CN109287916A - A kind of preparation method of Sessileflower Acanthopanax Bark extracting solution and its beverage - Google Patents
A kind of preparation method of Sessileflower Acanthopanax Bark extracting solution and its beverage Download PDFInfo
- Publication number
- CN109287916A CN109287916A CN201811464699.1A CN201811464699A CN109287916A CN 109287916 A CN109287916 A CN 109287916A CN 201811464699 A CN201811464699 A CN 201811464699A CN 109287916 A CN109287916 A CN 109287916A
- Authority
- CN
- China
- Prior art keywords
- acanthopanax bark
- sessileflower acanthopanax
- beverage
- extracting solution
- sessileflower
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000013361 beverage Nutrition 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 41
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 24
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims abstract description 8
- UQZIYBXSHAGNOE-USOSMYMVSA-N Stachyose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@H](CO[C@@H]2[C@@H](O)[C@@H](O)[C@@H](O)[C@H](CO)O2)O1 UQZIYBXSHAGNOE-USOSMYMVSA-N 0.000 claims abstract description 8
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 8
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims abstract description 8
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims abstract description 8
- 238000011049 filling Methods 0.000 claims abstract description 8
- 239000001814 pectin Substances 0.000 claims abstract description 8
- 235000010987 pectin Nutrition 0.000 claims abstract description 8
- 229920001277 pectin Polymers 0.000 claims abstract description 8
- UQZIYBXSHAGNOE-XNSRJBNMSA-N stachyose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO[C@@H]3[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O3)O)O2)O)O1 UQZIYBXSHAGNOE-XNSRJBNMSA-N 0.000 claims abstract description 8
- 230000001954 sterilising effect Effects 0.000 claims abstract description 5
- 239000000843 powder Substances 0.000 claims description 34
- 239000000706 filtrate Substances 0.000 claims description 16
- 238000000605 extraction Methods 0.000 claims description 14
- 239000007787 solid Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 12
- 238000004108 freeze drying Methods 0.000 claims description 7
- 238000002390 rotary evaporation Methods 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 5
- 238000004659 sterilization and disinfection Methods 0.000 claims description 3
- 235000019441 ethanol Nutrition 0.000 claims 4
- 238000004090 dissolution Methods 0.000 abstract description 6
- 235000016709 nutrition Nutrition 0.000 abstract description 5
- 230000035764 nutrition Effects 0.000 abstract description 5
- 239000000470 constituent Substances 0.000 abstract description 3
- 230000002929 anti-fatigue Effects 0.000 abstract description 2
- 239000008280 blood Substances 0.000 abstract description 2
- 210000004369 blood Anatomy 0.000 abstract description 2
- 239000000796 flavoring agent Substances 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 abstract description 2
- 230000036039 immunity Effects 0.000 abstract description 2
- 150000002632 lipids Chemical class 0.000 abstract description 2
- -1 oligofructose Chemical compound 0.000 abstract description 2
- 235000015165 citric acid Nutrition 0.000 abstract 1
- 238000007598 dipping method Methods 0.000 abstract 1
- 239000002304 perfume Substances 0.000 description 6
- 235000009508 confectionery Nutrition 0.000 description 5
- 230000001376 precipitating effect Effects 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- HOEVRHHMDJKUMZ-UHFFFAOYSA-N Isofraxidin Chemical compound C1=CC(=O)OC2=C1C=C(OC)C(O)=C2OC HOEVRHHMDJKUMZ-UHFFFAOYSA-N 0.000 description 2
- ANCHXLMTFNOVDK-UHFFFAOYSA-N Isofraxidin Natural products COC1=C(O)C(OC)=CC2=C1OC=CC2=O ANCHXLMTFNOVDK-UHFFFAOYSA-N 0.000 description 2
