CN103934450A - 烧结钕铁硼回收料的再利用方法 - Google Patents
烧结钕铁硼回收料的再利用方法 Download PDFInfo
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- CN103934450A CN103934450A CN201410117366.7A CN201410117366A CN103934450A CN 103934450 A CN103934450 A CN 103934450A CN 201410117366 A CN201410117366 A CN 201410117366A CN 103934450 A CN103934450 A CN 103934450A
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- 239000000463 material Substances 0.000 title claims abstract description 53
- 229910001172 neodymium magnet Inorganic materials 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 33
- 239000000843 powder Substances 0.000 claims abstract description 81
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 38
- 150000002910 rare earth metals Chemical class 0.000 claims abstract description 35
- 239000000654 additive Substances 0.000 claims abstract description 25
- 230000000996 additive effect Effects 0.000 claims abstract description 25
- 238000005245 sintering Methods 0.000 claims abstract description 24
- 238000002156 mixing Methods 0.000 claims abstract description 18
- 239000001257 hydrogen Substances 0.000 claims abstract description 11
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 238000001514 detection method Methods 0.000 claims abstract description 5
- 238000007873 sieving Methods 0.000 claims abstract description 3
- QJVKUMXDEUEQLH-UHFFFAOYSA-N [B].[Fe].[Nd] Chemical compound [B].[Fe].[Nd] QJVKUMXDEUEQLH-UHFFFAOYSA-N 0.000 claims description 33
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 28
- 238000012360 testing method Methods 0.000 claims description 22
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 20
- 238000000465 moulding Methods 0.000 claims description 16
- 230000003068 static effect Effects 0.000 claims description 16
- 229910052757 nitrogen Inorganic materials 0.000 claims description 14
- 239000002699 waste material Substances 0.000 claims description 14
- 238000004064 recycling Methods 0.000 claims description 13
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 12
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 10
- 239000003963 antioxidant agent Substances 0.000 claims description 10
- 230000003078 antioxidant effect Effects 0.000 claims description 10
- 229910052786 argon Inorganic materials 0.000 claims description 10
- 239000012496 blank sample Substances 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 9
- 239000008187 granular material Substances 0.000 claims description 8
- 230000005389 magnetism Effects 0.000 claims description 8
- -1 on batch mixer Substances 0.000 claims description 8
- 239000011858 nanopowder Substances 0.000 claims description 5
- ATVJXMYDOSMEPO-UHFFFAOYSA-N 3-prop-2-enoxyprop-1-ene Chemical compound C=CCOCC=C ATVJXMYDOSMEPO-UHFFFAOYSA-N 0.000 claims description 4
- 150000005215 alkyl ethers Chemical class 0.000 claims description 4
- 238000006356 dehydrogenation reaction Methods 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 238000003801 milling Methods 0.000 claims description 4
- 239000011812 mixed powder Substances 0.000 claims description 4
- 238000004806 packaging method and process Methods 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 3
- 238000005516 engineering process Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 2
- 238000005265 energy consumption Methods 0.000 abstract description 2
