Summary of the invention
The invention provides a kind of with the integration of drinking and medicinal herbs Chinese herbal medicines such as matrimony vine, marine alga, red date be raw material functional health vinegar beverage and production technology thereof, this beverage products have promote the production of body fluid to quench thirst, the effect such as liver-protecting and alcoholism-relieving, be a kind of both effectiveness good, mouthfeel is good, commodity property is good functional health vinegar beverage, pursue the multi-level requirement such as mouthfeel, nutrition, health care to meet people.
For achieving the above object, technical scheme of the present invention is as follows:
One protects liver herbal health care vinegar beverage, it is characterized in that, the herbal raw material selected and mass ratio are: marine alga 25 ~ 35 parts, red date 17 ~ 23 parts, matrimony vine 15 ~ 25 parts, STEVIA REBAUDIANA 10 ~ 20 parts, umbellate pore furgus 8 ~ 12 parts, 4 ~ 6 parts, peach kernel.
Vinegar method processed yields poorly, the production cycle is long, labour intensity is large, raw material availability is low and the technology drawback of liquid fermentation method product special flavour difference for solid-state, the invention provides one and protect liver herbal health care vinegar beverage production technology, it is characterized in that solid-state, liquid state fermentation coexists zymotechnique.Specifically comprise the following steps:
(1) get the raw materials ready: get the raw materials ready according to aforementioned proportion, remove infested raw material;
(2) pretreatment of raw material: the different qualities according to raw material carries out pretreatment of raw material respectively:
marine alga: by the marine alga peeling after cleaning, adopt first to add in 0.02% sodium sulfite solution after 90 DEG C of blanching 2 ~ 3min and soak lh and carry out color retention, add 2 ~ 3 times of water making beating, add the AMS of 1.5 ~ 2%, liquefy under 60 ~ 70 DEG C of conditions 20 ~ 30min;
red date, matrimony vine: after the red date after cleaning, matrimony vine adds 1.5 ~ 2 times of water, and making beating, adds pectase in 0.2 ~ 0.4g/100mL ratio, enzymolysis 1.5 ~ 2h under 45 ~ 50 DEG C of conditions;
umbellate pore furgus, STEVIA REBAUDIANA, peach kernel: the umbellate pore furgus after cleaning, STEVIA REBAUDIANA, peach kernel are pulverized, crosses 40 mesh sieves;
(3) batch mixing: by raw material mixing every in step (2), add water to solid-to-liquid ratio 1:5 ~ 8, and add 0.15 ~ 0.20% ammonium sulfate, 0.05 ~ 0.08% potassium dihydrogen phosphate, 0.02 ~ 0.03% magnesium sulfate;
(4) enzymolysis: add amylase, carbohydrase, cellulase respectively in 0.1 ~ 0.2g/100mL, 0.4 ~ 0.8g/100mL, 0.2 ~ 0.4g/100mL ratio, then at 40 ~ 60 DEG C, coordinated enzymatic hydrolysis 2 ~ 3h under stirring condition;
(5) alcoholic fermentation: regulate initial total sugar degree 13 ~ 15BX after enzymolysis, inoculation saccharomyces cerevisiae, inoculum concentration 6 ~ 8%, then (supernatant liquid stirs fermentation to carry out alcoholic fermentation, lower floor's solid standing for fermentation, 12h stirs once), at 20 ~ 28 DEG C of condition bottom fermentation 36 ~ 48h;
(6) acetic fermentation: inoculate acetic acid bacteria after alcoholic fermentation, inoculum concentration 8 ~ 10%, standing for fermentation 72 ~ 96h under 28 ~ 32 DEG C of conditions;
(7) be separated: be separated after fermentation ends, obtain acetic acid fermentation liquid;
(8) spray: to the solid spray be separated, acetic acid and other functional activity materials are leached as far as possible, and merging spray liquid and zymotic fluid obtain acetate solution;
(9) ageing: ageing 20 ~ 30 days under normal temperature condition;
(10) filter: adopt diatomite filtration;
(11) allocate: the total acid content 1.0 ~ 2.0% adjusting above-mentioned acetate solution, and add 1.0 ~ 1.5% sweeteners, 0.1% citric acid, 0.15 ~ 0.02% calcium lactate, 1 ~ 2% xanthans, 0.01 ~ 0.02% sodium Diacetate;
(12) homogeneous: deployed beverage is placed in homogenizer, at homogenization pressure 25MPa, homogeneous at temperature 60 ~ 70 DEG C, makes various nutritional labeling homogenising, prevents product from occurring layering and precipitating, product stability is further ensured;
(13) essence filter: the functional health vinegar beverage after homogeneous is first filtered through 200 order duplex strainers, then through the filter of diatom filter essence with removing impurity wherein and not tolerant;
(14) sterilization: deployed functional health vinegar beverage carries out high-temperature short-time sterilization, sterilising temp is 120 ~ 140 DEG C, and the time is 4 ~ 6s;
(15) filling: adopt vacuum filling, vacuum is 0.04-0.05Mpa, and filling temperature controls at 60-75 DEG C, then is cooled to normal temperature and gets product.
