifuged through the centrifugal speed of 2000 r/min
Supernatant B is obtained after 5 min, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 5, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 6：2：3 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：30 material liquid volume ratio（kg/L）In the bar that temperature is 33 DEG C, power is 500 W
Ultrasonic extraction is carried out under part, leaching liquor is obtained after 2 h.
(3) after leaching liquor grinds 2 times through the colloid mill that rotor speed is 4000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 150 MPa, be then 38 in hydrolysis temperature
DEG C, enzymolysis time be 2.0 h under conditions of use amylase, pectase, cellulase degradation, obtain homogeneous enzymolysis liquid；Most
Use centrifuge with the centrifugal speed of 8000 r/min to the min of enzymolysis liquid centrifugation 25 afterwards, respectively obtain supernatant A and filter
Slag.Supernatant A is collected, filter residue is discarded.
Wherein：Amylase, pectase, the mass ratio of cellulase（kg/kg）It is 1：7：3.
Enzyme dosage is the 0.5% of the compound extracting solution quality of colloidal.
(5) it is as 50 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 0.3 t/h is 0.2 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 0.15 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 5：3 volume ratio（L/L）Allocated, through 10000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 16, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 6, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 7：2：2 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：8 material liquid volume ratio（kg/L）Heating water bath extraction, 3 are carried out at a temperature of 53 DEG C
Leaching liquor is obtained after h.
(3) after leaching liquor grinds 3 times through the colloid mill that rotor speed is 10000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 80 MPa, be then 56 in hydrolysis temperature
DEG C, enzymolysis time be 18 h under conditions of using amylase, pectase, hemicellulase enzymolysis, obtain homogeneous enzymolysis liquid；Most
Use centrifuge with the centrifugal speed of 6000 r/min to the min of enzymolysis liquid centrifugation 15 afterwards, respectively obtain supernatant A and filter
Slag.Supernatant A is collected, filter residue is discarded.
Wherein：Amylase, pectase, the mass ratio of hemicellulase（kg/kg）It is 1：6：2.
Enzyme dosage is the 0.4% of the compound extracting solution quality of colloidal.
(5) it is as 55 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 1.0t/h is 2.0 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 1.0 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 5：2 volume ratio（L/L）Allocated, be centrifuged through the centrifugal speed of 6000 r/min
Supernatant B is obtained after 25 min, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 7, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 6：1：2 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：25 material liquid volume ratio（kg/L）In the bar that temperature is 37 DEG C, power is 300 W
Ultrasonic extraction is carried out under part, leaching liquor is obtained after 3 h.
(3) after leaching liquor grinds 1 time through the colloid mill that rotor speed is 8000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 100 MPa, be then 60 in hydrolysis temperature
DEG C, enzymolysis time be 1.5 h under conditions of using amylase, pectase, hemicellulase enzymolysis, obtain homogeneous enzymolysis liquid；
Finally use centrifuge with the centrifugal speed of 4000 r/min to the min of enzymolysis liquid centrifugation 14, respectively obtain supernatant A and
Filter residue.Supernatant A is collected, filter residue is discarded.
Wherein：Amylase, pectase, the mass ratio of hemicellulase（kg/kg）It is 1：7：2.
Enzyme dosage is the 0.6% of the compound extracting solution quality of colloidal.
(5) it is as 55 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 2.0 t/h is 5.0 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 1.5 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 12：5 volume ratio（L/L）Allocated, through 8000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 5, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 8, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 9：2：3 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：10 material liquid volume ratio（kg/L）Heating water bath is carried out at a temperature of 50 DEG C to carry
Take, leaching liquor is obtained after 4 h.
(3) after leaching liquor grinds 2 times through the colloid mill that rotor speed is 15000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 150 MPa, be then 20 in hydrolysis temperature
DEG C, enzymolysis time be 12 h under conditions of use amylase, pectase, cellulase degradation, obtain homogeneous enzymolysis liquid；Finally
Use centrifuge with the centrifugal speed of 8000 r/min to the min of enzymolysis liquid centrifugation 20, respectively obtain supernatant A and filter residue.
Supernatant A is collected, filter residue is discarded.
Wherein：Amylase, pectase, the mass ratio of cellulase（kg/kg）It is 1：6：4.
Enzyme dosage is the 0.3% of the compound extracting solution quality of colloidal.
(5) it is as 57 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 0.1 t/h is 0.2 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 0.5 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 8：3 volume ratio（L/L）Allocated, be centrifuged through the centrifugal speed of 6000 r/min
Supernatant B is obtained after 15 min, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 9, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 5：1：2 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：20 material liquid volume ratio（kg/L）In the bar that temperature is 40 DEG C, power is 600 W
Ultrasonic extraction is carried out under part, leaching liquor is obtained after 10 h.
(3) after leaching liquor grinds 1 time through the colloid mill that rotor speed is 10000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 100 MPa, be then 48 in hydrolysis temperature
DEG C, enzymolysis time be 27 h under conditions of using amylase, pectase, hemicellulase enzymolysis, obtain homogeneous enzymolysis liquid；Most
Use centrifuge with the centrifugal speed of 8000 r/min to the min of enzymolysis liquid centrifugation 25 afterwards, respectively obtain supernatant A and filter
Slag.Supernatant A is collected, filter residue is discarded.
Wherein：Amylase, pectase, the mass ratio of hemicellulase（kg/kg）It is 1：5：2.
Enzyme dosage is the 0.06% of the compound extracting solution quality of colloidal.
(5) it is as 58 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 1.0 t/h is 2.0 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 1.5 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 11：5 volume ratio（L/L）Allocated, through 8000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 15, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 10, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 8：3：2 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：4 material liquid volume ratio（kg/L）Heating water bath extraction, 5 are carried out at a temperature of 48 DEG C
Leaching liquor is obtained after h.
(3) after leaching liquor grinds 2 times through the colloid mill that rotor speed is 15000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 100 MPa, be then 24 in hydrolysis temperature
DEG C, enzymolysis time be 24 h under conditions of use amylase, pectinase enzymatic hydrolysis, obtain homogeneous enzymolysis liquid；Finally using centrifugation
Machine, to the min of enzymolysis liquid centrifugation 20, respectively obtains supernatant A and filter residue with the centrifugal speed of 6000 r/min.Collect supernatant
Liquid A, discards filter residue.
Wherein：The mass ratio of amylase, pectase（kg/kg）It is 1：10.
Enzyme dosage is the 0.09% of the compound extracting solution quality of colloidal.
(5) it is as 56 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 0.2 t/h is 8.0 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 1.0 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 5：1 volume ratio（L/L）Allocated, be centrifuged through the centrifugal speed of 8000 r/min
Supernatant B is obtained after 8 min, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 11, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 9：2：3 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：60 material liquid volume ratio（kg/L）In the bar that temperature is 60 DEG C, power is 500 W
Ultrasonic extraction is carried out under part, leaching liquor is obtained after 36 h.
(3) after leaching liquor grinds 8 times through the colloid mill that rotor speed is 20000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 200 MPa, be then 50 in hydrolysis temperature
DEG C, enzymolysis time be 24 h under conditions of use amylase enzymolysis, obtain homogeneous enzymolysis liquid；Finally use centrifuge with
The centrifugal speed of 20000 r/min respectively obtains supernatant A and filter residue to the min of enzymolysis liquid centrifugation 50.Collect supernatant
A, discards filter residue.
Wherein：Enzyme dosage is the 0.03% of the compound extracting solution quality of colloidal.
(5) it is as 15 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 9 t/h is 10 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 0.005 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 12：5 volume ratio（L/L）Allocated, through 20000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 40, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 12, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 6：1：2 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：1 material liquid volume ratio（kg/L）Heating water bath extraction is carried out at a temperature of 20 DEG C,
Leaching liquor is obtained after 0.2h.
(3) after leaching liquor grinds 1 time through rotor speed for the colloid mill of 2000r/min, the compound extraction for obtaining colloidal is molten
Liquid.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 1 MPa, be then 60 in hydrolysis temperature
DEG C, enzymolysis time be 0.1 h under conditions of use pectinase enzymatic hydrolysis, obtain homogeneous enzymolysis liquid；Finally use centrifuge with
The centrifugal speed of 2000 r/min respectively obtains supernatant A and filter residue to the min of enzymolysis liquid centrifugation 5.Collect supernatant A,
Discard filter residue.