- 239000007791 liquid phase Substances 0.000 abstract description 2
- 238000000462 isostatic pressing Methods 0.000 abstract 2
- 238000009740 moulding (composite fabrication) Methods 0.000 abstract 2
- 239000012300 argon atmosphere Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 239000012071 phase Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 3
- 229910052777 Praseodymium Inorganic materials 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
- PXAWCNYZAWMWIC-UHFFFAOYSA-N [Fe].[Nd] Chemical compound [Fe].[Nd] PXAWCNYZAWMWIC-UHFFFAOYSA-N 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 238000007885 magnetic separation Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
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Abstract
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104107908A (zh) * | 2014-07-26 | 2014-10-22 | 宿州学院 | 一种钕铁硼合金制粉用抗氧化剂 |
CN104439256A (zh) * | 2014-11-24 | 2015-03-25 | 湖南航天磁电有限责任公司 | 一种烧结钕铁硼氧化毛坯的回收再利用方法 |
CN108364738A (zh) * | 2018-04-17 | 2018-08-03 | 抚顺市先锋永磁材料有限公司 | 一种利用回收料制备烧结钕铁硼磁体的方法 |
CN109604616A (zh) * | 2018-12-04 | 2019-04-12 | 洪作娟 | 提高钕铁硼磁体耐腐性的制备方法 |
CN112563009A (zh) * | 2019-09-10 | 2021-03-26 | 宁波科宁达工业有限公司 | 一种利用回收压坯制备烧结磁体的方法 |
CN113436878A (zh) * | 2021-07-05 | 2021-09-24 | 宁波市易赞磁业有限公司 | 一种利用钕铁硼废料制备的烧结钕铁硼及其制备方法 |
CN114429858A (zh) * | 2022-01-13 | 2022-05-03 | 宁波金轮磁材技术有限公司 | 一种烧结钕铁硼磁钢及其制备方法 |
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RO115996B1 (ro) * | 1998-02-27 | 2000-08-30 | S C Icpe Sa | PROCEDEU DE RECUPERARE A DESEURILOR DE ALIAJE MAGNETICE NdFeB |
CN1687470A (zh) * | 2005-05-18 | 2005-10-26 | 西北有色金属研究院 | 一种利用废料制备钕铁硼合金的方法 |
JP2006077264A (ja) * | 2004-09-07 | 2006-03-23 | Kenichi Machida | 希土類焼結磁石および遷移金属系スクラップのリサイクル方法、GHz帯域対応電波吸収体用磁性体粉末および電波吸収体の製造方法 |
CN101015859A (zh) * | 2007-02-15 | 2007-08-15 | 山西汇镪磁性材料制作有限公司 | 烧结钕铁硼永磁体机械加工后所产生粉削再生利用的处理方法 |
CN102211192A (zh) * | 2011-06-09 | 2011-10-12 | 天津一阳磁性材料有限责任公司 | 二次回收料制备高性能钕铁硼的方法 |
CN102719725A (zh) * | 2012-07-10 | 2012-10-10 | 宁波科田磁业有限公司 | 烧结钕铁硼废料再成型的方法 |
CN103390478A (zh) * | 2013-08-08 | 2013-11-13 | 内蒙古科技大学 | 回收钕铁硼粉末废料的方法及利用其制备永磁材料的方法 |
-
2014
- 2014-03-26 CN CN201410117366.7A patent/CN103934450B/zh active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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RO115996B1 (ro) * | 1998-02-27 | 2000-08-30 | S C Icpe Sa | PROCEDEU DE RECUPERARE A DESEURILOR DE ALIAJE MAGNETICE NdFeB |
JP2006077264A (ja) * | 2004-09-07 | 2006-03-23 | Kenichi Machida | 希土類焼結磁石および遷移金属系スクラップのリサイクル方法、GHz帯域対応電波吸収体用磁性体粉末および電波吸収体の製造方法 |
CN1687470A (zh) * | 2005-05-18 | 2005-10-26 | 西北有色金属研究院 | 一种利用废料制备钕铁硼合金的方法 |
CN101015859A (zh) * | 2007-02-15 | 2007-08-15 | 山西汇镪磁性材料制作有限公司 | 烧结钕铁硼永磁体机械加工后所产生粉削再生利用的处理方法 |
CN102211192A (zh) * | 2011-06-09 | 2011-10-12 | 天津一阳磁性材料有限责任公司 | 二次回收料制备高性能钕铁硼的方法 |
CN102719725A (zh) * | 2012-07-10 | 2012-10-10 | 宁波科田磁业有限公司 | 烧结钕铁硼废料再成型的方法 |
CN103390478A (zh) * | 2013-08-08 | 2013-11-13 | 内蒙古科技大学 | 回收钕铁硼粉末废料的方法及利用其制备永磁材料的方法 |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104107908A (zh) * | 2014-07-26 | 2014-10-22 | 宿州学院 | 一种钕铁硼合金制粉用抗氧化剂 |
CN104107908B (zh) * | 2014-07-26 | 2015-12-02 | 宿州学院 | 一种钕铁硼合金制粉用抗氧化剂 |
CN104439256A (zh) * | 2014-11-24 | 2015-03-25 | 湖南航天磁电有限责任公司 | 一种烧结钕铁硼氧化毛坯的回收再利用方法 |
CN108364738A (zh) * | 2018-04-17 | 2018-08-03 | 抚顺市先锋永磁材料有限公司 | 一种利用回收料制备烧结钕铁硼磁体的方法 |
