CN103300469A - Ginkgo leaf cigarette and preparation method thereof - Google Patents

Ginkgo leaf cigarette and preparation method thereof Download PDF

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Publication number
CN103300469A
CN103300469A CN2013102652289A CN201310265228A CN103300469A CN 103300469 A CN103300469 A CN 103300469A CN 2013102652289 A CN2013102652289 A CN 2013102652289A CN 201310265228 A CN201310265228 A CN 201310265228A CN 103300469 A CN103300469 A CN 103300469A
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China
Prior art keywords
cigarette
ginkgo leaf
ginkgo
preparation
pipe tobacco
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CN2013102652289A
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CN103300469B (en
Inventor
徐莉
蒋国斌
王财富
李国政
雷萌
陈泳
王燕芹
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NANJING JINGUIYUAN AGRICULTURAL DEVELOPMENT Co Ltd
Nanjing Forestry University
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NANJING JINGUIYUAN AGRICULTURAL DEVELOPMENT Co Ltd
Nanjing Forestry University
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Publication of CN103300469A publication Critical patent/CN103300469A/en
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Abstract

The invention discloses a ginkgo leaf cigarette and a preparation method thereof. The ginkgo leaf cigarette is prepared by spraying the conventional tobacco shreds with a ginkgo leaf extract solution. Through sensory quality evaluation on the ginkgo leaf cigarette and detection on main harmful components in smoke gas, a proper adding concentration range of the ginkgo leaf extract is determined; the ginkgo leaf extract is used as a cigarette additive, is formulated into a solution and sprayed onto the tobacco shreds, and the tobacco shreds are rolled into the cigarette, so that the processing technology and the performance of the cigarette are not changed, the harmful components in the smoke gas of the cigarette are reduced, and the safety and the comfort of the cigarette smoking process are improved; a functional component beneficial to a human body is added, so that the Chinese cigarette with certain characteristics is obtained.

