CN102406575B - Sweet osmanthus perfume - Google Patents
Sweet osmanthus perfume Download PDFInfo
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- CN102406575B CN102406575B CN2011103706925A CN201110370692A CN102406575B CN 102406575 B CN102406575 B CN 102406575B CN 2011103706925 A CN2011103706925 A CN 2011103706925A CN 201110370692 A CN201110370692 A CN 201110370692A CN 102406575 B CN102406575 B CN 102406575B
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Abstract
The invention discloses sweet osmanthus perfume which comprises the following 100 parts by volume of components: basic essential oil, sweet osmanthus essential oil, sweet osmanthus hydrolat, essential oil emulsifier and 95% ethanol. According to the invention, the advantages of high extraction quality, low equipment cost, simple operation, high extraction efficiency, no solvent residue, low top note loss and the like are achieved. The sweet osmanthus essential oil extracted from fresh sweet osmanthus is taken as a main ingredient, and the main ingredient, namely the sweet osmanthus essential oil has fragrant and elegant flavor, super penetrability, has the functions of deeply supplementing nutrition and water for skin, reducing the epidermal pigmentation of the skin, eliminating toxins, accelerating the metabolism of the skin, avoiding the aging of the skin, moistening and refreshing the skin so that the skin looks vital, moist, fresh and alive; and the obtained perfume has the advantages of good overall feeling, quietly elegant color and luster, harmonious and natural fragrance and long fragrance maintaining time, and has very high application value and broad market prospects.
Description
Technical field
The present invention relates to a kind of perfume, especially a kind of Flos Osmanthi Fragrantis perfume.
Background technology
Flos Osmanthi Fragrantis (OsmanthusfragransLour) is that the Oleaceae sweet-scented osmanthus belongs to evergreen shrubs or dungarunga; Be one of China's ten great tradition famous flowers; Flos Osmanthi Fragrantis is not only good afforestation seeds; Have certain edibility and medical value simultaneously, be widely used in industries such as food, cosmetics, chemical industry.With a long history like Jiujiang Flos Osmanthi Fragrantis brittleness and Flos Osmanthi Fragrantis tea cake, have won fame both at home and abroad, once be cited as Jiujiang quality product.The osmanthus essential oil fragrant odour is simple and elegant, has superpower penetration, can supplement the nutrients and moisture to skin depth, can alleviate the epiderm skin pigmentation; Get rid of toxin, accelerate skin metabolism, avoid skin ageing; Make skin water tender pure and fresh, dynamic, the water profit is fresh and alive.
Supercritical CO is mainly used in the extraction of osmanthus essential oil at present
2Abstraction technique, the microwave-assisted way of distillation, organic solvent extraction technology etc., these methods exist as extracting of poor quality, and cost of equipment is high, complicated operation, extraction efficiency is low, and variety of issues such as organic solvent residual are unfavorable to large scale application.The present invention utilizes steam distillation to extract osmanthus essential oil, Flos Osmanthi Fragrantis hydrosol simultaneously; It is high to have the quality of extraction, and cost of equipment is low, and is simple to operate; Extraction efficiency is high; No solvent residue, characteristics such as the fragrant loss of head is few are utilized and are extracted the osmanthus essential oil that obtains and cooperate with the quintessence oil of other plant or flowers and obtain a kind of Flos Osmanthi Fragrantis fragrance of a flower water.This method for distilling will have bigger utilization and extention to be worth.
Summary of the invention
Characteristics such as the object of the present invention is to provide a kind of Flos Osmanthi Fragrantis perfume, it is high that this perfume has the quality of extraction, and cost of equipment is low, and is simple to operate, and extraction efficiency is high, and organic solvent-free is residual, and the fragrant loss of head is few.
Technical scheme of the present invention is: a kind of Flos Osmanthi Fragrantis perfume, and the volume component of this perfume is: 1-2 part basis quintessence oil, 2-5 part osmanthus essential oil, 5-10 part Flos Osmanthi Fragrantis hydrosol, 0-1.5 part quintessence oil emulsifying agent, add 95% ethanol to 100 part; Wherein basic quintessence oil is mixed for 5 parts by 5 parts of Oleum menthae, 10 parts of Herba Cymbopogonis Citrari quintessence oils, 20 parts of oleum bergamottae, 10 parts of grapefruit quintessence oils, 30 parts of jasmin quintessence oils, 20 parts of clove oils, 20 parts of tea tree ethereal oils, 40 parts of Herba Lysimachiae foenum-graeci quintessence oil, 40 parts of Flos Rosae Rugosae quintessence oils, 5 parts of cinnamon essential oils, 5 parts of rosemary ethereal oils, 1 part of Lignum Santali Albi quintessence oil, eucalyptus quintessence oil; The preparation technology of osmanthus essential oil, Flos Osmanthi Fragrantis hydrosol: pulverize (1): it is broken that osmanthus flowers is not had the iodine common salt pigment through pulverizer adding 2.5~5% concentration expressed in percentage by weights, and add the no iodine common salt water yield for by weight, water: flower is 0.1~0.5: 1; Obtain the Flos Osmanthi Fragrantis slurry; (2) distillation: the Flos Osmanthi Fragrantis slurry adds distillating still and obtains the profit mist through steam distillation, and distillation time 120-150 minute, the control steam pressure was 0.1~0.35Mpa, and the control vapo(u)rizing temperature is 105 ℃-110 ℃; Through spiral cooler, the tap water condensation obtains the fraction of oil water mixture; (3) oil-water separation: the fraction of oil water mixture leaves standstill through oil water separator, and the profit layering is after oil water separator is collected the Flos Osmanthi Fragrantis hydrosol that obtains rough osmanthus essential oil in upper strata and lower floor; (4) purification: osmanthus essential oil is that 20 ℃~30 ℃, pressure are to obtain pure osmanthus essential oil through the molecular distillation purification under the condition of 5~10Pa in temperature.
The invention has the advantages that: it is high to have the extraction quality, and cost of equipment is low, and is simple to operate, and extraction efficiency is high, no solvent residue, and head perfume loses advantages such as few.The osmanthus essential oil that from bright Flos Osmanthi Fragrantis, extracts is a main component, and main component osmanthus essential oil fragrant odour is simple and elegant, has superpower penetration, and the degree of depth supplements the nutrients and moisture to skin; Can alleviate the epiderm skin pigmentation, get rid of toxin, accelerate skin metabolism, avoid skin ageing; Make skin water tender pure and fresh, dynamic, the fresh and alive perfume integral body that obtains of water profit is felt all right, and color and luster is simple and elegant; Fragrance harmony and natural, the fragrance length of holding time has very high using value and vast market prospect.
The specific embodiment
A kind of Flos Osmanthi Fragrantis perfume, the volume component of this perfume is:
Modulation 21100ml Flos Osmanthi Fragrantis perfume,
Basis quintessence oil 211ml, osmanthus essential oil 633ml, Flos Osmanthi Fragrantis hydrosol 1055ml, quintessence oil emulsifying agent 0ml, add 95% ethanol 19201ml.Wherein basic quintessence oil is mixed by Oleum menthae 5ml, Herba Cymbopogonis Citrari quintessence oil 10ml, oleum bergamottae 20ml, grapefruit quintessence oil 10ml, jasmin quintessence oil 30ml, clove oil 20ml, tea tree ethereal oil 20ml, Herba Lysimachiae foenum-graeci quintessence oil 40ml, Flos Rosae Rugosae quintessence oil 40ml, cinnamon essential oil 5ml, rosemary ethereal oil 5ml, Lignum Santali Albi quintessence oil 1ml, eucalyptus quintessence oil 5ml.
The preparation technology of osmanthus essential oil, Flos Osmanthi Fragrantis hydrosol:
(1) pulverizes: osmanthus flowers is added no iodine common salt water 8% through common pulverizer pulverize, obtain the Flos Osmanthi Fragrantis slurry;
(2) distillation: the Flos Osmanthi Fragrantis slurry adds distillating still and obtains the profit mist through steam distillation, and through spiral cooler, the tap water condensation obtains the fraction of oil water mixture;
(3) oil-water separation: the fraction of oil water mixture leaves standstill through oil water separator, and the profit layering is after oil water separator is collected the Flos Osmanthi Fragrantis hydrosol that obtains rough osmanthus essential oil in upper strata and lower floor;
(4) purification: osmanthus essential oil is to obtain pure osmanthus essential oil through the molecular distillation purification under 25 ℃ of pressure condition that is 8Pa in temperature.
Claims (1)
1. Flos Osmanthi Fragrantis perfume, it is characterized in that: the volume component of this perfume is:
Basis quintessence oil 1-2 part, osmanthus essential oil 2-5 part, Flos Osmanthi Fragrantis hydrosol 5-10 part, quintessence oil emulsifying agent 0-1.5 part, add 95% ethanol to 100 part;
Wherein basic quintessence oil is mixed for 5 parts by 5 parts of Oleum menthae, 10 parts of Herba Cymbopogonis Citrari quintessence oils, 20 parts of oleum bergamottae, 10 parts of grapefruit quintessence oils, 30 parts of jasmin quintessence oils, 20 parts of clove oils, 20 parts of tea tree ethereal oils, 40 parts of Herba Lysimachiae foenum-graeci quintessence oil, 40 parts of Flos Rosae Rugosae quintessence oils, 5 parts of cinnamon essential oils, 5 parts of rosemary ethereal oils, 1 part of Lignum Santali Albi quintessence oil, eucalyptus quintessence oil;
The preparation technology of osmanthus essential oil, Flos Osmanthi Fragrantis hydrosol:
(1) pulverize: it is broken that osmanthus flowers is not had the iodine common salt pigment through pulverizer adding 2.5~5% concentration expressed in percentage by weights, and add the no iodine common salt water yield for by weight, water: flower is 0.1~0.5: 1; Obtain the Flos Osmanthi Fragrantis slurry;
(2) distillation: the Flos Osmanthi Fragrantis slurry adds distillating still and obtains the profit mist through steam distillation, and distillation time 120-150 minute, the control steam pressure was 0.1~0.35Mpa, and the control vapo(u)rizing temperature is 105 ℃-110 ℃; Through spiral cooler, the tap water condensation obtains the fraction of oil water mixture;
(3) oil-water separation: the fraction of oil water mixture leaves standstill through oil water separator, and the profit layering is after oil water separator is collected the Flos Osmanthi Fragrantis hydrosol that obtains rough osmanthus essential oil in upper strata and lower floor;
(4) purification: osmanthus essential oil is that 20 ℃~30 ℃, pressure are to obtain pure osmanthus essential oil through the molecular distillation purification under the condition of 5~10Pa in temperature.
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CN2011103706925A CN102406575B (en) | 2011-11-21 | 2011-11-21 | Sweet osmanthus perfume |
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CN2011103706925A CN102406575B (en) | 2011-11-21 | 2011-11-21 | Sweet osmanthus perfume |
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CN102406575A CN102406575A (en) | 2012-04-11 |
CN102406575B true CN102406575B (en) | 2012-11-21 |
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CN2011103706925A Expired - Fee Related CN102406575B (en) | 2011-11-21 | 2011-11-21 | Sweet osmanthus perfume |
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CN103622866B (en) * | 2013-06-30 | 2015-03-04 | 金玛瑙香水(明光)有限公司 | Perfume capable of whitening and preparation method thereof |
CN103695175B (en) * | 2013-12-13 | 2015-07-29 | 仙芝科技(福建)股份有限公司 | The method of extraction and isolation DANGUIHUA or each component of Flower of Arabian Jasmine |
CN104161696A (en) * | 2013-12-13 | 2014-11-26 | 金玛瑙香水(明光)有限公司 | Long acting perfume |
CN103720618A (en) * | 2013-12-21 | 2014-04-16 | 樊秀娟 | Skin-nourishing compound essential oil |
CN104398445A (en) * | 2014-12-10 | 2015-03-11 | 遵义医学院 | Honeysuckle perfume |
CN104928039A (en) * | 2015-05-30 | 2015-09-23 | 防城港市防城区那梭香料厂 | Preparation method for lemongrass essential oil |
CN106176508A (en) * | 2016-06-24 | 2016-12-07 | 浙江美之源化妆品有限公司 | Perfume containing natural Ambra Grisea |
CN106176509A (en) * | 2016-06-24 | 2016-12-07 | 浙江美之源化妆品有限公司 | Perfume containing natural castoreum |
CN106377783A (en) * | 2016-08-31 | 2017-02-08 | 张益方 | Production method of sweet osmanthus-flavor car perfume |
CN107049915A (en) * | 2017-03-21 | 2017-08-18 | 湖南科技学院 | A kind of snake gall jessamine and its ageing |
CN106913484A (en) * | 2017-03-31 | 2017-07-04 | 金玛瑙香水(明光)有限公司 | A kind of production method of perfume stick |
CN107648126A (en) * | 2017-11-14 | 2018-02-02 | 何芬 | A kind of sweet osmanthus perfume |
CN108653074A (en) * | 2018-05-29 | 2018-10-16 | 李应峰 | A kind of production method of l'origan perfume |
CN109453091B (en) * | 2019-01-02 | 2021-08-24 | 广东美宝化妆品有限公司 | Perfume based on composite flower extracting solution and preparation method thereof |
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CN101775337A (en) * | 2010-02-05 | 2010-07-14 | 四川日香桂农业科技开发有限公司 | Method for simultaneously preparing osmanthus essential oil, dry osmanthus product and osmanthus essential lotion |
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