CN103624863A - Welding flux used in filigree golden blank cloisonn product and manufacturing method for cloisonn product - Google Patents
Welding flux used in filigree golden blank cloisonn product and manufacturing method for cloisonn product Download PDFInfo
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- CN103624863A CN103624863A CN201310644635.0A CN201310644635A CN103624863A CN 103624863 A CN103624863 A CN 103624863A CN 201310644635 A CN201310644635 A CN 201310644635A CN 103624863 A CN103624863 A CN 103624863A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/24—Selection of soldering or welding materials proper
- B23K35/30—Selection of soldering or welding materials proper with the principal constituent melting at less than 1550 degrees C
- B23K35/3013—Au as the principal constituent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C1/00—Processes, not specifically provided for elsewhere, for producing decorative surface effects
- B44C1/26—Inlaying with ornamental structures, e.g. niello work, tarsia work
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C5/00—Processes for producing special ornamental bodies
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Adornments (AREA)
- Tires In General (AREA)
Abstract
The invention relates to a welding flux used in a filigree golden blank cloisonn product and a manufacturing method for the cloisonn product. The method comprises the following steps of making a blank, inlaying a wire, installing the wire, soldering, pickling, painting blue, polishing blue, painting bright white glaze, polishing blue again, polishing, plating gold and the like. The soldering medicine powder comprises the following ingredients of 55-60% of gold, 6-8% of sliver, 27-32% of red metal, 4-7% of cadmium and arsenic trioxide which accounts 22-26wt% of above ingredients. During pickling, the soldered gold blank is pickled for three times and pickled for 10-12 minutes each time; and after blue painting, the sintering temperature is 790-820DEG C. The welding flux used for soldering has the advantages of good liquidity, firmness in welding and easiness in welding. The obtained cloisonn filigree has the advantages of preciseness in positioning, abrasion resistance, high hardness and no colour fading. The white glaze varnishing technology and two-time blue polishing are adopted, so that the obtained artware has the advantages of better color and high collection value, is always new and is free from rusting, and the high-level artistic enjoyment of people can be satisfied.
Description
Technical field
The present invention relates to a kind of cloisonne ' products, particularly relate to a kind of for the welding agent of golden tire melting welding cloisonne ' products and the preparation method of cloisonne ' products of wiring inlay.
Background technology
Cloisonne enamel, has another name called " copper tire thread weaving enamel ", is the Particular craft product of a kind of porcelain copper combination, with red copper, makes base, makes various moulding, then pinches into various flowers with copper wire, fills enamel glaze, and fired, polishing, the operation such as gold-plated are made.Its adopts gold, silver and bronze and multiple natural mineral matter is raw material, integrates the fine arts, technique, carves, inlays, the professional technique such as glass melting, metallurgy.Cloisonne enamel moulding is special, make exquisite, exquisite workmanship, exquisite beyond compare, pattern is serious, color is gorgeous, splendid, is one of artifacts of tool national characters, selected first batch of List of National Intangible Cultural Heritage in 2006.Cloisonne handicraft is applicable to appreciate collection, can also be as commercial gift, articles for daily use, indoor and outdoor architectural engineering decoration etc.
The current copper tire cloisonne enamel holding time has been grown its inwall blue or green rust, not only affects attractive in appearancely, and blue or green rust is poisonous; The silver tire cloisonne enamel inwall time has been grown and has had black show.Along with development and the market demand of cloisonne handicraft, people need more high-grade cloisonne ' products, require that cloisonne enamel surface is will never fade, wear-resisting, sound construction, hardness be high, need to explore better process to obtain better handicraft.
Summary of the invention
The technical problem to be solved in the present invention: overcome shortcoming of the prior art, the welding agent of the golden tire melting welding of wiring inlay of a kind of good fluidity, firm welding cloisonne ' products is provided;
The preparation method of a kind of Never-rusty, colour-fast, the wear-resisting golden tire melting welding cloisonne ' products that wires inlay in surface is also provided.
technical scheme of the present invention:
For a welding agent for the golden tire melting welding cloisonne ' products that wires inlay, by the composition of following percentage by weight, formed: the gold of 55-60%, the silver of 6-8%, the red metal of 27-32%, the cadmium of 4-7%, add the arsenic trioxide of above composition weight 22-26% in addition.
