CN103478904A - Tea-flower-aroma tobacco excipient and tobacco product - Google Patents
Tea-flower-aroma tobacco excipient and tobacco product Download PDFInfo
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- CN103478904A CN103478904A CN201310446797.3A CN201310446797A CN103478904A CN 103478904 A CN103478904 A CN 103478904A CN 201310446797 A CN201310446797 A CN 201310446797A CN 103478904 A CN103478904 A CN 103478904A
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Abstract
The invention belongs to the field of spices and tobacco, and relates to a tea-flower-aroma tobacco excipient and a tobacco product, in particular to a tobacco excipient containing tea flower extracts, application of the tobacco excipient in preparation of the tobacco product like cigarettes, and the tobacco product, containing the tobacco excipient, like the cigarettes. The cigarettes has a tea flower aroma which is consistent with an own fragrance of tobacco of the cigarettes, aroma and taste of the cigarettes are obviously improved, remaining taste is comfortable, smoke is delicate and soft, and spicy stimulation and mouth dryness sensation of the smoke is effectively reduced. The tobacco excipient which is a tobacco flavor is simple in preparation process, and original processing techniques and equipment of the cigarettes are unchanged in the process of adding of the tobacco excipient.
Description
Technical field
The invention belongs to spices and Field of Tobacco, relate to a kind of tobacco auxiliary material and tobacco product of Tea Flower odor type.
Background technology
In recent years, along with the raising of people's living standard, more and more deep to healthy understanding, the smoker is also more and more higher for the quality requirements of cigarette, the cigarette that adopts the whole bag of tricks or additive to prepare different taste.
Cigarette paper is commonly called as obbbin, and as the auxiliary material of cigarette, from the cigarette outward appearance, cigarette paper plays the effect of parcel pipe tobacco.It is compared as cork paper, forming paper with the auxiliary material of other cigarette, most important characteristics are burnings that cigarette paper participates in cigarette, thereby the chemical composition of suction flavor, cigarette outward appearance and the flue gas of the smolderability of cigarette, burning velocity, cigarette is all played a very important role.Typical cigarette paper contains about 74% cellulose and 25% pearl filler, 1% combustion adjuvant in addition.The air permeability of cigarette paper, tensile strength, the performance of glowing, opacity and certain requirement is quantitatively arranged in cigarette industry.
At present, most of cigarette paper all can produce the suction disadvantageous xylon gas of taste when burning.In order to adjust and improve the performance of cigarette paper, can reduce or utilize the smell of other material generation to cover the xylon gas that the burning of regular-size cigarette paper produces by adding appropriate additive, inhale thereby reach the purpose that flavor compensates.Additive can comprise natural baccy extract, natural plant extracts and monomer perfume material.As Chinese patent CN200810133587.8 discloses a kind of cigarette paper that contains compound Chinese herb extract additive and preparation method thereof.Chinese patent CN201010101358.5 discloses a kind of cigarette paper for mint cigarette and preparation method thereof.Chinese patent CN201010120249.8 discloses a kind of cigarette paper that contains rhodiola root and preparation method thereof.But not yet there is the Tea Flower extract to be added on the report in cigarette paper at present.
Tipping paper has another name called cork paper, is to specialize in a kind of special industry paper using of cigarette as filter tip cigarette packing, and its effect is mainly used for the connection of filter tip and cigarette.Tipping paper is generally printing or painting last layer coating on body paper, and color is generally brown or pure white, or with orris, imitative cork floral designs and trade mark title.The body paper of tipping paper be take wood pulp cellulose as raw material, and calcium carbonate is filler, generally also contains the titanium dioxide composition, to control the opacity of paper.Tipping paper requires to have certain quality, thickness, tensile strength, water suction and waterproof ability.Directly contact with the smoker when the cigarette smoking due to tipping paper, therefore in recent years the requirement of tipping paper not only be confined to the packing that tradition is simple, more to its health environment-friendly and fall on burnt flavouring and have higher requirement.
Chinese patent CN200410003057.3 discloses a kind of tipping paper that contains micro-antibiotic effective ingredient and preparation method thereof.Chinese patent CN200810210590.5 discloses a kind of tipping paper that contains compound Chinese herb extract additive and preparation method thereof.
In addition, cigarette filter tip rod, as the filtration system of cigarette smoke, be take cigarette filter tip rod as carrier, adds different functional additives, aspect lifting cigarette smoking quality and reduction cigarette smoke harmful substance, has important effect.Yet along with the reduction of cigarette tar content, also corresponding reduction of the fragrance matter content in flue gas, on the suction quality band of cigarette bad impact.Flavouring during Cigarette design is mended the fragrant person's that becomes the Cigarette design to satisfy the demands of consumers crucial research topic.Add different types of essence and flavoring agent in filter stick, can improve to a certain extent the fragrance of cigarette, if but add the essence and flavoring agent manually recalled, add and can make too much cigarette lose the taste of itself.
Yuan Yi comes (CN1887126A) to disclose the preparation method of a kind of fruit flavouring cigarette and filter stick, fruity essence is prepared into to brewed heart yearn after solution, after making fragrant heart yearn, it is added in the acetate fiber rod of filter stick, the essence on heart yearn can make the consumer live pure and fresh simple and elegant and refrigerant mouthfeel.But a large amount of interpolation essence and flavoring agents has been desalinated the original natural fragrance of cigarette.He Jinxings etc. (CN102423137A) disclose Yunnan Fructus Canrii Albi extract and the application on cigarette filter stick thereof for a kind of cigarette, reach the content of beary metal reduced in flue gas, the effect that relieve sore throat promotes the production of body fluid.
Yu Yao etc. (CN102871221A) disclose a kind of by the coaxial filter stick binary compound filter candle of acetate fiber and active carbon, can significantly reduce the harmful components in cigarette smoke.(CN102860584A) such as fourth petrels discloses a kind of capsule that supplements a large amount of aroma components and humectation composition, and embeds the cellulose acetate filter rod section and make Three-element composite filter core, reaches the purpose that increases fragrance and flue gas comfort.
