CN103948642A - Application of refrigeration technique in phellinus igniarius drying - Google Patents
Application of refrigeration technique in phellinus igniarius drying Download PDFInfo
- Publication number
- CN103948642A CN103948642A CN201410204744.5A CN201410204744A CN103948642A CN 103948642 A CN103948642 A CN 103948642A CN 201410204744 A CN201410204744 A CN 201410204744A CN 103948642 A CN103948642 A CN 103948642A
- Authority
- CN
- China
- Prior art keywords
- dry
- phellinus igniarius
- quel
- application
- drying
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention relates to an application of a refrigeration technique in phellinus igniarius drying. The application comprises the following steps: taking freshly-harvested phellinus igniarius, refrigerating, piling up for 2-5 days and drying. The prepared phellinus igniarius has high content of active ingredients polysaccharide and flavonoid.
Description
Invention field
The present invention relates to medicine method for making, the particularly application of Refrigeration Technique in Phellinus igniarius (L. ex Fr.) Quel. is dry, belongs to medical technical field.
Background technology
Traditional Chinese medicine drying has very long history in China, the Chinese herbal medicine of drying can keep certain medicinal ingredient and be difficult for putrid and deteriorated, the dry important measures as ensureing Chinese herbal medicine quality, it is a requisite technical process in Chinese herbal medicine processing, it is in close relations that dry and Chinese medicine are produced, and dry quality will directly affect the quality of product.
Phellinus igniarius (L. ex Fr.) Quel. is the macro fungi that a class has important medical value, is Basidiomycotina (Basidiomycotina) Hymenomycetes (Hymenomycetes) Aphyllophorales (Polyporales) perforated Cordycepps (Hymenochaetacae) Phellinus (Phellinus).The functions such as the traditional Chinese medical science thinks, Phellinus igniarius (L. ex Fr.) Quel. can sharp the five internal organs, softening the hard mass, toxin expelling, stop blooding, invigorate blood circulation, rush down blood, leukorrhagia, amenorrhea, diarrhea due to hypofunction of the spleen etc. for controlling metrorrhagia, stranguria with blood, proctoptosis.Modern pharmacology studies have shown that, Phellinus igniarius (L. ex Fr.) Quel. has many-sided medicinal functions such as the tumor of inhibition, the liver protecting, raising immunity, is the best medicinal fungi of current internationally recognized antitumous effect.The effective ingredient of Phellinus igniarius (L. ex Fr.) Quel. mainly contains polysaccharide, Flavonoid substances.
Phellinus igniarius (L. ex Fr.) Quel. is used as medicine with dry product.
Summary of the invention
The object of this invention is to provide a kind of dry method of Phellinus igniarius (L. ex Fr.) Quel., the Phellinus igniarius (L. ex Fr.) Quel. that the method is dry, main effective ingredient polysaccharide, Flavonoid substances content are high.
The present invention is achieved in that
The application of Refrigeration Technique in Phellinus igniarius (L. ex Fr.) Quel. is dry, is characterized in that: get the Phellinus igniarius (L. ex Fr.) Quel. of newly gathering, and freezing, the 2-5 days that banks up is dry.
The application of Refrigeration Technique of the present invention in Phellinus igniarius (L. ex Fr.) Quel. is dry, is characterized in that: freezing is to be refrigerated to freeze.
The application of Refrigeration Technique of the present invention in Phellinus igniarius (L. ex Fr.) Quel. is dry, is characterized in that: freezing is to be refrigerated to-5 DEG C to freeze below.
The application of Refrigeration Technique of the present invention in Phellinus igniarius (L. ex Fr.) Quel. is dry, is characterized in that: dry is that heap postpone is dried or dries or dries.
Of the present inventionly being refrigerated to subzero certain DEG C, is to be refrigerated to and to freeze at this subzero certain DEG C.
So far completed the present invention, the Phellinus igniarius (L. ex Fr.) Quel. of preparing by drying means of the present invention, main effective ingredient polysaccharide, Flavonoid substances content are high.
Further illustrate usefulness of the present invention below by test example, test example is intended to further illustrate usefulness of the present invention, but not limitation of the present invention.