The composition of described gold solder medicinal powder is preferably: 58.5% gold, 7.5% silver, 29% red metal, 5% cadmium, add the arsenic trioxide of above composition weight 25% in addition.
The wire inlay preparation method of golden tire melting welding cloisonne ' products, comprises the following steps:
(1) make base: gold sheet is cut into cloisonne ' products size, carries out spinning, welding, obtains complete gold tire;
(2) wire inlay: with thin flat gold silk, as lines, with tweezers, according to the bending turnover of decorative pattern, pinch into pattern;
(3) upper silk: the gold silk wiring inlay is put into stove fire and fire, after the deliquescing of gold silk, clamp gold silk with tweezers and dip in bletilla striata slurry, according to pattern, gold silk is bonded on gold tire;
(4) freeze: on gold tire, evenly spray water, then evenly sprinkle layer of gold welding agent powder and borax, the weight ratio of gold solder medicinal powder and borax is 3:1; Gold tire is heated to 780-900 ℃, makes the fusing of gold solder medicinal powder, gold wire bond is connected on gold tire;
Wherein to take the composition of percentage by weight be the gold of 55-60%, the silver of 6-8%, the red metal of 27-32%, the cadmium of 4-7% to gold solder medicinal powder, adds in addition the arsenic trioxide of above composition weight 22-26%; During this gold solder medicinal powder fusing, first, by gold, silver, red metal fusing, then add cadmium and arsenic trioxide;
(5) pickling: the gold tire after freezing is carried out to pickling three times, each 10-12 minute;
(6) fill enamel: according to the color indicating, the enamel glaze of getting ready is filled in the gold reel frame on gold tire, carries out sintering, sintering temperature is 790-820 ℃, after heating, enamel glaze is molten into liquid, becomes after cooling the color glaze layer anchoring on carcass; If color glaze layer, lower than the frame height of gold silk, is filled enamel glaze sintering again, 3-4 time so repeatedly, until color glaze layer is equal with gold reel frame;
(7) mill is blue: the semi-finished product that obtain are placed on to mill Lan Jishang, polish respectively with 50 orders, the quartzy stone mill of 150 objects;
(8) upper brilliant white glaze: last layer brilliant white glaze equably on the semi-finished product after polishing, sintering again after drying, sintering temperature is 790-820 ℃;
(9) mill is blue again: semi-finished product are placed on to mill Lan Jishang, first with the quartzy stone mill of 400 objects, polish; Then with 400 orders, 800 orders, 1500 object waterproof abrasive papers, carry out fine grinding respectively;
(10) polishing, gold-plated: the semi-finished product after fine grinding are carried out to polishing, plating, finally obtain finished product.
While welding in described step (1), welding medicinal powder composition is by weight percentage: gold 90%, silver 5%, copper 4%, zinc 1%.
While firing in stove fire in described step (3), temperature is 300-600 ℃, and the firing time is 30-60 second.
The composition of described gold solder medicinal powder is: 58.5% gold, 7.5% silver, 29% red metal, 5% cadmium, add the arsenic trioxide of above composition weight 25% in addition.
Described pickling temperature is 40 ℃, the hydrochloric acid that acid used is 20%.
positive beneficial effect of the present invention:
(1) the present invention is for the welding agent of cloisonne enamel, and good fluidity, is not only easy to welding, and firm welding, the cloisonne enamel the obtaining registration that wires inlay, wear-resisting, hardness is high, will never fade.
(2) the golden tire cloisonne enamel that the wires inlay of the present invention technique of wiring inlay, forms the decorative pattern of cloisonne ' products with gold silk, substitute traditional copper tire cloisonne enamel technique of wiring inlay, the welding agent of making base adopting in technique, and fusing point is high, is difficult for cracking while freezing, and welding is easily.The method is compared with traditional handicraft, can greatly shorten technical process, enhances productivity.
(3) the present invention adopts brilliant white glaze handicraft and twice mill indigo plant, and the handicraft color obtaining is better, with the passing of time as new, and Never-rusty.
(4) golden tire cloisonne enamel of the present invention can be made the various handicrafts such as various drinking utensils, tea set, vase, bracelet, and high-grade, both artistic and practical, reserve value is high, can meet the high-level artistic treat of people.
