CN103113821B - 一种阻燃性涂料的制备方法 - Google Patents
一种阻燃性涂料的制备方法 Download PDFInfo
- Publication number
- CN103113821B CN103113821B CN201310094271.3A CN201310094271A CN103113821B CN 103113821 B CN103113821 B CN 103113821B CN 201310094271 A CN201310094271 A CN 201310094271A CN 103113821 B CN103113821 B CN 103113821B
- Authority
- CN
- China
- Prior art keywords
- product
- preparation
- flame retardant
- weight
- retardant resistance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000003063 flame retardant Substances 0.000 title claims abstract description 26
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 239000011248 coating agent Substances 0.000 title claims abstract description 18
- 238000000576 coating method Methods 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000005057 Hexamethylene diisocyanate Substances 0.000 claims abstract description 8
- 229920001730 Moisture cure polyurethane Polymers 0.000 claims abstract description 8
- 239000003054 catalyst Substances 0.000 claims abstract description 8
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004970 Chain extender Substances 0.000 claims abstract description 6
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 6
- 239000012975 dibutyltin dilaurate Substances 0.000 claims abstract description 6
- 238000004945 emulsification Methods 0.000 claims abstract description 6
- 238000006386 neutralization reaction Methods 0.000 claims abstract description 6
- 239000003960 organic solvent Substances 0.000 claims abstract description 6
- -1 nitrogen-containing compound Chemical class 0.000 claims abstract description 5
- 125000000896 monocarboxylic acid group Chemical group 0.000 claims abstract description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 9
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 8
- XQSFXFQDJCDXDT-UHFFFAOYSA-N hydroxysilicon Chemical compound [Si]O XQSFXFQDJCDXDT-UHFFFAOYSA-N 0.000 claims description 7
- 238000006243 chemical reaction Methods 0.000 claims description 5
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 claims description 4
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 claims description 4
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 4
- RNFNDJAIBTYOQL-UHFFFAOYSA-N chloral hydrate Chemical compound OC(O)C(Cl)(Cl)Cl RNFNDJAIBTYOQL-UHFFFAOYSA-N 0.000 claims description 4
- 229960002327 chloral hydrate Drugs 0.000 claims description 4
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 claims description 4
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 4
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims description 4
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 3
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 3
- 235000006408 oxalic acid Nutrition 0.000 claims description 3
- FGYHQFZISBDLDR-UHFFFAOYSA-N OCCC[PH2]=O Chemical compound OCCC[PH2]=O FGYHQFZISBDLDR-UHFFFAOYSA-N 0.000 claims description 2
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- SCPYDCQAZCOKTP-UHFFFAOYSA-N silanol Chemical compound [SiH3]O SCPYDCQAZCOKTP-UHFFFAOYSA-N 0.000 abstract 1
- 229920002635 polyurethane Polymers 0.000 description 8
- 239000004814 polyurethane Substances 0.000 description 8
- 239000000779 smoke Substances 0.000 description 8
- 238000002485 combustion reaction Methods 0.000 description 7