Tea Flower is the flower of Theaceae Camellia Plants tea tree, is a kind of without plantation cultivation, abundant and reproducible natural resources.Tea tree is wide at China's distributed pole, be September to next year 1, February tea tree florescence in most of tea district, Tea Flower is a kind of without plantation cultivation, abundant and reproducible natural resources, for a long time, the tea grower only plucks the fresh and tender bud-leaf of tea tree, let alone to run its course for Tea Flower, seldom be used.Tea Flower is containing various active compositions such as abundant aroma substance and protein, Tea Polyphenols, tea polysaccharide, Tea Saponin, flavonoids, amino acid, vitamin, trace element and superoxide dismutase (SOD), theobromines.
Still need at present the additive of wanting suitable with and application on cigarette paper, cigarette tipping paper and/or filter stick for cigarettes, to produce the cigarette of Tea Flower odor type.
Summary of the invention
The inventor, through in depth studying and performing creative labour, has obtained the preparation technology of Tea Flower extract and has correspondingly obtained Tea Flower extract (essential oil of the flower of Camellia sinensis, Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil).The inventor is surprised to find, the Tea Flower extract (one or more mixture) made is put among one or more auxiliary materials of tobacco, can make cigarette there is Tea Flower feature note, with this fragrant harmony of cigarette tobacco, the jealous obvious improvement of the perfume (or spice) of cigarette, flue gas is fine and smooth, soft, and pleasant impression is comfortable, effectively reduces pungent stimulation and the xerostomia sense of flue gas.Following invention is provided thus:
One aspect of the present invention relates to the auxiliary material that grows tobacco, and it contains the Tea Flower extract.
Described tobacco auxiliary material for be selected from for example, in cigarette paper, tipping paper (being called again cork paper) and filter stick (heart yearn filter stick or binary compound filter candle) any or multiple.
Described Tea Flower extract can be used and be selected from following method preparation: normal temperature lixiviate, heating and refluxing extraction, Soxhlet extraction, ultrasonic auxiliary extraction, microwave auxiliary extraction, enzyme process auxiliary extraction, accelerated solvent extraction, supercritical fluid extraction, while distillation extraction etc.But the Tea Flower extract of preferably, putting down in writing below for this paper.
Described Tea Flower extract can be from the extract of single variety Tea Flower acquisition or the mixture of the extract of different varieties of tea plant flower acquisition.
The mixture of one or more that described Tea Flower extract can be essential oil of the flower of Camellia sinensis, medicinal extract, absolute oil, tincture etc. (for example wherein any 2 kinds, any 3 kinds or any 4 kinds).
The Tea Flower extract is dissolved and is deployed into the Tea Flower essence that the mass concentration scope is 1%-10% with 60%-80% ethanol.
In one embodiment of the invention, through following preparation section, can make the cigarette paper that contains the Tea Flower odor type:
After adding a little, the combustionregulator of paper machine introduces quantitative spraying device, take a certain amount of Tea Flower extract according to the Tea Flower extract of 0.01 weight portion-0.5 weight portion and the ratio of 100 weight portion cigarette paper, be configured to 60%-80% ethanol the Tea Flower essence solution that the mass concentration scope is 1%-10%, at quantitative spraying device, evenly be sprayed on cigarette paper, again through the low temperature cylinder dried, volatilize fully to alcohol; Maybe the Tea Flower essence solution prepared is carried out to even dip-coating to cigarette paper on coating machine, then through the low temperature cylinder dried, volatilize fully to alcohol.Dryer temperature is controlled between 40-70 ℃.Then through batching, cut the manufacture of Tea Flower odor type cigarette paper.
In one embodiment of the invention, through following preparation section, can make the cork paper that contains the Tea Flower odor type:
The Tea Flower extract of pressing the 0.1%-10% mass fraction of the general printing-ink of cork paper mixes with printing ink, after being uniformly mixed, in cork paper typography process, is printed onto on cork paper, is prepared into the cigarette paper of Tea Flower odor type.In cork paper, Tea Flower extract addition is that 100 weight portion yew paper add 0.01-0.5 weight portion Tea Flower extract.
The filter stick of Tea Flower odor type can make by following steps:
1. chitin fiber is made to well-formed's filter stick heart yearn;
2. the Tea Flower extract is prepared to Tea Flower essence according to the following ratio: Tea Flower extract 1-4 part, water soluble chitosan 0.1-0.5 part, all the other are water or ethanol (100 weight portions altogether).
3. will contain the functional agent of Tea Flower essence by sponge roller, make it evenly to spread upon on the filter stick heart yearn;
4. above-mentioned filter stick heart yearn is placed in to the dry 2-4h of hothouse that under normal temperature, humidity is 25%-30%;
5. by the outer core of acetate fiber and the moulding simultaneously of step 3 gained filter stick heart yearn, make the filter stick heart yearn that contains Tea Flower essence combine into cigarette filter rod with the outer core of acetate fiber.
The cigarette the present invention relates to refers to the filter stick that comprises acetate fiber and modified activated carbon filter stick binary recombiner unit with binary compound filter candle; Particularly, it also comprises outer wrapping layer and interior integument, wherein acetate fiber and active carbon filter stick binary recombiner unit are the round clavas consisted of cellulose acetate filter rod section and the alternate combination of active carbon filter stick section, interior integument is wrapped in respectively on the fine filter rod segments of vinegar and active carbon stick section, and the outer wrapping layer is wrapped on interior integument.
Described modified activated carbon filter stick is to take the diacetate fiber tow to be composited as carrier adds the modified activated carbon particle, and wherein modified activated carbon particle consumption changes as required between the 0.5-5mg/mm filter stick.
Described modified activated carbon is that active carbon forms by soaking or spray to implant through Tea Flower essence, the consumption of Tea Flower essence can be according to need to changing of applying between the 1%-30% of active carbon weight, and active carbon can be a kind of of cocoanut active charcoal, active fruit shell carbon or bamboo charcoal etc.
Described Tea Flower essence is the Tea Flower extract to be deployed into to the solution of concentration range 1%-10% with the ethanol of 60%-80%.
The described tobacco auxiliary material of any one according to the present invention, wherein, the 0.01-5% that the content of described Tea Flower extract or consumption are tobacco auxiliary material weight; Preferably, be 0.05%-3%; More preferably, be 0.1%-1%, be particularly preferably 0.2%-0.8%, 0.2%-0.6%, 0.2%-0.5%, 0.2%-0.4%, 0.4%-0.6%, 0.5%-0.8%; Particularly, be 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7% or 0.8%.