- 244000269722 Thea sinensis Species 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000001151 other effect Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 244000167222 Acanthopanax sessiliflorus Species 0.000 description 1
- 235000017615 Acanthopanax sessiliflorus Nutrition 0.000 description 1
- 244000144730 Amygdalus persica Species 0.000 description 1
- 241000208340 Araliaceae Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- OVSQVDMCBVZWGM-SJWGPRHPSA-N Hyperin Natural products O[C@H]1[C@H](O)[C@@H](O)[C@@H](CO)O[C@H]1OC1=C(C=2C=C(O)C(O)=CC=2)OC2=CC(O)=CC(O)=C2C1=O OVSQVDMCBVZWGM-SJWGPRHPSA-N 0.000 description 1
- FVQOMEDMFUMIMO-UHFFFAOYSA-N Hyperosid Natural products OC1C(O)C(O)C(CO)OC1OC1C(=O)C2=C(O)C=C(O)C=C2OC1C1=CC=C(O)C(O)=C1 FVQOMEDMFUMIMO-UHFFFAOYSA-N 0.000 description 1
- 235000006040 Prunus persica var persica Nutrition 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 235000021022 fresh fruits Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- NQYPTLKGQJDGTI-FCVRJVSHSA-N hyperoside Natural products OC[C@H]1O[C@@H](OC2=C(Oc3cc(O)cc(O)c3[C@H]2O)c4ccc(O)c(O)c4)[C@H](O)[C@@H](O)[C@H]1O NQYPTLKGQJDGTI-FCVRJVSHSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- OVSQVDMCBVZWGM-DTGCRPNFSA-N quercetin 3-O-beta-D-galactopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1OC1=C(C=2C=C(O)C(O)=CC=2)OC2=CC(O)=CC(O)=C2C1=O OVSQVDMCBVZWGM-DTGCRPNFSA-N 0.000 description 1
- BBFYUPYFXSSMNV-UHFFFAOYSA-N quercetin-7-o-galactoside Natural products OC1C(O)C(O)C(CO)OC1OC1=CC(O)=C2C(=O)C(O)=C(C=3C=C(O)C(O)=CC=3)OC2=C1 BBFYUPYFXSSMNV-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Botany (AREA)
- Mycology (AREA)
- Non-Alcoholic Beverages (AREA)
- Medicinal Preparation (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention provides the preparation methods of a kind of Sessileflower Acanthopanax Bark extracting solution and its beverage, and technical characteristic is: Sessileflower Acanthopanax Bark dry fruit being crushed, is extracted with alcohol solution dipping, filters, be concentrated, dry, is dissolved in water to obtain Sessileflower Acanthopanax Bark extracting solution；Sessileflower Acanthopanax Bark extracting solution is uniformly mixed with stachyose, oligofructose, citric acid, pectin, carboxymethyl cellulose, be sieved, after sterilizing it is filling to get arrive Sessileflower Acanthopanax Bark beverage.Preparation method provided by the invention, effective component dissolution rate is high, improves the utilization rate of Sessileflower Acanthopanax Bark nutrition and active constituent；Product color, flavor and taste are all good, and stability is good；With improve the immunity of the human body, antifatigue, to adjust multiple efficacies, the target user such as blood lipid extensive.
Description
Technical field
The present invention relates to technical field of food beverage, and in particular to it is a kind of using Sessileflower Acanthopanax Bark dry fruit prepare extracting solution and its
The method of beverage.
Background technique
Sessileflower Acanthopanax Bark is Araliaceae Acanthopanax typical case's medicinal plant, belongs to perennial machaka, north native to China
Portion, eastern region.Sessileflower Acanthopanax Bark is on the books in Shennong's Herbal, Compendium of Material Medica, is listed in top grade, in China, Russia
The ground such as Ross, South Korea are widely applied for a long time as a kind of traditional medicine.Sessileflower Acanthopanax Bark contain flavones, lignanoid, organic acid,
A variety of active ingredients such as volatile oil, pigment, while rich in the microelements such as selenium, iron, calcium, zinc, have antifatigue, protection liver,
Anticancer, anti-inflammatory, tranquilizing the mind and other effects.