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 239000003973 paint Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000004753 textile Substances 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000010985 leather Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000007306 functionalization reaction Methods 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000001384 succinic acid Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/0804—Manufacture of polymers containing ionic or ionogenic groups
- C08G18/0819—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups
- C08G18/0823—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups containing carboxylate salt groups or groups forming them
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
- C08G18/3271—Hydroxyamines
- C08G18/3275—Hydroxyamines containing two hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/34—Carboxylic acids; Esters thereof with monohydroxyl compounds
- C08G18/341—Dicarboxylic acids, esters of polycarboxylic acids containing two carboxylic acid groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
- C08G18/3819—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen
- C08G18/3842—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen containing heterocyclic rings having at least one nitrogen atom in the ring
- C08G18/3851—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen containing heterocyclic rings having at least one nitrogen atom in the ring containing three nitrogen atoms in the ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/61—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/6541—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen the low-molecular compounds being compounds of group C08G18/34
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
- C08G18/675—Low-molecular-weight compounds
- C08G18/6755—Unsaturated carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/80—Masked polyisocyanates
- C08G18/8003—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen
- C08G18/8054—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/38
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Polyurethanes Or Polyureas (AREA)
- Paints Or Removers (AREA)
Abstract
Description
本发明 | 市场(SPUA-352) | |
最大烟密度 | 43 | 63 |
达到最大烟密度时间/s | 180 | 160 |
氧指数/% | 28.3 | 26.2 |
有焰燃烧时间/s | 16.3 | 25.4 |
无焰燃烧时间/s | 5.6 | 11.0 |
本发明 | 市场(SPUA-352) | |
断裂伸长率/% | 127.06 | 107.67 |
Claims (4)
Priority Applications (7)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410602685.7A CN104312407B (zh) | 2013-03-22 | 2013-03-22 | 一种水性聚氨酯涂料的制备方法 |
CN201410602542.6A CN104356912B (zh) | 2013-03-22 | 2013-03-22 | 一种涂料的制备方法 |
CN201410602717.3A CN104293152B (zh) | 2013-03-22 | 2013-03-22 | 一种涂料的制备方法 |
CN201410602716.9A CN104327710B (zh) | 2013-03-22 | 2013-03-22 | 一种制备工艺简单的涂料的制备方法 |
CN201410602684.2A CN104277193B (zh) | 2013-03-22 | 2013-03-22 | 聚氨酯涂料的制备方法 |
CN201410602683.8A CN104449310B (zh) | 2013-03-22 | 2013-03-22 | 工艺简单的涂料的制备方法 |
CN201310094271.3A CN103113821B (zh) | 2013-03-22 | 2013-03-22 | 一种阻燃性涂料的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310094271.3A CN103113821B (zh) | 2013-03-22 | 2013-03-22 | 一种阻燃性涂料的制备方法 |
Related Child Applications (6)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201410602716.9A Division CN104327710B (zh) | 2013-03-22 | 2013-03-22 | 一种制备工艺简单的涂料的制备方法 |
CN201410602684.2A Division CN104277193B (zh) | 2013-03-22 | 2013-03-22 | 聚氨酯涂料的制备方法 |
CN201410602717.3A Division CN104293152B (zh) | 2013-03-22 | 2013-03-22 | 一种涂料的制备方法 |
CN201410602683.8A Division CN104449310B (zh) | 2013-03-22 | 2013-03-22 | 工艺简单的涂料的制备方法 |
CN201410602542.6A Division CN104356912B (zh) | 2013-03-22 | 2013-03-22 | 一种涂料的制备方法 |
CN201410602685.7A Division CN104312407B (zh) | 2013-03-22 | 2013-03-22 | 一种水性聚氨酯涂料的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103113821A CN103113821A (zh) | 2013-05-22 |
