CN103622866B - Perfume capable of whitening and preparation method thereof - Google Patents

Perfume capable of whitening and preparation method thereof Download PDF

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CN103622866B
CN103622866B CN201310557255.3A CN201310557255A CN103622866B CN 103622866 B CN103622866 B CN 103622866B CN 201310557255 A CN201310557255 A CN 201310557255A CN 103622866 B CN103622866 B CN 103622866B
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CN103622866A (en
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胡云福
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AGATE PERFUME (MINGGUANG) Co Ltd
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AGATE PERFUME (MINGGUANG) Co Ltd
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Abstract

The invention provides a preparation method of a perfume, in particular relates to a perfume capable of whitening, and belongs to the technical field of daily cosmetics. The perfume comprises bergamot, lemon, grapefruit, jasmine, rose, rosemary, basil, mint, foeniculum vulgare, bush cinquefoil, russianolive flower, cnidium officinale root, elsholtzia, green tea, vitamin E, bletilla striata, olive oil, angelica sinensis, simmered ginger, radix ophiopogonis, pseudo-ginseng, selaginella tamariscina, cortex fraxini, centella asiatica, semen cuscutae, SPAN-80, ethyl p-hydroxybenzoate, sodium alginate, methylpropanediol, dipotassium glycyrrhizinate, panaxoside, sodium pyrrolidone carboxylic acid, hydrogenated soybean lecithin, and ethanol solution. The perfume capable of whitening is fragrant and has a certain whitening effect.

Description

A kind of perfume with whitening effect and preparation method thereof
Technical field
The invention provides a kind of preparation method of perfume, particularly relate to a kind of perfume with whitening function, belong to household chemicals technical field.
Background technology
Skin is organ the most widely in human body.But it affected by factors such as systemic physiological state, nutrition, environment, emotions.During as nutritional disorder, subcutaneous fat reduces; Skin edema can be caused during anemia; Emotion changes also can affect skin, and then skin is easily aging for the long-term depressed unhappiness of emotion, even promotes that poliosis generates.
The color of skin is different because of ethnic group, sex, age, season etc.Difference between each ethnic group is very large.Ethnic group is in the world broadly divided into white race, the yellow race, black race, and therefore, the colour of skin is adularescent, yellow, black also.These colours of skin are that the light at random in pigment and skin face contained by skin and skin internal reflected light formed.The inherent colour of skin that cannot change then is decided by pigment contained in skin histology.Skin pigment metabolism mainly by genetic determination, the not impact of light, the main cause of ethnic group colour of skin difference that Here it is.In sex, male enriches than the pigment of women; Older enriches than the pigment of year the lighter in years.
The color of normal skin depends on three factors: 1, the concentration and distribution situation of various pigment in skin: the coloring matter of skin mainly contains melanin, carotene.The color of skin and hair is not depend on melanocytic quantity, but depends on the quantity of melanosome, size, distribution and melanocyte degree.The yellow race is more containing carotene, is stored in corium and subcutaneous tissue more.Thorax abdomen and buttocks more, face less.2, the ratio of hemoglobin oxidation reduction in skin blood: hemoglobin (hematochrome) pinkiness, HbO2 Oxyhemoglobin are cerise, reduced hemoglobin is kermesinus.3, the thickness of skin and light are in the scattering of skin surface.Present yellow when horny layer is thicker, granular layer, clear layer are thicker, whitening color.Epidermis is thinner, more has transparent feel, can through more blood pigment, thus make skin blushing.The position that skin is thicker, light therethrough rate variance, can only see the carotene in horny layer, and skin is in yellow.The skin of old people, due to corium elastic fibrosis fracture, flexibility decrease, skin blood is transported poor and is yellow in addition.
How to reach whitening effect, at present mainly through two approach: (one) check melanin generates; 1, restraint of tyrosinase is active; 2, melanocyte proliferation is suppressed; (adding endothelin antagonist) 3, antioxidant.(2) impel the melanin generated to excrete skin pigment to get rid of external mode and also have two kinds: 1, pigment can shift to horny layer voluntarily gradually under certain condition, finally come off with aging horn cell and excrete.2, after pigment is decomposed, dissolves and absorbs in skin, excrete through blood circulation in vivo.
Perfume is a kind of liquid being mixed with essential oil, fixative and ethanol or ethyl acetate, is used for allowing object (normally human body) have the abnormal smells from the patient of lasting and happy people.Quintessence oil is taken from flowers and plants plant, inhales method extraction, also can use fragrant Organic substance with the way of distillation or fat.Time immemorial, people just used spice to change human scent, and the use of spice also to use and as the patent of the ruling class.People constantly create more novel unique essence, thus constitute the part in the perfume world, and this trend has become the mark in the epoch of our life.Allow perfume have the function of benefit, develop more perfume type and have an important significance.
Summary of the invention
The object of this invention is to provide a kind of perfume with skin-whitening effect, the technical scheme of employing is:
A kind of perfume with whitening effect, include following component by weight: Fructus Citri Sarcodactylis 30 ~ 50 parts, 20 ~ 30 parts, Fructus Citri Limoniae, grapefruit 10 ~ 20 parts, jasmine 30 ~ 50 parts, 30 ~ 50 parts, Flos Rosae Rugosae, Herba Rosmarini Officinalis 10 ~ 20 parts, Herba Ocimi (Herba Ocimi Pilosi) 10 ~ 20 parts, Herba Menthae 10 ~ 20 parts, 10 ~ 20 parts, Fructus Foeniculi, bush cinqefoil 5 ~ 10 parts, Flos Elaeagni Angustifoliae 10 ~ 20 parts, Rhizoma Chuanxiong root 5 ~ 10 parts, Herba Moslae 5 ~ 10 parts, green tea 60 ~ 100 parts, vitamin e1 5 ~ 30 parts, the Pseudobulbus Bletillae (Rhizoma Bletillae) 5 ~ 10 parts, 15 ~ 20 parts, olive oil, Radix Angelicae Sinensis 5 ~ 10 parts, Roast Rhizoma Zingiberis Recens 5 ~ 10 parts, Radix Ophiopogonis 5 ~ 10 parts, Radix Notoginseng 5 ~ 10 parts, Herba Selaginellae 6 ~ 12 parts, Cortex Fraxini 3 ~ 6 parts, Herba Centellae 3 ~ 6 parts, Semen Cuscutae 3 ~ 6 parts, SPAN-802 ~ 3 part, ethylparaben 2 ~ 3 parts, sodium alginate 2 ~ 3 parts, methyl propanediol 1 ~ 2 part, glycyrrhizic acid dipotassium 1 ~ 3 part, ginsenoside 2 ~ 4 parts, pyrrolidone sodium carboxylate 3 ~ 6 parts, hydrogenated soy phosphatidyl choline 3 ~ 6 parts, alcoholic solution 80 ~ 100 parts.
