CN103624863B - Welding agent in the gold tire melting welding cloisonne ' products that wires inlay and the manufacture method of cloisonne ' products - Google Patents
Welding agent in the gold tire melting welding cloisonne ' products that wires inlay and the manufacture method of cloisonne ' products Download PDFInfo
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- CN103624863B CN103624863B CN201310644635.0A CN201310644635A CN103624863B CN 103624863 B CN103624863 B CN 103624863B CN 201310644635 A CN201310644635 A CN 201310644635A CN 103624863 B CN103624863 B CN 103624863B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/24—Selection of soldering or welding materials proper
- B23K35/30—Selection of soldering or welding materials proper with the principal constituent melting at less than 1550 degrees C
- B23K35/3013—Au as the principal constituent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C1/00—Processes, not specifically provided for elsewhere, for producing decorative surface effects
- B44C1/26—Inlaying with ornamental structures, e.g. niello work, tarsia work
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C5/00—Processes for producing special ornamental bodies
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Adornments (AREA)
- Tires In General (AREA)
Abstract
The present invention relates to a kind of welding agent in the gold tire melting welding cloisonne ' products that wires inlay and the manufacture method of cloisonne ' products.The method includes making base, wires inlay, upper silk, freeze, pickling, fill enamel, grind brilliant white glaze blue, upper, again grind indigo plant, polishing, the step such as gold-plated, the medication powder composition that wherein freezes is: 55 60% gold, 6 8% silver, 27 32% rose copper, 4 7% cadmiums, the another arsenic trioxide adding above weight 22 26%；Gold tire pickling after freezing during pickling three times, each 10 12 minutes；After filling enamel, sintering temperature is 790 820 DEG C.The present invention freezes with welding agent, good fluidity, firm welding, it is easy to welding, the cloisonné obtained wires inlay registration, wear-resisting, hardness is high, will never fade；In employing, brilliant white glaze handicraft and twice mill are blue, and the artware color obtained is more preferable, and with the passing of time as new, Never-rusty, reserve value is high, can meet the artistic treat that people are high-level.
Description
Technical field
The present invention relates to a kind of cloisonne ' products, particularly relate to a kind of welding agent in the gold tire melting welding cloisonne ' products that wires inlay and the manufacture method of cloisonne ' products.
Background technology
Cloisonné, has another name called " copper tire thread weaving enamel ", is the Particular craft product that combine of a kind of porcelain copper, makees base with red copper, make various moulding, then pinch into various flower with copper wire, fills enamel glaze, and fired, polishing, the operation such as gold-plated are made.It uses gold, silver and bronze and multiple natural mineral matter to be raw material, integrate the fine arts, technique, carve, inlay, the professional technique such as glass melting, metallurgy.Cloisonné moulding is special, makes fineness, exquisite workmanship, and exquisite beyond compare, pattern is serious, and color is gorgeous, splendid, is one of the artifacts of most national characters, selected first batch of List of National Intangible Cultural Heritage in 2006.Cloisonne handicraft is applicable to appreciate collection, it is also possible to as commercial affairs gift, articles for daily use, indoor and outdoor architectural engineering decoration etc..
Its inwall of current copper tire cloisonné holding time length has blue or green rust, not only affects attractive in appearance, and blue or green rust is poisonous；Silver tire cloisonné inwall time length has black show.Along with development and the market demand of cloisonne handicraft, people need more high-grade cloisonne ' products, it is desirable to cloisonné surface is will never fade, wear-resisting, sound construction, hardness high, needs to explore more preferable process to obtain more preferable handicraft.
Summary of the invention
The technical problem to be solved in the present invention: overcome shortcoming of the prior art, it is provided that a kind of good fluidity, firm welding wire inlay gold tire melting welding cloisonne ' products welding agent；
Additionally provide the manufacture method of colour-fast, the wear-resisting gold tire melting welding cloisonne ' products that wires inlay in a kind of Never-rusty, surface.
Technical scheme:
A kind of welding agent in the gold tire melting welding cloisonne ' products that wires inlay, is made up of the composition of following percentage by weight: the gold of 55-60%, the silver of 6-8%, the rose copper of 27-32%, the cadmium of 4-7%, it is possible to additionally incorporate the arsenic trioxide of above Ingredient Wt 22-26%.
The composition of described gold solder medicated powder is preferably: the gold of 58.5%, the silver of 7.5%, the rose copper of 29%, the cadmium of 5%, it is possible to additionally incorporate the arsenic trioxide of above Ingredient Wt 25%.
The manufacture method of a kind of gold tire melting welding cloisonne ' products that wires inlay, comprises the following steps:
(1) make base: gold sheet is cut into cloisonne ' products size, carry out spinning, welding, obtain complete gold tire；
(2) wire inlay: with the most flat gold silk as lines, transfer according to the bending of decorative pattern with tweezers, pinch into pattern；
(3) upper silk: the gold silk wired inlay is put into stove fire and fires, after gold silk deliquescing, clamps gold silk with tweezers and dips in Pseudobulbus Bletillae (Rhizoma Bletillae) slurry, be bonded on gold tire by gold silk according to pattern；
(4) freezing: uniformly spray water on gold tire, the most uniformly spread last layer gold solder medicated powder and Borax, the weight ratio of gold solder medicated powder and Borax is 3:1；Gold tire is heated to 780-900 DEG C, makes gold solder medicated powder melt, gold wire bond is connected on gold tire；
Wherein gold solder medicated powder with the composition of percentage by weight is: the gold of 55-60%, the silver of 6-8%, the rose copper of 27-32%, the cadmium of 4-7%, it is possible to additionally incorporate the arsenic trioxide of above Ingredient Wt 22-26%；During the fusing of this gold solder medicated powder, first by gold, silver, rose copper fusing, it is subsequently adding cadmium and arsenic trioxide；
(5) pickling: the gold tire after freezing carries out pickling three times, each 10-12 minute；
(6) fill enamel: according in the gold reel frame that the enamel glaze got ready is filled on gold tire by the color indicated, it is sintered, sintering temperature is 790-820 DEG C, and after heating, enamel glaze is molten into liquid, becomes the color glaze layer anchored on carcass after cooling；If color glaze layer is less than the frame height of gold silk, then it is again filled with enamel glaze and sinters, 3-4 time the most repeatedly, until color glaze layer is equal with gold reel frame；
(7) mill indigo plant: the semi-finished product obtained are placed on mill Lan Jishang, polish with the quartzy stone grinder of 50 mesh, 150 mesh respectively；
(8) upper brilliant white glaze: last layer brilliant white glaze equably on the semi-finished product after polishing, sinters after drying again, and sintering temperature is 790-820 DEG C；
(9) indigo plant is again ground: semi-finished product are placed on mill Lan Jishang, first polish with the quartzy stone grinder of 400 mesh；Fine grinding is carried out the most respectively with 400 mesh, 800 mesh, the waterproof abrasive paper of 1500 mesh；
(10) polishing, gold-plated: the semi-finished product after fine grinding are polished, electroplate, finally obtains finished product.
In described step (1) during welding, welding medicated powder composition by weight percentage is: gold 90%, silver 5%, copper 4%, zinc 1%.
When firing in stove fire in described step (3), temperature is 300-600 DEG C, and the firing time is the 30-60 second.
The composition of described gold solder medicated powder is: the gold of 58.5%, the silver of 7.5%, the rose copper of 29%, the cadmium of 5%, it is possible to additionally incorporate the arsenic trioxide of above Ingredient Wt 25%.
Described pickling temperature is 40 DEG C, and acid used is the hydrochloric acid of 20%.
The positive beneficial effect of the present invention:
(1) present invention is for the welding agent of cloisonné, good fluidity, is not only easy to welding, and firm welding, and the cloisonné obtained wires inlay registration, wear-resisting, hardness is high, will never fade.
(2) the gold tire cloisonné that wires inlay of the present invention wires inlay technique, constitutes the decorative pattern of cloisonne ' products with gold silk, substitutes traditional copper tire cloisonné and wires inlay technique, and the welding agent of making base used in technique, fusing point is high, is difficult to crack when freezing, and welding is easily.The method is compared with traditional handicraft, can be greatly shortened technical process, improves production efficiency.
(3) present invention uses brilliant white glaze handicraft and twice mill blue, and the artware color obtained is more preferable, with the passing of time as new, and Never-rusty.
(4) the golden tire cloisonné of the present invention can make the various artwares such as various drinking utensils, tea set, vase, bracelet, high-grade, both artistic and practical, and reserve value is high, can meet the artistic treat that people are high-level.
