CN102925274A - Optical glass grinding fluid and preparation method thereof - Google Patents

Optical glass grinding fluid and preparation method thereof Download PDF

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Publication number
CN102925274A
CN102925274A CN2012104447941A CN201210444794A CN102925274A CN 102925274 A CN102925274 A CN 102925274A CN 2012104447941 A CN2012104447941 A CN 2012104447941A CN 201210444794 A CN201210444794 A CN 201210444794A CN 102925274 A CN102925274 A CN 102925274A
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CN
China
Prior art keywords
agent
grinding fluid
opticglass
rust
inorganic salt
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2012104447941A
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Chinese (zh)
Inventor
韩生
吴志桥
王建华
夏乃洁
郁平
孙揭阳
高峰
朱贤
王爱民
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Shanghai Institute of Technology
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Shanghai Institute of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Shanghai Institute of Technology filed Critical Shanghai Institute of Technology
Priority to CN2012104447941A priority Critical patent/CN102925274A/en
Publication of CN102925274A publication Critical patent/CN102925274A/en
Pending legal-status Critical Current

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Abstract

The invention discloses optical glass grinding fluid and a preparation method thereof. The optical glass grinding fluid comprises 9%-15% by weight of surface active agent, 8%-12% by weight of antirust agent, 3%-7% by weight of lubricating agent, 0.5%-1% by weight of inorganic salt, 0.3%-0.7% by weight of sedimentation agent, and the balance water. The preparation method includes steps of sequentially adding the surface active agent, the antirust agent, the inorganic salt, the sedimentation agent and the water into the lubricating agent, stirring and mixing evenly, and obtaining the optical glass grinding fluid. The optical glass grinding fluid is greatly improved in rust-resistant property, lubricity, cooling property and cleaning property.

Description

A kind of opticglass grinding fluid and preparation method thereof
Technical field
The present invention relates to a kind of opticglass grinding fluid and preparation method thereof.
Background technology
Glass, the quartzy optical goods that wait are often used Water-soluble grinding fluid when ground finish, owing to produce a large amount of grinding heat and glass powder in grinding process, therefore require very high to cooling performance and the cleaning performance of glass grinding fluid, in order to improve cooling and cleaning performance, the flow of grinding fluid and pressure are all higher, add that the operative employee is directly used in the contact processing component, therefore require grinding fluid nontoxic, smell is little, and is low to the pungency of skin and eyes, do not produce aerosol.
At present, opticglass, the Water-soluble grinding fluid that quartzy industry is used is main component mainly with polyethers, exists cooling poor, and smell is large, and this causes detrimentally affect to operator and environment, and Long Term Contact can bring operative employee's health problem.
Goal of the invention
One of purpose of the present invention is to provide a kind of opticglass grinding fluid in order to solve above-mentioned technical problem.
Two of purpose of the present invention provides the preparation method of above-mentioned a kind of opticglass grinding fluid.
Technical scheme of the present invention
A kind of opticglass grinding fluid, wherein each feed composition is counted by weight percentage, and its composition and content are as follows:
Tensio-active agent 9%-15%
Rust-preventive agent 8%-12%
Lubricant 3%-7%
Inorganic salt 0.5%-1%
Sinking agent 0.3%-0.7%
Surplus is water;
Wherein said tensio-active agent is polyoxyethylene glycol or cithrol;
Described rust-preventive agent is the mixture of one or more compositions in monoethanolamine, diethanolamine and the trolamine, is preferably diethanolamine and trolamine;
Described lubricant is glycerol, propylene glycol or 1,3-PD;
Described inorganic salt are the mixture of one or more compositions in sodium-chlor, yellow soda ash, the sodium bicarbonate;
Described sinking agent is the twin quaternary ammonium salt of chain alkyl, chain alkyl three lives quaternary ammonium salt or polyquaternium.
The preparation method of above-mentioned a kind of opticglass grinding fluid, step is as follows:
In lubricant, add successively nonionogenic tenside, rust-preventive agent, inorganic salt, sinking agent and water after, mix, namely get the opticglass grinding fluid.
Technique effect of the present invention
A kind of opticglass grinding fluid of the present invention, owing to use surfactant polyethylene, cithrol has replaced the polyethers in traditional opticglass grinding fluid, and therefore, opticglass grinding fluid of the present invention is improving a lot aspect oilness, cooling, the cleaning.
Further, a kind of opticglass grinding fluid of the present invention owing to added sinking agent, therefore has better settling property.
Further, the inorganic salt described in a kind of opticglass grinding fluid of the present invention have good chemical dressing effect to diamond abrasive tool, and the grinding efficiency in the time of can improving glass grinding is so generally be applicable to various opticglass processing.
Further, a kind of opticglass grinding fluid of the present invention, owing to added the rust-preventive agent hydramine, lubricant is glycerol, propylene glycol or 1,3-PD, so also all have high-performance at aspects such as rust-preventing characteristic, oilness, cooling performances.
Embodiment
Below by embodiment the present invention is further set forth, but do not limit the present invention.
Below among each embodiment used raw material and manufacturer's information as follows:
Tensio-active agent: polyoxyethylene glycol and cithrol, the Si Likai of Shenzhen trade Co., Ltd produces;
Rust-preventive agent: diethanolamine and trolamine, reflect safe trade (Shanghai) Co., Ltd. and produce;
Lubricant: glycerol, propylene glycol and 1,3-PD, the great chemical industry in Shenzhen one company limited produces;
Inorganic salt: sodium-chlor, yellow soda ash and sodium bicarbonate, the great chemical industry in Shenzhen one company limited produces;
Sinking agent: the twin quaternary ammonium salt of chain alkyl, chain alkyl three lives quaternary ammonium salt or polyquaternium, Shanghai Hong Ze chemical industry company limited produces.
Embodiment 1
A kind of opticglass grinding fluid, wherein each feed composition is counted by weight percentage, and its composition and content are as follows:
Tensio-active agent 9%
Rust-preventive agent 8%
Lubricant 3%
Inorganic salt 0.5%
Sinking agent 0.3
Water 79.2%;
Wherein said tensio-active agent is polyoxyethylene glycol;
Described rust-preventive agent is trolamine;
Described lubricant is glycerol;
Described inorganic salt are yellow soda ash;
Described sinking agent is the twin quaternary ammonium salt of chain alkyl.
The preparation method of above-mentioned a kind of opticglass grinding fluid comprises the steps:
In lubricant, add successively tensio-active agent, rust-preventive agent, inorganic salt, sinking agent and water after, mix, namely get the opticglass grinding fluid.
Embodiment 2
A kind of opticglass grinding fluid, wherein each feed composition is counted by weight percentage, and its composition and content are as follows:
Tensio-active agent 15%
Rust-preventive agent 12%
Lubricant 7%
Inorganic salt 1%
Sinking agent 0.7%
Water 64.3%;
Wherein said tensio-active agent is cithrol;
Described rust-preventive agent is diethanolamine;
Described lubricant is propylene glycol;
Described inorganic salt are sodium-chlor;
Described sinking agent is chain alkyl three lives quaternary ammonium salt.
The preparation method of above-mentioned a kind of opticglass grinding fluid comprises the steps:
In lubricant, add successively tensio-active agent, rust-preventive agent, inorganic salt, sinking agent and water after, mix, namely get the opticglass grinding fluid.
Embodiment 3
A kind of opticglass grinding fluid is characterized in that each feed composition is counted by weight percentage in the described opticglass grinding fluid, and its composition and content are as follows:
Tensio-active agent 12.5%
Rust-preventive agent 10%
Lubricant 5%
Inorganic salt 0.75%
Sinking agent 0.5%
Water 71.25%;
Wherein said tensio-active agent is cithrol;
Described rust-preventive agent is diethanolamine;
Described lubricant is 1,3-PD;
Described inorganic salt are sodium bicarbonate;
Described sinking agent is polyquaternium.
The preparation method of above-mentioned a kind of opticglass grinding fluid comprises the steps:
In lubricant, add successively tensio-active agent, rust-preventive agent, inorganic salt, sinking agent and water after, mix, namely get the opticglass grinding fluid.
Foregoing only is the basic explanation of the present invention under conceiving, and according to any equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.