The volumetric concentration of described alcoholic solution is preferably between 95%-98%, and solvent is water.
Span-80 of the present invention has another name called class 80 of department, and sorbitan fatty ester is senior lipophilic emulsifier.
Fructus Citri Sarcodactylis is the fruit of rutaceae Fructus Citri Sarcodactylis Citrus medica L.var.sarcodactylis Swingle.The fruit colour of hands is golden yellow, gives off a strong fragrance, and shape is peculiar in hands, in different poses and with different expressions, allows people feel very witty.Fructus Citri Sarcodactylis not only has higher ornamental value, and has precious medical value, economic worth.The each provinces and regions of south China are cultivated in flower garden or orchard more.Peel and leaf contain aromatic oil, have strong fresh fruit delicate fragrance, are perfumery raw material; Fruit and the equal hyoscine of flower.
Fructus Citri Limoniae (Citrus limon) is the fruit of the evergreen dungarunga of Rutaceae both citrus, originates in Southeast Asia, and the existing main place of production is the U.S., Italy, Spain and Greece.Fruit is rich in vitamin C and citric acid.The Fructus Citri Limoniae oil of tool peat-reek is had, also containing Citrin in peel oil vacuole.Citric acid has the effect preventing and eliminate cutaneous pigmentation.Fructus Citri Limoniae contains nicotinic acid and abundant organic acid, and its taste is extremely sour, containing abundant potassium, sodium, so Fructus Citri Limoniae is base-forming food.Be conducive to human body acid-base degree.Citric acid juice has very strong bactericidal action, very beneficial to food hygiene, and experiment display, the extremely strong Fructus Citri Limoniae juice of acidity can kill antibacterials all in SeaShell in 15 minutes.
Grapefruit English Grapefruit, Pomelo by name, have skin thin, the features such as red pulp.One of primary raw material of its being Zhuan Pin ﹑ perfume.Grapefruit and fruit juice thereof in North America, European Countries and Japan, be fruit and the beverage of a lot of families breakfast indispensability, become consumption figure in citrus fruit and be only second to the key farm products of Fructus Citri sinensis.Grapefruit comes from Asia, plants in India, and Japan, the history in North America and basin, Mediterranean is also quite permanent.Mainly because its fruit, just widely planted.Grapefruit has clean effect with moistening for skin.Active ingredient contained by it, as: carbohydrate, aminoacid and fruit acid, all have effect that is moist and the clean skin of deep layer, flavonoid can increase permeability and the resistance of capillary wall.The combined effect that these compositions produce, allows grapefruit have perfect purification function.Containing valuable natural complex P and abundant vitamin C and soluble cellulose in grapefruit.Citrin can strengthen the function of skin and pore, is conducive to skin care and beauty treatment.Vitamin C can participate in human body collagen protein synthesis, the generation of enhancing antibody, to strengthen the function of detoxification of human body.
Jasmine Jasminum sambac (Linn.) Aiton, be the flower of Oleaceae gelsemium evergreen shrubs or liana, originate in India, Pakistan, China introduces a fine variety already, and plants widely.Jasmine happiness warm and moist and sunny environment, its leaf color jade green, flower color is pure white, gives off a strong fragrance, and is modal armaticity potted flowers.In gelsemium, foremost one is bivalve jasmine, namely the Flos Jasmini Sambac that is usually commonly called as of people.Jasmine has good health care and beauty functions, can be used for diet, can be used for the making of Jasmine tea.
Flos Rosae Rugosae (formal name used at school: Rosa rugosa) is the flower of Rosaceae gul, is a series of general designation spending cultivar gorgeous greatly of Rosa in daily life.Rosaceae chamiso, as crops, its flower is mainly used in food and refines essence Oleum Rosae Rugosae, Oleum Rosae Rugosae than etc. weight gold value high, be applied to the industry such as cosmetics, food, stock solution, fine chemistry industry.
Herba Rosmarini Officinalis is the leaf of labiate Rosmarinus officinalis, and repeatedly Herba Pelargonii Graveolentis is fragrant with tea, and peppery, the micro-hardship of acrid in the mouth, is often used in culinary art, also can be used to bubble Herb Tea and drinks.Evergreen shrubs, thinks Herba Rosmarini Officinalis energy hypermnesis ancient times, and the most antioxidant content had in the plant rosemary of antioxidation of generally acknowledging at present is mainly the compositions such as carnosic acid, carnosol, rosmanol, ursolic acid, rosmarinic acid.Herba Rosmarini Officinalis also is usually placed in indoor to purify air.
Herba Ocimi (Herba Ocimi Pilosi) (Ocimun basilicum L.), English Basil by name, be Labiatae basil, draft, with all herbal medicine, is famous medicine-food two-purpose fragrant plant.Stem, leaf and spica are containing aromatic oil, its main component is careless ligusticumic element (content is about 55%), linalool (content 34.5-40%) and other are as linalyl acetate, eugenol etc., main as perfumery raw material, preparing cosmetics, soap are used and edible essence, also for making correctives in toothpaste processed, collutory.Tender leaf is edible, and drink of also can making tea, has wind dispelling, fragrance, stomach invigorating and perspiration.
Herba Menthae is the aerial parts for Labiatae (Labiatae) perennial root herbaceous plant Mentha (Mentha), is a kind of fragrant crop having extraordinary economic worth.Mentholum and Oleum menthae have special fragrance, pungent sense and cool feeling, are mainly used in the perfuming of toothpaste, food, Nicotiana tabacum L., wine, refreshment drink, cosmetics, fancy soap; Pharmaceutically be widely used in the medicines such as wind dispelling, anticorrosion, antiinflammatory, analgesia, antipruritic, stomach invigorating.Fresh leaf is containing volatile oil 0.8 ~ 1%, and scapus leaf is containing 1.3 ~ 2%.In oil, main constituent is menthol (Menthol), content about 77 ~ 78%, secondly be menthone (Menthone), content is 8 ~ 12%, also containing acetic acid peppermint ester (Menthyl acetate), camphene (Camphene), limonene (Limonene), isomenthone (Isomenthone), pinene (Pinene) piperitenone (Menthenone), resin and a small amount of tannin, rosmarinic acid (Rosmarinicacid).