Detailed description of the invention
Example 1 :A kind of welding agent in the gold tire melting welding cloisonne ' products that wires inlay, is made up of the composition of following percentage by weight: the gold of 58.5%, the silver of 7.5%, the rose copper of 29%, the cadmium of 5%, it is possible to additionally incorporate the arsenic trioxide of above weight composition 25%.
Example 2 :A kind of welding agent in the gold tire melting welding cloisonne ' products that wires inlay, its percentage by weight forms: the gold of 55%, the silver of 8%, the rose copper of 32%, the cadmium of 5%, it is possible to additionally incorporate the arsenic trioxide of above weight composition 26%.
Example 3 :A kind of welding agent in the gold tire melting welding cloisonne ' products that wires inlay, its percentage by weight forms: the gold of 60%, the silver of 6%, the rose copper of 27%, the cadmium of 7%, the another arsenic trioxide adding above weight composition 22%.
Example 4 :The manufacture method of a kind of gold tire melting welding cloisonne ' products that wires inlay, comprises the following steps:
(1) make base: gold sheet is cut into cloisonne ' products size, carry out spinning, welding, obtain complete gold tire；
Wherein during welding, medicated powder composition by weight percentage is: gold 90%, silver 5%, copper 4%, zinc 1%.
(2) wire inlay: with the most flat gold silk as lines, transfer according to the bending of decorative pattern with tweezers, pinch into pattern；
(3) upper silk: the gold silk wired inlay is put into stove fire and fires, after gold silk deliquescing, clamps gold silk with tweezers and dips in Pseudobulbus Bletillae (Rhizoma Bletillae) slurry, be bonded on gold tire by gold silk according to pattern；When firing, temperature is 300-600 DEG C, and the firing time is the 30-60 second；
(4) freezing: uniformly spray water on gold tire, the most uniformly spread last layer gold solder medicated powder and Borax, the weight ratio of gold solder medicated powder and Borax is 3:1；Gold tire is heated to 780-900 DEG C, makes gold solder medicated powder melt, gold wire bond is connected on gold tire；
Wherein gold solder medication powder composition is: the gold of 58.5%, the silver of 7.5%, the rose copper of 29%, the cadmium of 5%, it is possible to additionally incorporate the arsenic trioxide of above Ingredient Wt 25%；During the fusing of gold solder medicated powder, first by gold, silver, rose copper fusing, it is subsequently adding cadmium and arsenic trioxide；
(5) pickling: the gold tire after freezing carries out pickling three times, each 10-12 minute；Wherein pickling temperature is 40 DEG C, and acid used is the hydrochloric acid of 20%；
(6) fill enamel: according in the gold reel frame that the enamel glaze got ready is filled on gold tire by the color indicated, it is sintered, sintering temperature is 790-820 DEG C, and after heating, enamel glaze is molten into liquid, becomes the color glaze layer anchored on carcass after cooling；If color glaze layer is less than the frame height of gold silk, then it is again filled with enamel glaze, sintering, 3-4 time the most repeatedly, until color glaze layer is equal with gold reel frame；
(7) mill indigo plant: the semi-finished product obtained are placed on the blue machine of mill and polish with the quartzy stone grinder of 50 mesh, 150 mesh respectively；
(8) upper brilliant white glaze: last layer brilliant white glaze equably on the semi-finished product after polishing, sinters after drying again, and sintering temperature is 790-820 DEG C；
(9) indigo plant is again ground: semi-finished product are placed on mill Lan Jishang, first polish with the quartzy stone grinder of 400 mesh；Fine grinding is carried out the most respectively with 400 mesh, 800 mesh, the waterproof abrasive paper of 1500 mesh；
(10) polishing, gold-plated: the semi-finished product after fine grinding are polished, electroplate, finally obtains finished product.
Example 5 :Identical with embodiment 4 step, difference is following technological parameter:
(1) upper silk: firing temperature is 300 DEG C, and the firing time is 60 seconds；
(2) freeze: gold tire is heated to 780 DEG C, make gold solder medicated powder melt, gold wire bond is connected on gold tire；
Wherein gold solder medication powder composition is: the gold of 55%, the silver of 8%, the rose copper of 32%, the cadmium of 5%, it is possible to additionally incorporate the arsenic trioxide of above weight 26%；
(3) pickling: the gold tire after freezing carries out pickling three times, each 10 minutes；
(4) fill enamel: sintering temperature is 800 DEG C；
(5) upper brilliant white glaze: uniform last layer brilliant white glaze on the semi-finished product of polishing, sinters after drying again, and sintering temperature is 800 DEG C.