According to above-mentioned zymotechnique, before alcoholic fermentation process, do not carry out the Separation of Solid and Liquid of zymotic fluid.
In above-mentioned (11) adaptation step, sweetener is one or more in oligoisomaltose, sucrose, xylitol.
The invention provides one and protect liver herbal health care vinegar beverage, product color is reddish brown, sweet and sour taste, mellow in taste, and juice is limpid bright, free from admixture; Not only remain red date, the original local flavor of matrimony vine, also possessed sour and the flavor substance such as ester class that fermentable produces, have promote the production of body fluid to quench thirst, the effect such as liver-protecting and alcoholism-relieving.Results of animal shows more than 2 times of liver-protecting and alcoholism-relieving effect of health-care vinegar beverage of the present invention, and Chinese herbal medicine proportioning and zymotechnique process all can protect the significant impact of effect generation of liver herbal health care vinegar beverage on the application.
The invention provides one and protect liver herbal health care vinegar beverage, it is advantageous that: one is that employing is solid-state, liquid state fermentation coexists zymotechnique, mix solid state fermentation raciness and liquid state fermentation output is high, with short production cycle, labour intensity is low, product health is good advantage, shorten fermentation time more than 10 days, local flavor reaches solid fermentation level; Two is do not carry out Separation of Solid and Liquid in product sweat, extend the extraction time of Chinese herbal medicine active component, and the leaching of active component is accelerated by the fermentation of microorganism, 23.94% is reduced compared to extracting technology solid content, this shows that more Chinese herbal medicine functional activity material enters into health-care vinegar beverage, compared the liver-protecting and alcoholism-relieving effect under two kinds of process conditions by animal experiment, the former is 1.86 times of the latter, achieves unforeseeable technique effect; Three is contain STEVIA REBAUDIANA in raw material, is a kind of good natural sweetener, and has effect of lowering blood sugar, make product be more suitable for patients with diabetes mellitus; Four is do not have Chinese herbal medicine extracting technology in production technology, reduces production cost, is convenient to suitability for industrialized production.
Detailed description of the invention
embodiment 1:
One protects liver herbal health care vinegar beverage, and its concrete production technology is as follows:
(1) get the raw materials ready: get the raw materials ready according to marine alga 35 parts, red date 17 parts, matrimony vine 25 parts, STEVIA REBAUDIANA 10 parts, umbellate pore furgus 8 parts, peach kernel 5 parts of ratios, remove infested raw material;
(2) pretreatment of raw material: the different qualities according to raw material carries out pretreatment of raw material respectively:
marine alga: by the marine alga peeling after cleaning, adopt first to add in 0.02% sodium sulfite solution after 90 DEG C of blanching 3min and soak lh and carry out color retention, add 3 times of water making beating, add the AMS of 1.5%, liquefy under 60 ~ 70 DEG C of conditions 20 ~ 30min;
red date, matrimony vine: after the red date after cleaning, matrimony vine adds 2 times of water, and making beating, adds pectase in 0.4g/100mL ratio, enzymolysis 1.5 ~ 2h under 45 ~ 50 DEG C of conditions;
umbellate pore furgus, STEVIA REBAUDIANA, peach kernel: the umbellate pore furgus after cleaning, STEVIA REBAUDIANA, peach kernel are pulverized, crosses 40 mesh sieves;
(3) batch mixing: by raw material mixing every in step (2), add water to solid-to-liquid ratio 1:8, and add 0.15% ammonium sulfate, 0.05% potassium dihydrogen phosphate, 0.02% magnesium sulfate;
(4) enzymolysis: add amylase, carbohydrase, cellulase respectively in 0.1g/100mL, 0.4g/100mL, 0.2g/100mL ratio, then at 40 ~ 60 DEG C, coordinated enzymatic hydrolysis 2 ~ 3h under stirring condition;
(5) alcoholic fermentation: regulate initial total sugar degree 13 ~ 15BX after enzymolysis, inoculation saccharomyces cerevisiae (commercially available Angel saccharomyces cerevisiae), inoculum concentration 8%, then (supernatant liquid stirs fermentation to carry out alcoholic fermentation, lower floor's solid standing for fermentation, 12h stirs once), at 20 ~ 28 DEG C of condition bottom fermentation 36 ~ 48h;
(6) acetic fermentation: inoculate acetic acid bacteria after alcoholic fermentation, inoculum concentration 10%, standing for fermentation 72 ~ 96h under 28 ~ 32 DEG C of conditions;
(7) be separated: be separated after fermentation ends, obtain acetic acid fermentation liquid;