Description

A kind of cigarette of ginkgo leaf and preparation method thereof
Technical field
The invention belongs to the natural plant extracts application, relate generally to a kind of cigarette of ginkgo leaf and preparation method thereof.
Background technology
China is the abundant country of resources of medicinal plant in the world, and kind reaches 11146 kinds.There are deep traditional Chinese medical theory and practical basis in China, Chinese medicine because of treat both principal and secondary aspect of disease, toxic and side effect is little that incomparable advantage is being arranged aspect the disease preventing and treating.Follow traditional Chinese medicine theory, in conjunction with modern extraction and separation technology, medicinal plant extract is added in the tobacco as cigarette additive, the Chinese style low harm cigarette with advantage is made in exploitation, reaching the purpose of flavouring humectation, functional health, is important means and the direction that improves the Chinese cigarette competitiveness.
Ginkgo leaf is that Ginkgoaceae plant Ginkgo biloba Ginkgo biloba L.(revises herein) dry leaf, be conventional Chinese medicine, have promoting blood circulation and removing blood stasisly, remove obstruction in channels to relieve pain the effect of astringing the lung and relievining asthma.Modern pharmacological research shows, ginkgo leaf is improving cardiovascular and cerebrovascular and myocardial ischemia, raising memory prevention amnesia, reducing the aspects such as the anti-tampon of blood viscosity, anti-oxidant removing interior free yl and have preferably curative effect.The ginkgo biloba p.e main chemical compositions is flavonol glycosides, terpene lactones, biflavone, OPC, alkyl phenol, dolichol, phenolic acid etc.Ginkgolides can increase cerebrovascular flow, improves cerebrovascular circulatory function, and coronary artery dilator prevents angina pectoris and miocardial infarction, improves body immunity; Ginkgoterpene lactone is the specific receptor antagonist of platelet activating factor; OPC has the peroxy radical of removing and antioxidation.Ginkgo biloba p.e suddenly becomes the most fast-selling autonomic drug in the whole world because stablizing as the diseases of cardiovascular and cerebrovascular systems curative effect of medication.
Have now ginkgo leaf is directly made the report that pipe tobacco prepares cigarette, but with directly roll after the ginkgo leaf chopping or with roll into the ginkgo Leaves health care cigarette after the certain proportions such as pipe tobacco mix, although certain health-care effect is arranged like this, but changed the original jealous of traditional cigarette, after the ginkgo leaf burning generation bitter taste is arranged, mouthfeel is not good, and tobacco hobby person is difficult acceptance; Ginkgo biloba p.e is added cigarette as additive, by control extract addition, make it not produce peculiar smell, keep cigarette original jealous, to a certain degree reduce excitant simultaneously, improve pleasant impression, improve sucking quality.
Smoking and health are one of world today's common problem of showing great attention to.How endanger to alleviate and ensure that publilc health has become noticeable important topic in the world wide by reducing cigarette.Wherein the characteristic of outstanding Chinese-style cigarette reduces the harmful components in the cigarette smoke, improves security and comfortableness in the smoking property of cigarette process, increases the functional components to the human body beneficial, has become the inexorable trend of current countries tobacco industrial development.
Summary of the invention
Technical problem to be solved by this invention, be to provide a kind of cigarette of ginkgo leaf, this cigarette is applied to Field of Tobacco with ginkgo biloba p.e, so that the harmful components in the reduction cigarette smoke, improve security and comfortableness in the smoking property of cigarette process, increase is given prominence to the fragrance characteristic of Chinese-style cigarette simultaneously to human body beneficial's functional components.
The technical problem that the present invention also will solve provides the preparation method of above-mentioned cigarette of ginkgo leaf.
For solving the problems of the technologies described above, the technical solution used in the present invention is as follows:
A kind of cigarette of ginkgo leaf rolls into cigarette behind the sprinkling ginkgo biloba p.e solution in conventional pipe tobacco.
Wherein, described conventional pipe tobacco is the full hall of Bright Yellow gold pipe tobacco.
Wherein, described ginkgo biloba p.e can directly be bought from the market, perhaps is prepared as follows to obtain: get ginkgo leaf, choose decontamination, drying at room temperature was pulverized 20 mesh sieves, extracted with alcohol heating reflux, merge extract, discard precipitation after the sedimentation, behind the supernatant reduced pressure concentration, through large pore resin absorption column absorption, the mixed liquor wash-out of water and ethanol is collected eluent, Recycled ethanol is condensed into thick paste, vacuum drying, be ground into Powderedly, sieve, make finished product.As long as ginkgo biloba p.e satisfies the regulation of Chinese Pharmacopoeia 2010 editions: total flavonoids 〉=24%, terpene lactones 〉=6%, ginkgolic acid≤10ppm gets final product.
Wherein, ginkgo biloba p.e accounts for the 0.025-0.5% of conventional pipe tobacco weight.
The preparation method of above-mentioned cigarette of ginkgo leaf is dissolved ginkgo biloba p.e with ethanol, add in the conventional pipe tobacco in the mode of spraying, and depositing spends the night makes the abundant absorbent solution of pipe tobacco, rolls into cigarette, and balance is 48 hours under the constant temperature and humidity condition, and get final product.
Wherein, described ethanolic solution is replaced with the ethanol water more than 90%.The consumption of ethanol and ethanol water is not strict with, and general warranty can fully dissolve ginkgo biloba p.e, and is easy to spray to be dispersed in the pipe tobacco get final product.
Wherein, described constant temperature is 22 ± 1 ℃.
Wherein, described constant humidity condition is relative humidity 60 ± 2%.
Ginkgo biloba p.e is as the application of additive in the preparation cigarette.
Ginkgo biloba p.e contains multiple functional components to the human body beneficial, has promoting blood circulation and removing blood stasisly, removes obstruction in channels to relieve pain the effect of astringing the lung and relievining asthma.As conventional Chinese medicine, has preferably effect at aspects such as improving cardiovascular and cerebrovascular and myocardial ischemia, raising memory prevention amnesia, the anti-tampon of reduction blood viscosity, removing interior free yl.Therefore, consider described ginkgo biloba p.e is added in the cigarette shreds, although the mechanism that burns and sucks the process effect is still not clear, it can obviously improve the quality of cigarette, reduces excitant and harmful components, improves and sucks comfort level and security.
Beneficial effect: the present invention has following advantage with respect to prior art:
The ginkgo biloba p.e preparation method that the present invention uses is simple and practical, extracts fully, and main pharmacodynamics composition flavonoids, terpene lactones content are higher, and phenolic content is low; The present invention carries out sensory quality assessment to cigarette of ginkgo leaf, and main harmful components in the flue gas are detected, and finds the suitable interpolation concentration range of ginkgo biloba p.e; The present invention is mixed with spray solution with ginkgo biloba p.e on pipe tobacco as cigarette additive, roll into cigarette, do not change Cigarette processing technique and performance, the harmful components in the cigarette smoke have been reduced, security and comfortableness in the smoking property of cigarette process have been improved, increase the functional components to the human body beneficial, formed the Chinese-style cigarette with certain characteristic.
The specific embodiment
According to following embodiment, the present invention may be better understood.Yet, those skilled in the art will readily understand, the described content of embodiment only is used for explanation the present invention, and should also can not limit the present invention described in detail in claims.
Below used ginkgo biloba p.e raw material be all the commercially available ginkgo biloba p.e of buying, available from producing in sky, Xi'an one Bioisystech Co., Ltd, lot number is TYG120413.
Embodiment 1
Take by weighing ginkgo leaf extract powder 1g, add absolute ethyl alcohol 100ml, ultrasonicly make its whole dissolvings, be mixed with the ginkgo biloba p.e solution of 10mg/ml.Measure respectively 0,2.5,5,10,50ml solution, be sprayed at respectively after the dilution on the full hall of the 100g Bright Yellow gold pipe tobacco.Ginkgo biloba p.e quality percentage composition is respectively in the final pipe tobacco: 0,0.025%, 0.05%, 0.1%, 0.5%.
Deposit after the been sprayed and spend the night, make the abundant absorbent solution of pipe tobacco, roll into cigarette, balance is 48 hours under constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) condition, not add ginkgo biloba p.e cigarette (adding the equivalent absolute ethyl alcohol) as contrast, please the expert carry out the aesthetic quality and smoke panel test, and main harmful components tar, nicotine, CO are detected.The 20 duct linear pattern smoking machines that smoking machine adopts Britain CERULEAN company to produce, nicotine, water content detection employing national standard gas chromatography, CO detects the non-scattering infrared method of employing national standard, and tar detects and adopts TPM to deduct nicotine and moisture acquisition.
Smoke panel test through the expert, add the cigarette free from extraneous odour of ginkgo biloba p.e, can increase to some extent fragrance matter and perfume quantity, the assorted gas of minimizing and excitant, raising comfort level, wherein obvious with 0.025%, 0.05% interpolation concentration effect, 0.1% interpolation concentration organoleptic quality remains basically stable with the contrast cigarette, and 0.5% interpolation concentration cigarette aesthetic quality has certain decline.
The results are shown in Table 1.
Table 1 sample Sensory Quality of Cigarette evaluation result
Figure BDA00003416422000041
After testing, the cigarette that adds ginkgo biloba p.e can reduce the content of harmful components tar, nicotine, CO to some extent, along with the increase of adding concentration, the harmful components amount constantly reduces, but changing down presents slowly-fast-slow trend substantially, it is larger to be that the interpolation concentration harmful components changing down of 0.05%-0.1% is compared with 0.025%-0.05%, and the interpolation concentration harmful components changing down of 0.1%-0.5% eases up.
Table 2 sample cigarette is harmful composition detection result mainly
Figure BDA00003416422000042
The results are shown in Table 2.

Claims (9)

1. a cigarette of ginkgo leaf is characterized in that, rolls into cigarette behind the sprinkling ginkgo biloba p.e solution in conventional pipe tobacco.
2. cigarette of ginkgo leaf according to claim 1 is characterized in that, described conventional pipe tobacco is the full hall of Bright Yellow gold pipe tobacco.
3. cigarette of ginkgo leaf according to claim 1 is characterized in that, described ginkgo biloba p.e is prepared as follows and obtains: get ginkgo leaf, choose decontamination, drying at room temperature was pulverized 20 mesh sieves, extracted with alcohol heating reflux, merge extract, discard precipitation after the sedimentation, behind the supernatant reduced pressure concentration, through large pore resin absorption column absorption, the mixed liquor wash-out of water and ethanol is collected eluent, Recycled ethanol is condensed into thick paste, vacuum drying, be ground into Powderedly, sieve, make finished product.
4. cigarette of ginkgo leaf according to claim 1 is characterized in that, ginkgo biloba p.e accounts for the 0.025-0.5% of conventional pipe tobacco weight.
5. the preparation method of the described cigarette of ginkgo leaf of any one in the claim 1~4, it is characterized in that, ginkgo biloba p.e is dissolved with ethanol, add in the conventional pipe tobacco in the mode of spraying, depositing spends the night makes the abundant absorbent solution of pipe tobacco, roll into cigarette, balance is 48 hours under the constant temperature and humidity condition, and get final product.
6. preparation method according to claim 5 is characterized in that, described ethanolic solution is replaced with the ethanol water more than 90%.
7. preparation method according to claim 5 is characterized in that, described constant temperature is 22 ± 1 ℃.
8. preparation method according to claim 5 is characterized in that, described constant humidity condition is relative humidity 60 ± 2%.
9. the application of ginkgo biloba p.e in the preparation cigarette.
CN201310265228.9A 2013-06-27 2013-06-27 A kind of cigarette of ginkgo leaf and preparation method thereof Expired - Fee Related CN103300469B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104087422A (en) * 2014-07-24 2014-10-08 中国烟草总公司郑州烟草研究院 Preparation method and application of hollyhock root/stem water extract
CN104957762A (en) * 2015-06-01 2015-10-07 湖北中烟工业有限责任公司 Suspension type gas fog health care cigarette and preparing method thereof
CN107802025A (en) * 2017-12-06 2018-03-16 湖北中烟工业有限责任公司 A kind of preparation method of ginkgo biloba p.e and its application in cigarette

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CN102031194A (en) * 2009-09-28 2011-04-27 福建中烟工业公司 Ginkgo leaf volatile oil extraction method and method for flavoring cigarettes by utilizing volatile oil
CN102078341A (en) * 2010-12-22 2011-06-01 天津泰阳制药有限公司 High-purity ginkgo flavone and composition thereof
CN102511924A (en) * 2011-10-28 2012-06-27 浙江中烟工业有限责任公司 Plant extractive and preparation method thereof as well as application to cigarettes

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CN1911257A (en) * 2005-08-10 2007-02-14 北京联合伟华药业有限公司 Extractive of ginkgo tree leaves, prepn. method and application thereof
CN102031194A (en) * 2009-09-28 2011-04-27 福建中烟工业公司 Ginkgo leaf volatile oil extraction method and method for flavoring cigarettes by utilizing volatile oil
CN102078341A (en) * 2010-12-22 2011-06-01 天津泰阳制药有限公司 High-purity ginkgo flavone and composition thereof
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104087422A (en) * 2014-07-24 2014-10-08 中国烟草总公司郑州烟草研究院 Preparation method and application of hollyhock root/stem water extract
CN104087422B (en) * 2014-07-24 2016-03-16 中国烟草总公司郑州烟草研究院 A kind of preparation method of hollyhock rhizome Aqueous extracts and application thereof
CN104957762A (en) * 2015-06-01 2015-10-07 湖北中烟工业有限责任公司 Suspension type gas fog health care cigarette and preparing method thereof
CN104957762B (en) * 2015-06-01 2016-04-27 湖北中烟工业有限责任公司 A kind of suspension type aerosol health care cigarette and preparation method thereof
CN107802025A (en) * 2017-12-06 2018-03-16 湖北中烟工业有限责任公司 A kind of preparation method of ginkgo biloba p.e and its application in cigarette
CN107802025B (en) * 2017-12-06 2019-12-24 湖北中烟工业有限责任公司 Preparation method of ginkgo leaf extract and application of ginkgo leaf extract in cigarettes

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