Wherein：Enzyme dosage is the 0.2% of the compound extracting solution quality of colloidal.
(5) it is as 60 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 0.1 t/h is 0.01 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 3 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 5：1 volume ratio（L/L）Allocated, be centrifuged through the centrifugal speed of 2000 r/min
Supernatant B is obtained after 5 min, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 13, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 10：5：2 volume ratio（L/L）After fully mixing, obtain
Mixing juice.
(2) mixing juice is pressed 1 with water：25 material liquid volume ratio（kg/L）Temperature be 25 DEG C, power be 1000 W
Under the conditions of carry out ultrasonic extraction, obtain leaching liquor after 12 h.
(3) after leaching liquor grinds 5 times through the colloid mill that rotor speed is 18000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 80 MPa, be then 30 in hydrolysis temperature
DEG C, enzymolysis time be 32 h under conditions of use cellulase degradation, obtain homogeneous enzymolysis liquid；Finally use centrifuge with
The centrifugal speed of 18000 r/min respectively obtains supernatant A and filter residue to the min of enzymolysis liquid centrifugation 35.Collect supernatant
A, discards filter residue.
Wherein：Enzyme dosage is the 1% of the compound extracting solution quality of colloidal.
By supernatant A with ceramic membrane that the flow velocity via hole diameter of 8 t/h is 8 μm temperature be 25 DEG C, pressure is for 2.5
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 10：3 volume ratio（L/L）Allocated, through 18000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 35, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 14, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 8：2：4 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：40 material liquid volume ratio（kg/L）Heating water bath is carried out at a temperature of 40 DEG C to carry
Take, leaching liquor is obtained after 36 h.
(3) after leaching liquor grinds 6 times through the colloid mill that rotor speed is 12000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 180 MPa, be then 10 in hydrolysis temperature
DEG C, enzymolysis time be 30 h under conditions of using hemicellulase digest, obtain homogeneous enzymolysis liquid；Finally use centrifuge with
The centrifugal speed of 12000 r/min respectively obtains supernatant A and filter residue to the min of enzymolysis liquid centrifugation 20.Collect supernatant
A, discards filter residue.
Wherein：Enzyme dosage is the 0.1% of the compound extracting solution quality of colloidal.
By supernatant A with ceramic membrane that the flow velocity via hole diameter of 7 t/h is 7 μm temperature be 45 DEG C, pressure is for 2 MPa
Under conditions of remove suspension, tannin, the impurity such as mucilaginous substance, collect the solution of per-meate side, obtain filtrate.
(6) by filtrate and haw juice with 7：1 volume ratio（L/L）Allocated, through 12000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 20, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 15, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 7：4：3 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：1 ~ 60 material liquid volume ratio（kg/L）Temperature be 15 ~ 60 DEG C, power be 50 W
Under conditions of carry out ultrasonic extraction, obtain leaching liquor after 0.2 ~ 36 h.
(3) after leaching liquor grinds 4 times through the colloid mill that rotor speed is 6000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 150 MPa, be then 39 in hydrolysis temperature
DEG C, enzymolysis time be 5 h under conditions of use protease hydrolyzed, obtain homogeneous enzymolysis liquid；Centrifuge is finally used with 6000
The centrifugal speed of r/min respectively obtains supernatant A and filter residue to the min of enzymolysis liquid centrifugation 10.Supernatant A is collected, is discarded
Filter residue.
Wherein：Enzyme dosage is the 0.08% of the compound extracting solution quality of colloidal.
By supernatant A with ceramic membrane that the flow velocity via hole diameter of 3 t/h is 3 μm temperature be 30 DEG C, pressure is for 3 MPa
Under conditions of remove suspension, tannin, the impurity such as mucilaginous substance, collect the solution of per-meate side, obtain filtrate.
(6) by filtrate and haw juice with 8：4 volume ratio（L/L）Allocated, be centrifuged through the centrifugal speed of 6000 r/min
Supernatant B is obtained after 10 min, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 16, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 5：2：2 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：40 material liquid volume ratio（kg/L）Heating water bath is carried out at a temperature of 40 DEG C to carry
Take, leaching liquor is obtained after 42 h.