Sessileflower Acanthopanax Bark is approved as new raw-food material (new resource food) by health ministry bulletin in December, 2008, becomes
The high-quality resource of new type functional food has been developed as the production such as Sessileflower Acanthopanax Bark alternative tea, acanthopanax sessiliflorus white spirit, health liquor at present
Product.But at present Sessileflower Acanthopanax Bark extraction be mostly fresh fruit directly squeeze the juice or hot water extract, effective component dissolution limited, nutriture value
Value and health-care effect are not fully used, meanwhile, alternative tea, alcohol product are limited using crowd, and field is single, production rule
Mould is smaller.Therefore, the present invention is on the basis of improving the dissolution of Sessileflower Acanthopanax Bark effective component, by the compound allotment of auxiliary material, to open
Issue that a kind of dissolution of effective component is more, and color is various, and target user is extensive, with healthcare function, short stalk full of nutrition
Slender acanthopanax beverage.
Summary of the invention
Extracting solution is prepared using Sessileflower Acanthopanax Bark dry fruit it is an object of the invention to overcome the deficiencies of the prior art and provide a kind of
And the method for beverage, Sessileflower Acanthopanax Bark extracting solution produced by the present invention, effective component dissolution rate is high, improve Sessileflower Acanthopanax Bark nutrition and
The utilization rate of active constituent；Sessileflower Acanthopanax Bark beverage obtained, color is various, and target user is extensive, has preferable nutrition
And healthcare function.
To achieve the goals above, the technical solution adopted by the present invention includes the following steps:
Step 1 prepares Sessileflower Acanthopanax Bark extracting solution:
A. Sessileflower Acanthopanax Bark dry fruit is crushed, crosses 80 meshes, obtains Sessileflower Acanthopanax Bark powder；
B. the ethanol solution of 5 times of weight is added into the Sessileflower Acanthopanax Bark powder that step a is obtained, under the conditions of 70 DEG C of temperature, stirring leaching
Bubble filters after extracting 10h, and it is spare to collect filtrate；The ethanol solution of 5 times of weight is added again into filtered filter residue, at 70 DEG C
Under the conditions of temperature, is filtered after stirring soak extraction 10h, collect and merge filtrate twice；
C. the obtained merging filtrate of step b is placed in rotary evaporation devices, is concentrated under reduced pressure into medicinal extract state, freeze-drying, powder
It is broken to obtain Sessileflower Acanthopanax Bark solid powder；
D. Sessileflower Acanthopanax Bark solid powder step c obtained, is dissolved in water according to the ratio of solid-liquid ratio 1:5, crosses 200 mesh screens,
Obtain Sessileflower Acanthopanax Bark extracting solution；
The ethanol solution is the food-grade ethanol solution that volume fraction is 20-30%.
Step 2 prepares Sessileflower Acanthopanax Bark beverage:
A. according to the mass fraction, 96.7-98.4 parts of Sessileflower Acanthopanax Bark extracting solution are taken, 0.2-0.4 parts of stachyose, oligofructose 0.5-1
Part, it 0.5-1 parts of citric acid, 0.1-0.3 parts of pectin, 0.3-0.6 parts of carboxymethyl cellulose, is uniformly mixed;
B. the resulting mixed liquor of step a is crossed into 200 mesh screens, sterilized, it is filling, Sessileflower Acanthopanax Bark beverage is made.
The sterilization process is high-temperature short-time sterilization 6-8 seconds under the conditions of 130-135 DEG C.
Beneficial effects of the present invention:
The present invention is using Sessileflower Acanthopanax Bark dry fruit as raw material, and by the optimization of extraction process and parameter, improving Sessileflower Acanthopanax Bark dry fruit has
The dissolution rate for imitating ingredient, improves the utilization rate of Sessileflower Acanthopanax Bark nutrition and active constituent；Improving, Sessileflower Acanthopanax Bark effective component is molten
On the basis of out, by the compound allotment of auxiliary material, sensory properties is improved, product color, flavor and taste are all good, stability
It is good, while the nutritive value and health-care efficacy of product are further enhanced, products obtained therefrom is tired with improving the immunity of the human body, resisting
Labor, adjusting blood lipid and other effects, are suitable for various sub-health populations, applied widely.