Claims (5)

1. an opticglass grinding fluid is characterized in that each feed composition is counted by weight percentage in the described opticglass grinding fluid, and its composition and content are as follows:
Tensio-active agent 9-15%
Rust-preventive agent 8%-12%
Lubricant 3%-7%
Inorganic salt 0.5%-1%
Sinking agent 0.3-0.7%
Surplus is water;
Wherein said tensio-active agent is polyoxyethylene glycol or cithrol;
Described rust-preventive agent is the mixture of one or more compositions in monoethanolamine, diethanolamine and the trolamine;
Described lubricant is glycerol, propylene glycol or 1,3-PD;
Described inorganic salt are the mixture of one or more compositions in sodium-chlor, yellow soda ash, the sodium bicarbonate;
Described sinking agent is the twin quaternary ammonium salt of chain alkyl, chain alkyl three lives quaternary ammonium salt or polyquaternium.
2. a kind of opticglass grinding fluid as claimed in claim 1 is characterized in that each feed composition is counted by weight percentage in the described opticglass grinding fluid, and its composition and content are as follows:
Nonionogenic tenside 9%
Rust-preventive agent 8%
Lubricant 3%
Inorganic salt 0.5%
Sinking agent 0.3%
Surplus is water;
Wherein said tensio-active agent is polyoxyethylene glycol;
Described rust-preventive agent is trolamine;
Described lubricant is glycerol;
Described inorganic salt are yellow soda ash;
Described sinking agent is the twin quaternary ammonium salt of chain alkyl.
3. a kind of opticglass grinding fluid as claimed in claim 1 is characterized in that each feed composition is counted by weight percentage in the described opticglass grinding fluid, and its composition and content are as follows:
Nonionogenic tenside 15%
Rust-preventive agent 12%
Lubricant 7%
Inorganic salt 1%
Sinking agent 0.7%
Surplus is water;
Wherein said tensio-active agent is cithrol;
Described rust-preventive agent is diethanolamine;
Described lubricant is propylene glycol;
Described inorganic salt are sodium-chlor;
Described sinking agent is chain alkyl three lives quaternary ammonium salt.
4. a kind of opticglass grinding fluid as claimed in claim 1 is characterized in that each feed composition is counted by weight percentage in the described opticglass grinding fluid, and its composition and content are as follows:
Nonionogenic tenside 12.5%
Rust-preventive agent 10%
Lubricant 5%
Inorganic salt 0.75%
Sinking agent 0.5%
Surplus is water;
Wherein said tensio-active agent is cithrol;
Described rust-preventive agent is diethanolamine;
Described lubricant is 1,3-PD;
Described inorganic salt are sodium bicarbonate;
Described sinking agent is polyquaternium.
5. such as the preparation method of the arbitrary described a kind of opticglass grinding fluid of claim 1-4, it is characterized in that in lubricant, after adding successively tensio-active agent, rust-preventive agent, inorganic salt, sinking agent and water, mix, namely get the opticglass grinding fluid.
CN2012104447941A 2012-11-09 2012-11-09 Optical glass grinding fluid and preparation method thereof Pending CN102925274A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012104447941A CN102925274A (en) 2012-11-09 2012-11-09 Optical glass grinding fluid and preparation method thereof

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Application Number Priority Date Filing Date Title
CN2012104447941A CN102925274A (en) 2012-11-09 2012-11-09 Optical glass grinding fluid and preparation method thereof

Publications (1)

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CN102925274A true CN102925274A (en) 2013-02-13

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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104087368A (en) * 2014-03-28 2014-10-08 南京航空航天大学 Cutting fluid for free abrasive electric grinding multi-line cutting
CN104450144A (en) * 2014-12-24 2015-03-25 常熟市梅李镇亚贸玻璃配件厂 Glass edging process
CN104830505A (en) * 2015-05-27 2015-08-12 深圳市飞世尔实业有限公司 Water-base glass cutting fluid and manufacturing method thereof
CN104911011A (en) * 2015-06-29 2015-09-16 北京工业大学 ELID (Electrolytic In-process Dressing)-based high-volume-fraction aluminum-based silicon carbide composite grinding fluid and preparation method of grinding fluid
CN105542934A (en) * 2015-12-24 2016-05-04 东莞市安美润滑科技有限公司 Smart phone glass cover plate grinding fluid and preparation method and method of application thereof
CN105925358A (en) * 2016-04-26 2016-09-07 东莞市剑鑫电子材料有限公司 Aqueous grinding liquid for optical sapphire
CN106281628A (en) * 2016-08-12 2017-01-04 浙江模德石化有限公司 A kind of Water-soluble grinding fluid and preparation method thereof
CN106675753A (en) * 2016-12-26 2017-05-17 广东山之风环保科技有限公司 Compound glass cutting fluid
CN107574006A (en) * 2017-09-29 2018-01-12 广东星弛光电科技有限公司 A kind of optical glass grinding fluid and preparation method thereof
CN107629861A (en) * 2016-07-18 2018-01-26 天津市澳路浦润滑科技股份有限公司 A kind of Hard-alloy Grinding Fluid
CN115678658A (en) * 2022-11-03 2023-02-03 福建省佑达环保材料有限公司 Glass cutting fluid with high settling property

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020019199A1 (en) * 1999-04-23 2002-02-14 3M Innovative Properties Company Abrasive article suitable for abrading glass and glass ceramic workpieces
CN102102008A (en) * 2009-12-18 2011-06-22 安集微电子(上海)有限公司 Water-based glass grinding fluid and using method thereof
CN101633831B (en) * 2009-08-26 2012-07-04 广州机械科学研究院 Optical product grinding fluid and preparation method and application thereof
CN102559354A (en) * 2010-12-30 2012-07-11 安集微电子(上海)有限公司 Water-based glass grinding fluid

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020019199A1 (en) * 1999-04-23 2002-02-14 3M Innovative Properties Company Abrasive article suitable for abrading glass and glass ceramic workpieces
CN101633831B (en) * 2009-08-26 2012-07-04 广州机械科学研究院 Optical product grinding fluid and preparation method and application thereof
CN102102008A (en) * 2009-12-18 2011-06-22 安集微电子(上海)有限公司 Water-based glass grinding fluid and using method thereof
CN102559354A (en) * 2010-12-30 2012-07-11 安集微电子(上海)有限公司 Water-based glass grinding fluid

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104087368B (en) * 2014-03-28 2016-08-17 南京航空航天大学 Multi-wire saw cutting fluid cut by a kind of free abrasive electric mill
CN104087368A (en) * 2014-03-28 2014-10-08 南京航空航天大学 Cutting fluid for free abrasive electric grinding multi-line cutting
CN104450144A (en) * 2014-12-24 2015-03-25 常熟市梅李镇亚贸玻璃配件厂 Glass edging process
CN104830505A (en) * 2015-05-27 2015-08-12 深圳市飞世尔实业有限公司 Water-base glass cutting fluid and manufacturing method thereof
CN104911011B (en) * 2015-06-29 2018-01-05 北京工业大学 High-volume fractional aluminum-base silicon carbide composite grinding fluid based on ELID and preparation method thereof
CN104911011A (en) * 2015-06-29 2015-09-16 北京工业大学 ELID (Electrolytic In-process Dressing)-based high-volume-fraction aluminum-based silicon carbide composite grinding fluid and preparation method of grinding fluid
CN105542934A (en) * 2015-12-24 2016-05-04 东莞市安美润滑科技有限公司 Smart phone glass cover plate grinding fluid and preparation method and method of application thereof
CN105925358A (en) * 2016-04-26 2016-09-07 东莞市剑鑫电子材料有限公司 Aqueous grinding liquid for optical sapphire
CN107629861A (en) * 2016-07-18 2018-01-26 天津市澳路浦润滑科技股份有限公司 A kind of Hard-alloy Grinding Fluid
CN106281628A (en) * 2016-08-12 2017-01-04 浙江模德石化有限公司 A kind of Water-soluble grinding fluid and preparation method thereof
CN106675753A (en) * 2016-12-26 2017-05-17 广东山之风环保科技有限公司 Compound glass cutting fluid
CN106675753B (en) * 2016-12-26 2020-09-08 广东山之风环保科技有限公司 Composite glass cutting fluid
CN107574006A (en) * 2017-09-29 2018-01-12 广东星弛光电科技有限公司 A kind of optical glass grinding fluid and preparation method thereof
CN115678658A (en) * 2022-11-03 2023-02-03 福建省佑达环保材料有限公司 Glass cutting fluid with high settling property

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Application publication date: 20130213