By with a collection of Phellinus igniarius (L. ex Fr.) Quel. of newly gathering, remove impurity, process by the following method.
1) dry: shady and cool ventilation place, spread out and dry;
2) dry: dry;
3) dry: 60 DEG C of following oven dry;
4) the freezing oven dry of banking up: be refrigerated to-5 DEG C to freezing, bank up 3 days at dark and damp place, 60 DEG C of following oven dry.
One, the dry phellin polysaccharides content comparison of distinct methods
Take respectively each sample powder (60 order) 5g, add 150mL distilled water mix homogeneously, reflux, extract, 3h, cooling, the centrifugal 15min of 6000r/min, get supernatant, precipitation part repeats to extract twice again, merges supernatant, rotation vacuum concentration is to 1/10 of original volume, add ethanol to concentration of alcohol 80%, hold over night, collecting precipitation; Absolute ethanol washing, vacuum drying, obtains crude polysaccharides.
Get a certain amount of dried crude polysaccharides, be settled to certain volume with distilled water, adopt phenol-sulfuric acid process to measure polyoses content, with glucose as a standard product drawing standard curve, in dry product, the results are shown in Table 1.
Table 1 distinct methods is dried phellin polysaccharides content (%)
| Drying means | Dry | Dry | Dry | The freezing oven dry of banking up |
| Content (%) | 3.75 | 3.81 | 3.76 | 5.42 |
Found out by table 1, Phellinus igniarius (L. ex Fr.) Quel. " freezing heap postpone is dry ", polyoses content is apparently higher than " drying ", " drying " and " oven dry ", and known the inventive method has advance.
Two, the dry flavonoids from phellinus content comparison of distinct methods
Take respectively each sample powder (60 order) 5g, add volume fraction 70% alcoholic solution 70mL, reflux, extract, 4 times, merges supernatant, filter, and filtrate recycling ethanol, vacuum drying, obtains flavone extract.
Get a certain amount of dried flavone extract, with dissolve with methanol and be settled to certain volume, adopt NaNO
The content of 2-Al (NO3) colorimetric method for determining flavone, taking rutin as standard substance drawing standard curve, in dry product, the results are shown in Table 2.
Table 2 distinct methods is dried flavonoids from phellinus content (%)
| Drying means | Dry | Dry | Dry | The freezing oven dry of banking up |
| Content (%) | 2.12 | 2.53 | 2.57 | 4.31 |
Found out by table 2, Phellinus igniarius (L. ex Fr.) Quel. " freezing heap postpone is dry ", flavones content is apparently higher than " drying ", " drying " and " oven dry ", and known the inventive method has advance.
Detailed description of the invention
The application of Refrigeration Technique in Phellinus igniarius (L. ex Fr.) Quel. is dry, is characterized in that: get the Phellinus igniarius (L. ex Fr.) Quel. of newly gathering, be refrigerated to and freeze, the 2-5 days that banks up is dry.
embodiment 1
Get the Phellinus igniarius (L. ex Fr.) Quel. of newly gathering, put in freeze dryer, be refrigerated to-5 DEG C to freezing, banking up 2 days in dark and damp place, dries.
embodiment 2
Get the Phellinus igniarius (L. ex Fr.) Quel. of newly gathering, put in freeze dryer, be refrigerated to-10 DEG C, bank up in the cool 3 days, dry.
embodiment 3
Get the Phellinus igniarius (L. ex Fr.) Quel. of newly gathering, put in freeze dryer, be refrigerated to-20 DEG C, bank up 4 days indoor, dry.
embodiment 4
Get the Phellinus igniarius (L. ex Fr.) Quel. of newly gathering, put in freeze dryer, be refrigerated to-32 DEG C to freezing, bank up 3 days outdoor, dry.
embodiment 6
Get the Phellinus igniarius (L. ex Fr.) Quel. of newly gathering, put in freeze dryer, be refrigerated to-15 DEG C, bank up 5 days at dark and damp place, dry.