(3) after leaching liquor grinds 4 times through the colloid mill that rotor speed is 10000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 10 MPa, be then 58 in hydrolysis temperature
DEG C, enzymolysis time be 9 h under conditions of use amylase, cellulase degradation, obtain homogeneous enzymolysis liquid；Finally using centrifugation
Machine, to the min of enzymolysis liquid centrifugation 40, respectively obtains supernatant A and filter residue with the centrifugal speed of 10000 r/min.In collection
Clear liquid A, discards filter residue.
Wherein：The mass ratio of amylase, cellulase（kg/kg）It is 1：5.
Enzyme dosage is the 0.07% of the compound extracting solution quality of colloidal.
(5) it is as 40 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 1 t/h is 0.2 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 0.03 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 7：2 volume ratio（L/L）Allocated, through 10000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 10, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 17, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 11：5：4 volume ratio（L/L）After fully mixing, obtain
Mixing juice.
(2) mixing juice is pressed 1 with water：60 material liquid volume ratio（kg/L）In the bar that temperature is 60 DEG C, power is 200 W
Ultrasonic extraction is carried out under part, leaching liquor is obtained after 36 h.
(3) after leaching liquor grinds 8 times through the colloid mill that rotor speed is 20000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 200 MPa, be then 60 in hydrolysis temperature
DEG C, enzymolysis time be 0.5 h under conditions of using amylase, hemicellulase digest, obtain homogeneous enzymolysis liquid；Finally use
Centrifuge, to the min of enzymolysis liquid centrifugation 50, respectively obtains supernatant A and filter residue with the centrifugal speed of 20000 r/min.Receive
Collection supernatant A, discards filter residue.
Wherein：The mass ratio of amylase, hemicellulase（kg/kg）It is 1：2.
Enzyme dosage is the 0.2% of the compound extracting solution quality of colloidal.
By supernatant A with ceramic membrane that the flow velocity via hole diameter of 9 t/h is 10 μm temperature be 60 DEG C, pressure is for 3
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 12：5 volume ratio（L/L）Allocated, through 20000 r/min centrifugal speed from
Obtain supernatant B after the min of the heart 40, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
A kind of black fruit fructus lycii of embodiment 18, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively, obtain black fruit fructus lycii juice,
Haw juice and lemon juice；Black fruit fructus lycii juice, haw juice and lemon juice press 4：1：1 volume ratio（L/L）After fully mixing, mixed
Close juice.
(2) mixing juice is pressed 1 with water：10 material liquid volume ratio（kg/L）Heating water bath is carried out at a temperature of 20 DEG C to carry
Take, leaching liquor is obtained after 2 h.
(3) after leaching liquor grinds 1 time through the colloid mill that rotor speed is 2000 r/min, the compound extraction of colloidal is obtained
Solution.
(4) the compound extracting solution of colloidal is carried out into homogeneous under the pressure of 10 MPa, be then 40 in hydrolysis temperature
DEG C, enzymolysis time be 16 h under conditions of use amylase, protease hydrolyzed, obtain homogeneous enzymolysis liquid；Finally using centrifugation
Machine, to the min of enzymolysis liquid centrifugation 5, respectively obtains supernatant A and filter residue with the centrifugal speed of 2000 r/min.Collect supernatant
Liquid A, discards filter residue.
Wherein：The mass ratio of amylase, protease（kg/kg）It is 1：3.
Enzyme dosage is the 0.6% of the compound extracting solution quality of colloidal.
(5) it is as 15 DEG C, pressure in temperature with the ceramic membrane that the flow velocity via hole diameter of 0.1 t/h is 0.01 μm by supernatant A
The impurity such as suspension, tannin, mucilaginous substance are removed under conditions of 0.005 MPa, the solution of per-meate side is collected, filtrate is obtained.