Specific embodiment
Technical solution of the present invention is described further below with reference to embodiment:
Embodiment one
The preparation method of a kind of Sessileflower Acanthopanax Bark extracting solution and its beverage, includes the following steps:
Step 1 prepares Sessileflower Acanthopanax Bark extracting solution:
A. Sessileflower Acanthopanax Bark dry fruit is crushed, crosses 80 meshes, obtains Sessileflower Acanthopanax Bark powder；
B. 5 times of weight are added into the Sessileflower Acanthopanax Bark powder that step a is obtained, the ethanol solution that volume fraction is 20%, in 70 DEG C of temperature
Under the conditions of, it is filtered after stirring soak extraction 10h, it is spare to collect filtrate；5 times of weight, bodies are added again into filtered filter residue
The ethanol solution that fraction is 20% filters after stirring soak extraction 10h under the conditions of 70 DEG C of temperature, collects and merge and filter twice
Liquid；
C. the obtained merging filtrate of step b is placed in rotary evaporation devices, is concentrated under reduced pressure into medicinal extract state, freeze-drying, powder
It is broken to obtain Sessileflower Acanthopanax Bark solid powder；
D. Sessileflower Acanthopanax Bark solid powder step c obtained, is dissolved in water according to the ratio of solid-liquid ratio 1:5, crosses 200 mesh screens,
Obtain Sessileflower Acanthopanax Bark extracting solution；
Step 2 prepares Sessileflower Acanthopanax Bark beverage:
A. according to the mass fraction, 97 parts of Sessileflower Acanthopanax Bark extracting solution are taken, 0.4 part of stachyose, 0.9 part of oligofructose, citric acid 0.9
Part, it 0.3 part of pectin, 0.5 part of carboxymethyl cellulose, is uniformly mixed;
B. the resulting mixed liquor of step a is crossed into 200 mesh screens, 135 DEG C sterilize 6 seconds, and it is filling, Sessileflower Acanthopanax Bark beverage is made.
Embodiment two
The preparation method of a kind of Sessileflower Acanthopanax Bark extracting solution and its beverage, includes the following steps:
Step 1 prepares Sessileflower Acanthopanax Bark extracting solution:
A. Sessileflower Acanthopanax Bark dry fruit is crushed, crosses 80 meshes, obtains Sessileflower Acanthopanax Bark powder；
B. 5 times of weight are added into the Sessileflower Acanthopanax Bark powder that step a is obtained, the ethanol solution that volume fraction is 25%, in 70 DEG C of temperature
Under the conditions of, it is filtered after stirring soak extraction 10h, it is spare to collect filtrate；5 times of weight, bodies are added again into filtered filter residue
The ethanol solution that fraction is 25% filters after stirring soak extraction 10h under the conditions of 70 DEG C of temperature, collects and merge and filter twice
Liquid；
C. the obtained merging filtrate of step b is placed in rotary evaporation devices, is concentrated under reduced pressure into medicinal extract state, freeze-drying, powder
It is broken to obtain Sessileflower Acanthopanax Bark solid powder；
D. Sessileflower Acanthopanax Bark solid powder step c obtained, is dissolved in water according to the ratio of solid-liquid ratio 1:5, crosses 200 mesh screens,
Obtain Sessileflower Acanthopanax Bark extracting solution；
Step 2 prepares Sessileflower Acanthopanax Bark beverage:
A. according to the mass fraction, 98.2 parts of Sessileflower Acanthopanax Bark extracting solution are taken, 0.3 part of stachyose, 0.5 part of oligofructose, citric acid 0.5
Part, it 0.1 part of pectin, 0.4 part of carboxymethyl cellulose, is uniformly mixed;
B. the resulting mixed liquor of step a is crossed into 200 mesh screens, 130 DEG C sterilize 8 seconds, and it is filling, Sessileflower Acanthopanax Bark beverage is made.