Claims (4)
1. the application of Refrigeration Technique in Phellinus igniarius (L. ex Fr.) Quel. is dry, is characterized in that: get the Phellinus igniarius (L. ex Fr.) Quel. of newly gathering, and freezing, the 2-5 days that banks up is dry.
2. the application in Phellinus igniarius (L. ex Fr.) Quel. is dry according to the Refrigeration Technique of claim 1, is characterized in that: freezing is to be refrigerated to freeze.
3. the application in Phellinus igniarius (L. ex Fr.) Quel. is dry according to the Refrigeration Technique of claim 1, is characterized in that: freezing is to be refrigerated to-5 DEG C to freeze below.
4. the application in Phellinus igniarius (L. ex Fr.) Quel. is dry according to the Refrigeration Technique of claim 1, is characterized in that: dry is that heap postpone is dried or dries or dries.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410204744.5A CN103948642A (en) | 2014-05-15 | 2014-05-15 | Application of refrigeration technique in phellinus igniarius drying |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410204744.5A CN103948642A (en) | 2014-05-15 | 2014-05-15 | Application of refrigeration technique in phellinus igniarius drying |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103948642A true CN103948642A (en) | 2014-07-30 |
Family
ID=51326084
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410204744.5A Pending CN103948642A (en) | 2014-05-15 | 2014-05-15 | Application of refrigeration technique in phellinus igniarius drying |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103948642A (en) |
Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104132507A (en) * | 2014-08-25 | 2014-11-05 | 济南康众医药科技开发有限公司 | Method for drying mulberry leaves by applying refrigeration technique |
| CN104142048A (en) * | 2014-08-25 | 2014-11-12 | 济南康众医药科技开发有限公司 | Lamiophlomis herba drying method |
| CN104154715A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Freeze-drying method of honeysuckles |
| CN104154722A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Application of freeze-drying technology in lamiophlomis rotata drying |
| CN104147058A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Portulaca oleracea for treating diabetes |
| CN104147113A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Preparation method of salvia miltiorrhiza |
| CN104147059A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Drying method of penthorum chinense pursh |
| CN104147087A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Drying method of eucommia ulmoides |
| CN104154708A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Drying method of honeysuckles |
| CN104180613A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Freeze-drying method for roots of red-rooted salvia |
| CN104180610A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Penthorum chinense pursh drying method |
| CN104180614A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Freeze-drying method for roots of red-rooted salvia |
| CN104180616A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Drying method for lamiophlomis rotata |
| CN104180612A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Method for using refrigeration technique to dry mulberry leaves |
| CN104180619A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Scutellaria baicalensis drying method |
| CN104197637A (en) * | 2014-08-25 | 2014-12-10 | 济南康众医药科技开发有限公司 | Method for drying portulaca oleracea |
| CN104197647A (en) * | 2014-08-25 | 2014-12-10 | 济南康众医药科技开发有限公司 | Drying method of magnolia officinalis and application of magnolia officinalis product |
| CN104189069A (en) * | 2014-08-25 | 2014-12-10 | 济南康众医药科技开发有限公司 | Method for drying lamiophlomis rotata |
| CN106943438A (en) * | 2017-02-24 | 2017-07-14 | 浙江大学 | Phellinus active anticancer flavone compound PBF 1 and preparation method and application |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101703530A (en) * | 2009-06-08 | 2010-05-12 | 上海荷仙菇生物科技股份有限公司 | Mixed fungus ultrafine powder and preparation method thereof |
-
2014
- 2014-05-15 CN CN201410204744.5A patent/CN103948642A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101703530A (en) * | 2009-06-08 | 2010-05-12 | 上海荷仙菇生物科技股份有限公司 | Mixed fungus ultrafine powder and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 张兆旺主编: "《中药药剂学》", 30 April 2007, 中国中医药出版社 * |
| 杜伟锋等: "中药产地加工方法"发汗"的研究进展", 《中华中医药学刊》 * |
| 王忠壮等: "《现代中药学》", 31 January 2006, 第二军医大学出版社 * |
Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104132507A (en) * | 2014-08-25 | 2014-11-05 | 济南康众医药科技开发有限公司 | Method for drying mulberry leaves by applying refrigeration technique |