The described tobacco auxiliary material of any one according to the present invention, wherein, described Tea Flower extract be selected from essential oil of the flower of Camellia sinensis, Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil any one, two kinds, three kinds or four kinds.
The described tobacco auxiliary material of any one according to the present invention, wherein, the mixture that described Tea Flower extract is Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil.
The described tobacco auxiliary material of any one according to the present invention, wherein, described Tea Flower extract comprises Tea Flower tincture 25%-70%, 25%-45% or 45%-70%.
The described tobacco auxiliary material of any one according to the present invention, wherein, described Tea Flower extract comprises Tea Flower medicinal extract 5%-25%, 5%-30% or 25%-30%.
The described tobacco auxiliary material of any one according to the present invention, wherein, described Tea Flower extract comprises Tea Flower absolute oil 20%-30%, 20%-25%, 25%-30%, 20%-22% or 22%-25%, and for example 20%, 21%, 22%, 23%, 24%, 25%, 26%, 27%, 28%, 29%, 30%.
The described tobacco auxiliary material of any one according to the present invention, wherein, described Tea Flower extract comprises or is Tea Flower tincture 45%-70%, Tea Flower medicinal extract 5%-30%, Tea Flower absolute oil 25%-30%.
In one embodiment of the invention, described tobacco auxiliary material, wherein, described Tea Flower extract is Tea Flower tincture 70%, Tea Flower medicinal extract 5%, Tea Flower absolute oil 25%.
In one embodiment of the invention, described tobacco auxiliary material, wherein, described Tea Flower extract is Tea Flower tincture 45%, Tea Flower medicinal extract 30%, Tea Flower absolute oil 25%.
In one embodiment of the invention, described tobacco auxiliary material, wherein, described Tea Flower extract is Tea Flower tincture 45%, Tea Flower medicinal extract 25%, Tea Flower absolute oil 30%.
The inventor also is surprised to find, and when using above-mentioned three kinds of extracts and consumption thereof, the cigarette obtained has the note of Tea Flower feature, and with the fragrant harmony of cigarette, fragrance matter is obviously improved, the fragrance exquisiteness, and mouthfeel is fresh and sweet, and assorted gas and dry sensation obviously improve, and pleasant impression is clean.Wherein allowing especially the inventor impressive is the fresh and sweet characteristics of mouthfeel.
The tincture that the Tea Flower of different cultivars extracts, medicinal extract, absolute oil and essential oil have certain difference.Tincture, medicinal extract, absolute oil and essential oil can mix use, and it can be same seeds, also can different tree species.
The described tobacco auxiliary material of any one according to the present invention, wherein, tincture used, medicinal extract, absolute oil and essential oil are tincture, medicinal extract, absolute oil and the essential oil that is selected from the Tea Flower of Fujian Anxi Tieguanyin Tea tea tree, District, Xinyang Area, Henan Province high-quality green tea tea tree, Wuyi Mountain, fujian Wuyi cliff tea tea tree and yunnan puer tea tea tree independently.
In specific embodiment of the present invention, described tobacco auxiliary material, wherein, described Tea Flower extract is Xinyang Maojian Tea tea tree tincture 70%, Wuyi cliff tea Tea Flower medicinal extract 5%, Wuyi cliff tea Tea Flower absolute oil 25%.
In specific embodiment of the present invention, described tobacco auxiliary material, wherein, described Tea Flower extract is Anxi Tieguanyin Tea Tea Flower tincture 45%, Xinyang Maojian Tea tea tree flower concrete 30%, Wuyi cliff tea Tea Flower absolute oil 25%.
In specific embodiment of the present invention, described tobacco auxiliary material, wherein, described Tea Flower extract is Anxi Tieguanyin Tea Tea Flower tincture 45%, Xinyang Maojian Tea tea tree flower concrete 25%, Wuyi cliff tea Tea Flower absolute oil 30%.
In one embodiment of the invention, described tobacco auxiliary material, wherein, described Tea Flower extract is Anxi Tieguanyin Tea Tea Flower tincture 45%, Xinyang Maojian Tea tea tree flower concrete 25%-30%, Wuyi cliff tea Tea Flower absolute oil 25%-30%.
In one embodiment of the invention, described tobacco auxiliary material, wherein, described Tea Flower extract is Anxi Tieguanyin Tea Tea Flower tincture 40%-50%, Xinyang Maojian Tea tea tree flower concrete 25%-30%, Wuyi cliff tea Tea Flower absolute oil 25%-30%.
In one embodiment of the invention, described tobacco auxiliary material, wherein, described Tea Flower extract is Anxi Tieguanyin Tea Tea Flower tincture 45%-50%, Xinyang Maojian Tea tea tree flower concrete 25%-30%, Wuyi cliff tea Tea Flower absolute oil 25%-30%.
The invention still further relates to the extractive composition (mixture of Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil) of above-mentioned use.
The described tobacco auxiliary material of any one according to the present invention, wherein, described essential oil of the flower of Camellia sinensis makes as follows:
(1) take a certain amount of Tea Flower pack into be furnished with the trapping cold-trap the decompression extraction element in;
(2) add the water of at least 5 times of Tea Flower weight, and the temperature of the water added is more than 80 ℃, at least 5min is soaked in sealing, is cooled to 30-70 ℃;
(3-1) carry out the reduced steam distillation, temperature used is identical with cooled temperature in step (2), and vacuum is 1-17kpa, collects distillate;
Preferably, also comprise step (3-2): repeating step (2) and (3-1) in operation 1 time or repeatedly, and merge distillate;
(4) in the use, low polar organic solvent carries out 1 time the distillate obtained in step (3-1) or step (3-2) or repeatedly back extraction (for example 2,3,4 or 5 times, preferably 3 times), obtains stripping workshop; Stripping workshop is concentrated, obtained concentrate;
(5) use concentrate weight 2-4 absolute ethyl alcohol doubly to carry out backwash to the concentrate obtained in step (4), reduced pressure concentration remove wherein residual in after low polar organic solvent essential oil of the flower of Camellia sinensis.