Example 6 :Identical with embodiment 4 step, difference is following technological parameter:
(1) upper silk: firing temperature is 600 DEG C, and the firing time is 30 seconds；
(2) freeze: gold tire is heated to 900 DEG C, make gold solder medicated powder melt, gold wire bond is connected on gold tire；
Wherein gold solder medication powder composition is: the gold of 60%, the silver of 6%, the rose copper of 27%, the cadmium of 7%, it is possible to additionally incorporate the arsenic trioxide of above weight composition 22%；
(3) pickling: the gold tire after freezing carries out pickling three times, each 12 minutes；
(4) fill enamel: sintering temperature is 820 DEG C；
(5) upper brilliant white glaze: uniform last layer brilliant white glaze on the semi-finished product of polishing, sinters after drying again, and sintering temperature is 820 DEG C.
Example 7 :Identical with embodiment 4 step, difference is following technological parameter:
(1) upper silk: firing temperature is 500 DEG C, and the firing time is 50 seconds；
(2) freeze: gold tire is heated to 790 DEG C, make gold solder medicated powder melt, gold wire bond is connected on gold tire；
Wherein gold solder medication powder composition is: the gold of 58%, the silver of 7%, the rose copper of 30%, the cadmium of 5%, it is possible to additionally incorporate the arsenic trioxide of above weight composition 24%；
(3) pickling: the gold tire after freezing carries out pickling three times, each 10-12 minute；
(4) fill enamel: sintering temperature is 810 DEG C；
(5) upper brilliant white glaze: uniform last layer brilliant white glaze on the semi-finished product of polishing, sinters after drying again, and sintering temperature is 810 DEG C.
Claims (6)
1. the welding agent in the gold tire melting welding cloisonne ' products that wires inlay, it is characterized in that: this welding agent is made up of the composition of following percentage by weight: the gold of 55-60%, the silver of 6-8%, the rose copper of 27-32%, the cadmium of 4-7%, it is possible to additionally incorporate the arsenic trioxide of above Ingredient Wt 22-26%.
2. welding agent as claimed in claim 1, is characterized in that: the composition of described welding agent is: the gold of 58.5%, the silver of 7.5%, the rose copper of 29%, the cadmium of 5%, it is possible to additionally incorporate the arsenic trioxide of above Ingredient Wt 25%.
3. the manufacture method of the gold tire melting welding cloisonne ' products that wires inlay, it is characterised in that the method comprises the following steps:
(1) make base: gold sheet is cut into cloisonne ' products size, carry out spinning, welding, obtain complete gold tire；
(2) wire inlay: with the most flat gold silk as lines, transfer according to the bending of decorative pattern with tweezers, pinch into pattern；
(3) upper silk: the gold silk wired inlay is put into stove fire and fires, after gold silk deliquescing, clamps gold silk with tweezers and dips in Pseudobulbus Bletillae (Rhizoma Bletillae) slurry, be bonded on gold tire by gold silk according to pattern；
(4) freezing: uniformly spray water on gold tire, the weight ratio the most uniformly spreading last layer welding agent and Borax, welding agent and Borax is 3:1；Gold tire is heated to 780-900 DEG C, makes welding agent melt, gold wire bond is connected on gold tire；
Wherein welding agent with the composition of percentage by weight is: the gold of 55-60%, the silver of 6-8%, the rose copper of 27-32%, the cadmium of 4-7%, it is possible to additionally incorporate the arsenic trioxide of above Ingredient Wt 22-26%；During the fusing of this welding agent, first by gold, silver, rose copper fusing, it is subsequently adding cadmium and arsenic trioxide；
(5) pickling: the gold tire after freezing carries out pickling three times, each 10-12 minute；
(6) fill enamel: according in the gold reel frame that the enamel glaze got ready is filled on gold tire by the color indicated, it is sintered, sintering temperature is 790-820 DEG C, and after heating, enamel glaze is molten into liquid, becomes the color glaze layer anchored on carcass after cooling；If color glaze layer is less than the frame height of gold silk, then it is again filled with enamel glaze and sinters, 3-4 time the most repeatedly, until color glaze layer is equal with gold reel frame；
(7) mill indigo plant: the semi-finished product obtained are placed on mill Lan Jishang, polish with the quartzy stone grinder of 50 mesh, 150 mesh respectively；
(8) upper brilliant white glaze: last layer brilliant white glaze equably on the semi-finished product after polishing, sinters after drying again, and sintering temperature is 790-820 DEG C；
(9) indigo plant is again ground: semi-finished product are placed on mill Lan Jishang, first polish with the quartzy stone grinder of 400 mesh；Fine grinding is carried out the most respectively with 400 mesh, 800 mesh, the waterproof abrasive paper of 1500 mesh；
(10) polishing, gold-plated: the semi-finished product after fine grinding are polished, electroplate, finally obtains finished product；
Described pickling temperature is 40 DEG C, and acid used is the hydrochloric acid of 20%.