Embodiment three
The preparation method of a kind of Sessileflower Acanthopanax Bark extracting solution and its beverage, includes the following steps:
Step 1 prepares Sessileflower Acanthopanax Bark extracting solution:
A. Sessileflower Acanthopanax Bark dry fruit is crushed, crosses 80 meshes, obtains Sessileflower Acanthopanax Bark powder；
B. 5 times of weight are added into the Sessileflower Acanthopanax Bark powder that step a is obtained, the ethanol solution that volume fraction is 22%, in 70 DEG C of temperature
Under the conditions of, it is filtered after stirring soak extraction 10h, it is spare to collect filtrate；5 times of weight, bodies are added again into filtered filter residue
The ethanol solution that fraction is 22% filters after stirring soak extraction 10h under the conditions of 70 DEG C of temperature, collects and merge and filter twice
Liquid；
C. the obtained merging filtrate of step b is placed in rotary evaporation devices, is concentrated under reduced pressure into medicinal extract state, freeze-drying, powder
It is broken to obtain Sessileflower Acanthopanax Bark solid powder；
D. Sessileflower Acanthopanax Bark solid powder step c obtained, is dissolved in water according to the ratio of solid-liquid ratio 1:5, crosses 200 mesh screens,
Obtain Sessileflower Acanthopanax Bark extracting solution；
Step 2 prepares Sessileflower Acanthopanax Bark beverage:
A. according to the mass fraction, 97.5 parts of Sessileflower Acanthopanax Bark extracting solution are taken, 0.2 part of stachyose, 0.7 part of oligofructose, citric acid 0.7
Part, it 0.3 part of pectin, 0.6 part of carboxymethyl cellulose, is uniformly mixed;
B. the resulting mixed liquor of step a is crossed into 200 mesh screens, 132 DEG C sterilize 7 seconds, and it is filling, Sessileflower Acanthopanax Bark beverage is made.
Example IV
The preparation method of a kind of Sessileflower Acanthopanax Bark extracting solution and its beverage, includes the following steps:
Step 1 prepares Sessileflower Acanthopanax Bark extracting solution:
A. Sessileflower Acanthopanax Bark dry fruit is crushed, crosses 80 meshes, obtains Sessileflower Acanthopanax Bark powder；
B. 5 times of weight are added into the Sessileflower Acanthopanax Bark powder that step a is obtained, the ethanol solution that volume fraction is 28%, in 70 DEG C of temperature
Under the conditions of, it is filtered after stirring soak extraction 10h, it is spare to collect filtrate；5 times of weight, bodies are added again into filtered filter residue
The ethanol solution that fraction is 28% filters after stirring soak extraction 10h under the conditions of 70 DEG C of temperature, collects and merge and filter twice
Liquid；
C. the obtained merging filtrate of step b is placed in rotary evaporation devices, is concentrated under reduced pressure into medicinal extract state, freeze-drying, powder
It is broken to obtain Sessileflower Acanthopanax Bark solid powder；
D. Sessileflower Acanthopanax Bark solid powder step c obtained, is dissolved in water according to the ratio of solid-liquid ratio 1:5, crosses 200 mesh screens,
Obtain Sessileflower Acanthopanax Bark extracting solution；
Step 2 prepares Sessileflower Acanthopanax Bark beverage:
A. according to the mass fraction, 98 parts of Sessileflower Acanthopanax Bark extracting solution are taken, 0.3 part of stachyose, 0.6 part of oligofructose, citric acid 0.6
Part, it 0.2 part of pectin, 0.3 part of carboxymethyl cellulose, is uniformly mixed;
B. the resulting mixed liquor of step a is crossed into 200 mesh screens, 135 DEG C sterilize 6 seconds, and it is filling, Sessileflower Acanthopanax Bark beverage is made.