(6) by filtrate and haw juice with 5：1 volume ratio（L/L）Allocated, be centrifuged through the centrifugal speed of 2000 r/min
Supernatant B is obtained after 5 min, supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
Claims (6)
1. a kind of black fruit fructus lycii, hawthorn, the preparation method of lemon composite beverage, comprise the following steps：
(1) black fruit fructus lycii, hawthorn, lemon are picked into removal of impurities through artificial cleaning, treatment of squeezing the juice respectively obtains black fruit fructus lycii juice, hawthorn
Juice and lemon juice；The black fruit fructus lycii juice, haw juice and lemon juice press 4 ~ 11：1~5：After 1 ~ 4 volume ratio is fully mixed, obtain
Mixing juice；
(2) the mixing juice and water are pressed 1：1 ~ 60 material liquid volume ratio carries out heating water bath extraction at a temperature of 20 ~ 60 DEG C,
Leaching liquor is obtained after 0.2 ~ 72 h；
(3) after the leaching liquor grinds 1 ~ 8 time through colloid mill, the compound extracting solution of colloidal is obtained；
(4) after the compound extracting solution of the colloidal being carried out into homogeneous under the pressure of 1 ~ 200 MPa, through enzymolysis, centrifugation point
From respectively obtaining supernatant A and filter residue；
By the supernatant A with the flow velocity via hole diameter of 0.1 ~ 9 t/h as 0.01 ~ 10 μm ceramic membrane temperature be 15 ~ 60
DEG C, pressure be 0.005 ~ 3 MPa under conditions of removal of impurities, obtain filtrate；
By the filtrate with the haw juice with 5 ~ 12：1 ~ 5 volume ratio is allocated, and supernatant B is obtained after centrifugation, should
Supernatant B is sterilized according to a conventional method, it is filling after obtain final product.
2. as claimed in claim 1 a kind of black fruit fructus lycii, hawthorn, the preparation method of lemon composite beverage, it is characterised in that：With
(2) following preparation methods prepare leaching liquor instead of step described in claim 1：The mixing juice and water are pressed 1：1 ~ 60
Material liquid volume ratio temperature be 15 ~ 60 DEG C, power be 50 ~ 1000 W under conditions of carry out ultrasonic extraction, obtained final product after 0.2 ~ 36 h.
3. as claimed in claim 1 a kind of black fruit fructus lycii, hawthorn, the preparation method of lemon composite beverage, it is characterised in that：Institute
The rotor speed of the colloid mill in stating step (3) is 2000 ~ 20000 r/min.
4. as claimed in claim 1 a kind of black fruit fructus lycii, hawthorn, the preparation method of lemon composite beverage, it is characterised in that：Institute
(4) middle enzymatic hydrolysis condition refers to that hydrolysis temperature is 10 ~ 60 DEG C to state step, and enzymolysis time is 0.1 ~ 32 h, and the enzyme for being used is starch
One kind in enzyme, pectase, cellulase, hemicellulase, protease, two or more；Its consumption is the colloidal
The 0.01% ~ 1% of compound extracting solution quality.
5. as claimed in claim 1 a kind of black fruit fructus lycii, hawthorn, the preparation method of lemon composite beverage, it is characterised in that：Institute
The condition for stating step (4) middle centrifugation refers to that centrifugal speed is 2000 ~ 20000 r/min, and centrifugation time is 5 ~ 50 min.
6. as claimed in claim 1 a kind of black fruit fructus lycii, hawthorn, the preparation method of lemon composite beverage, it is characterised in that：Institute
The condition for stating step (6) middle centrifugation refers to that centrifugal speed is 2000 ~ 20000 r/min, and centrifugation time is 5 ~ 40 min.
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| CN105410546B (en) * | 2015-11-27 | 2018-03-09 | 魏海青 | Composite plant beverage rich in anthocyanidin and preparation method thereof |
| CN106465783A (en) * | 2016-10-12 | 2017-03-01 | 肥西久盛食品有限公司 | A kind of manufacture method of deacidification Fructus Citri Limoniae juice sugar |
| CN106360189A (en) * | 2016-10-12 | 2017-02-01 | 中国科学院西北高原生物研究所 | Lycium ruthenicum juice and preparing method thereof |
| CN110810677A (en) * | 2019-11-22 | 2020-02-21 | 中国科学院西北高原生物研究所 | Preparation method of lycium ruthenicum collagen peptide beverage |
| CN113100444A (en) * | 2021-05-17 | 2021-07-13 | 天津正大珍吾堂食品股份有限公司 | Enteral nutrition support composition for tumor patients and/or postoperative population and preparation method thereof |
| CN114009638A (en) * | 2021-11-03 | 2022-02-08 | 江苏食品药品职业技术学院 | Micro-fermented wolfberry fruit and hawthorn fruit beverage and preparation method thereof |
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