CN103525533B - Full-synthetic glass grinding fluid - Google Patents
Full-synthetic glass grinding fluid Download PDFInfo
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- CN103525533B CN103525533B CN201310503658.XA CN201310503658A CN103525533B CN 103525533 B CN103525533 B CN 103525533B CN 201310503658 A CN201310503658 A CN 201310503658A CN 103525533 B CN103525533 B CN 103525533B
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Abstract
The invention discloses an environment-friendly glass grinding fluid, which is efficient, and long in service. The full-synthetic glass grinding fluid is prepared from an organic acid, a boride, an organic amine, a water-based lubricant, a hard water-resisting surfactant, a water-based mould inhibitor, an organic alcohol, a settling agent, a defoaming agent and water in a mixing manner. The glass grinding fluid disclosed by the invention has excellent cooling property, anti-rotting ability and lubricating abrasion resistance, and outstanding hard water resistance, can be recycled for a long period of time, can ensure the working accuracy and the service life of a tool, and has excellent cleaning performance; the blocking phenomenon of a grinding wheel can be effectively prevented; the product is good in settleability; processing is facilitated; the product is free of poison, environment-friendly, free of pollution, small in smell, good in working performance, good in compatibility with a paint of equipment, low in pH value, free of bad effects on skin and the like; the phenomenon that the paint of the equipment peels off is not generated. The grinding fluid disclosed by the invention is simple in reparation method, low in cost, excellent in performance, and good in market prospect at present.
Description
Technical field
The present invention relates to the grinding fluid of a kind of simple glass (comprising opticglass, ambetti etc.) and quartz glass product.
Background technology
In the ground finish of glasswork, what bring into use most is pure oil type product, but its cooling is relatively poor, and the settleability of abrasive particle powder is poor, easily cause and abrade the surface second of glasswork and affect smooth finish, it easily produces mist of oil simultaneously, causes ill effect to production environment.
At present, promotion Water-soluble grinding fluid energetically in this complete processing, owing to can produce a large amount of glass powders in grinding process, is therefore proposed high requirement to the cleaning performance of grinding fluid and cooling performance.In order to improve cleaning performance, the flow of grinding fluid and pressure are usually all higher; Add in the course of processing, operative employee often directly catches tactile grinding working fluid, and this just requires that the smell of grinding fluid is little, pH value is low and skin irritation is little.Current, the water-soluble glass grinding fluid of domestic-developed is also fewer, and be main component mainly with benzene analog derivative, the nitrite even forbidden in the water-soluble glass grinding fluid developed, and there is cleaning difference, working accuracy is forbidden, mostly only for roughly grinding processing, be unsuitable for ground finish, have stimulation to the skin of operator and eyes, and easily cause the health problem that " nitrite " brings, waste liquid causes problem of environmental pollution simultaneously.
Summary of the invention
For problem existing in prior art, the object of the invention is to for the corase grind of glass grinding and ground finish provide a kind of good work, working accuracy high, paint with equipment compatibility good, to operator ' s health safety, long service life, low toxicity, low stain, there is the all-synthetic grinding fluid of superior settleability, cooling and cleaning.
In order to achieve the above object, present invention employs following technical scheme:
A kind of complete synthesis glass grinding fluid, it comprises following component by mass percentage:
Preferably, a kind of complete synthesis glass grinding fluid, it comprises following component by mass percentage:
Preferably, a kind of complete synthesis glass grinding fluid, it comprises following component by mass percentage:
Preferably, described organic acid is selected from C
8~ C
24unit lipid acid, C
8~ C
24polyhydric aliphatic acid or dimeracid in the mixture of any one or at least two kinds.
The lipid acid of unit lipid acid namely containing a carboxyl, the lipid acid of polyhydric aliphatic acid namely containing at least two carboxyls.
Preferably, described boride is that boric acid is or/and boric acid acid amides.
Preferably, described organic amine is selected from the mixture of any one or at least two kinds in monoethanolamine, diethanolamine, trolamine, monoisopropanolamine, diisopropanolamine (DIPA), tri-isopropanolamine, alkyl alcoholamine or 2-amino-2-methyl-1-propanol.The mixture of described mixture such as monoethanolamine and diethanolamine, the mixture of trolamine and monoisopropanolamine, the mixture of diisopropanolamine (DIPA) and tri-isopropanolamine, the mixture of alkyl alcoholamine and 2-amino-2-methyl-1-propanol, monoethanolamine, the mixture of diethanolamine and trolamine, monoisopropanolamine, the mixture of diisopropanolamine (DIPA) and tri-isopropanolamine, alkyl alcoholamine, the mixture of 2-amino-2-methyl-1-propanol and monoethanolamine, diethanolamine, the mixture of trolamine and monoisopropanolamine, diisopropanolamine (DIPA), tri-isopropanolamine, the mixture of alkyl alcoholamine and 2-amino-2-methyl-1-propanol.