The specific embodiment
example 1:for a welding agent for the golden tire melting welding cloisonne ' products that wires inlay, by the composition of following percentage by weight, formed: 58.5% gold, 7.5% silver, 29% red metal, 5% cadmium, add the arsenic trioxide of above weight composition 25% in addition.
example 2:for a welding agent for the golden tire melting welding cloisonne ' products that wires inlay, its percentage by weight forms: 55% gold, 8% silver, 32% red metal, 5% cadmium, add the arsenic trioxide of above weight composition 26% in addition.
example 3:for a welding agent for the golden tire melting welding cloisonne ' products that wires inlay, its percentage by weight forms: 60% gold, 6% silver, 27% red metal, 7% cadmium, separately add the arsenic trioxide of above weight composition 22%.
example 4:the wire inlay preparation method of golden tire melting welding cloisonne ' products, comprises the following steps:
(1) make base: gold sheet is cut into cloisonne ' products size, carries out spinning, welding, obtains complete gold tire;
While wherein welding, medicinal powder composition is by weight percentage: gold 90%, silver 5%, copper 4%, zinc 1%.
(2) wire inlay: with thin flat gold silk, as lines, with tweezers, according to the bending turnover of decorative pattern, pinch into pattern;
(3) upper silk: the gold silk wiring inlay is put into stove fire and fire, after the deliquescing of gold silk, clamp gold silk with tweezers and dip in bletilla striata slurry, according to pattern, gold silk is bonded on gold tire; While firing, temperature is 300-600 ℃, and the firing time is 30-60 second;
(4) freeze: on gold tire, evenly spray water, then evenly sprinkle layer of gold welding agent powder and borax, the weight ratio of gold solder medicinal powder and borax is 3:1; Gold tire is heated to 780-900 ℃, makes the fusing of gold solder medicinal powder, gold wire bond is connected on gold tire;
Wherein gold solder medicinal powder composition is: 58.5% gold, 7.5% silver, 29% red metal, 5% cadmium, add the arsenic trioxide of above composition weight 25% in addition; During the fusing of gold solder medicinal powder, first, by gold, silver, red metal fusing, then add cadmium and arsenic trioxide;
(5) pickling: the gold tire after freezing is carried out to pickling three times, each 10-12 minute; Wherein pickling temperature is 40 ℃, the hydrochloric acid that acid used is 20%;
(6) fill enamel: according to the color indicating, the enamel glaze of getting ready is filled in the gold reel frame on gold tire, carries out sintering, sintering temperature is 790-820 ℃, after heating, enamel glaze is molten into liquid, becomes after cooling the color glaze layer anchoring on carcass; If color glaze layer, lower than the frame height of gold silk, is filled enamel glaze, sintering again, 3-4 time so repeatedly, until color glaze layer is equal with gold reel frame;
(7) mill is blue: the semi-finished product that obtain are placed on the blue machine of mill and with 50 orders, the quartzy stone mill of 150 objects, are polished respectively;
(8) upper brilliant white glaze: last layer brilliant white glaze equably on the semi-finished product after polishing, sintering again after drying, sintering temperature is 790-820 ℃;
(9) mill is blue again: semi-finished product are placed on to mill Lan Jishang, first with the quartzy stone mill of 400 objects, polish; Then with 400 orders, 800 orders, 1500 object waterproof abrasive papers, carry out fine grinding respectively;
(10) polishing, gold-plated: the semi-finished product after fine grinding are carried out to polishing, plating, finally obtain finished product.
example 5:identical with embodiment 4 steps, difference is following technological parameter:
(1) upper silk: firing temperature is 300 ℃, and the firing time is 60 seconds;
(2) freeze: gold tire is heated to 780 ℃, makes the fusing of gold solder medicinal powder, gold wire bond is connected on gold tire;
Wherein gold solder medicinal powder composition is: 55% gold, 8% silver, 32% red metal, 5% cadmium, add the arsenic trioxide of above weight 26% in addition;
(3) pickling: the gold tire after freezing is carried out to pickling three times, each 10 minutes;
(4) fill enamel: sintering temperature is 800 ℃;
(5) upper brilliant white glaze: even last layer brilliant white glaze on the semi-finished product of polishing, sintering again after drying, sintering temperature is 800 ℃.