| CN104142048A (en) * | 2014-08-25 | 2014-11-12 | 济南康众医药科技开发有限公司 | Lamiophlomis herba drying method |
| CN104154715A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Freeze-drying method of honeysuckles |
| CN104154722A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Application of freeze-drying technology in lamiophlomis rotata drying |
| CN104147058A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Portulaca oleracea for treating diabetes |
| CN104147113A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Preparation method of salvia miltiorrhiza |
| CN104147059A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Drying method of penthorum chinense pursh |
| CN104147087A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Drying method of eucommia ulmoides |
| CN104154708A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Drying method of honeysuckles |
| CN104180613A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Freeze-drying method for roots of red-rooted salvia |
| CN104180610A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Penthorum chinense pursh drying method |
| CN104180614A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Freeze-drying method for roots of red-rooted salvia |
| CN104180616A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Drying method for lamiophlomis rotata |
| CN104180612A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Method for using refrigeration technique to dry mulberry leaves |
| CN104180619A (en) * | 2014-08-25 | 2014-12-03 | 济南康众医药科技开发有限公司 | Scutellaria baicalensis drying method |
| CN104197637A (en) * | 2014-08-25 | 2014-12-10 | 济南康众医药科技开发有限公司 | Method for drying portulaca oleracea |
| CN104197647A (en) * | 2014-08-25 | 2014-12-10 | 济南康众医药科技开发有限公司 | Drying method of magnolia officinalis and application of magnolia officinalis product |
| CN104189069A (en) * | 2014-08-25 | 2014-12-10 | 济南康众医药科技开发有限公司 | Method for drying lamiophlomis rotata |
| CN106943438A (en) * | 2017-02-24 | 2017-07-14 | 浙江大学 | Phellinus active anticancer flavone compound PBF 1 and preparation method and application |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103948642A (en) | Application of refrigeration technique in phellinus igniarius drying | |
| CN104365883B (en) | A kind of processing method of photovoltaic green tea | |
| CN103968647A (en) | Golden ganoderma drying method | |
| KR101583050B1 (en) | Preparation method of black ginseng for increasing ginsenoside Rg3 and decreasing benzopyrene, and the product thereof | |
| CN103977037A (en) | Phellinus drying method | |
| KR100840490B1 (en) | Method of manufacturing white ginseng and red ginseng by extra-high pressure treatment | |
| CN104231104A (en) | Extraction method of polysaccharides in coriolus versicolor | |
| CN108634157A (en) | A kind of vacuum freeze-drying processing method of fresh ginseng | |
| CN112212615A (en) | Microwave vacuum-hot air sectional type drying method for pseudo-ginseng | |
| CN201652645U (en) | Dehumidified, mould-proof and mothproof device used for Chinese traditional medicine cabinets | |
| CN103637953B (en) | Torch tree fruit extract and preparation method thereof and preparing the purposes in cosmetics | |
| CN103948644A (en) | Method for drying phellinus igniarius | |
| CN110638941A (en) | Microwave hot air drying method for gastrodia elata | |
| CN103977036A (en) | Drying method of inonotus obliquus | |
| CN104839360A (en) | Processing method for fresh Huangkui tea leaves in early stage of stir-frying | |
| CN101912156B (en) | Blackberry lily essential oil extraction method and application of blackberry lily essential oil in cigarette | |
| Di et al. | Effects of drying methods on the quality and microstructure of Armillaria luteo-virens | |
| CN113251749A (en) | Method for freeze drying salvia miltiorrhiza | |
| CN104138418B (en) | A kind of drying means of mulberry leaf | |
| CN115702912B (en) | Method for extracting polyphenol in Echinacea purpurea stems by using response surface method and application thereof | |
| CN113244334A (en) | Rhizoma gastrodiae tablet and drying method | |
| CN107149654A (en) | A kind of drying means of rhizoma Gastrodiae | |
| CN106819236A (en) | The scenting method of Feicheng Buddhist peach scented tea | |
| CN111349568A (en) | Endophytic fungi strain and strain as well as separation and application methods thereof | |
| CN103948645A (en) | Application of freezing technology in drying of phylloporia ribis sporocarp |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20140730 |