Preferably, described water-based lubricant be selected from the trans polyethers of low molecule, water-soluble self-emulsifying ester, molecular weight be 400 ~ 2000 higher alcohols, fatty acid ester, any one or at least two kinds in cis polyethers or fatty acid amide mixture.The mixture of the trans polyethers of described mixture such as low molecule and water-soluble self-emulsifying ester, molecular weight is the higher alcohols of 400 ~ 2000 and the mixture of cis polyethers, the mixture of cis polyethers and fatty acid amide, the trans polyethers of low molecule, water-soluble self-emulsifying ester and molecular weight are the mixture of the higher alcohols of 400 ~ 2000.
Preferably, when described complete synthesis glass grinding fluid includes the trans polyethers of low molecule, described in comprise C
8~ C
24unit lipid acid be selected from the mixture of any one or at least two kinds in neodecanoic acid, different n-nonanoic acid, oleic acid, stearic acid or n-capric acid; Described C
8~ C
24polyhydric aliphatic acid be selected from C
21monocycle diprotic acid, C24 dimeracid or C
8~ C
24ternary aliphatic acid in the mixture of any one or at least two kinds.
Preferably, when described complete synthesis glass grinding fluid does not include the trans polyethers of low molecule, described in comprise C
8~ C
24unit lipid acid be C
12~ C
24unit lipid acid, described C
8~ C
24polyhydric aliphatic acid be C
12~ C
24polyhydric aliphatic acid.
Preferably, the trans polyethers of described low molecule to be number-average molecular weight be 1000 ~ 3000 EO(oxyethane) and PO(propylene oxide) segmented copolymer.As EO and the PO segmented copolymer can selecting high EO content (molar content of EO is more than 50%) during more excellent water-soluble and settleability need be provided, but its oilness and anti-bubble relatively weak; Otherwise, then EO and the PO segmented copolymer of low EO content is selected.
Preferably, described cis polyethers is selected from number-average molecular weight is that the cis polyethers of 20000 ~ 55000 is or/and number-average molecular weight is the cis polyethers of 1000 ~ 6000.In formula, by the proportioning of conservative control high and low molecule cis polyethers, be for different glass grinding process obtains one of means of suitable settleability grinding fluid.Pfpe molecule amount is lower, and surface tension is less, and settling property is more excellent.
Higher alcohols, also known as high fatty alcohol, refers to the mixture containing the above monohydroxy-alcohol of six carbon atom.
Preferably, described anti-hard water tensio-active agent is that four sodium edtas are or/and C
12~ C
24alcohol ether carboxylate ammonium salt.
Preferably, described water mildow-proof agent is water-soluble 3-iodopropynyl butyl formate solution, preferred described water-soluble 3-iodopropynyl butyl formate solution is allocated by 3-iodopropynyl butyl formate organic solution and lower alcohol and is obtained, the mass ratio of described 3-iodopropynyl butyl formate organic solution and lower alcohol is for being less than 2:1, and described lower alcohol refers to that carbonatoms is less than 4 alcohol.
Preferably, the low-carbon alcohol that the preferred carbonatoms of described Organic Alcohol is less than 6, the mixture of any one or at least two kinds further preferably in ethylene glycol, ethanol, glycol ether, n-propyl alcohol, Virahol, propylene glycol, 1,3-PD or glycerol.The mixture of described mixture such as ethylene glycol and ethanol, the mixture of glycol ether and n-propyl alcohol, the mixture of Virahol and propylene glycol, 1, the mixture of ammediol and glycerol, the mixture of ethylene glycol, ethanol and glycol ether, the mixture of n-propyl alcohol, Virahol and propylene glycol, the mixture of 1,3-PD, glycerol and ethanol.Be one of means regulating grinding fluid settleability and cleaning by controlling the add-on of low-carbon alcohol, it can strengthen settleability and cleaning.