CN103113821B true CN103113821B (zh) | 2014-12-24 |
Family
ID=48412243
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201310094271.3A Active CN103113821B (zh) | 2013-03-22 | 2013-03-22 | 一种阻燃性涂料的制备方法 |
CN201410602716.9A Active CN104327710B (zh) | 2013-03-22 | 2013-03-22 | 一种制备工艺简单的涂料的制备方法 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201410602716.9A Active CN104327710B (zh) | 2013-03-22 | 2013-03-22 | 一种制备工艺简单的涂料的制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (2) | CN103113821B (zh) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104004449B (zh) * | 2014-06-15 | 2016-04-20 | 段宝荣 | 一种耐光与阻燃性水性聚氨酯涂料的制备方法 |
CN104046224B (zh) * | 2014-07-09 | 2016-05-18 | 段宝荣 | 一种阻燃性水性聚氨酯涂料的制备方法 |
CN104087145B (zh) * | 2014-07-21 | 2016-03-02 | 段宝荣 | 一种阻燃与抗菌性水性聚氨酯涂料的制备方法 |
CN104086698B (zh) * | 2014-07-27 | 2016-05-18 | 朱蕾 | 一种阻燃性核壳型水性丙烯酸酯类树脂涂料的制备方法 |
CN104449325B (zh) * | 2014-12-17 | 2016-09-28 | 高仕邦邯郸新材料科技有限公司 | 纳米材料提高水性聚氨酯涂料阻燃性的制备方法 |
CN104830220B (zh) * | 2015-05-02 | 2017-03-01 | 广州威迪仕汽车用品有限公司 | 阻燃性水性聚氨酯涂料与胶黏剂的制备方法 |
CN104861851A (zh) * | 2015-05-05 | 2015-08-26 | 段宝荣 | 阻燃性水性聚氨酯涂料与胶黏剂的制备方法 |
CN104861852A (zh) * | 2015-06-22 | 2015-08-26 | 朱明德 | 一种建筑用阻燃性水性聚氨酯涂料与胶黏剂的制备方法 |
CN108129635B (zh) * | 2017-12-15 | 2020-10-27 | 合众(佛山)化工有限公司 | 一种疏水阻燃型水性固化剂及其制备方法 |
CN110591044B (zh) * | 2019-08-28 | 2022-01-14 | 浙江华峰合成树脂有限公司 | 一种高物性低发雾水性面层聚氨酯树脂及其制备方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100335522C (zh) * | 2005-09-29 | 2007-09-05 | 上海申真企业发展有限公司 | 阻燃型聚氨酯水性分散体及其制备方法 |
CN102516489A (zh) * | 2011-12-14 | 2012-06-27 | 华南理工大学 | 一种硅胶按键保护涂料用耐磨端羟基聚氨酯树脂的制备方法应用 |
CN102827571B (zh) * | 2012-09-28 | 2014-12-10 | 广东多正化工科技有限公司 | 一种水性聚氨酯胶黏剂的制备方法 |
CN102898936B (zh) * | 2012-10-13 | 2014-08-27 | 浙江新力塑料股份有限公司 | 一种阻燃型水性聚氨酯的制备方法 |
CN102924903B (zh) * | 2012-11-23 | 2014-05-21 | 段宝荣 | 一种纳米材料提高水性聚氨酯阻燃性的制备方法 |
-
2013
- 2013-03-22 CN CN201310094271.3A patent/CN103113821B/zh active Active
- 2013-03-22 CN CN201410602716.9A patent/CN104327710B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN104327710A (zh) | 2015-02-04 |
CN103113821A (zh) | 2013-05-22 |
CN104327710B (zh) | 2016-05-25 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103113821B (zh) | 一种阻燃性涂料的制备方法 | |
CN102898936B (zh) | 一种阻燃型水性聚氨酯的制备方法 | |
CN102250309B (zh) | 一种阻燃型紫外光固化水性聚氨酯涂料及其制备方法 | |
CN101381444B (zh) | 一种环保无卤反应型磷-氮协效阻燃水性聚氨酯及其制备方法 | |
CN104558488B (zh) | 一种有机磷改性水性聚氨酯阻燃涂层剂及其制备方法 | |
CN105315421B (zh) | 一种软硬段共改性后扩链阻燃水性聚氨酯涂层剂及其制备方法 | |
CN104046224B (zh) | 一种阻燃性水性聚氨酯涂料的制备方法 | |
CN102924903B (zh) | 一种纳米材料提高水性聚氨酯阻燃性的制备方法 | |
CN104592475A (zh) | 含有磷杂菲和/或苯基磷酸酯基的阻燃水性聚氨酯的制法 | |
CN104861851A (zh) | 阻燃性水性聚氨酯涂料与胶黏剂的制备方法 | |
CN102226314A (zh) | 环保无卤反应型软硬段共改性阻燃水性聚氨酯织物涂层剂及其制备方法 | |
CN102220700A (zh) | 环保无卤有机磷阻燃改性水性聚氨酯织物涂层剂及其制备方法 | |
Patel et al. | Synthesis and characterization of flame retardant hyperbranched polyurethanes for nano-composite and nano-coating applications | |
CN104293152A (zh) | 一种涂料的制备方法 | |
CN104830220A (zh) | 阻燃性水性聚氨酯涂料与胶黏剂的制备方法 | |
Liu et al. | Flame‐retardant polyurethanes from phosphorus‐containing isocyanates | |
CN105131808B (zh) | 一种阻燃型水性聚氨酯涂料的制备方法 | |
CN105238245A (zh) | 一种环氧树脂改性的水性聚氨酯阻燃涂料及其制备方法 | |
CN107686547A (zh) | 阻燃聚氨酯及其制备方法 | |
CN104861852A (zh) | 一种建筑用阻燃性水性聚氨酯涂料与胶黏剂的制备方法 | |
CN101333443A (zh) | 水分散含磷、硅、氮嵌段聚合物阻燃剂的制备方法及其用途 | |
CN105176368A (zh) | 一种阻燃与耐光性聚氨酯涂料与胶粘剂的制备方法 | |
CN104312407A (zh) | 一种水性聚氨酯涂料的制备方法 | |
KR20200111298A (ko) | 후가교성 반응형 인계 폴리올 및 그의 제조방법, 및 후가교성 반응형 인계 폴리올로 제조되는 난연 열가소성 폴리우레탄 | |