Manufacture method the most according to claim 3, it is characterised in that in described step (1) during welding, welding medicated powder composition by weight percentage is: gold 90%, silver 5%, copper 4%, zinc 1%.
5., according to the manufacture method described in claim 3 or 4, it is characterised in that when firing in stove fire in described step (3), temperature is 300-600 DEG C, the firing time is the 30-60 second.
6., according to the manufacture method described in claim 3 or 4, it is characterised in that the composition of described welding agent is: the gold of 58.5%, the silver of 7.5%, the rose copper of 29%, the cadmium of 5%, it is possible to additionally incorporate the arsenic trioxide of above Ingredient Wt 25%.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310644635.0A CN103624863B (en) | 2013-12-05 | 2013-12-05 | Welding agent in the gold tire melting welding cloisonne ' products that wires inlay and the manufacture method of cloisonne ' products |
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| CN201310644635.0A CN103624863B (en) | 2013-12-05 | 2013-12-05 | Welding agent in the gold tire melting welding cloisonne ' products that wires inlay and the manufacture method of cloisonne ' products |
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| CN103624863A CN103624863A (en) | 2014-03-12 |
| CN103624863B true CN103624863B (en) | 2016-09-21 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110370848A (en) * | 2019-07-23 | 2019-10-25 | 江苏贲泰珐琅文化有限公司 | Transparent enamel method is sintered in the copper tire of production cloisonne enamel and copper wire surface |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106218295A (en) * | 2016-07-29 | 2016-12-14 | 安庆帝雅艺术品有限公司 | One is wired inlay technique |
| CN106240217A (en) * | 2016-08-26 | 2016-12-21 | 河南梦祥纯银制品有限公司 | A kind of thread weaving enamel silverware and preparation method thereof |
| CN106183600A (en) * | 2016-08-28 | 2016-12-07 | 郭漫笳 | A kind of preparation method of copper art parquet decorative board |
| CN108749447B (en) * | 2018-06-27 | 2020-07-21 | 河南梦祥纯银制品有限公司 | Silver-body enamel and manufacturing method thereof |
| CN109530965B (en) * | 2018-12-28 | 2020-11-10 | 云南乌铜走银文化产业有限公司 | Soldering lug for manufacturing black copper by silver and preparation method thereof |
| CN110747471B (en) * | 2019-11-05 | 2022-02-11 | 深圳宝福珠宝有限公司 | Method for processing color-changing enamel applied to metal surface |
| CN111962078A (en) * | 2020-08-21 | 2020-11-20 | 深圳明丰珠宝首饰有限公司 | Technology for combining ancient gold with enamel |
| CN115255694A (en) * | 2022-08-13 | 2022-11-01 | 苏州欧纳菲文化发展有限公司 | Welding process of gold small beads |
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| CN1644402A (en) * | 2005-01-31 | 2005-07-27 | 苗新田 | Cloisonne enamel production |
| US8231969B2 (en) * | 2008-03-26 | 2012-07-31 | University Of Utah Research Foundation | Asymmetrically functionalized nanoparticles |
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| CN110370848A (en) * | 2019-07-23 | 2019-10-25 | 江苏贲泰珐琅文化有限公司 | Transparent enamel method is sintered in the copper tire of production cloisonne enamel and copper wire surface |
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