The described tobacco auxiliary material of any one according to the present invention, wherein, step (2) meets following any one in 1.-4. or multinomial:
The 5-50 that the amount of the water 1. added is Tea Flower weight doubly, is preferably 5-40 doubly or 8-40 times, and more preferably 10-30 doubly;
The temperature of the water 2. added is preferably more than 85 ℃, more preferably, more than 90 ℃, more preferably, more than 95 ℃, is particularly preferably boiling water;
3. the time that sealing is soaked is 5min-4h, is preferably 5min-4h, 5min-3h or 5min-2h, and more preferably 5-60min, 5-50min or 5-40min, be particularly preferably 5-30min;
4. be cooled to 30-70 ℃; For example 30-40 ℃, 45-55 ℃ or 60-70 ℃.
The described tobacco auxiliary material of any one according to the present invention, wherein, step is cooled to 30-70 ℃ in (2), for example 30-40 ℃, 30-50 ℃, 30-60 ℃, 40-50 ℃, 45-55 ℃, 40-60 ℃, 40-70 ℃, 50-60 ℃, 50-70 ℃ or 60-70 ℃.
Those skilled in the art know, and vacuum is corresponding to a certain extent with vapo(u)rizing temperature, need to guarantee to allow distilled water and aroma component in cucurbit steam under giving fixed temperature and vacuum.
Be not limited to theoretical restriction, temperature is lower, and required vacuum is less, and temperature is higher, and required vacuum is larger.Inventor's discovery, when temperature is 30 ℃, vacuum 2.5kpa; Can be faster than the little speed distilled of 2.5kpa; When temperature is 70 ℃, vacuum 17kpa; Can be faster than the little speed distilled of 17kpa.
Be not limited to theoretical restriction, on the other hand, under the prerequisite of Temperature Setting, if vacuum is too low, may cause the meeting bumping, pot liquid is gone out; If vacuum is too high, may make the pot liquid distillation not out, do not have the effect of decompression distillation.Therefore, the corresponding proper vacuum ranges of each temperature value.
Therefore, about step (3-1) or the vacuum of reduced steam (3-2) distillation, those skilled in the art can be set according to the theory above selected temperature reference or this area knowledge, also can be with reference to following vacuum ranges, or adjusted on this basis:
For example 1-12kPa, 1-10kPa, 1-9.5kPa, 1-9kPa, 1-8.5kPa, 1-8kPa, 1-7.5kPa or 1-7kPa, 2.5-7kPa for example, 1-2kPa, 1-3kPa, 1-4kPa, 1-5kPa, 1-6kPa, 2-3kPa, 2-4kPa, 2-5kPa, 2-6kPa, 2-7kPa, 3-4kPa, 3-5kPa, 3-6kPa, 3-7kPa, 4-5kPa, 4-6kPa, 4-7kPa, 5-6kPa, 5-7kPa, 6-7kPa, 6-12kPa, 8-12kPa, 10-12kPa, 1kPa, 2kPa, 3kPa, 4kPa, 5kPa, 6kPa, 7kPa, 8kPa, 9kPa, 10kPa, 11kPa or 12kPa.
The described tobacco auxiliary material of any one according to the present invention, wherein, in step (4), described in low polar organic solvent be to be selected from any one in absolute ether and ethyl acetate, or two kinds of mixtures with arbitrary proportion.Ethyl acetate.In described, the consumption of low polar organic solvent can be the 1/4-1/3 of distillate volume.
The decompression extraction element used can be to be commercially available, and those skilled in the art also can combine realization by the routine instrument device be purchased.
The described tobacco auxiliary material of any one according to the present invention, wherein, described Tea Flower tincture, Tea Flower medicinal extract or Tea Flower absolute oil, respectively as follows 1), step 1)-2) or step 1)-3) make:
1) super-pressure extracts: take a certain amount of Tea Flower and put into the super-pressure extractor, the edible alcohol that adds at least 2 times of (w/w) Tea Flower weight, carry out the super-pressure extraction, obtain Tea Flower tincture 1, the concentration of wherein said edible alcohol is the 20-70%(mass concentration); Preferably, the 1/5-1/10 that Tea Flower tincture 1 is concentrated into to original volume obtains Tea Flower tincture 2;
2) prepare Tea Flower medicinal extract: the Tea Flower tincture 1 or the Tea Flower tincture 2 that obtain in step 1) are further concentrated, obtain Tea Flower medicinal extract;
3) prepare the Tea Flower absolute oil: by a certain amount of 95% ethanol back dissolving step 2) the Tea Flower medicinal extract that obtains, then carry out freezing processing (for example-10 ℃ to-20 ℃), cooling time is that 16-48h(is preferably 20-36h), then filter, concentrated, obtain the Tea Flower absolute oil.
The described tobacco auxiliary material of any one according to the present invention, wherein, step 1) meets following any one in 1.-6. or multinomial:
1. described is that adopted Tea Flower is Tea Flower fresh flower, dried flower, spray Ethanol Treatment Tea Flower, saline sook Tea Flower or alcohol immersion Tea Flower;
2. release immediately after the super-pressure extraction;
3. add the doubly edible alcohol of (w/w) Tea Flower weight of 1-15 at least, be preferably 1-10 doubly, 2-10 doubly, 2-8 doubly, 3-8 doubly (w/w), more preferably 4-7 doubly (w/w);
④150－500Mpa；
5. the dwell time is 5-120min, is preferably 5-60min, more preferably 10-30min.
6. the concentration of edible alcohol used is the 40%-70%(mass concentration).
The described tobacco auxiliary material of any one according to the present invention, wherein, in step 1), particularly, the concentration of described edible alcohol is the 20-70%(mass concentration), 20-40%, 20-50%, 40-50%, 50-70%, 20%, 30%, 40%, 50%, 60%, 70%.
The described tobacco auxiliary material of any one according to the present invention, wherein, in step 1), release immediately after super-pressure extracts.
The described tobacco auxiliary material of any one according to the present invention, wherein, in step 1), the pressure of described super-pressure is 150-500Mpa; Particularly, be 150-250Mpa, 150-300Mpa, 250-300Mpa, 250-350Mpa, 250-500Mpa, 300-350Mpa, 300-500Mpa, 350-500Mpa, 150Mpa, 200Mpa, 250Mpa, 300Mpa, 350Mpa, 400Mpa, 450Mpa, 500Mpa etc.
The super-pressure extraction element used can be to be commercially available.
Another aspect of the present invention relates to the described tobacco auxiliary material of middle any one and is preparing for example purposes in cigarette of tobacco product.
The tobacco articles that relates in one aspect to again of the present invention, it contains the described tobacco auxiliary material of any one in one or more the present invention; Particularly, described tobacco product is cigarette.
In the present invention,
" tea tree " in described " Tea Flower ", if not otherwise specified, refer to the plant of Theales (Theales), Theaceae (Theaceae) or Camellia (Camellis).
In the present invention, in concrete embodiment, described tea tree is Fujian Anxi Tieguanyin Tea tea tree, District, Xinyang Area, Henan Province high-quality green tea tea tree, Wuyi Mountain, fujian Wuyi cliff tea tea tree or yunnan puer tea tea tree.
In one aspect of the invention, " flower " in described " Tea Flower " comprising: perianth, oecium, gynoecium.Perianth comprises: calyx (being comprised of sepal), corolla (being comprised of petal).The color of flower and fragrance are from corolla.Stamen comprises: filigree and flower pesticide.Gynoecium comprises: column cap, style and ovary.
In one aspect of the invention, term " Tea Flower ", can be fresh flower, can be also dry flower; If there is no specified otherwise, it refers to the part of complete Tea Flower or Tea Flower; It at least comprises petal; Alternatively, also comprise and be selected from one or more in sepal, stamen and gynoecium.
In the present invention, in concrete embodiment, described Tea Flower is the Tea Flower that picks up from Fujian Anxi Tieguanyin Tea tea tree, District, Xinyang Area, Henan Province high-quality green tea tea tree, Wuyi Mountain, fujian Wuyi cliff tea tea tree or yunnan puer tea tea tree.
Tea Flower of the present invention can be Tea Flower fresh flower, dried flower, spray Ethanol Treatment Tea Flower, saline sook Tea Flower or alcohol immersion Tea Flower.
Term " essential oil ", in broad terms, essential oil refers to from spice berry and secretes the general name of the organ of fragrant animal, passing through the resulting volatility fragrant containing substance goods of processing extraction, in the narrow sense, essential oil only refers to the goods of water steam distillation method, milling process, cold grinding method or cracking process prepared fragrant containing substance from spice berry organ (as flower, leaf, branch, skin, scapus, root, fruit, seed etc.).In actual applications, often adopt its narrow sense.
Term " tincture " or " tincture " refer to uses certain density ethanol, lixiviate spice berry organ or exudate and secrete fragrant animal containing fragrant organ or its containing the resulting aroma material preparation that contains some ethanol of fragrant secretion.Under normal temperature, be worth tincture to be called " cold process tincture "; The tincture made under the heating counterflow condition is called " hot method tincture ".
Term " medicinal extract ", in a broad sense, medicinal extract refers to organic solvent extraction spice berry organ or its exudate (as resin, natural gum, balm), removes solvent for use and the general designation of the aroma material preparation that obtains.From narrowly, medicinal extract only refers to organic solvent extraction spice berry organ resulting not containing the aroma material preparation of solvent for use and moisture.
Term " absolute oil ", in a broad sense, refer to the solution that extracts the fragrant composition in medicinal extract, botany bar gum, balm or face cream with high concentration ethanol, through freezing processing, the elimination insoluble matter, then after pressure reducing and steaming ethanol the general designation of the aroma material preparation of gained.
In the present invention, Tea Flower essence also refers to the Tea Flower extract, includes but not limited to: Tea Flower tincture, medicinal extract and/or absolute oil; Alternatively, it also comprises auxiliary material (carrier, solvent, pigment, antioxidant, anticorrisive agent, humectant, fumet etc.).
In the present invention, particularly, the tobacco product of described tobacco product for sucking, be preferably cigarette.
The beneficial effect of the invention
The Tea Flower essence made is added in cigarette paper and/or tipping paper, can make cigarette there is Tea Flower feature note, with this fragrant harmony of cigarette tobacco, the jealous obvious improvement of the perfume (or spice) of cigarette, flue gas is fine and smooth, soft, and pleasant impression is comfortable, effectively reduces pungent stimulation and the xerostomia sense of flue gas.And this cigarette additive preparation technology is simple, the adding technology in cigarette does not change the original processing technology of cigarette and equipment.
The cigarette rolled with the heart yearn filter stick containing Tea Flower essence, during suction, contain tea tree essence active ingredient in flue gas, make flue gas pure and fresh simple and elegant, there is the Tea Flower characteristic perfume with this fragrant harmony of tobacco, can improve the mouthfeel of cigarette, the drying that reduces flue gas stimulates, the comfort while improving cigarette smoking simultaneously.The Tea Polyphenols isoreactivity material contained in Tea Flower essence can reduce the free radical in flue gas, submits the smoking property of cigarette security to.Tea Flower essence adds in cigarette filter rod, does not participate in burning, does not produce other harmful substance.The cigarette rolled for binary compound filter candle, the harmful components in the adsorbable flue gas of active carbon wherein, improve the smoking property of cigarette security.
The specific embodiment
Below in conjunction with embodiment, embodiment of the present invention are described in detail, but it will be understood to those of skill in the art that the following example is only for the present invention is described, and should not be considered as limiting scope of the present invention.Unreceipted actual conditions person in embodiment, carry out according to the condition of normal condition or manufacturer's suggestion.The unreceipted person of production firm of agents useful for same or instrument, being can be by the conventional products of commercial acquisition.
preparation example 1: the preparation of essential oil of the flower of Camellia sinensis
1. experiment material
Tea Flower picks up from the Tie Guanyin tea plant in Anxi, Fujian.
2. the preparation of essential oil of the flower of Camellia sinensis
Step is as follows:
(1) take the certain quantity of fresh Tea Flower and pack in the decompression extraction element, add the boiling water of 10 times of Tea Flower weight, sealing is cooled to 30 ℃ after soaking 5min;
(2) carry out the reduced steam distillation on the decompressor of being furnished with the trapping cold-trap, temperature is: 30 ℃, vacuum is: 1kpa, collect distillate;
(3) boiling water that 5 times of Tea Flower weight are added in decompression distillation after complete is collected liquid to repeating twice rear merging of decompression distillation according to step (3) in extraction element;
(4) add 0.3 times and collect the long-pending absolute ether back extraction of liquid three times, merge stripping workshop and be concentrated into 1/10 of fresh Tea Flower weight;
(5) essential oil of the flower of Camellia sinensis is refining: the absolute ethyl alcohol that adds 3 times of the middle concentrates of step (4) carries out backwash, and reduced pressure concentration is removed wherein and obtained essential oil of the flower of Camellia sinensis after residual absolute ether.
preparation example 2: the preparation of Tea Flower tincture
1. experiment material
Tea Flower picks up from the Tie Guanyin tea plant in Anxi, Fujian.
2. the preparation of Tea Flower tincture
Step is as follows:
(1) described Tea Flower includes but not limited to fresh Tea Flower, dried flower, alcohol immersion processing Tea Flower, spray Ethanol Treatment Tea Flower etc.;
(2) super-pressure extracts: take the certain quantity of fresh Tea Flower and put into the super-pressure extractor, add the edible alcohol that 7 times of concentration to Tea Flower weight are 20%, carry out release immediately after the super-pressure extraction; The pressure of described super-pressure is: 150MPa, dwell time: 30min;
(3) the 1/5-1/10 that the extract in step (2) is carried out after suction filtration being concentrated into original volume obtains the Tea Flower tincture.
preparation example 3: the preparation of Tea Flower tincture and Tea Flower medicinal extract
1. experiment material
Tea Flower picks up from the high-quality green tea tea tree of District, Xinyang Area, Henan Province.
2. the preparation of Tea Flower medicinal extract
Step is as follows:
(1) described Tea Flower includes but not limited to fresh Tea Flower, dried flower, alcohol immersion processing Tea Flower, spray Ethanol Treatment Tea Flower etc.;
(2) super-pressure extracts: take the certain quantity of fresh Tea Flower and put into the super-pressure extractor, 4 times of concentration to Tea Flower weight are 40% edible alcohol, carry out release immediately after the super-pressure extraction; The pressure of described super-pressure is: 500MPa, dwell time: 10min;
(3) the 1/5-1/10 that the extract in step (2) is carried out after suction filtration being concentrated into original volume obtains the Tea Flower tincture;
(4) prepare Tea Flower medicinal extract: the Tea Flower tincture continuation obtained in step (3) is concentrated and can obtain Tea Flower medicinal extract.
preparation example 4: the preparation of Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil
1. experiment material
Tea Flower picks up from the Wuyi cliff tea tea tree of Wuyi Mountain, fujian.
2. the preparation of Tea Flower absolute oil
Step is as follows:
(1) described Tea Flower includes but not limited to fresh Tea Flower, dried flower, alcohol immersion processing Tea Flower, spray Ethanol Treatment Tea Flower etc.;
(2) super-pressure extracts: take the certain quantity of fresh Tea Flower and put into the super-pressure extractor, 5 times of concentration to Tea Flower weight are 70% edible alcohol, carry out release immediately after the super-pressure extraction; The pressure of described super-pressure is: 300MPa, dwell time: 20min;
(3) the 1/5-1/10 that the extract in step (2) is carried out after suction filtration being concentrated into original volume obtains the Tea Flower tincture;
(4) prepare Tea Flower medicinal extract: the Tea Flower tincture continuation obtained in step (3) is concentrated and can obtain Tea Flower medicinal extract;
(5) prepare the Tea Flower absolute oil: with a certain amount of 95% ethanol back dissolving Tea Flower medicinal extract, for example, after freezing (-10 ℃ to-20 ℃) 24-48h, filter, concentrated, obtain the Tea Flower absolute oil.
The Tea Flower extract that preparation example 1-4 makes is for the following examples.
embodiment 1: the preparation of the cigarette paper of Tea Flower odor type and 1# cigarette
1. get the essential oil of the flower of Camellia sinensis (preparation example 1 preparation) of 15 parts by weight, the Tea Flower tincture of 85 parts by weight (preparation example 3 preparations) mixes as the Tea Flower extract, be dissolved in 70% ethanol and be configured to the solution that mass concentration is 8%, obtain Tea Flower essence;
2. in the ratio of Tea Flower essence and the 100 weight portion cigarette paper of 5 weight portions, at quantitative spraying device, evenly be sprayed on cigarette paper, then through the low temperature cylinder dried, volatilize fully to alcohol, then cut into the cigarette paper of Tea Flower odor type.The Tea Flower extract that in this cigarette paper, every 100 weight portions contain 0.4 weight portion;
3. with the above-mentioned cigarette paper that adds Tea Flower essence, by existing cigarette job contract skill parameter, roll and obtain the 1# cigarette.
With the cigarette that contrasts that the cigarette paper of 70% ethanol that only adds identical weight part makes, compare, the cigarette rolled with the cigarette paper that is coated with Tea Flower essence, during cigarette smoking, Tea Flower essence in cigarette paper is transferred in flue gas through burning, make flue gas there is Tea Flower feature note, with this fragrant harmony of cigarette tobacco, the jealous style of the perfume (or spice) of cigarette is improved, and fragrance is coordinated, and pleasant impression is comfortable, the flue gas exquisiteness, soft, effectively reduce the pungent stimulation of flue gas, the xerostomia sense, and do not change original processing technology and equipment in cigarette paper production, simple.
embodiment 2: the preparation of the cork paper of Tea Flower odor type and 2# cigarette
1. the Tea Flower absolute oil (prepared by preparation example 4) of getting the Tea Flower tincture (preparation example 3 preparation) of 70 parts by weight, the Tea Flower medicinal extract of 5 parts by weight (preparation example 4 preparations) and 25 parts by weight mixes and prepares the Tea Flower extract;
2. according to the ratio of Tea Flower extract and the 100 weight portion yew paper paper of 0.03 weight portion, the general printing ink of Tea Flower extract and cork paper is mixed, after being uniformly mixed, be printed onto on cork paper in cork paper typography process.