(8) spray: to the solid spray be separated, acetic acid and other functional activity materials are leached as far as possible, and merging spray liquid and zymotic fluid obtain acetate solution;
(9) ageing: ageing 20 ~ 30 days under normal temperature condition;
(10) filter: adopt diatomite filtration;
(11) allocate: the total acid content 1.0 ~ 2.0% adjusting above-mentioned acetate solution, and add 1.0% oligoisomaltose, 0.1% citric acid, 0.02% calcium lactate, 1% xanthans, 0.02% sodium Diacetate;
(12) homogeneous: deployed beverage is placed in homogenizer, at homogenization pressure 25MPa, homogeneous at temperature 60 ~ 70 DEG C, makes various nutritional labeling homogenising, prevents product from occurring layering and precipitating, product stability is further ensured;
(13) essence filter: the functional health vinegar beverage after homogeneous is first filtered through 200 order duplex strainers, then through the filter of diatom filter essence with removing impurity wherein and not tolerant;
(14) sterilization: deployed functional health vinegar beverage carries out high-temperature short-time sterilization, sterilising temp is 120 ~ 140 DEG C, and the time is 4 ~ 6s;
(15) filling: adopt vacuum filling, vacuum is 0.04-0.05Mpa, and filling temperature controls at 60-75 DEG C, then is cooled to normal temperature and gets product.
embodiment 2:
One protects liver herbal health care vinegar beverage, and its concrete production technology is as follows:
(1) get the raw materials ready: get the raw materials ready according to marine alga 30 parts, red date 20 parts, matrimony vine 20 parts, STEVIA REBAUDIANA 15 parts, umbellate pore furgus 10 parts, peach kernel 5 parts of ratios, remove infested raw material;
(2) pretreatment of raw material: the different qualities according to raw material carries out pretreatment of raw material respectively:
marine alga: by the marine alga peeling after cleaning, adopt first to add in 0.02% sodium sulfite solution after 90 DEG C of blanching 2.5min and soak lh and carry out color retention, add 2.5 times of water making beating, add the AMS of 1.8%, liquefy under 60 ~ 70 DEG C of conditions 20 ~ 30min;
red date, matrimony vine: after the red date after cleaning, matrimony vine adds 1.5 times of water, and making beating, adds pectase in 0.3g/100mL ratio, enzymolysis 1.5 ~ 2h under 45 ~ 50 DEG C of conditions;
umbellate pore furgus, STEVIA REBAUDIANA, peach kernel: the umbellate pore furgus after cleaning, STEVIA REBAUDIANA, peach kernel are pulverized, crosses 40 mesh sieves;
(3) batch mixing: by raw material mixing every in step (2), add water to solid-to-liquid ratio 1:6, and add 0.18% ammonium sulfate, 0.07% potassium dihydrogen phosphate, 0.02% magnesium sulfate;
(4) enzymolysis: add amylase, carbohydrase, cellulase respectively in 0.15g/100mL, 0.6g/100mL, 0.3g/100mL ratio, then at 40 ~ 60 DEG C, coordinated enzymatic hydrolysis 2 ~ 3h under stirring condition;
(5) alcoholic fermentation: regulate initial total sugar degree 13 ~ 15BX after enzymolysis, inoculation saccharomyces cerevisiae (commercially available Angel saccharomyces cerevisiae), inoculum concentration 7%, then (supernatant liquid stirs fermentation to carry out alcoholic fermentation, lower floor's solid standing for fermentation, 12h stirs once), at 20 ~ 28 DEG C of condition bottom fermentation 36 ~ 48h;
(6) acetic fermentation: inoculate acetic acid bacteria after alcoholic fermentation, inoculum concentration 9%, standing for fermentation 72 ~ 96h under 28 ~ 32 DEG C of conditions;
(7) be separated: be separated after fermentation ends, obtain acetic acid fermentation liquid;
(8) spray: to the solid spray be separated, acetic acid and other functional activity materials are leached as far as possible, and merging spray liquid and zymotic fluid obtain acetate solution;
(9) ageing: ageing 20 ~ 30 days under normal temperature condition;
(10) filter: adopt diatomite filtration;
(11) allocate: the total acid content 1.5% adjusting above-mentioned acetate solution, and add 1.2% sucrose, 0.1% citric acid, 0.18% calcium lactate, 1.5% xanthans, 0.015% sodium Diacetate;
(12) homogeneous: deployed beverage is placed in homogenizer, at homogenization pressure 25MPa, homogeneous at temperature 60 ~ 70 DEG C, makes various nutritional labeling homogenising, prevents product from occurring layering and precipitating, product stability is further ensured;
(13) essence filter: the functional health vinegar beverage after homogeneous is first filtered through 200 order duplex strainers, then through the filter of diatom filter essence with removing impurity wherein and not tolerant;
(14) sterilization: deployed functional health vinegar beverage carries out high-temperature short-time sterilization, sterilising temp is 120 ~ 140 DEG C, and the time is 4 ~ 6s;
(15) filling: adopt vacuum filling, vacuum is 0.04-0.05Mpa, and filling temperature controls at 60-75 DEG C, then is cooled to normal temperature and gets product.