CN104449310A (zh) | 工艺简单的涂料的制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C53 | Correction of patent of invention or patent application | ||
CB02 | Change of applicant information |
Address after: Lishui Economic Development Zone, Nanjing City, Jiangsu province 211215 zhe Ning Road No. 355 Applicant after: Duan Baorong Address before: 264005 Shandong Province, Yantai city Laishan District Road No. 30 spring Applicant before: Duan Baorong |
|
CB03 | Change of inventor or designer information |
Inventor after: Zhao Genyi Inventor after: Yao Hongru Inventor after: Ji Tingting Inventor after: Zhao Xin Inventor after: Gao Ya Inventor after: Li Cheng Inventor after: Zou Zhonghua Inventor before: Duan Baorong Inventor before: Gao Long Inventor before: Song Yu Inventor before: Wang Shanshan |
|
COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: DUAN BAORONG GAO LONG SONG YU WANG SHANSHAN TO: ZHAO GENYI YAO HONGRU JI TINGTING ZHAO XIN GAO YA LI CHENG ZOU ZHONGHUA |
|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: ZHONGSHAN BOHAI FINE CHEMICALS CO., LTD. Free format text: FORMER OWNER: DUAN BAORONG Effective date: 20150508 |
|
C41 | Transfer of patent application or patent right or utility model | ||
COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 211215 NANJING, JIANGSU PROVINCE TO: 528447 ZHONGSHAN, GUANGDONG PROVINCE |
|
TR01 | Transfer of patent right |
Effective date of registration: 20150508 Address after: Wood River port town in Guangdong province Zhongshan City West Jing 528447 No. 5 Patentee after: ZHONGSHAN BOHAI FINE CHEMICAL CO.,LTD. Address before: Lishui Economic Development Zone, Nanjing City, Jiangsu province 211215 zhe Ning Road No. 355 Patentee before: Duan Baorong |
|
C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20161017 Address after: 526000 Guangdong city of Zhaoqing Province Gaoyao District Gaoyao Jinli Gaoyao Avenue and Han industrial base room 211 Patentee after: GUANGDONG BOHAI CHEMICAL TECHNOLOGY Co.,Ltd. Address before: Wood River port town in Guangdong province Zhongshan City West Jing 528447 No. 5 Patentee before: ZHONGSHAN BOHAI FINE CHEMICAL CO.,LTD. |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20170605 Address after: Wood River port town in Guangdong province Zhongshan City West Jing 528400 No. 5 Patentee after: ZHONGSHAN BOHAI FINE CHEMICAL CO.,LTD. Address before: 526000 Guangdong city of Zhaoqing Province Gaoyao District Gaoyao Jinli Gaoyao Avenue and Han industrial base room 211 Patentee before: GUANGDONG BOHAI CHEMICAL TECHNOLOGY Co.,Ltd. |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method of flame-retardant coating Effective date of registration: 20170920 Granted publication date: 20141224 Pledgee: Postal Savings Bank of China Limited by Share Ltd. Zhongshan branch Pledgor: ZHONGSHAN BOHAI FINE CHEMICAL CO.,LTD. Registration number: 2017440000088 |
|
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20220803 Granted publication date: 20141224 Pledgee: Postal Savings Bank of China Limited by Share Ltd. Zhongshan branch Pledgor: ZHONGSHAN BOHAI FINE CHEMICAL CO.,LTD. Registration number: 2017440000088 |
|
TR01 | Transfer of patent right |
Effective date of registration: 20220831 Address after: Room 211, Hanhe Gaoyao Industrial Base, Jinli Avenue, Jinli Town, Gaoyao District, Zhaoqing City, Guangdong Province, 528400 Patentee after: GUANGDONG BOHAI CHEMICAL TECHNOLOGY Co.,Ltd. Address before: 528400 No. 5 Muhe Lingxi Port Town, Zhongshan City, Guangdong Province Patentee before: ZHONGSHAN BOHAI FINE CHEMICAL CO.,LTD. |
|
TR01 | Transfer of patent right |