Fructus Foeniculi Foeniculum vulgare is the fruit of Foeniculum plant Fructus Foeniculi, and the main component of Fructus Foeniculi is protein, fat, dietary fiber, anethole, fenchone, anisaldehyde etc.Its fragrance is mainly from the fragrance matter such as anethole, anisaldehyde.Integrate medicine, seasoning, edible, the multipurpose plant of making up.Tender stem, leaf make vegetable, filling food, containing Oleum Anisi Stellati 2.8% in Fructus Foeniculi fruit, and anethole 50 ~ 60%, a-fenchone 18 ~ 20%, methyl Fructus Piperis powder 10% and a-pinene double focusing amylene, anisaldehyde, camphene etc.
Bush cinqefoil (PotentillafruticosaL.) is also called Dasiphora fruticosa (L.) Rydb, golden wax prunus mume (sieb.) sieb.et zucc., Rosaceae (Rosaceae) Potentilla (PotentillaL.) machaka, because of brightly yellowish color, gain the name like prunus mume (sieb.) sieb.et zucc., be born between the rock of mountain top or in shrubbery.Machaka.Imparipinnate leaf, there is thread pubescence on two sides.Produce Northeast China, North China, northwest, southwestern various places; Also there is distribution Japan, Mongolia, Europe, North America.Its flower or leaf can extract spice.
Fructus Elaeagni Angustifoliae Elaeagnus angustifolia L. calls silver-colored willow, is the shrub of Elaeangnaceae Elaeagnus, containing ethereal oil in its flower, can extract.Fruit is containing flavonoid.Sugary 43 ~ the 59%(of sarcocarp 20% is wherein fructose), protein about 10%, a small amount of tannin and phlegmatic temperament.Root and aerial parts are the good sources of Harman alkaloid, containing 3-methyl-4-carboline, harmol, harmine etc.Leaf is containing caffeic acid, chlorogenic acid, neochlorogenic acid, vitamin C 140 ~ 350 milligrams, flavonoid.
Rhizoma Chuanxiong root is Umbelliferae, and the root of Rhizoma Chuanxiong platymiscium Rhizoma Chuanxiong Ligusticum wallichii Franch, has 40 kinds containing the fuel-displaced middle composition of volatile oil about 1%. qualification, account for 93.64% of volatile oil, and wherein main constituent is that ligustilide (ligustilide) accounts for 58%, lactone compound contained in 3-Ding Fu lactone (3-butylphthalide) 5.29% and sabinene (sabinene) 6.08%. rhizome, except above-mentioned two kinds of mentioning, still containing Ding Xi Fu lactone (butylidene phthalide), cnidium lactone (sankyunolide), neocindilide (neocnidilide), 4-hydroxyl-3-Ding Fu lactone (4-hydroxy-3-butyl phthalide), chuanxingol (chuanxingol), Diligustilide (2,2 '-diligustilide), and 3-butyl-3,6,7. trihydroxy-4,5,6,7-tetrahydrochysene Phthalide etc. nitrogen-containing compound has tetramethylpyazine (tetramethylpyrazine, ligustrazine, chuanxiongzine), perlolyrine, trimethylamine hydrochloride, choline hydrochloride, L-isoleucyl--Valine acid anhydride (L-isobutyl-L-valine anhydride), L-valyl-Valine acid anhydride, 1-acetyl group-β-Ka quinoline, uracil, Xian Piao ridge and adenosine. acid or phenoloid has 4-hydroxy 3-methoxybenzene ethylene, 1-hydroxyl-1-(3-methoxyl group 4-hydroxy benzenes)-ethane, 4-HBA, caffeic acid, vanillic acid, ferulic acid (ferulic acid), sedanoic acid (sadanic acid), chrysophanic acid (chrysophic acid), Palmic acid, vanillin and linoleic acid. in addition, Rhizome of Ligusticum Sinense Oliv. Cv. Chuanxiong is still containing neutral oil, and its composition is 15, 16, 17, octadecanoid acid ethyl ester, different 17, isooctadecane acetoacetic ester and different methyl margarate. separately feed formyl ether (bis-5,5 '-formylfurfuryl ether) containing 5,5 '-Lian furan, spathulenol (spathulenol), Sitosterolum, sucrose and a kind of fatty glyceride.
Herba Moslae is the dry aerial parts of labiate Herba Moslae Mosla chinensis Maxim..Herb has enhanced aroma.Herba Moslae congener Herba Moslae herb is containing volatile oil 0.2%-1%, and fresh stem and leaf is containing volatile oil 0.26%-0.59%, and scapus leaf is containing 0.8%-2%, main containing elsholtziakesone (elsholtzione) about 85% in oil, 1-Phenylethanone. (acetophenone) about 1% [3.4]。Also containing 6-methyl tritriacontane (6-methyl-tritria contane), 13-cyclohexyl hexacosane (13-cyclohexylhexacosane), cupreol (β-sitosterol), cupreol-3-β-D-Glucose glycoside (β-sitosterol-3-β-D-glucoside), Palmic acid (palmitic acid), linoleic acid (linoleic acid), linolenic acid (linolenic acid), ursolic acid (urso-lic acid)), 5-hydroxyl-6, 7-dimethoxy flavone (5-hydroxy-6, 7-dimetho-xyflavone), 5-hydroxyl-7, 8-dimethoxy flavone (5-ydroxy-7, 8-dimethoxy-flavone), 5, 7-dihydroxy-4-methoxyl group flavanone (5-hydroxy-7, 4-dimethoxyflavanone), 5-hydroxyl-6-methoxyl group flavanone-7-O-α-D-galactopyranosyl glucoside (5-hydroxy-6-methoxyflavanone-7-α-D-galactopyranosi-de), acacetin-7-O-β-D-Glucose (acacetin-7-O-β-D-glucoside).Volatile oil has broad-spectrum antiseptic and bactericidal action, and has the effect directly suppressing influenza virus.
The tea polyphenols contained in green tea, catechin, chlorophyll, caffeine, aminoacid, vitamins and other nutritious components are also more.These natural nutrition compositions in green tea, having special-effect to anti-aging, anti-cancer, anticancer, sterilization, antiinflammatory etc., is less than other teas.Oleum Camelliae content in green tea is more, has special fragrance.
The Pseudobulbus Bletillae (Rhizoma Bletillae) has the functions such as convergence, hemostasis, delay skin aging, moisturizing, to treatment with prevent skin chilblain and chap, blood circulation promoting, improve skin-nourishing situation and prevent wrinkle etc. to have obvious curative effects, and without side reaction and toxicity.Therefore, its energy Glycerin, beauty treatment speckle removing, makes skin as smooth as jade.
Olive oil can wrinkle resistant, smooth careful skin, pore refining, increases gloss and the elasticity of skin, compact and moisturizing, skin whitening, anti-canthus wrinkle.
SPAN-80 is oil-in-water emulsifiers, is conducive to the dispersed of olive oil, be conducive to improving form the stability of perfume.
Radix Angelicae Sinensis has antigonadotropic effect, and its main component ferulic acid can suppress pituitary lutropin and prolactin antagonist, and antagonising gonadotropin discharges, and restraint of tyrosinase is active, prevents oxidizing tyrosine from forming pigment.
Roast Rhizoma Zingiberis Recens has removes interior free yl, antioxidative effect, and the effect of antiinflammatory sterilization and promotion Transdermal absorption.
Radix Notoginseng: containing Saponin, is mainly ginsenoside Rb1, Rg1, Rg2 and a small amount of ginsenoside Ra, Rb2, Rb and Re.
In addition, still containing flavonoid glycoside, starch, protein, oils and fats etc.Nature and flavor: warm in nature, sweet in the mouth, micro-hardship.Function cures mainly: dissipating blood stasis stops blooding, subduing swelling and relieving pain.For various inside and outside hemorrhage, breast ventral spine pain, tumbling and swelling.
The composition possessing astriction in ginsenoside is more, also has contractive effect to skin, and can regulate corium water balance, prevents skin dehydration, and the originality can restraining again dark black element can make skin become smooth, tender, pure white.So its energy delay skin aging, increase the elasticity of skin, thus play the effect that protection skin gloss is tender, prevent and cut down wrinkle of skin, Radix Ginseng active substance also possesses the reducing property of restraining dark black element, makes skin pure white smooth.
Herba Selaginellae and Herba Selaginellae, have inhibitory action to lipoxidase.Lipoxidase is by the enzyme of unsaturated fatty acids acid oxidase, and unsaturated fatty acid oil is the main component forming cell membrane, therefore be also an aspect of skin anti-aging to the suppression of lipoxidase, Herba Selaginellae extract has eliminating effect to superoxide radical, may be used for the aging resistance of skin; There is powerful suppression to melanocyte activity during Herba Selaginellae extract low concentration, may be used for the cosmetics removing skin splash; Its performance of keeping humidity is better than Aloe.
Cortex Fraxini has heat clearing away, removing fire from the liver effect.
Another object of the present invention is to provide a kind of preparation method of above-mentioned whitening perfume, comprises the steps:
S1: get Fructus Citri Sarcodactylis, Fructus Citri Limoniae, grapefruit, after cleaning, pulverize, be placed in boiler, steam is led directly to from the boiler the bottom of a pan, steam pressure 3 ~ 5atm, distills, and the gas that distillation produces is collected in condensation, distillation time is 1 ~ 1.5h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils I;
S2: get jasmine, Flos Rosae Rugosae, Herba Rosmarini Officinalis, Herba Ocimi (Herba Ocimi Pilosi), Herba Menthae, Fructus Foeniculi, bush cinqefoil, Flos Elaeagni Angustifoliae, Rhizoma Chuanxiong root, Herba Moslae, green tea, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3 ~ 5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 1 ~ 1.5h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils II;
S3: get the Pseudobulbus Bletillae (Rhizoma Bletillae), olive oil, Radix Angelicae Sinensis, Roast Rhizoma Zingiberis Recens, Radix Ophiopogonis, Radix Notoginseng, Herba Selaginellae, Cortex Fraxini, Herba Centellae, Semen Cuscutae, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3 ~ 5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 2 ~ 3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils III;
S4: get blend of essential oils I, blend of essential oils II, edible vegetable oil mixtures III, vitamin E, SPAN-80, ethylparaben, sodium alginate, methyl propanediol, glycyrrhizic acid dipotassium, ginsenoside, pyrrolidone sodium carboxylate, hydrogenated soy phosphatidyl choline, mix homogeneously, add alcoholic solution again, stir, leave standstill after 24 ~ 48 hours, put into sealed container, ageing is after 4 ~ 8 weeks.
Grope through lot of experiments, optimum proportioning raw materials and preparation technology are:
Take following raw materials according: Fructus Citri Sarcodactylis 44 weight portion, Fructus Citri Limoniae 21 weight portion, grapefruit 17 weight portion, jasmine 38 weight portion, Flos Rosae Rugosae 45 weight portion, Herba Rosmarini Officinalis 16 weight portion, Herba Ocimi (Herba Ocimi Pilosi) 12 weight portion, Herba Menthae 13 weight portion, Fructus Foeniculi 17 weight portion, bush cinqefoil 8 weight portion, Flos Elaeagni Angustifoliae 19 weight portion, Rhizoma Chuanxiong root 7 weight portion, Herba Moslae 6 weight portion, green tea 95 weight portion, vitamin E2 4 weight portion, the Pseudobulbus Bletillae (Rhizoma Bletillae) 7 weight portion, olive oil 18 weight portion, Radix Angelicae Sinensis 8 weight portion, Roast Rhizoma Zingiberis Recens 9 weight portion, Radix Ophiopogonis 6 weight portion, Radix Notoginseng 6 weight portion, Herba Selaginellae 9 weight portion, Cortex Fraxini 4 weight portion, Herba Centellae 4 weight portion, Semen Cuscutae 4 weight portion, SPAN-803 weight portion, ethylparaben 3 weight portion, sodium alginate 3 weight portion, methyl propanediol 2 weight portion, glycyrrhizic acid dipotassium 1 weight portion, ginsenoside 3 weight portion, pyrrolidone sodium carboxylate 3 weight portion, hydrogenated soy phosphatidyl choline 5 weight portion, alcoholic solution 95 weight portion.
Preparation method:
S1: get Fructus Citri Sarcodactylis, Fructus Citri Limoniae, grapefruit, after cleaning, pulverize, be placed in boiler, steam is led directly to from the boiler the bottom of a pan, steam pressure 4.1atm, distills, and the gas that distillation produces is collected in condensation, distillation time is 1.2h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils I;
S2: get jasmine, Flos Rosae Rugosae, Herba Rosmarini Officinalis, Herba Ocimi (Herba Ocimi Pilosi), Herba Menthae, Fructus Foeniculi, bush cinqefoil, Flos Elaeagni Angustifoliae, Rhizoma Chuanxiong root, Herba Moslae, green tea, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 4.4atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 1.3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils II;
S3: get the Pseudobulbus Bletillae (Rhizoma Bletillae), olive oil, Radix Angelicae Sinensis, Roast Rhizoma Zingiberis Recens, Radix Ophiopogonis, Radix Notoginseng, Herba Selaginellae, Cortex Fraxini, Herba Centellae, Semen Cuscutae, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3.5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 2.3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils III;
S4: get blend of essential oils I, blend of essential oils II, edible vegetable oil mixtures III, vitamin E, SPAN-80, ethylparaben, sodium alginate, methyl propanediol, glycyrrhizic acid dipotassium, ginsenoside, pyrrolidone sodium carboxylate, hydrogenated soy phosphatidyl choline, mix homogeneously, add alcoholic solution again, stir, leave standstill after 37 hours, put into sealed container, ageing is after 6 weeks.
Beneficial effect
Whitening perfume provided by the invention, not only fragrant odour, also has certain whitening function to skin.
Detailed description of the invention
Embodiment 1
Take following raw materials according: Fructus Citri Sarcodactylis 30kg, Fructus Citri Limoniae 20kg, grapefruit 10kg, jasmine 30kg, Flos Rosae Rugosae 30kg, Herba Rosmarini Officinalis 10kg, Herba Ocimi (Herba Ocimi Pilosi) 10kg, Herba Menthae 10kg, Fructus Foeniculi 10kg, bush cinqefoil 5kg, Flos Elaeagni Angustifoliae 10kg, Rhizoma Chuanxiong root 5kg, Herba Moslae 5kg, green tea 60kg, vitamin e1 5kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 5kg, olive oil 15kg, Radix Angelicae Sinensis 5kg, Roast Rhizoma Zingiberis Recens 5kg, Radix Ophiopogonis 5kg, Radix Notoginseng 5kg, Herba Selaginellae 6kg, Cortex Fraxini 3kg, Herba Centellae 3kg, Semen Cuscutae 3kg, SPAN-802kg, ethylparaben 2kg, sodium alginate 2kg, methyl propanediol 1kg, glycyrrhizic acid dipotassium 1kg, ginsenoside 2kg, pyrrolidone sodium carboxylate 3kg, hydrogenated soy phosphatidyl choline 3kg, alcoholic solution 80kg.
The volumetric concentration of described alcoholic solution is 98%, and solvent is water.
Preparation method:
S1: get Fructus Citri Sarcodactylis, Fructus Citri Limoniae, grapefruit, after cleaning, pulverize, be placed in boiler, steam is led directly to from the boiler the bottom of a pan, steam pressure 3atm, distills, and the gas that distillation produces is collected in condensation, distillation time is 1h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils I;
S2: get jasmine, Flos Rosae Rugosae, Herba Rosmarini Officinalis, Herba Ocimi (Herba Ocimi Pilosi), Herba Menthae, Fructus Foeniculi, bush cinqefoil, Flos Elaeagni Angustifoliae, Rhizoma Chuanxiong root, Herba Moslae, green tea, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 1h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils II;
S3: get the Pseudobulbus Bletillae (Rhizoma Bletillae), olive oil, Radix Angelicae Sinensis, Roast Rhizoma Zingiberis Recens, Radix Ophiopogonis, Radix Notoginseng, Herba Selaginellae, Cortex Fraxini, Herba Centellae, Semen Cuscutae, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 2h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils III;
S4: get blend of essential oils I, blend of essential oils II, edible vegetable oil mixtures III, vitamin E, SPAN-80, ethylparaben, sodium alginate, methyl propanediol, glycyrrhizic acid dipotassium, ginsenoside, pyrrolidone sodium carboxylate, hydrogenated soy phosphatidyl choline, mix homogeneously, add alcoholic solution again, stir, leave standstill after 24 hours, put into sealed container, ageing is after 4 weeks.
Embodiment 2
Take following raw materials according: Fructus Citri Sarcodactylis 50kg, Fructus Citri Limoniae 30kg, grapefruit 20kg, jasmine 50kg, Flos Rosae Rugosae 50kg, Herba Rosmarini Officinalis 20kg, Herba Ocimi (Herba Ocimi Pilosi) 20kg, Herba Menthae 20kg, Fructus Foeniculi 20kg, bush cinqefoil 10kg, Flos Elaeagni Angustifoliae 20kg, Rhizoma Chuanxiong root 10kg, Herba Moslae 10kg, green tea 100kg, vitamin E 30kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 10kg, olive oil 20kg, Radix Angelicae Sinensis 10kg, Roast Rhizoma Zingiberis Recens 10kg, Radix Ophiopogonis 10kg, Radix Notoginseng 10kg, Herba Selaginellae 12kg, Cortex Fraxini 6kg, Herba Centellae 6kg, Semen Cuscutae 6kg, SPAN-803kg, ethylparaben 3kg, sodium alginate 3kg, methyl propanediol 2kg, glycyrrhizic acid dipotassium 3kg, ginsenoside 4kg, pyrrolidone sodium carboxylate 6kg, hydrogenated soy phosphatidyl choline 6kg, alcoholic solution 100kg.
The volumetric concentration of described alcoholic solution is 98%, and solvent is water.
Preparation method:
S1: get Fructus Citri Sarcodactylis, Fructus Citri Limoniae, grapefruit, after cleaning, pulverize, be placed in boiler, steam is led directly to from the boiler the bottom of a pan, steam pressure 5atm, distills, and the gas that distillation produces is collected in condensation, distillation time is 1.5h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils I;
S2: get jasmine, Flos Rosae Rugosae, Herba Rosmarini Officinalis, Herba Ocimi (Herba Ocimi Pilosi), Herba Menthae, Fructus Foeniculi, bush cinqefoil, Flos Elaeagni Angustifoliae, Rhizoma Chuanxiong root, Herba Moslae, green tea, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 1.5h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils II;
S3: get the Pseudobulbus Bletillae (Rhizoma Bletillae), olive oil, Radix Angelicae Sinensis, Roast Rhizoma Zingiberis Recens, Radix Ophiopogonis, Radix Notoginseng, Herba Selaginellae, Cortex Fraxini, Herba Centellae, Semen Cuscutae, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils III;
S4: get blend of essential oils I, blend of essential oils II, edible vegetable oil mixtures III, vitamin E, SPAN-80, ethylparaben, sodium alginate, methyl propanediol, glycyrrhizic acid dipotassium, ginsenoside, pyrrolidone sodium carboxylate, hydrogenated soy phosphatidyl choline, mix homogeneously, add alcoholic solution again, stir, leave standstill after 48 hours, put into sealed container, ageing is after 8 weeks.
Embodiment 3
Take following raw materials according: Fructus Citri Sarcodactylis 40kg, Fructus Citri Limoniae 25kg, grapefruit 15kg, jasmine 35kg, Flos Rosae Rugosae 35kg, Herba Rosmarini Officinalis 15kg, Herba Ocimi (Herba Ocimi Pilosi) 15kg, Herba Menthae 15kg, Fructus Foeniculi 15kg, bush cinqefoil 6kg, Flos Elaeagni Angustifoliae 15kg, Rhizoma Chuanxiong root 8kg, Herba Moslae 8kg, green tea 80kg, vitamin E2 0kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 8kg, olive oil 17kg, Radix Angelicae Sinensis 7kg, Roast Rhizoma Zingiberis Recens 8kg, Radix Ophiopogonis 8kg, Radix Notoginseng 8kg, Herba Selaginellae 10kg, Cortex Fraxini 5kg, Herba Centellae 5kg, Semen Cuscutae 5kg, SPAN-803kg, ethylparaben 3kg, sodium alginate 3kg, methyl propanediol 2kg, glycyrrhizic acid dipotassium 1kg, ginsenoside 2kg, pyrrolidone sodium carboxylate 3kg, hydrogenated soy phosphatidyl choline 5kg, alcoholic solution 90kg.
The volumetric concentration of described alcoholic solution is 98%, and solvent is water.
Preparation method:
S1: get Fructus Citri Sarcodactylis, Fructus Citri Limoniae, grapefruit, after cleaning, pulverize, be placed in boiler, steam is led directly to from the boiler the bottom of a pan, steam pressure 4atm, distills, and the gas that distillation produces is collected in condensation, distillation time is 1.2h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils I;
S2: get jasmine, Flos Rosae Rugosae, Herba Rosmarini Officinalis, Herba Ocimi (Herba Ocimi Pilosi), Herba Menthae, Fructus Foeniculi, bush cinqefoil, Flos Elaeagni Angustifoliae, Rhizoma Chuanxiong root, Herba Moslae, green tea, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 4atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 1.3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils II;
S3: get the Pseudobulbus Bletillae (Rhizoma Bletillae), olive oil, Radix Angelicae Sinensis, Roast Rhizoma Zingiberis Recens, Radix Ophiopogonis, Radix Notoginseng, Herba Selaginellae, Cortex Fraxini, Herba Centellae, Semen Cuscutae, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3.5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 2.6h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils III;
S4: get blend of essential oils I, blend of essential oils II, edible vegetable oil mixtures III, vitamin E, SPAN-80, ethylparaben, sodium alginate, methyl propanediol, glycyrrhizic acid dipotassium, ginsenoside, pyrrolidone sodium carboxylate, hydrogenated soy phosphatidyl choline, mix homogeneously, add alcoholic solution again, stir, leave standstill after 35 hours, put into sealed container, ageing is after 7 weeks.
Embodiment 4
Take following raw materials according: Fructus Citri Sarcodactylis 44kg, Fructus Citri Limoniae 21kg, grapefruit 17kg, jasmine 38kg, Flos Rosae Rugosae 45kg, Herba Rosmarini Officinalis 16kg, Herba Ocimi (Herba Ocimi Pilosi) 12kg, Herba Menthae 13kg, Fructus Foeniculi 17kg, bush cinqefoil 8kg, Flos Elaeagni Angustifoliae 19kg, Rhizoma Chuanxiong root 7kg, Herba Moslae 6kg, green tea 95kg, vitamin E2 4kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 7kg, olive oil 18kg, Radix Angelicae Sinensis 8kg, Roast Rhizoma Zingiberis Recens 9kg, Radix Ophiopogonis 6kg, Radix Notoginseng 6kg, Herba Selaginellae 9kg, Cortex Fraxini 4kg, Herba Centellae 4kg, Semen Cuscutae 4kg, SPAN-803kg, ethylparaben 3kg, sodium alginate 3kg, methyl propanediol 2kg, glycyrrhizic acid dipotassium 1kg, ginsenoside 3kg, pyrrolidone sodium carboxylate 3kg, hydrogenated soy phosphatidyl choline 5kg, alcoholic solution 95kg.
The volumetric concentration of described alcoholic solution is 98%, and solvent is water.
