CN103478503A - Special nano slow-release fish guano for silver carps and preparation method thereof - Google Patents
Special nano slow-release fish guano for silver carps and preparation method thereof Download PDFInfo
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- 241000251468 Actinopterygii Species 0.000 title claims abstract description 40
- 241000252234 Hypophthalmichthys nobilis Species 0.000 title claims abstract description 26
- 239000002515 guano Substances 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- 241000894006 Bacteria Species 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims abstract description 11
- 239000002699 waste material Substances 0.000 claims abstract description 11
- 239000002131 composite material Substances 0.000 claims abstract description 10
- 241000190950 Rhodopseudomonas palustris Species 0.000 claims abstract description 9
- 241000194032 Enterococcus faecalis Species 0.000 claims abstract description 8
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims abstract description 8
- 241000223259 Trichoderma Species 0.000 claims abstract description 8
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 7
- 230000000813 microbial effect Effects 0.000 claims abstract description 7
- 235000009566 rice Nutrition 0.000 claims abstract description 7
- 239000000052 vinegar Substances 0.000 claims abstract description 7
- 235000021419 vinegar Nutrition 0.000 claims abstract description 7
- 240000007594 Oryza sativa Species 0.000 claims abstract 3
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical class CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 24
- 239000000203 mixture Substances 0.000 claims description 21
- 238000013270 controlled release Methods 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 18
- 238000000855 fermentation Methods 0.000 claims description 15
- 230000004151 fermentation Effects 0.000 claims description 15
- 239000013049 sediment Substances 0.000 claims description 10
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 8
- 241000235342 Saccharomycetes Species 0.000 claims description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 7
- 210000003608 fece Anatomy 0.000 claims description 7
- 239000010871 livestock manure Substances 0.000 claims description 7
- 239000001301 oxygen Substances 0.000 claims description 7
- 229910052760 oxygen Inorganic materials 0.000 claims description 7
- 235000015277 pork Nutrition 0.000 claims description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 235000008694 Humulus lupulus Nutrition 0.000 claims description 6
- 241001263603 Stellera Species 0.000 claims description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 6
- 244000067645 Wedelia chinensis Species 0.000 claims description 6
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 claims description 6
- 229910000020 calcium bicarbonate Inorganic materials 0.000 claims description 6
- 239000004202 carbamide Substances 0.000 claims description 6
- 235000013339 cereals Nutrition 0.000 claims description 6
- -1 concave convex rod Chemical compound 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 239000000428 dust Substances 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 6
- 238000001291 vacuum drying Methods 0.000 claims description 6
- 229910052588 hydroxylapatite Inorganic materials 0.000 claims description 5
- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 claims description 5
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 claims description 4
- 239000004472 Lysine Substances 0.000 claims description 4
- 150000001413 amino acids Chemical class 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 4
- 239000005995 Aluminium silicate Substances 0.000 claims description 3
- 229910021532 Calcite Inorganic materials 0.000 claims description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 3
- 235000012211 aluminium silicate Nutrition 0.000 claims description 3
- 238000009264 composting Methods 0.000 claims description 3
- GDVKFRBCXAPAQJ-UHFFFAOYSA-A dialuminum;hexamagnesium;carbonate;hexadecahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Al+3].[Al+3].[O-]C([O-])=O GDVKFRBCXAPAQJ-UHFFFAOYSA-A 0.000 claims description 3
- 229960001760 dimethyl sulfoxide Drugs 0.000 claims description 3
- 238000004821 distillation Methods 0.000 claims description 3
- 239000012153 distilled water Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 229910001701 hydrotalcite Inorganic materials 0.000 claims description 3
- 229960001545 hydrotalcite Drugs 0.000 claims description 3
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 3
- 230000014759 maintenance of location Effects 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical class [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 claims description 3
- 235000011056 potassium acetate Nutrition 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 239000004408 titanium dioxide Substances 0.000 claims description 3
- 230000012010 growth Effects 0.000 abstract description 9
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 6
- 201000010099 disease Diseases 0.000 abstract description 5
- 230000009286 beneficial effect Effects 0.000 abstract description 4
- 244000005700 microbiome Species 0.000 abstract description 4
- 230000003247 decreasing effect Effects 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 239000003337 fertilizer Substances 0.000 description 15
- 230000008901 benefit Effects 0.000 description 6
- 239000003814 drug Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 241000209094 Oryza Species 0.000 description 4
- 238000009395 breeding Methods 0.000 description 4
- 230000001488 breeding effect Effects 0.000 description 4
- 241000252233 Cyprinus carpio Species 0.000 description 3
- 229940079593 drug Drugs 0.000 description 3
- 208000010824 fish disease Diseases 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 244000037640 animal pathogen Species 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 210000001035 gastrointestinal tract Anatomy 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- JMANVNJQNLATNU-UHFFFAOYSA-N oxalonitrile Chemical compound N#CC#N JMANVNJQNLATNU-UHFFFAOYSA-N 0.000 description 2
- 210000002784 stomach Anatomy 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 208000035143 Bacterial infection Diseases 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 208000025309 Hair disease Diseases 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 208000022362 bacterial infectious disease Diseases 0.000 description 1
- 230000033558 biomineral tissue development Effects 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 208000034653 disorder of pilosebaceous unit Diseases 0.000 description 1
- 230000037336 dry skin Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000000366 juvenile effect Effects 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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- Fodder In General (AREA)
- Fertilizers (AREA)
- Feed For Specific Animals (AREA)
Abstract
The invention discloses a special nano slow-release fish guano for silver carps and a preparation method thereof. The special composite microbial fish guano for silver carps comprises the following components in parts by weight: 0.5-0.8 part of silicate bacterium, 1-3 parts of Streptococcus faecalis, 0.6-0.8 part of Trichoderma, 2-5 parts of Rhodopseudomonas palustris, 0.3-0.5 part of microzyme, 50-60 parts of fishbone powder, 65-70 parts of vinegar residue powder, 50-55 parts of waste liquid precipitate, 40-60 parts of rice bran and the like. According to the invention, the fish guano can promote the quick growth of silver carps, increase the EPA content of the fish bodies, reduce the diseases of the fishes and ensure that sick and dead fishes are decreased; and meanwhile, beneficial microorganisms in the water body can be increased, thus finally ensuring that the quality and mass of the silver carps are improved.
Description
Technical field
The present invention relates to a kind of microbial manure, particularly relate to a kind of complex microorganism fish guano, be specifically related to a kind of silver carp special-purpose nanometer slowly-releasing fish guano and preparation method thereof.
Background technology
Silver carp can provide abundant colloid albumen, can body-building, can improve looks again, and be the ultimate food that the women nourishes skin; It is all effective in cure to pachylosis, furfur, the hair disease such as simply easily come off, and is women's very important delicacies of improving looks; Health-preserving food for tonifying Qi in temperature, warm stomach, damp skin, be applicable to deficiency-cold in spleen and stomach physique, semiliquid stool, dry skin person, also can be used for the symptoms such as breast due to deficiency of spleen-QI and stomach-QI is few, is one of fish of liking very much of people.
Need to throw in feed in the breeding process of silver carp and grow for it, but long-term input feed can grow some harmful bacterias in fishpond and fish pond, these harmful bacterias not only can affect water body environment, also are unfavorable for the growth of silver carp.Especially easily the bacterial infection disease is as cause of disease branchiomycosis, stigmatosis, doctylogyrosis, myxoboliosis in breeding process for silver carp, and these diseases have a strong impact on the quality and yield of silver carp.The control of these diseases generally be take drug-treated as main, but long-term medication can make the fish body develop immunity to drugs, and some medicament can accumulate in the fish body, unfavorable to human body.
In the breeding process of carp, at present a lot of plants adopt fertilizer, by the picture pond, throwing in a certain amount of fertilizer, improve the output of carp; Traditional fertilizer has its advantage, but the shortcoming function singleness is longer by the process that phytoplankton utilized, and consumes a large amount of oxygen in water body in mineralization process, this in water to put product in a suitable place to breed as unfavorable as growths such as fish.
Except the fertilizer and inorganic fertilizer of simple function, from last century the eighties also start to promote " rational application of fertilizers ", i.e. " composite organic-inorganic fertilizer ", although composite fertilizer has absorbed the advantage of single fertilizer and inorganic fertilizer two aspects, their shortcoming is not fine to be overcome.Existing single type fish guano and compound fish guano also have a common shortcoming, and that can not be killed harmful bacteria exactly, therefore, lack the effectively effect of control of fish disease.Can increase the content of beneficial bacterium in fishpond by the compound fish guano of microorganism, effectively reduce the generation of fish diseases, at present about special-purpose nanometer slowly-releasing fish guano of being exclusively used in silver carp and preparation method thereof report not also.
Summary of the invention
The technical problem that the present invention mainly solves is to provide a kind of silver carp specific complex microbial fish guano and preparation method thereof, comprehensive nutrition is provided can on the one hand the growth of silver carp, can improve on the other hand the useful content in pond, suppress the breeding growth of pathogen in water body, reduce the generation of disease, improve the yield and quality of fertilizer efficiency, carp.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is:
A kind of silver carp nano controlled-release fish guano, is characterized in that, its raw material comprises the composition of following weight ratio:
Silicate bacteria 0.5-0.8 part, streptococcus fecalis 1-3 part, Trichoderma 0.6-0.8 part, Rhodopseudomonas palustris 2-5 part, saccharomycete 0.3-0.5 part, fishbone dust 50-60 part, vinegar grain powder 65-70 part, waste liquid sediment 50-55 part, rice bran 40-60 part, brown sugar 12-14 part, salt 10-14 part, pig manure 80-85 part, pork slaughterhouse discarded object 45-55 part, pasture and water 60-65 part, calcium bicarbonate 12-16 part, urea 14-17 part, ironic citrate 1-3 part, Cobastab
10.6-0.8 part, Cobastab
120.2-0.6 part, Chinese Stellera Root 1-1.5 part, hops 0.5-1.0 part, South America wedelia chinensis 1.0-2.0 part, nano controlled-release carrier 20-25 part;
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, dry 24 hours of 60 ℃ of temperature, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition.Filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at the 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain the nano controlled-release carrier complexes.
Described a kind of silver carp specific complex microbial fish guano, described waste liquid sediment derives from the amino acid whose production processes such as Gourmet Powder Factory, lysine factory.
The preparation method of described fish guano comprises the following steps:
(1) pasture and water are dried, make its water content below 40%, it is cut to 2-4cm, then according to described ratio, add fishbone dust, vinegar grain powder, rice bran, brown sugar, salt, fully stir, mix;
(2) said mixture is fermented, described fermentation is aerobic composting fermentation, and the fermentation water accounts for the 20-30% of material gross weight, and be 50-60 hour winter oxygen supply time, and be 20-25 hour summer, and fermentation temperature is 45-60 ℃, and fermentation time is 7-10 days;
(3) waste liquid sediment, pig manure, pork slaughterhouse discarded object are mixed according to described ratio, add saccharomycete, streptococcus fecalis to be fermented; Above-mentioned substance is inserted to mixing corruption in pond and macerate, plastic sheeting on upper cap, carry out fermenting in advance in 3-5 days; Then plastic sheeting is thrown off, and stirred, allow mixture contact oxygen, temperature gradually raises, from normal temperature to 50 ℃, keep continuing turning after 1-3 days, then be raised to 60 ℃ from 50 ℃, the retention time is 2-4 days, then cool the temperature to normal temperature, keep 6-8 days, until slaking is fully fermented complete;
(4) organic mixture after step (1) and step (2) are fermented, sterilized is carried out to drying, baking temperature is 45-60 ℃, and being dried to water content is 15-25%;
(5) silicate bacteria, Trichoderma, Rhodopseudomonas palustris are joined in above-mentioned material according to described ratio, fully mix, stir;
(6) by calcium bicarbonate, urea, ironic citrate, Cobastab
1, Cobastab
12, Chinese Stellera Root, hops, South America wedelia chinensis, nano controlled-release carrier join in mixture according to described ratio, fully mixes, stir;
(7) above-mentioned material is carried out under the condition of 18-45 ℃ to low temperature drying, making its water content is below 10%.
The invention has the beneficial effects as follows:
(1) Rhodopseudomonas palustris added is nutritious, protein content is up to 65%, and be rich in various bioactivators, and there is strong adaptability, can tolerate the organic wastewater of high concentration and stronger decomposition and inversion ability, the poisonous substances such as phenol, cyanogen are also had to the characteristics such as certain tolerance and capacity of decomposition, can purify water, dispose of sewage, be conducive to the growth of fish.The various mushrooms such as the silicate bacteria added, Trichoderma, Rhodopseudomonas palustris, streptococcus fecalis, saccharomycete can continue to expand in water body numerous, the balance that maintains microorganisms in water is had a very important role, and can regulate and adjust microecological balance in fish body enteron aisle, the Harmful Residue in can also decomposer, strengthen the fingerling premunition;
(2) take full advantage of the waste liquid sediment that the amino acid whose production process such as pasture and water, pork slaughterhouse discarded object, Gourmet Powder Factory and lysine factory produces, can improve the utilization rate of refuse, the silver carp needed nutriment of growing can also be provided, increase the protein content of fish body.And added organic feed, inorganic mineral, trace element, comprehensive nutrition is provided can to the growth of fish;
(3) utilize hydroxyapatite etc. itself to there is the character of loose structure, fertilizer components is adsorbed in the inner mesh of carrier, reach the purpose of slow release.Hydroxyapatite also has biodegradable characteristic, and the gained catabolite is the various trace elements ion, and these elements can be absorbed again.The nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, each component that makes it load has controlled-release function, through twice-modified nano-complex medicine carrying amount and adsorbance, all improve a lot, the fertilizer efficiency time lengthening is more than 3 months, effectively suppress the increment of animal pathogen, improve the producer's benefit.
The specific embodiment
Below preferred embodiment of the present invention is described in detail, thereby so that advantages and features of the invention can be easier to be it will be appreciated by those skilled in the art that, protection scope of the present invention is made to more explicit defining.
embodiment 1
A kind of silver carp nano controlled-release fish guano, is characterized in that, its raw material comprises the composition of following weight ratio:
Silicate bacteria 0.5-0.8 part, streptococcus fecalis 1-3 part, Trichoderma 0.6-0.8 part, Rhodopseudomonas palustris 2-5 part, saccharomycete 0.3-0.5 part, fishbone dust 50-60 part, vinegar grain powder 65-70 part, waste liquid sediment 50-55 part, rice bran 40-60 part, brown sugar 12-14 part, salt 10-14 part, pig manure 80-85 part, pork slaughterhouse discarded object 45-55 part, pasture and water 60-65 part, calcium bicarbonate 12-16 part, urea 14-17 part, ironic citrate 1-3 part, Cobastab
10.6-0.8 part, Cobastab
120.2-0.6 part, Chinese Stellera Root 1-1.5 part, hops 0.5-1.0 part, South America wedelia chinensis 1.0-2.0 part, nano controlled-release carrier 20-25 part;
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, dry 24 hours of 60 ℃ of temperature, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition.Filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at the 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain the nano controlled-release carrier complexes.
Described a kind of silver carp specific complex microbial fish guano, described waste liquid sediment derives from the amino acid whose production processes such as Gourmet Powder Factory, lysine factory.
The preparation method of described fish guano comprises the following steps:
(1) pasture and water are dried, make its water content below 40%, it is cut to 2-4cm, then according to described ratio, add fishbone dust, vinegar grain powder, rice bran, brown sugar, salt, fully stir, mix;
(2) said mixture is fermented, described fermentation is aerobic composting fermentation, and the fermentation water accounts for the 20-30% of material gross weight, and be 50-60 hour winter oxygen supply time, and be 20-25 hour summer, and fermentation temperature is 45-60 ℃, and fermentation time is 7-10 days;
(3) waste liquid sediment, pig manure, pork slaughterhouse discarded object are mixed according to described ratio, add saccharomycete, streptococcus fecalis to be fermented; Above-mentioned substance is inserted to mixing corruption in pond and macerate, plastic sheeting on upper cap, carry out fermenting in advance in 3-5 days; Then plastic sheeting is thrown off, and stirred, allow mixture contact oxygen, temperature gradually raises, from normal temperature to 50 ℃, keep continuing turning after 1-3 days, then be raised to 60 ℃ from 50 ℃, the retention time is 2-4 days, then cool the temperature to normal temperature, keep 6-8 days, until slaking is fully fermented complete;
(4) organic mixture after step (1) and step (2) are fermented, sterilized is carried out to drying, baking temperature is 45-60 ℃, and being dried to water content is 15-25%;
(5) silicate bacteria, Trichoderma, Rhodopseudomonas palustris are joined in above-mentioned material according to described ratio, fully mix, stir;
(6) by calcium bicarbonate, urea, ironic citrate, Cobastab
1, Cobastab
12, Chinese Stellera Root, hops, South America wedelia chinensis, nano controlled-release carrier join in mixture according to described ratio, fully mixes, stir;
(7) above-mentioned material is carried out under the condition of 18-45 ℃ to low temperature drying, making its water content is below 10%.
Juvenile stage in the silver carp growth, fish is pulled out, divide and support in the middle of five ponds, 300, every pond, microbial fish guano and the common fish guano of in four ponds, according to the injected volume of every mu of 200kg, throwing in respectively embodiment of the present invention 1-3 (contrast 1, originate from Beijing Century AMMS Biotechnology Co., Ltd.), fish guano (contrasting 2) is not thrown in the another one pond, but throw in the common fish food of same amount, remaining feeding amount is identical, culture environment is identical, cultivation through 2-4 month, contrast the upgrowth situation of its output and silver carp, add the Fast Growth that composite microbe fertilizer of the present invention can promote silver carp, fish body EPA content increases, fish disease reduces, the fish that dies of illness reduces, also make the beneficial microbe in water body increase simultaneously, quality and the quality of final silver carp all are improved.The nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, each component that makes it load has controlled-release function, through twice-modified nano-complex medicine carrying amount and adsorbance, all improve a lot, the fertilizer efficiency time lengthening is more than 3 months, effectively suppress the increment of animal pathogen, improve the producer's benefit.
The foregoing is only embodiments of the invention; not thereby limit the scope of the claims of the present invention; every equivalent structure or conversion of equivalent flow process that utilizes description of the present invention to do; or directly or indirectly be used in other relevant technical fields, all in like manner be included in scope of patent protection of the present invention.
Claims (3)
1. a silver carp nano controlled-release fish guano, is characterized in that, its raw material comprises the composition of following weight ratio:
Silicate bacteria 0.5-0.8 part, streptococcus fecalis 1-3 part, Trichoderma 0.6-0.8 part, Rhodopseudomonas palustris 2-5 part, saccharomycete 0.3-0.5 part, fishbone dust 50-60 part, vinegar grain powder 65-70 part, waste liquid sediment 50-55 part, rice bran 40-60 part, brown sugar 12-14 part, salt 10-14 part, pig manure 80-85 part, pork slaughterhouse discarded object 45-55 part, pasture and water 60-65 part, calcium bicarbonate 12-16 part, urea 14-17 part, ironic citrate 1-3 part, Cobastab
10.6-0.8 part, Cobastab
120.2-0.6 part, Chinese Stellera Root 1-1.5 part, hops 0.5-1.0 part, South America wedelia chinensis 1.0-2.0 part, nano controlled-release carrier 20-25 part;
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, dry 24 hours of 60 ℃ of temperature, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition, filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at the 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain the nano controlled-release carrier complexes.
2. a kind of silver carp specific complex microbial fish guano according to claim 1, is characterized in that, described waste liquid sediment derives from the amino acid whose production processes such as Gourmet Powder Factory, lysine factory.
3. the preparation method of fish guano according to claim 1, is characterized in that, comprises the following steps:
(1) pasture and water are dried, make its water content below 40%, it is cut to 2-4cm, then according to described ratio, add fishbone dust, vinegar grain powder, rice bran, brown sugar, salt, fully stir, mix;
(2) said mixture is fermented, described fermentation is aerobic composting fermentation, and the fermentation water accounts for the 20-30% of material gross weight, and be 50-60 hour winter oxygen supply time, and be 20-25 hour summer, and fermentation temperature is 45-60 ℃, and fermentation time is 7-10 days;
(3) waste liquid sediment, pig manure, pork slaughterhouse discarded object are mixed according to described ratio, add saccharomycete, streptococcus fecalis to be fermented; Above-mentioned substance is inserted to mixing corruption in pond and macerate, plastic sheeting on upper cap, carry out fermenting in advance in 3-5 days; Then plastic sheeting is thrown off, and stirred, allow mixture contact oxygen, temperature gradually raises, from normal temperature to 50 ℃, keep continuing turning after 1-3 days, then be raised to 60 ℃ from 50 ℃, the retention time is 2-4 days, then cool the temperature to normal temperature, keep 6-8 days, until slaking is fully fermented complete;
(4) organic mixture after step (1) and step (2) are fermented, sterilized is carried out to drying, baking temperature is 45-60 ℃, and being dried to water content is 15-25%;
(5) silicate bacteria, Trichoderma, Rhodopseudomonas palustris are joined in above-mentioned material according to described ratio, fully mix, stir;
(6) by calcium bicarbonate, urea, ironic citrate, Cobastab
1, Cobastab
12, Chinese Stellera Root, hops, South America wedelia chinensis, nano controlled-release carrier join in mixture according to described ratio, fully mixes, stir;
(7) above-mentioned material is carried out under the condition of 18-45 ℃ to low temperature drying, making its water content is below 10%.
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| CN101011102A (en) * | 2006-10-12 | 2007-08-08 | 玉门拓璞科技开发有限责任公司 | Use of hop slag for preparing animal fodder |
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| CN101011102A (en) * | 2006-10-12 | 2007-08-08 | 玉门拓璞科技开发有限责任公司 | Use of hop slag for preparing animal fodder |
| CN101965927A (en) * | 2010-10-21 | 2011-02-09 | 杭州环特生物科技有限公司 | Hatch feed for zebra fish fry |
| CN103300248A (en) * | 2013-06-17 | 2013-09-18 | 苏州市阳澄湖现代农业发展有限公司 | Compound microbial fish fertilizer special for silver carp and preparation method thereof |
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