Preferably, described sinking agent preferably water soluble cationic tensio-active agent, the further mixture of preferred any one or at least two kinds in water-soluble polyacrylamide, the twin quaternary ammonium salt of tween, tween three lives quaternary ammonium salt, polyoxyethylene Quito alkyl multi-quaternary ammonium salt, chain alkyl three lives quaternary ammonium salt, the twin quaternary ammonium salt of sapn, the twin quaternary ammonium salt of chain alkyl, the twin quaternary ammonium salt of natural rosin base or natural rosin base three lives quaternary ammonium salt.The mixture of the twin quaternary ammonium salt of described mixture such as water-soluble polyacrylamide and tween, the mixture of tween three lives quaternary ammonium salt and polyoxyethylene Quito alkyl multi-quaternary ammonium salt, the mixture of chain alkyl three lives quaternary ammonium salt and the twin quaternary ammonium salt of sapn, the mixture of the twin quaternary ammonium salt of chain alkyl and the twin quaternary ammonium salt of natural rosin base, the mixture of natural rosin base three lives quaternary ammonium salt and water-soluble polyacrylamide, the mixture of the twin quaternary ammonium salt of tween and tween three lives quaternary ammonium salt, the mixture of polyoxyethylene Quito alkyl multi-quaternary ammonium salt and chain alkyl three lives quaternary ammonium salt, the mixture of the twin quaternary ammonium salt of sapn and the twin quaternary ammonium salt of chain alkyl, the mixture of the twin quaternary ammonium salt of natural rosin base and natural rosin base three lives quaternary ammonium salt.Being the another effective means regulating grinding fluid settleability by the control of water soluble surfactant active's kind and add-on, by controlling appropriate surface tension, and then the object improving settleability can being reached.
Preferably, described defoamer is the mixture of any one or at least two kinds in emulsification three-dimensional siloxanes, organosilicon, polyethers or polyvalent alcohol.
Preferably, the pH of described complete synthesis glass grinding fluid is 7.5 ~ 8.5, such as 7.6,7.7,7.8,7.9,8.1,8.2,8.3 or 8.4.
Compared with prior art, the present invention has following beneficial effect:
Glass grinding fluid highly versatile of the present invention, not only may be used for the ground finish of simple glass (comprising opticglass, ambetti etc.), silica glass, is also applicable to the ground finish of various metals; There is excellent anti-wear lubricating and cooling performance, be applicable to corase grind and ground finish, guarantee the work-ing life of working accuracy and emery wheel.
The component of glass grinding fluid of the present invention is mostly fungus resistance composition, adds the use of unique preparation water-soluble mildew preventive, makes it have outstanding anti-corrupt ability, can recycle for a long time, greatly reduce and change liquid cost.
Unique proportioning of glass grinding fluid emollient component of the present invention, adds adding of low-carbon alcohol and sinking agent, can meet the settleability requirement of most of grinding process.Select other component more identical than the present invention, but do not comprise low-carbon alcohol and sinking agent, the settling velocity of the glass grinding fluid obtained is fast, is inferior to the settling property adding the glass grinding fluid having low-carbon alcohol and sinking agent of the present invention.
Glass grinding fluid of the present invention has outstanding stability in hard water energy, can be suitable for the use in hard water degree district higher; There is good cleaning performance, effectively can prevent the sticky stifled phenomenon of emery wheel; There is higher grinding ratio, effectively can improve working (machining) efficiency; Not containing objectionable impuritiess such as nitrous acid, benzene class, phenols, to environment and healthy and beneficial; Low or the euosmia invariably of smell, good work, low ph value, to no skin irritation; There is good liquid waste disposal performance, can by commonly industrial wastewater process.
Embodiment
For better the present invention being described, be convenient to understand technical scheme of the present invention, typical but non-limiting embodiment of the present invention is as follows:
Embodiment 1
A kind of complete synthesis glass grinding fluid, composed as follows by mass percentage:
Organic acid is selected from C
8~ C
24unit lipid acid, C
8~ C
24polyhydric aliphatic acid or dimeracid in the mixture of any one or at least two kinds.Boride is that boric acid is or/and boric acid acid amides.Described organic amine is selected from the mixture of any one or at least two kinds in monoethanolamine, diethanolamine, trolamine, monoisopropanolamine, diisopropanolamine (DIPA), tri-isopropanolamine, alkyl alcoholamine or 2-amino-2-methyl-1-propanol.The mixture of any one or at least two kinds in described water-based lubricant is selected from the trans polyethers of low molecule, water-soluble self-emulsifying ester, number-average molecular weight are 400 ~ 2000 higher alcohols, cis polyethers, fatty acid ester or fatty acid amide.The trans polyethers of described low molecule to be number-average molecular weight be 1000 ~ 3000 EO(oxyethane) and PO(propylene oxide) segmented copolymer.Described anti-hard water tensio-active agent is that four sodium edtas are or/and C
12~ C
24alcohol ether carboxylate ammonium salt.The low-carbon alcohol that the preferred carbonatoms of described Organic Alcohol is less than 6, the mixture of any one or at least two kinds further preferably in ethylene glycol, ethanol, glycol ether, n-propyl alcohol, Virahol, propylene glycol, 1,3-PD or glycerol.Described sinking agent preferably water soluble cationic tensio-active agent, the further mixture of preferred any one or at least two kinds in water-soluble polyacrylamide, the twin quaternary ammonium salt of tween, tween three lives quaternary ammonium salt, polyoxyethylene Quito alkyl multi-quaternary ammonium salt, chain alkyl three lives quaternary ammonium salt, the twin quaternary ammonium salt of sapn, the twin quaternary ammonium salt of chain alkyl, the twin quaternary ammonium salt of natural rosin base or natural rosin base three lives quaternary ammonium salt.Described defoamer is the three-dimensional siloxanes of emulsification.