Preparation method:
S1: get Fructus Citri Sarcodactylis, Fructus Citri Limoniae, grapefruit, after cleaning, pulverize, be placed in boiler, steam is led directly to from the boiler the bottom of a pan, steam pressure 4.1atm, distills, and the gas that distillation produces is collected in condensation, distillation time is 1.2h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils I;
S2: get jasmine, Flos Rosae Rugosae, Herba Rosmarini Officinalis, Herba Ocimi (Herba Ocimi Pilosi), Herba Menthae, Fructus Foeniculi, bush cinqefoil, Flos Elaeagni Angustifoliae, Rhizoma Chuanxiong root, Herba Moslae, green tea, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 4.4atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 1.3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils II;
S3: get the Pseudobulbus Bletillae (Rhizoma Bletillae), olive oil, Radix Angelicae Sinensis, Roast Rhizoma Zingiberis Recens, Radix Ophiopogonis, Radix Notoginseng, Herba Selaginellae, Cortex Fraxini, Herba Centellae, Semen Cuscutae, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3.5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 2.3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils III;
S4: get blend of essential oils I, blend of essential oils II, edible vegetable oil mixtures III, vitamin E, SPAN-80, ethylparaben, sodium alginate, methyl propanediol, glycyrrhizic acid dipotassium, ginsenoside, pyrrolidone sodium carboxylate, hydrogenated soy phosphatidyl choline, mix homogeneously, add alcoholic solution again, stir, leave standstill after 37 hours, put into sealed container, ageing is after 6 weeks.
Reference examples 1
Reference examples 1 is with the difference of embodiment 3, does not add green tea in step s 2, specifically:
Take following raw materials according: Fructus Citri Sarcodactylis 40kg, Fructus Citri Limoniae 25kg, grapefruit 15kg, jasmine 35kg, Flos Rosae Rugosae 35kg, Herba Rosmarini Officinalis 15kg, Herba Ocimi (Herba Ocimi Pilosi) 15kg, Herba Menthae 15kg, Fructus Foeniculi 15kg, bush cinqefoil 6kg, Flos Elaeagni Angustifoliae 15kg, Rhizoma Chuanxiong root 8kg, Herba Moslae 8kg, vitamin E2 0kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 8kg, olive oil 17kg, Radix Angelicae Sinensis 7kg, Roast Rhizoma Zingiberis Recens 8kg, Radix Ophiopogonis 8kg, Radix Notoginseng 8kg, Herba Selaginellae 10kg, Cortex Fraxini 5kg, Herba Centellae 5kg, Semen Cuscutae 5kg, SPAN-803kg, ethylparaben 3kg, sodium alginate 3kg, methyl propanediol 2kg, glycyrrhizic acid dipotassium 1kg, ginsenoside 2kg, pyrrolidone sodium carboxylate 3kg, hydrogenated soy phosphatidyl choline 5kg, alcoholic solution 90kg.
The volumetric concentration of described alcoholic solution is 98%, and solvent is water.
Preparation method:
S1: get Fructus Citri Sarcodactylis, Fructus Citri Limoniae, grapefruit, after cleaning, pulverize, be placed in boiler, steam is led directly to from the boiler the bottom of a pan, steam pressure 3 ~ 5atm, distills, and the gas that distillation produces is collected in condensation, distillation time is 1 ~ 1.5h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils I;
S2: get jasmine, Flos Rosae Rugosae, Herba Rosmarini Officinalis, Herba Ocimi (Herba Ocimi Pilosi), Herba Menthae, Fructus Foeniculi, bush cinqefoil, Flos Elaeagni Angustifoliae, Rhizoma Chuanxiong root, Herba Moslae, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3 ~ 5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 1 ~ 1.5h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils II;
S3: get the Pseudobulbus Bletillae (Rhizoma Bletillae), olive oil, Radix Angelicae Sinensis, Roast Rhizoma Zingiberis Recens, Radix Ophiopogonis, Radix Notoginseng, Herba Selaginellae, Cortex Fraxini, Herba Centellae, Semen Cuscutae, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3 ~ 5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 2 ~ 3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils III; S4: get blend of essential oils I, blend of essential oils II, edible vegetable oil mixtures III, vitamin E, SPAN-80, ethylparaben, sodium alginate, methyl propanediol, glycyrrhizic acid dipotassium, ginsenoside, pyrrolidone sodium carboxylate, hydrogenated soy phosphatidyl choline, mix homogeneously, add alcoholic solution again, stir, leave standstill after 24 ~ 48 hours, put into sealed container, ageing is after 4 ~ 8 weeks.
Performance test
1. the inhibit activities test of pair tryrosinase
Tyrosinase inhibitory activity uses spectrogrph to detect.The whitening perfume 40 μ L that 5% dimethyl sulfoxide solution dissolves is added in 96 orifice plates, add the tryrosinase 40 μ L of trorsine 14 0 μ L, 1/15M kaliumphosphate buffer 80 μ L and 60U/mL of 0.1mg/mL successively, above solution all uses 1/15M kaliumphosphate buffer (pH6.8) to prepare, 37 DEG C hatch 30 minutes after, detect at 475nm wavelength place, with the 1/15M kaliumphosphate buffer (pH6.8) of 5% dimethyl sulfoxine for blank group by microplate reader.The suppression ratio computing formula of tryrosinase is as follows:
Suppression ratio=((A-B)-(C-D))/(A-B) × 100%
In formula, A is the trap after blank solution is hatched, and B is the trap before blank solution is hatched, and C is the trap after sample solution is hatched, and D is the trap before sample solution hatching.
1) experiment material and instrument
Tryrosinase is purchased from Sigma (U.S.);
Tyrosine is purchased from Sigma (U.S.);
Arbutin is purchased from Sigma (U.S.);
Microwell plate is purchased from the Costar(U.S.);
Microplate reader uses FlexStation3 microplate reader (Molecular Devices, California, the U.S.).
2) experimental technique
Whitening active adopts tyrosinase inhibitory activity method.
3) test sample
The whitening perfume of embodiment gained, positive controls arbutin (arbutin concentration is 500 μ g/ml).
4) experimental result, see table 1.
Table 1 whitening perfume of the present invention is to the inhibit activities measurement result of tryrosinase
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Arbutin
Tyrosinase inhibition rate (%) 47.4±1.1 45.9±1.3 46.4±1.2 50.2±1.5 51.2±2.1
As can be seen from the table, whitening perfume provided by the invention can effective restraint of tyrosinase.
5. whitening effect test
Whitening effect is tested, and comprises the transfer of acceleration dermal melanin, metabolism and the test of raising skin brightness.Following white-skinned face function test all adopts human test's mode, measures melanin content and the brightness of skin with the dark red pigment tester of skin and skin colourity test probe+MPA9 tester.
Choose 120 volunteers, men and women half and half, is divided into 5 groups at random, often organize 24 people, often organize and test with embodiment 1, embodiment 2, embodiment 3, embodiment 4, reference examples 1 and blank sample respectively, blank sample is 75% common ethanol, and the test data of each group is all averaged.Within before recipient site 2 ~ 3 days, any product can not be used; With dry medicated napkin, both hands inner forearm wiped clean is 4 × 4cm 2pilot region measures labelling, measures melanin content and the skin brightness of tested skin with skin dark red pigment tester and skin colourity test probe+MPA9 tester; Sample will be tested with blank group by 2.0 ± 0.1mg sample/cm with latex finger cot 2consumption spread upon respectively in left and right arm, smear and measure the melanin content in 1st ~ 4 weeks each regions and skin brightness respectively afterwards.
(1) melanin content mutation analysis
Dermal melanin changes of contents is reflected in test period, pilot region dermal melanin content Changing Pattern in time.Its value is larger, and dermal melanin content is larger, otherwise, dermal melanin content.Melanin content (T0) before each time point melanin content (Tn)-use product after melanin content difference (Δ T)=use product.
The difference of table 2 recipient site dermal melanin content and initial value
Within 4 weeks test periods, the melanin content of blank group recipient site skin on the occasion of, numerical value, without significant change, illustrates that the substrate of smearing does not have and shifts melanic ability.The melanin content of sample sets recipient site skin and the difference of initial value are negative value always; When the 4th week, melanin content difference is below-5, and value reduces along with the prolongation of time, illustrates that the skin care item containing whitening extract prepared by embodiment have transfer or reduce the ability of melanin content.Wherein, embodiment 4 is optimum.
(2) mutation analysis of skin brightness
Skin brightness change is reflected in test period, investigates Experimental Area skin brightness L-value Changing Pattern in time.Its value is larger, and skin brightness is larger, otherwise skin brightness is lower.
L-value (T0) before each time point L-value (Tn)-use product after skin brightness difference (Δ T)=use product.
The difference of table 3 recipient site skin brightness L-value and initial value
As shown in Table 3, within the cycle of test, the skin brightness numerical value of blank group recipient site slightly changes, but not obvious, illustrates that the substrate of smearing does not have the ability improving skin brightness.The skin brightness L-value of sample sets recipient site skin and the difference of initial value be always on the occasion of, and raise along with the prolongation of testing time, when the 4th week, the difference of skin brightness L-value and initial value reaches more than 0.70, illustrates that whitening perfume prepared by embodiment has good whitening effect.Wherein, embodiment 4 is optimum.
6. stability test
Perfume turbidity is measured according to QB/T1858-2004 " perfume, GULONG water ".
After perfume is completed ageing, take out and carry out turbidity test.
Table 4 perfume turbidity is tested
As can be seen from Table 4, after with the addition of green tea, the problem that cotton-shaped muddiness appears in whitening perfume can be solved.

Claims (1)

1. there is the preparation method of the perfume of whitening effect, it is characterized in that, comprise the steps:
Take following raw materials according: Fructus Citri Sarcodactylis 44 weight portion, Fructus Citri Limoniae 21 weight portion, grapefruit 17 weight portion, jasmine 38 weight portion, Flos Rosae Rugosae 45 weight portion, Herba Rosmarini Officinalis 16 weight portion, Herba Ocimi (Herba Ocimi Pilosi) 12 weight portion, Herba Menthae 13 weight portion, Fructus Foeniculi 17 weight portion, bush cinqefoil 8 weight portion, Flos Elaeagni Angustifoliae 19 weight portion, Rhizoma Chuanxiong root 7 weight portion, Herba Moslae 6 weight portion, green tea 95 weight portion, vitamin E 24 weight portion, the Pseudobulbus Bletillae (Rhizoma Bletillae) 7 weight portion, olive oil 18 weight portion, Radix Angelicae Sinensis 8 weight portion, Roast Rhizoma Zingiberis Recens 9 weight portion, Radix Ophiopogonis 6 weight portion, Radix Notoginseng 6 weight portion, Herba Selaginellae 9 weight portion, Cortex Fraxini 4 weight portion, Herba Centellae 4 weight portion, Semen Cuscutae 4 weight portion, SPAN-80 3 weight portion, ethylparaben 3 weight portion, sodium alginate 3 weight portion, methyl propanediol 2 weight portion, glycyrrhizic acid dipotassium 1 weight portion, ginsenoside 3 weight portion, pyrrolidone sodium carboxylate 3 weight portion, hydrogenated soy phosphatidyl choline 5 weight portion, alcoholic solution 95 weight portion,
Preparation method:
S1: get Fructus Citri Sarcodactylis, Fructus Citri Limoniae, grapefruit, after cleaning, pulverize, be placed in boiler, steam is led directly to from the boiler the bottom of a pan, steam pressure 4.1atm, distills, and the gas that distillation produces is collected in condensation, distillation time is 1.2h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils I;
S2: get jasmine, Flos Rosae Rugosae, Herba Rosmarini Officinalis, Herba Ocimi (Herba Ocimi Pilosi), Herba Menthae, Fructus Foeniculi, bush cinqefoil, Flos Elaeagni Angustifoliae, Rhizoma Chuanxiong root, Herba Moslae, green tea, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 4.4atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 1.3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils II;
S3: get the Pseudobulbus Bletillae (Rhizoma Bletillae), olive oil, Radix Angelicae Sinensis, Roast Rhizoma Zingiberis Recens, Radix Ophiopogonis, Radix Notoginseng, Herba Selaginellae, Cortex Fraxini, Herba Centellae, Semen Cuscutae, after cleaning, be placed in boiler, lead directly to steam from the boiler the bottom of a pan, steam pressure 3.5atm, distill, the gas that distillation produces is collected in condensation, and distillation time is 2.3h, after condensed fluid stratification, get the oil reservoir on upper strata, obtain blend of essential oils III;
S4: get blend of essential oils I, blend of essential oils II, blend of essential oils III, vitamin E, SPAN-80, ethylparaben, sodium alginate, methyl propanediol, glycyrrhizic acid dipotassium, ginsenoside, pyrrolidone sodium carboxylate, hydrogenated soy phosphatidyl choline, mix homogeneously, add alcoholic solution again, stir, leave standstill after 37 hours, put into sealed container, ageing is after 6 weeks.
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