Embodiment five
The preparation method of a kind of Sessileflower Acanthopanax Bark extracting solution and its beverage, includes the following steps:
Step 1 prepares Sessileflower Acanthopanax Bark extracting solution:
A. Sessileflower Acanthopanax Bark dry fruit is crushed, crosses 80 meshes, obtains Sessileflower Acanthopanax Bark powder；
B. 5 times of weight are added into the Sessileflower Acanthopanax Bark powder that step a is obtained, the ethanol solution that volume fraction is 30%, in 70 DEG C of temperature
Under the conditions of, it is filtered after stirring soak extraction 10h, it is spare to collect filtrate；5 times of weight, bodies are added again into filtered filter residue
The ethanol solution that fraction is 30% filters after stirring soak extraction 10h under the conditions of 70 DEG C of temperature, collects and merge and filter twice
Liquid；
C. the obtained merging filtrate of step b is placed in rotary evaporation devices, is concentrated under reduced pressure into medicinal extract state, freeze-drying, powder
It is broken to obtain Sessileflower Acanthopanax Bark solid powder；
D. Sessileflower Acanthopanax Bark solid powder step c obtained, is dissolved in water according to the ratio of solid-liquid ratio 1:5, crosses 200 mesh screens,
Obtain Sessileflower Acanthopanax Bark extracting solution；
Step 2 prepares Sessileflower Acanthopanax Bark beverage:
A. according to the mass fraction, 96.7 parts of Sessileflower Acanthopanax Bark extracting solution are taken, 0.4 part of stachyose, 1.0 parts of oligofructose, citric acid 1.0
Part, it 0.3 part of pectin, 0.6 part of carboxymethyl cellulose, is uniformly mixed;
B. the resulting mixed liquor of step a is crossed into 200 mesh screens, 130 DEG C sterilize 7 seconds, and it is filling, Sessileflower Acanthopanax Bark beverage is made.
Test example one
Subjective appreciation is carried out to the resulting Sessileflower Acanthopanax Bark beverage of embodiment one to five and stability test, specific evaluation result are as follows
Shown in table:
| Embodiment | Mouthfeel | Appearance | Stand 12 months |
| Embodiment one | Sweet mouthfeel is moderate, there is the unique perfume of Sessileflower Acanthopanax Bark | Transparent red | Without precipitating |
| Embodiment two | Sweet mouthfeel is moderate, there is the unique perfume of Sessileflower Acanthopanax Bark | Transparent red | Without precipitating |
| Embodiment three | Sweet mouthfeel is moderate, there is the unique perfume of Sessileflower Acanthopanax Bark | Transparent red | Without precipitating |
| Example IV | Sweet mouthfeel is moderate, there is the unique perfume of Sessileflower Acanthopanax Bark | Transparent red | Without precipitating |
| Embodiment five | Sweet mouthfeel is moderate, there is the unique perfume of Sessileflower Acanthopanax Bark | Transparent red | Without precipitating |
Test example two
Significant functional component content in Sessileflower Acanthopanax Bark beverage is measured, as a result as shown in the table:
| Group | Hyperoside (μ g/100ml) | Isofraxidin (μ g/100ml) |
| Embodiment one | 17.5 | 6.8 |
| Embodiment two | 21.6 | 9.8 |
| Embodiment three | 19.5 | 9.3 |
| Example IV | 23.5 | 8.8 |
| Embodiment five | 25.1 | 7.7 |
By the resulting Sessileflower Acanthopanax Bark beverage of embodiment one to five, meet the standard requirements of GB7101-2015 beverage, sweet mouthfeel
Moderate, the unique perfume with Sessileflower Acanthopanax Bark, appearance is transparent red；Wherein, main function component content index is as follows: gold
Silk peach glycosides content >=17 μ g/100ml, Determination of isofraxidin >=6 μ g/100ml.