CN109604616A (zh) * | 2018-12-04 | 2019-04-12 | 洪作娟 | 提高钕铁硼磁体耐腐性的制备方法 |
CN112563009A (zh) * | 2019-09-10 | 2021-03-26 | 宁波科宁达工业有限公司 | 一种利用回收压坯制备烧结磁体的方法 |
CN112563009B (zh) * | 2019-09-10 | 2024-04-02 | 宁波科宁达工业有限公司 | 一种利用回收压坯制备烧结磁体的方法 |
CN113436878A (zh) * | 2021-07-05 | 2021-09-24 | 宁波市易赞磁业有限公司 | 一种利用钕铁硼废料制备的烧结钕铁硼及其制备方法 |
CN114429858A (zh) * | 2022-01-13 | 2022-05-03 | 宁波金轮磁材技术有限公司 | 一种烧结钕铁硼磁钢及其制备方法 |
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Effective date of registration: 20150929 Address after: 112611 No. 68, new Taiwan Road, hi tech Industrial Development Zone, Liaoning, Tieling Patentee after: LIAONING WUHUAN ENGINEERING TECHNOLOGY Co.,Ltd. Address before: 112000 No. 68, new Taiwan Road, hi tech Industrial Development Zone, Liaoning, Tieling Patentee before: LIAONING WUHUAN TECHNOLOGY DEVELOPMENT Co.,Ltd. |
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Inventor after: Zhang Xianwei Inventor after: Zhang Xi Inventor after: Zhang Qiang Inventor after: Zhang Junfei Inventor after: Li Jia Inventor before: Zhang Xianwei Inventor before: Zhang Xi Inventor before: Zhang Qiang Inventor before: Liu Ying Inventor before: Zhang Junfei |
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Effective date of registration: 20180115 Address after: 113000 Liaoning Province Wang Li Fushun City Economic Development Zone, the east side of the street town of A2-7 floor Patentee after: SHENYANG ZHIGU INDUSTRIAL Co.,Ltd. Address before: 112611 No. 68, new Taiwan Road, hi tech Industrial Development Zone, Liaoning, Tieling Patentee before: LIAONING WUHUAN ENGINEERING TECHNOLOGY Co.,Ltd. |
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Address after: 113000 Building A2-7, Doctoral Town, East of Wangli Street, Fushun Economic Development Zone, Liaoning Province Patentee after: Shenyang Wuwei Engineering Technology Co.,Ltd. Address before: 113000 Building A2-7, Doctoral Town, East of Wangli Street, Fushun Economic Development Zone, Liaoning Province Patentee before: Shenyang Hongji Mining and Metallurgical Engineering Technology Co.,Ltd. Address after: 113000 Building A2-7, Doctoral Town, East of Wangli Street, Fushun Economic Development Zone, Liaoning Province Patentee after: Shenyang Hongji Mining and Metallurgical Engineering Technology Co.,Ltd. Address before: 113000 Building A2-7, Doctoral Town, East of Wangli Street, Fushun Economic Development Zone, Liaoning Province Patentee before: SHENYANG ZHIGU INDUSTRIAL Co.,Ltd. |
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Effective date of registration: 20191017 Address after: 1501, No. 75-1, Jinfeng street, Shenfu New District, Shenyang, Liaoning Patentee after: Shenyang Shengshi Wuhuan Technology Co.,Ltd. Address before: 113000 Building A2-7, Doctoral Town, East of Wangli Street, Fushun Economic Development Zone, Liaoning Province Patentee before: Shenyang Wuwei Engineering Technology Co.,Ltd. |
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Address after: 113122 No. 69, Shendong seventh Road, Shenfu demonstration area, Shenyang City, Liaoning Province Patentee after: Shenyang Shengshi Wuhuan Technology Co.,Ltd. Address before: No. 1501, No. 75-1, Jinfeng street, Shenfu New District, Shenyang City, Liaoning Province Patentee before: Shenyang Shengshi Wuhuan Technology Co.,Ltd. |
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