embodiment 3:
One protects liver herbal health care vinegar beverage, and its concrete production technology is as follows:
(1) get the raw materials ready: get the raw materials ready according to marine alga 25 parts, red date 23 parts, matrimony vine 15 parts, STEVIA REBAUDIANA 20 parts, umbellate pore furgus 12 parts, peach kernel 5 parts of ratios, remove infested raw material;
(2) pretreatment of raw material: the different qualities according to raw material carries out pretreatment of raw material respectively:
marine alga: by the marine alga peeling after cleaning, adopt first to add in 0.02% sodium sulfite solution after 90 DEG C of blanching 2min and soak lh and carry out color retention, add 3 times of water making beating, add the AMS of 2%, liquefy under 60 ~ 70 DEG C of conditions 20 ~ 30min;
red date, matrimony vine: after the red date after cleaning, matrimony vine adds 2 times of water, and making beating, adds pectase in 0.4g/100mL ratio, enzymolysis 1.5 ~ 2h under 45 ~ 50 DEG C of conditions;
umbellate pore furgus, STEVIA REBAUDIANA, peach kernel: the umbellate pore furgus after cleaning, STEVIA REBAUDIANA, peach kernel are pulverized, crosses 40 mesh sieves;
(3) batch mixing: by raw material mixing every in step (2), add water to solid-to-liquid ratio 1:8, and add 0.15% ammonium sulfate, 0.05% potassium dihydrogen phosphate, 0.02% magnesium sulfate;
(4) enzymolysis: add amylase, carbohydrase, cellulase respectively in 0.2g/100mL, 0.8g/100mL, 0.4g/100mL ratio, then at 40 ~ 60 DEG C, coordinated enzymatic hydrolysis 2 ~ 3h under stirring condition;
(5) alcoholic fermentation: regulate initial total sugar degree 13 ~ 15BX after enzymolysis, inoculation saccharomyces cerevisiae (commercially available Angel saccharomyces cerevisiae), inoculum concentration 6%, then (supernatant liquid stirs fermentation to carry out alcoholic fermentation, lower floor's solid standing for fermentation, 12h stirs once), at 20 ~ 28 DEG C of condition bottom fermentation 36 ~ 48h;
(6) acetic fermentation: inoculate acetic acid bacteria after alcoholic fermentation, inoculum concentration 8%, standing for fermentation 72 ~ 96h under 28 ~ 32 DEG C of conditions;
(7) be separated: be separated after fermentation ends, obtain acetic acid fermentation liquid;
(8) spray: to the solid spray be separated, acetic acid and other functional activity materials are leached as far as possible, and merging spray liquid and zymotic fluid obtain acetate solution;
(9) ageing: ageing 20 ~ 30 days under normal temperature condition;
(10) filter: adopt diatomite filtration;
(11) allocate: the total acid content 2.0% adjusting above-mentioned acetate solution, and add 1.5% xylitol, 0.1% citric acid, 0.15% calcium lactate, 2% xanthans, 0.02% sodium Diacetate;
(12) homogeneous: deployed beverage is placed in homogenizer, at homogenization pressure 25MPa, homogeneous at temperature 60 ~ 70 DEG C, makes various nutritional labeling homogenising, prevents product from occurring layering and precipitating, product stability is further ensured;
(13) essence filter: the functional health vinegar beverage after homogeneous is first filtered through 200 order duplex strainers, then through the filter of diatom filter essence with removing impurity wherein and not tolerant;
(14) sterilization: deployed functional health vinegar beverage carries out high-temperature short-time sterilization, sterilising temp is 120 ~ 140 DEG C, and the time is 4 ~ 6s;
(15) filling: adopt vacuum filling, vacuum is 0.04-0.05Mpa, and filling temperature controls at 60-75 DEG C, then is cooled to normal temperature and gets product.
Above embodiment only for illustration of technical scheme of the present invention, but not is limited; Although be described in detail by invention with reference to previous embodiment, for the person of ordinary skill of the art, still the technical scheme described in previous embodiment can be modified, or equivalent replacement has been carried out to wherein portion of techniques feature; And to these amendments or replacement, do not make the essence of appropriate technical solution depart from the spirit and scope of the present invention's technical scheme required for protection.