Embodiment 2
A kind of complete synthesis glass grinding fluid, composed as follows by mass percentage:
All the other are with embodiment 1, except not containing except sinking agent.
Embodiment 3
A kind of complete synthesis glass grinding fluid, composed as follows by mass percentage:
All the other are with embodiment 1.
Embodiment 4
A kind of complete synthesis glass grinding fluid, composed as follows by mass percentage:
Organic acid is C
8unit lipid acid and dimeracid, boride is boric acid, and organic amine is the mixture of monoethanolamine, diethanolamine and trolamine, and water-based lubricant is fatty acid amide, and anti-hard water tensio-active agent is four sodium edtas and C
12~ C
24alcohol ether carboxylate ammonium salt, Organic Alcohol is the mixture of ethylene glycol, ethanol and glycol ether, and sinking agent is polyoxyethylene Quito alkyl multi-quaternary ammonium salt, and defoamer is the three-dimensional siloxanes of emulsification.
Embodiment 5
A kind of complete synthesis glass grinding fluid, composed as follows by mass percentage:
Organic acid is neodecanoic acid and C
21monocycle diprotic acid, boride is boric acid acid amides, and organic amine is diisopropanolamine (DIPA), water-based lubricant is the trans polyethers of low molecule, and anti-hard water tensio-active agent is four sodium edtas, and Organic Alcohol is 1, ammediol, sinking agent is the twin quaternary ammonium salt of sapn, and defoamer is the three-dimensional siloxanes of emulsification.The trans polyethers of described low molecule to be number-average molecular weight be 1000 ~ 3000 EO(oxyethane) and PO(propylene oxide) segmented copolymer.
Embodiment 6
A kind of complete synthesis glass grinding fluid, composed as follows by mass percentage:
Organic acid is C
12unit lipid acid or, boride is boric acid acid amides, organic amine is selected from alkyl alcoholamine, water-based lubricant is water-soluble self-emulsifying ester, anti-hard water tensio-active agent is four sodium edtas, and Organic Alcohol is the mixture of 1,3-PD and glycerol, sinking agent is tween three lives quaternary ammonium salt, and defoamer is the three-dimensional siloxanes of emulsification.
It should be noted that and understand, when not departing from the spirit and scope of the present invention required by accompanying claim, various amendment and improvement can be made to the present invention of foregoing detailed description.Therefore, the scope of claimed technical scheme is not by the restriction of given any specific exemplary teachings.
Applicant states, the present invention illustrates method detailed of the present invention by above-described embodiment, but the present invention is not limited to above-mentioned method detailed, does not namely mean that the present invention must rely on above-mentioned method detailed and could implement.Person of ordinary skill in the field should understand, any improvement in the present invention, to equivalence replacement and the interpolation of ancillary component, the concrete way choice etc. of each raw material of product of the present invention, all drops within protection scope of the present invention and open scope.
Claims (13)
1. a complete synthesis glass grinding fluid, is characterized in that, it comprises following component by mass percentage:
Described organic acid is selected from C
8~ C
24unit lipid acid, C
8~ C
24polyhydric aliphatic acid or dimeracid in the mixture of any one or at least two kinds;
The mixture of any one or at least two kinds in described water-based lubricant is selected from the trans polyethers of low molecule, water-soluble self-emulsifying ester, molecular weight are 400 ~ 2000 higher alcohols, fatty acid ester, cis polyethers or fatty acid amide;
Described boride is that boric acid is or/and boric acid acid amides;
Described organic amine is selected from the mixture of any one or at least two kinds in alkyl alcoholamine;
Described anti-hard water tensio-active agent is that four sodium edtas are or/and C
12~ C
24alcohol ether carboxylate ammonium salt;
Described Organic Alcohol is the low-carbon alcohol that carbonatoms is less than 6;
Described sinking agent is water-soluble cationic tensio-active agent;
Described defoamer is the mixture of any one or at least two kinds in organosilicon, polyethers or polyvalent alcohol.