example 6:identical with embodiment 4 steps, difference is following technological parameter:
(1) upper silk: firing temperature is 600 ℃, and the firing time is 30 seconds;
(2) freeze: gold tire is heated to 900 ℃, makes the fusing of gold solder medicinal powder, gold wire bond is connected on gold tire;
Wherein gold solder medicinal powder composition is: 60% gold, 6% silver, 27% red metal, 7% cadmium, add the arsenic trioxide of above weight composition 22% in addition;
(3) pickling: the gold tire after freezing is carried out to pickling three times, each 12 minutes;
(4) fill enamel: sintering temperature is 820 ℃;
(5) upper brilliant white glaze: even last layer brilliant white glaze on the semi-finished product of polishing, sintering again after drying, sintering temperature is 820 ℃.
example 7:identical with embodiment 4 steps, difference is following technological parameter:
(1) upper silk: firing temperature is 500 ℃, and the firing time is 50 seconds;
(2) freeze: gold tire is heated to 790 ℃, makes the fusing of gold solder medicinal powder, gold wire bond is connected on gold tire;
Wherein gold solder medicinal powder composition is: 58% gold, 7% silver, 30% red metal, 5% cadmium, add the arsenic trioxide of above weight composition 24% in addition;
(3) pickling: the gold tire after freezing is carried out to pickling three times, each 10-12 minute;
(4) fill enamel: sintering temperature is 810 ℃;
(5) upper brilliant white glaze: even last layer brilliant white glaze on the semi-finished product of polishing, sintering again after drying, sintering temperature is 810 ℃.
Claims (7)
1. the welding agent for the golden tire melting welding cloisonne ' products that wires inlay, it is characterized in that: this welding agent is comprised of the composition of following percentage by weight: the gold of 55-60%, the silver of 6-8%, the red metal of 27-32%, the cadmium of 4-7%, add the arsenic trioxide of above composition weight 22-26% in addition.
2. welding agent as claimed in claim 1, is characterized in that: the composition of described gold solder medicinal powder is: 58.5% gold, 7.5% silver, 29% red metal, 5% cadmium, add the arsenic trioxide of above composition weight 25% in addition.
3. the wire inlay preparation method of golden tire melting welding cloisonne ' products, is characterized in that, the method comprises the following steps:
(1) make base: gold sheet is cut into cloisonne ' products size, carries out spinning, welding, obtains complete gold tire;
(2) wire inlay: with thin flat gold silk, as lines, with tweezers, according to the bending turnover of decorative pattern, pinch into pattern;
(3) upper silk: the gold silk wiring inlay is put into stove fire and fire, after the deliquescing of gold silk, clamp gold silk with tweezers and dip in bletilla striata slurry, according to pattern, gold silk is bonded on gold tire;
(4) freeze: on gold tire, evenly spray water, then evenly sprinkle layer of gold welding agent powder and borax, the weight ratio of gold solder medicinal powder and borax is 3:1; Gold tire is heated to 780-900 ℃, makes the fusing of gold solder medicinal powder, gold wire bond is connected on gold tire;
Wherein to take the composition of percentage by weight be the gold of 55-60%, the silver of 6-8%, the red metal of 27-32%, the cadmium of 4-7% to gold solder medicinal powder, adds in addition the arsenic trioxide of above composition weight 22-26%; During this gold solder medicinal powder fusing, first, by gold, silver, red metal fusing, then add cadmium and arsenic trioxide;
(5) pickling: the gold tire after freezing is carried out to pickling three times, each 10-12 minute;
(6) fill enamel: according to the color indicating, the enamel glaze of getting ready is filled in the gold reel frame on gold tire, carries out sintering, sintering temperature is 790-820 ℃, after heating, enamel glaze is molten into liquid, becomes after cooling the color glaze layer anchoring on carcass; If color glaze layer, lower than the frame height of gold silk, is filled enamel glaze sintering again, 3-4 time so repeatedly, until color glaze layer is equal with gold reel frame;
(7) mill is blue: the semi-finished product that obtain are placed on to mill Lan Jishang, polish respectively with 50 orders, the quartzy stone mill of 150 objects;
(8) upper brilliant white glaze: last layer brilliant white glaze equably on the semi-finished product after polishing, sintering again after drying, sintering temperature is 790-820 ℃;
(9) mill is blue again: semi-finished product are placed on to mill Lan Jishang, first with the quartzy stone mill of 400 objects, polish; Then with 400 orders, 800 orders, 1500 object waterproof abrasive papers, carry out fine grinding respectively;
(10) polishing, gold-plated: the semi-finished product after fine grinding are carried out to polishing, plating, finally obtain finished product.
4. preparation method according to claim 3, is characterized in that, while welding in described step (1), welding medicinal powder composition is by weight percentage: gold 90%, silver 5%, copper 4%, zinc 1%.
5. according to the preparation method described in claim 3 or 4, it is characterized in that, while firing in stove fire in described step (3), temperature is 300-600 ℃, and the firing time is 30-60 second.
6. according to the preparation method described in claim 3 or 4, it is characterized in that, the composition of described gold solder medicinal powder is: 58.5% gold, 7.5% silver, 29% red metal, 5% cadmium, add the arsenic trioxide of above composition weight 25% in addition.
7. according to the preparation method described in claim 3 or 4, it is characterized in that, described pickling temperature is 40 ℃, the hydrochloric acid that acid used is 20%.
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| CN201310644635.0A CN103624863B (en) | 2013-12-05 | 2013-12-05 | Welding agent in the gold tire melting welding cloisonne ' products that wires inlay and the manufacture method of cloisonne ' products |
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| CN201310644635.0A CN103624863B (en) | 2013-12-05 | 2013-12-05 | Welding agent in the gold tire melting welding cloisonne ' products that wires inlay and the manufacture method of cloisonne ' products |
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Cited By (8)
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| CN106183600A (en) * | 2016-08-28 | 2016-12-07 | 郭漫笳 | A kind of preparation method of copper art parquet decorative board |
| CN106218295A (en) * | 2016-07-29 | 2016-12-14 | 安庆帝雅艺术品有限公司 | One is wired inlay technique |
| CN106240217A (en) * | 2016-08-26 | 2016-12-21 | 河南梦祥纯银制品有限公司 | A kind of thread weaving enamel silverware and preparation method thereof |
| CN108749447A (en) * | 2018-06-27 | 2018-11-06 | 河南梦祥纯银制品有限公司 | A kind of silver tire enamel and preparation method thereof |
| CN109530965A (en) * | 2018-12-28 | 2019-03-29 | 云南乌铜走银文化产业有限公司 | The weld tabs and preparation method thereof of silvery work is walked for black copper |
| CN110747471A (en) * | 2019-11-05 | 2020-02-04 | 深圳宝福珠宝有限公司 | Method for processing color-changing enamel applied to metal surface |
| CN111962078A (en) * | 2020-08-21 | 2020-11-20 | 深圳明丰珠宝首饰有限公司 | Technology for combining ancient gold with enamel |
| CN115255694A (en) * | 2022-08-13 | 2022-11-01 | 苏州欧纳菲文化发展有限公司 | Welding process of gold small beads |
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| CN110370848B (en) * | 2019-07-23 | 2021-04-20 | 申震 | Method for sintering transparent enamel on surface of copper wire and copper tire for manufacturing cloisonne enamel |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106218295A (en) * | 2016-07-29 | 2016-12-14 | 安庆帝雅艺术品有限公司 | One is wired inlay technique |
| CN106240217A (en) * | 2016-08-26 | 2016-12-21 | 河南梦祥纯银制品有限公司 | A kind of thread weaving enamel silverware and preparation method thereof |
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| CN108749447A (en) * | 2018-06-27 | 2018-11-06 | 河南梦祥纯银制品有限公司 | A kind of silver tire enamel and preparation method thereof |
| CN109530965A (en) * | 2018-12-28 | 2019-03-29 | 云南乌铜走银文化产业有限公司 | The weld tabs and preparation method thereof of silvery work is walked for black copper |
| CN109530965B (en) * | 2018-12-28 | 2020-11-10 | 云南乌铜走银文化产业有限公司 | Soldering lug for manufacturing black copper by silver and preparation method thereof |
| CN110747471A (en) * | 2019-11-05 | 2020-02-04 | 深圳宝福珠宝有限公司 | Method for processing color-changing enamel applied to metal surface |
| CN110747471B (en) * | 2019-11-05 | 2022-02-11 | 深圳宝福珠宝有限公司 | Method for processing color-changing enamel applied to metal surface |
| CN111962078A (en) * | 2020-08-21 | 2020-11-20 | 深圳明丰珠宝首饰有限公司 | Technology for combining ancient gold with enamel |
| CN115255694A (en) * | 2022-08-13 | 2022-11-01 | 苏州欧纳菲文化发展有限公司 | Welding process of gold small beads |
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