CN103289637A - 一种高粘结性脱醇型硅橡胶的制备方法及其应用 - Google Patents
一种高粘结性脱醇型硅橡胶的制备方法及其应用 Download PDFInfo
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- CN103289637A CN103289637A CN2013101349180A CN201310134918A CN103289637A CN 103289637 A CN103289637 A CN 103289637A CN 2013101349180 A CN2013101349180 A CN 2013101349180A CN 201310134918 A CN201310134918 A CN 201310134918A CN 103289637 A CN103289637 A CN 103289637A
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- Prior art keywords
- dealcoholizing
- preparation
- adhesion
- silicon rubber
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- 229920002379 silicone rubber Polymers 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 239000004945 silicone rubber Substances 0.000 title abstract description 6
- 239000003054 catalyst Substances 0.000 claims description 24
- 239000003921 oil Substances 0.000 claims description 20
- XQSFXFQDJCDXDT-UHFFFAOYSA-N hydroxysilicon Chemical compound [Si]O XQSFXFQDJCDXDT-UHFFFAOYSA-N 0.000 claims description 18
- 239000003795 chemical substances by application Substances 0.000 claims description 15
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 14
- 229920002635 polyurethane Polymers 0.000 claims description 12
- 239000004814 polyurethane Substances 0.000 claims description 12
- 229910052710 silicon Inorganic materials 0.000 claims description 12
- 239000010703 silicon Substances 0.000 claims description 12
- 150000001875 compounds Chemical class 0.000 claims description 10
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 9
- 229920002545 silicone oil Polymers 0.000 claims description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 6
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 6
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- KSBAEPSJVUENNK-UHFFFAOYSA-L tin(ii) 2-ethylhexanoate Chemical compound [Sn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O KSBAEPSJVUENNK-UHFFFAOYSA-L 0.000 claims description 4
- JMXKSZRRTHPKDL-UHFFFAOYSA-N titanium ethoxide Chemical compound [Ti+4].CC[O-].CC[O-].CC[O-].CC[O-] JMXKSZRRTHPKDL-UHFFFAOYSA-N 0.000 claims description 4
- RJMRIDVWCWSWFR-UHFFFAOYSA-N methyl(tripropoxy)silane Chemical compound CCCO[Si](C)(OCCC)OCCC RJMRIDVWCWSWFR-UHFFFAOYSA-N 0.000 claims description 3
- BFXIKLCIZHOAAZ-UHFFFAOYSA-N methyltrimethoxysilane Chemical compound CO[Si](C)(OC)OC BFXIKLCIZHOAAZ-UHFFFAOYSA-N 0.000 claims description 3
- -1 tetramethyl ester Chemical class 0.000 claims description 3
- QUVMSYUGOKEMPX-UHFFFAOYSA-N 2-methylpropan-1-olate;titanium(4+) Chemical compound [Ti+4].CC(C)C[O-].CC(C)C[O-].CC(C)C[O-].CC(C)C[O-] QUVMSYUGOKEMPX-UHFFFAOYSA-N 0.000 claims description 2
- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 claims description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- 239000013522 chelant Substances 0.000 claims description 2
- JZZIHCLFHIXETF-UHFFFAOYSA-N dimethylsilicon Chemical compound C[Si]C JZZIHCLFHIXETF-UHFFFAOYSA-N 0.000 claims description 2
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims description 2
- 239000011863 silicon-based powder Substances 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 claims description 2
- VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 claims description 2
- CPUDPFPXCZDNGI-UHFFFAOYSA-N triethoxy(methyl)silane Chemical compound CCO[Si](C)(OCC)OCC CPUDPFPXCZDNGI-UHFFFAOYSA-N 0.000 claims description 2
- XXZNHVPIQYYRCG-UHFFFAOYSA-N trihydroxy(propoxy)silane Chemical compound CCCO[Si](O)(O)O XXZNHVPIQYYRCG-UHFFFAOYSA-N 0.000 claims description 2
- 238000005303 weighing Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 5
- 239000000565 sealant Substances 0.000 abstract 3
- 230000015556 catabolic process Effects 0.000 abstract 1
- 238000006731 degradation reaction Methods 0.000 abstract 1
- 230000035699 permeability Effects 0.000 abstract 1
- 239000003292 glue Substances 0.000 description 7
- 238000007789 sealing Methods 0.000 description 6
- 239000000443 aerosol Substances 0.000 description 5
- 238000004073 vulcanization Methods 0.000 description 3
- 239000006087 Silane Coupling Agent Substances 0.000 description 2
- 239000004902 Softening Agent Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 239000007822 coupling agent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 238000004381 surface treatment Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 125000005474 octanoate group Chemical group 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 125000003698 tetramethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