2. glass grinding fluid as claimed in claim 1, it is characterized in that, it comprises following component by mass percentage:
3. glass grinding fluid as claimed in claim 1, it is characterized in that, it comprises following component by mass percentage:
4. the glass grinding fluid as described in one of claim 1-3, it is characterized in that, described organic amine is selected from the mixture of any one or at least two kinds in monoethanolamine, diethanolamine, trolamine, monoisopropanolamine, diisopropanolamine (DIPA), tri-isopropanolamine or 2-amino-2-methyl-1-propanol.
5. glass grinding fluid as claimed in claim 1, is characterized in that, when described complete synthesis glass grinding fluid includes the trans polyethers of low molecule, described in comprise C
8~ C
24unit lipid acid be selected from the mixture of any one or at least two kinds in neodecanoic acid, different n-nonanoic acid, oleic acid, stearic acid or n-capric acid; Described C
8~ C
24polyhydric aliphatic acid be selected from C
21monocycle diprotic acid, C24 dimeracid or C
8~ C
24ternary aliphatic acid in the mixture of any one or at least two kinds.
6. glass grinding fluid as claimed in claim 1, is characterized in that, when described complete synthesis glass grinding fluid does not include the trans polyethers of low molecule, described in comprise C
8~ C
24unit lipid acid be C
12~ C
24unit lipid acid, described C
8~ C
24polyhydric aliphatic acid be C
12~ C
24polyhydric aliphatic acid.
7. glass grinding fluid as claimed in claim 1, is characterized in that, the segmented copolymer of the trans polyethers of described low molecule to be number-average molecular weight be EO and PO of 1000 ~ 4000.
8. glass grinding fluid as claimed in claim 1, it is characterized in that, it is that the cis polyethers of 20000 ~ 55000 is or/and number-average molecular weight is the cis polyethers of 1000 ~ 6000 that described cis polyethers is selected from number-average molecular weight.
9. the glass grinding fluid as described in one of claim 1-3, is characterized in that, described water mildow-proof agent is water-soluble 3-iodopropynyl butyl formate solution.
10. glass grinding fluid as claimed in claim 9, it is characterized in that, described water-soluble 3-iodopropynyl butyl formate solution is allocated by 3-iodopropynyl butyl formate organic solution and lower alcohol and is obtained, and the mass ratio of described 3-iodopropynyl butyl formate organic solution and lower alcohol is for being less than 2:1.
11. glass grinding fluids as claimed in claim 1, is characterized in that, described Organic Alcohol is the mixture of any one or at least two kinds in ethylene glycol, ethanol, glycol ether, n-propyl alcohol, Virahol, propylene glycol, 1,3-PD or glycerol.
12. glass grinding fluids as claimed in claim 1, it is characterized in that, described sinking agent is the mixture of any one or at least two kinds in water-soluble polyacrylamide, the twin quaternary ammonium salt of tween, tween three lives quaternary ammonium salt, polyoxyethylene Quito alkyl multi-quaternary ammonium salt, chain alkyl three lives quaternary ammonium salt, the twin quaternary ammonium salt of sapn, the twin quaternary ammonium salt of chain alkyl, the twin quaternary ammonium salt of natural rosin base or natural rosin base three lives quaternary ammonium salt.
13. glass grinding fluids as described in one of claim 1-3, it is characterized in that, the pH of described complete synthesis glass grinding fluid is 7.5 ~ 8.5.
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| CN103525533B true CN103525533B (en) | 2015-06-17 |
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| CN104911011B (en) * | 2015-06-29 | 2018-01-05 | 北京工业大学 | High-volume fractional aluminum-base silicon carbide composite grinding fluid based on ELID and preparation method thereof |
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| CN106675753B (en) * | 2016-12-26 | 2020-09-08 | 广东山之风环保科技有限公司 | Composite glass cutting fluid |
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| CN108925579A (en) * | 2018-05-11 | 2018-12-04 | 惠州市宝斯特实业有限公司 | A kind of antimildew liquid for glass |
| CN111704954A (en) * | 2020-07-02 | 2020-09-25 | 深圳市油博士润滑科技有限公司 | Water-soluble glass grinding fluid and preparation method thereof |
| CN113999727B (en) * | 2021-11-19 | 2023-11-03 | 广州米奇化工有限公司 | Cleaning composition, preparation method thereof and cleaning gel beads |
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