Claims (3)
1. the preparation method of a kind of Sessileflower Acanthopanax Bark extracting solution and its beverage, which comprises the steps of:
Step 1 prepares Sessileflower Acanthopanax Bark extracting solution:
Sessileflower Acanthopanax Bark dry fruit is crushed, 80 meshes is crossed, obtains Sessileflower Acanthopanax Bark powder；
The ethanol solution of 5 times of weight is added into the Sessileflower Acanthopanax Bark powder that step a is obtained, under the conditions of 70 DEG C of temperature, stirring is impregnated
It is filtered after extracting 10h, it is spare to collect filtrate；The ethanol solution of 5 times of weight is added again into filtered filter residue, in 70 DEG C of temperature
Under the conditions of degree, is filtered after stirring soak extraction 10h, collect and merge filtrate twice；
The obtained merging filtrate of step b is placed in rotary evaporation devices, medicinal extract state is concentrated under reduced pressure into, freeze-drying crushes
Obtain Sessileflower Acanthopanax Bark solid powder；
The Sessileflower Acanthopanax Bark solid powder that step c is obtained, is dissolved in water according to the ratio of solid-liquid ratio 1:5, crosses 200 mesh screens, obtains
To Sessileflower Acanthopanax Bark extracting solution；
Step 2 prepares Sessileflower Acanthopanax Bark beverage:
According to the mass fraction, 96.7-98.4 parts of Sessileflower Acanthopanax Bark extracting solution are taken, 0.2-0.4 parts of stachyose, 0.5-1 parts of oligofructose,
It 0.5-1 parts of citric acid, 0.1-0.3 parts of pectin, 0.3-0.6 parts of carboxymethyl cellulose, is uniformly mixed;
The resulting mixed liquor of step a is crossed into 200 mesh screens, is sterilized, it is filling, Sessileflower Acanthopanax Bark beverage is made.
2. the preparation method of Sessileflower Acanthopanax Bark extracting solution according to claim 1 and its beverage, which is characterized in that the ethyl alcohol
Solution is the food-grade ethanol solution that volume fraction is 20-30%.
3. the preparation method of Sessileflower Acanthopanax Bark extracting solution according to claim 1 and its beverage, which is characterized in that the sterilizing
Process is high-temperature short-time sterilization 6-8 seconds under the conditions of 130-135 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811464699.1A CN109287916A (en) | 2018-12-03 | 2018-12-03 | A kind of preparation method of Sessileflower Acanthopanax Bark extracting solution and its beverage |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811464699.1A CN109287916A (en) | 2018-12-03 | 2018-12-03 | A kind of preparation method of Sessileflower Acanthopanax Bark extracting solution and its beverage |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109287916A true CN109287916A (en) | 2019-02-01 |
Family
ID=65142283
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811464699.1A Pending CN109287916A (en) | 2018-12-03 | 2018-12-03 | A kind of preparation method of Sessileflower Acanthopanax Bark extracting solution and its beverage |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109287916A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111165701A (en) * | 2019-11-28 | 2020-05-19 | 重庆市药物种植研究所 | Anti-fatigue beverage |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101214270A (en) * | 2007-12-29 | 2008-07-09 | 哈尔滨仁皇药业股份有限公司 | Acanthopanax senticosus effective fraction extract, preparation and application thereof |
| CN107137439A (en) * | 2017-07-06 | 2017-09-08 | 吉林省农业科学院 | The application of fruit of Acanthopanax sessiliflorus polyphenol |
| CN107156841A (en) * | 2017-05-19 | 2017-09-15 | 丹东五加生物科技有限公司 | Sessileflower Acanthopanax Bark extract solution, the application of Sessileflower Acanthopanax Bark extract solution and Sessileflower Acanthopanax Bark beverage and preparation method thereof |
| CN108497082A (en) * | 2017-06-16 | 2018-09-07 | 北京工业大学 | The formula and preparation method of two kinds of wilsonii solid beverages |
-
2018
- 2018-12-03 CN CN201811464699.1A patent/CN109287916A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101214270A (en) * | 2007-12-29 | 2008-07-09 | 哈尔滨仁皇药业股份有限公司 | Acanthopanax senticosus effective fraction extract, preparation and application thereof |
| CN107156841A (en) * | 2017-05-19 | 2017-09-15 | 丹东五加生物科技有限公司 | Sessileflower Acanthopanax Bark extract solution, the application of Sessileflower Acanthopanax Bark extract solution and Sessileflower Acanthopanax Bark beverage and preparation method thereof |
| CN108497082A (en) * | 2017-06-16 | 2018-09-07 | 北京工业大学 | The formula and preparation method of two kinds of wilsonii solid beverages |
| CN107137439A (en) * | 2017-07-06 | 2017-09-08 | 吉林省农业科学院 | The application of fruit of Acanthopanax sessiliflorus polyphenol |
Non-Patent Citations (1)
| Title |
|---|
| 郝婧玮等: "短梗五加果实中异嗪皮啶的提取工艺研究", 《吉林农业》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111165701A (en) * | 2019-11-28 | 2020-05-19 | 重庆市药物种植研究所 | Anti-fatigue beverage |
| CN111165701B (en) * | 2019-11-28 | 2022-07-22 | 重庆市药物种植研究所 | Anti-fatigue beverage |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR100730647B1 (en) | Aged Concentrate of Ginseng Steamed Red, and a Preparation Method Thereof | |
| CN102048003B (en) | Soyabean coat herbal tea and preparation method thereof | |
| CN104186858A (en) | Herbal tea raw material formula, bagged tea, herbal tea and preparation method of herbal tea | |
| CN103540493A (en) | Preparation method of ganoderma lucidum tea wine | |
| CN103918830A (en) | Warming tea beverage | |
| CN107348090B (en) | Ginseng candy capable of preserving health and tonifying kidney and preparation method thereof | |
| CN104336230A (en) | Mulberry leaf sweet tea and preparation method thereof | |
| CN101366519B (en) | Hippophae rhamnoides flavone nourishing tea/powder and preparation process | |
| CN108991215A (en) | A kind of Yunnan olive preserved fruit and preparation method thereof | |
| KR101060309B1 (en) | Restorative herb medicine with jujube and manufacturing method thereof | |
| CN103859521B (en) | Natural drinks of a kind of Morinda and preparation method thereof | |
| CN107287074A (en) | The preparation method of the Hakkas's wine brewing | |
| KR20130104100A (en) | Method for producing red ginseng extract comprising medicinal herbs concentrate and plant extract | |
| CN103734345A (en) | Edible houseleek healthcare soybean milk and preparation method thereof | |
| KR20160006427A (en) | The health functional food for children comprising herbal plant treated by traditional processing | |
| KR20110056908A (en) | Composition of mixed herb medicine for leached tea | |
| CN103828981A (en) | Hemp tea | |
| CN109287916A (en) | A kind of preparation method of Sessileflower Acanthopanax Bark extracting solution and its beverage | |
| CN105661207A (en) | Compound vegetable and fruit juice beverage for enhancing immunity and making method thereof | |
| KR101409168B1 (en) | Method for manufacturing red ginseng extract with enhanced function and the extact thereof | |
| KR20170061961A (en) | Manufacturing method of liquors | |
| CN104489195A (en) | Lotus leaf-fresh ginger tea capable of reducing blood fat | |
| CN104605439A (en) | Mulberry and sharpleaf galangal fruit beverage and preparation method thereof | |
| CN104397786A (en) | Liquid-engendering and fat-reducing tea soup granule and making method thereof | |
| CN110772456B (en) | Miracle fruit leaf compound and application thereof in anti-melanin formation product |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190201 |
|
| RJ01 | Rejection of invention patent application after publication |