3. with the above-mentioned cork paper that adds the Tea Flower extract, by existing cigarette job contract skill parameter, roll and obtain the 2# cigarette.
With the cigarette that contrasts made without the interpolation cork paper, compare, with the cigarette tipping paper tipping cigarette that is added with Tea Flower essence, can make the perfume (or spice) of smelling of cigarette there is Tea Flower feature note, during suction, flue gas is taken the Tea Flower fragrance matter out of through filter stick, effectively covers assorted gas, with the fragrant harmony of cigarette, the flue gas exquisiteness, soft, mouthfeel is fresh and sweet, and the xerostomia sense obviously alleviates.
embodiment 3: the preparation of the binary compound filter candle of Tea Flower odor type and 3# cigarette
1. get the essential oil of the flower of Camellia sinensis (preparation example 1 preparation) of 15 parts by weight, the Tea Flower tincture of 85 parts by weight (preparation example 3 preparations) mixes, be deployed into 60% ethanol the Tea Flower essence that concentration is 4%, by 10% of active carbon weight, load on active carbon and make modified activated carbon;
2. the modified activated carbon made is loaded on the diacetate fiber tow and makes the modified active carbon rod by existing process conditions, wherein modified activated carbon particle consumption is the 0.8mg/mm filter stick;
3. the active carbon filter stick that makes and cellulose acetate filter rod being made to the alternate round clava in conjunction with forming by the outer wrapping layer is binary compound filter candle of the present invention;
4. the cigarette binary compound filter candle made with the present embodiment, roll and obtain the 3# cigarette by existing technique.
The cigarette that contrasts made with the filter stick that only adds unmodified active carbon is compared, during suction 3# cigarette, flue gas can make the Tea Flower extract volatilization of load in active carbon enter cigarette smoke through filter stick, make cigarette smoke there is the characteristic perfume of Tea Flower, with this fragrant harmony of tobacco, the pure and fresh gracefulness of flue gas, improve flavor quality of cigarette, improve the cigarette mouthfeel.Simultaneously, the harmful components in the adsorbable flue gas of active carbon, improve the smoking property of cigarette security.
embodiment 4: the preparation of the binary compound filter candle of Tea Flower odor type and 4# cigarette
1. getting the Tea Flower tincture (preparation example 2 preparations) of 45 parts by weight, the Tea Flower medicinal extract (preparation example 3 preparations) of 30 parts by weight and the Tea Flower absolute oil (preparation example 4 preparations) of 25 parts by weight mixes, be deployed into 60% ethanol the Tea Flower essence that concentration is 5% again, by 8% of active carbon weight, load on active carbon and make modified activated carbon;
2. the modified activated carbon made is loaded on the diacetate fiber tow and makes the modified active carbon rod by existing process conditions, wherein modified activated carbon particle consumption is the 2.0mg/mm filter stick;
3. the active carbon filter stick that makes and cellulose acetate filter rod being made to the alternate round clava in conjunction with forming by the outer wrapping layer is binary compound filter candle of the present invention;
4. the binary compound filter candle made with the present embodiment, roll and obtain the 4# cigarette by existing technique.
The cigarette that contrasts made with the filter stick that only adds unmodified active carbon is compared, during suction 4# cigarette, flue gas can make the Tea Flower extract volatilization of load in active carbon enter cigarette smoke through filter stick, make cigarette smoke there is the characteristic perfume of Tea Flower, with this fragrant harmony of tobacco, the pure and fresh gracefulness of flue gas, improve the cigarette mouthfeel, and mouthfeel is fresh and sweet, reduce the flue gas drying excitement, improve flavor quality of cigarette.Simultaneously, the harmful components in the adsorbable flue gas of active carbon, improve the smoking property of cigarette security.
embodiment 5: the preparation of the binary compound filter candle of Tea Flower odor type and 5# cigarette
1. getting the Tea Flower tincture (preparation example 4 preparations) of 65 parts by weight and the Tea Flower medicinal extract (preparation example 3 preparations) of 35 parts by weight mixes, ethanol with 80% is deployed into the Tea Flower essence that concentration is 2%, by 25% of active carbon weight, loads on active carbon and makes modified activated carbon;
2. the modified activated carbon made is loaded on the diacetate fiber tow and makes the modified active carbon rod by existing process conditions, wherein modified activated carbon particle consumption is the 3.5mg/mm filter stick;
3. the active carbon filter stick that makes and cellulose acetate filter rod being made to the alternate round clava in conjunction with forming by the outer wrapping layer is binary compound filter candle of the present invention;
4. the binary compound filter candle made with the present embodiment, roll and obtain the 5# cigarette by existing technique.
The cigarette that contrasts made with the filter stick that only adds unmodified active carbon is compared, during suction 5# cigarette, flue gas can make the Tea Flower extract volatilization of load in active carbon enter cigarette smoke through filter stick, make cigarette smoke there is the characteristic perfume of Tea Flower, with this fragrant harmony of tobacco, the pure and fresh gracefulness of flue gas, improve flavor quality of cigarette, improve the cigarette mouthfeel.Simultaneously, the harmful components in the adsorbable flue gas of active carbon, improve the smoking property of cigarette security.
embodiment 6: the heart yearn filter stick of Tea Flower odor type and the preparation of 6# cigarette
1. according to prior art, chitin fiber is made to well-formed's filter stick heart yearn;
2. get the Tea Flower tincture (preparation example 2 preparations) of 45 parts by weight, the Tea Flower medicinal extract (preparation example 3 preparations) of 25 parts by weight and the Tea Flower absolute oil (preparation example 4 preparations) of 30 parts by weight and mix, be prepared into the Tea Flower extract;
2. press 3 parts of Tea Flower extracts, 0.3 part of water soluble chitosan, all the other make Tea Flower essence (gross weight is 100 parts of meters) for water or ethanol.
3. Tea Flower essence is passed through to sponge roller, make it evenly to spread upon on the filter stick heart yearn, Tea Flower essence consumption is 20% of filter stick heart yearn weight;
4. above-mentioned filter stick heart yearn is placed under normal temperature to dry 3h in the hothouse that humidity is 28%;
5. by the outer core of acetate fiber and 3. gained filter stick heart yearn while moulding of step, make the cigarette filter rod that the heart yearn that contains Tea Flower essence combines with cellulose acetate filter rod.
6. the heart yearn filter stick made with the present embodiment, roll and obtain the 6# cigarette by existing technique.
The cigarette rolled with the heart yearn filter stick that contains Tea Flower essence is compared with the heart yearn filter stick that does not add Tea Flower essence, during suction, flue gas impels the Tea Flower essence volatilization in heart yearn, enter cigarette smoke, make flue gas pure and fresh simple and elegant, have the Tea Flower characteristic perfume with this fragrant harmony of tobacco, mouthfeel is fresh and sweet, the drying that can reduce flue gas simultaneously stimulates, the comfort while improving cigarette smoking.Tea Flower essence adds in cigarette filter rod, does not participate in burning, does not produce other harmful substance.
Although the specific embodiment of the present invention has obtained detailed description, it will be understood to those of skill in the art that.According to disclosed all instructions, can carry out various modifications and replacement to those details, these change all within protection scope of the present invention.Four corner of the present invention is provided by claims and any equivalent thereof.
Claims (12)
1. the auxiliary material that grows tobacco, it contains the Tea Flower extract.
2. tobacco auxiliary material according to claim 1, wherein, the 0.01%-5% that the content of described Tea Flower extract or consumption are tobacco auxiliary material weight; Preferably, be 0.01%-1%; More preferably, be 0.1%-1%.
3. tobacco auxiliary material according to claim 2, wherein, described tobacco auxiliary material for be selected from for example, in cigarette paper, tipping paper and filter stick (heart yearn filter stick or binary compound filter candle) any or multiple.
4. tobacco auxiliary material according to claim 1, wherein, described Tea Flower extract be selected from essential oil of the flower of Camellia sinensis, Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil any one, two kinds, three kinds or four kinds.
5. tobacco auxiliary material according to claim 4, wherein, the mixture that described Tea Flower extract is Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil; Preferably, Tea Flower tincture 45%-70%, Tea Flower medicinal extract 5%-30%, Tea Flower absolute oil 25%-30%.
6. tobacco auxiliary material according to claim 4, wherein, described essential oil of the flower of Camellia sinensis makes as follows:
(1) take a certain amount of Tea Flower pack into be furnished with the trapping cold-trap the decompression extraction element in;
(2) add the water of at least 5 times of Tea Flower weight, and the temperature of the water added is more than 80 ℃, at least 5min is soaked in sealing, is cooled to 30-70 ℃;
(3-1) carry out the reduced steam distillation, temperature used is identical with cooled temperature in step (2), and vacuum is 1-17kpa, collects distillate;
Preferably, also comprise step (3-2): repeating step (2) and (3-1) in operation 1 time or repeatedly, and merge distillate;
(4) in the use, low polar organic solvent carries out 1 time or repeatedly back extraction the distillate obtained in step (3-1) or step (3-2), obtains stripping workshop; Stripping workshop is concentrated, obtained concentrate;
(5) use concentrate weight 2-4 absolute ethyl alcohol doubly to carry out backwash to the concentrate obtained in step (4), reduced pressure concentration remove wherein residual in after low polar organic solvent essential oil of the flower of Camellia sinensis.
7. tobacco auxiliary material according to claim 6, wherein, step (2) meets following any one in 1.-4. or multinomial:
The 5-50 that the amount of the water 1. added is Tea Flower weight doubly, is preferably 5-40 doubly or 8-40 times, and more preferably 10-30 doubly;
The temperature of the water 2. added is preferably more than 85 ℃, more preferably, more than 90 ℃, more preferably, more than 95 ℃, is particularly preferably boiling water;
3. the time that sealing is soaked is 5min-4h, is preferably 5min-4h, 5min-3h or 5min-2h, and more preferably 5-60min, 5-50min or 5-40min, be particularly preferably 5-30min;
4. be cooled to 30-70 ℃; For example 30-40 ℃, 45-55 ℃ or 60-70 ℃.
8. tobacco auxiliary material according to claim 6, wherein, in step (4), described in low polar organic solvent be to be selected from any one in absolute ether and ethyl acetate.
9. tobacco auxiliary material according to claim 4, wherein, described Tea Flower tincture, Tea Flower medicinal extract or Tea Flower absolute oil, respectively as follows 1), step 1)-2) or step 1)-3) make:
1) super-pressure extracts: take a certain amount of Tea Flower and put into the super-pressure extractor, the edible alcohol that adds at least 2 times of (w/w) Tea Flower weight, carry out the super-pressure extraction, obtain Tea Flower tincture 1, the concentration of wherein said edible alcohol is the 20-70%(mass concentration); Preferably, the 1/5-1/10 that Tea Flower tincture 1 is concentrated into to original volume obtains Tea Flower tincture 2;
2) prepare Tea Flower medicinal extract: the Tea Flower tincture 1 or the Tea Flower tincture 2 that obtain in step 1) are further concentrated, obtain Tea Flower medicinal extract;
3) prepare the Tea Flower absolute oil: by a certain amount of 95% ethanol back dissolving step 2) the Tea Flower medicinal extract that obtains, then carry out freezing processing, cooling time is that 16-48h(is preferably 20-36h), then filter, concentrated, obtain the Tea Flower absolute oil.
10. tobacco auxiliary material according to claim 9, wherein, step 1) meets following any one in 1.-6. or multinomial:
1. described is that adopted Tea Flower is Tea Flower fresh flower, dried flower, spray Ethanol Treatment Tea Flower, alcohol immersion Tea Flower;
2. release immediately after the super-pressure extraction;
3. add the doubly edible alcohol of (w/w) Tea Flower weight of 2-15 at least, be preferably 2-10 doubly, 2-8 doubly, 3-8 doubly (w/w), more preferably 4-7 doubly (w/w);
④150－500Mpa；
5. the dwell time is 5-120min, is preferably 5-60min, more preferably 10-30min.
6. the concentration of edible alcohol used is the 40-70%(mass concentration).
11. in claim 1 to 10, the described tobacco auxiliary material of any one is preparing for example purposes in cigarette of tobacco product.
12. a tobacco articles, it contains the described tobacco auxiliary material of any one in one or more claims 1 to 10; Particularly, described tobacco product is cigarette.
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