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- Compositions Of Macromolecular Compounds (AREA)
- Sealing Material Composition (AREA)
- Non-Portable Lighting Devices Or Systems Thereof (AREA)
Abstract
Description
Claims (9)
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CN201310134918.0A CN103289637B (zh) | 2013-04-18 | 2013-04-18 | 一种高粘结性脱醇型硅橡胶的制备方法及其应用 |
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CN201310134918.0A CN103289637B (zh) | 2013-04-18 | 2013-04-18 | 一种高粘结性脱醇型硅橡胶的制备方法及其应用 |
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CN103289637A true CN103289637A (zh) | 2013-09-11 |
CN103289637B CN103289637B (zh) | 2014-10-15 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107936900A (zh) * | 2017-12-24 | 2018-04-20 | 苏州佳亿达电器有限公司 | 一种用于组装吸尘器的密封胶 |
CN109810669A (zh) * | 2018-12-28 | 2019-05-28 | 广州市高士实业有限公司 | 一种聚硅树脂及其制备方法和应用 |
CN112538333A (zh) * | 2020-12-10 | 2021-03-23 | 江西晨光新材料股份有限公司 | 一种双组分室温硫化硅橡胶及其制备方法和应用 |
CN115505370A (zh) * | 2022-10-28 | 2022-12-23 | 新纳奇材料科技江苏有限公司 | 一种防水透气胶的制备方法及其产品和应用 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101200594A (zh) * | 2006-12-15 | 2008-06-18 | 比亚迪股份有限公司 | 单组分脱醇型室温固化硅橡胶 |
CN101735618A (zh) * | 2008-11-26 | 2010-06-16 | 信越化学工业株式会社 | 室温可固化的有机基聚硅氧烷组合物 |
CN102086368A (zh) * | 2010-12-17 | 2011-06-08 | 广州新展有机硅有限公司 | 一种环保型有机硅改性聚氨酯粘接密封胶 |
CN102516772A (zh) * | 2011-12-26 | 2012-06-27 | 成都拓利化工实业有限公司 | 一种脱醇型单组份室温硫化硅橡胶及其制备方法 |
CN102952270A (zh) * | 2011-08-29 | 2013-03-06 | 比亚迪股份有限公司 | 一种聚硅氧烷聚合物及其制备方法、以及一种单组份脱醇型硅橡胶及其制备方法 |
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2013
- 2013-04-18 CN CN201310134918.0A patent/CN103289637B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101200594A (zh) * | 2006-12-15 | 2008-06-18 | 比亚迪股份有限公司 | 单组分脱醇型室温固化硅橡胶 |
CN101735618A (zh) * | 2008-11-26 | 2010-06-16 | 信越化学工业株式会社 | 室温可固化的有机基聚硅氧烷组合物 |
CN102086368A (zh) * | 2010-12-17 | 2011-06-08 | 广州新展有机硅有限公司 | 一种环保型有机硅改性聚氨酯粘接密封胶 |
CN102952270A (zh) * | 2011-08-29 | 2013-03-06 | 比亚迪股份有限公司 | 一种聚硅氧烷聚合物及其制备方法、以及一种单组份脱醇型硅橡胶及其制备方法 |
CN102516772A (zh) * | 2011-12-26 | 2012-06-27 | 成都拓利化工实业有限公司 | 一种脱醇型单组份室温硫化硅橡胶及其制备方法 |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107936900A (zh) * | 2017-12-24 | 2018-04-20 | 苏州佳亿达电器有限公司 | 一种用于组装吸尘器的密封胶 |
CN109810669A (zh) * | 2018-12-28 | 2019-05-28 | 广州市高士实业有限公司 | 一种聚硅树脂及其制备方法和应用 |
CN109810669B (zh) * | 2018-12-28 | 2021-07-16 | 广州市高士实业有限公司 | 一种聚硅树脂及其制备方法和应用 |
CN112538333A (zh) * | 2020-12-10 | 2021-03-23 | 江西晨光新材料股份有限公司 | 一种双组分室温硫化硅橡胶及其制备方法和应用 |
CN115505370A (zh) * | 2022-10-28 | 2022-12-23 | 新纳奇材料科技江苏有限公司 | 一种防水透气胶的制备方法及其产品和应用 |
CN115505370B (zh) * | 2022-10-28 | 2023-09-01 | 新纳奇材料科技江苏有限公司 | 一种防水透气胶的制备方法及其产品和应用 |
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CN103289637B (zh) | 2014-10-15 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CB03 | Change of inventor or designer information | ||
CB03 | Change of inventor or designer information |
Inventor after: Li Junyi Inventor after: Yao Yifan Inventor before: Hua Xilin Inventor before: Yang Xiongfa Inventor before: Lai Guoqiao Inventor before: Wu Lianbin Inventor before: Jiang Jianxiong |
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TR01 | Transfer of patent right |
Effective date of registration: 20171117 Address after: No. 2, No. 2589, ring road, ring road, No. 2589, Wu Tung Street, Zhejiang, Zhejiang Patentee after: JIAXING YAOYANG NEW MATERIAL TECHNOLOGY CO., LTD. Address before: Hangzhou City, Zhejiang province 310036 Xuelin Xiasha Economic Development Zone Road No. 16 Patentee before: Hangzhou Normal University |
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TR01 | Transfer of patent right | ||
CP01 | Change in the name or title of a patent holder |
Address after: No. 2, No. 2589, ring road, ring road, No. 2589, Wu Tung Street, Zhejiang, Zhejiang Patentee after: ZHEJIANG SUNLIKY NEW MATERIAL TECHNOLOGY Co.,Ltd. Address before: No. 2, No. 2589, ring road, ring road, No. 2589, Wu Tung Street, Zhejiang, Zhejiang Patentee before: JIAXING YAOYANG NEW MATERIAL TECHNOLOGY Co.,Ltd. |
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CP01 | Change in the name or title of a patent holder | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation and application of a highly adhesive dealcoholic silicone rubber Effective date of registration: 20200826 Granted publication date: 20141015 Pledgee: Bank of Hangzhou Limited by Share Ltd. Tongxiang branch Pledgor: ZHEJIANG SUNLIKY NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2020330000642 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |