CN103098162A - 复合电极材料及其制备方法和应用 - Google Patents
复合电极材料及其制备方法和应用 Download PDFInfo
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- CN103098162A CN103098162A CN2010800688115A CN201080068811A CN103098162A CN 103098162 A CN103098162 A CN 103098162A CN 2010800688115 A CN2010800688115 A CN 2010800688115A CN 201080068811 A CN201080068811 A CN 201080068811A CN 103098162 A CN103098162 A CN 103098162A
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- electrode material
- graphene
- combination electrode
- preparation
- mixed solution
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000007772 electrode material Substances 0.000 title claims abstract description 79
- 239000002131 composite material Substances 0.000 title abstract description 11
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 86
- 229910021389 graphene Inorganic materials 0.000 claims abstract description 55
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 claims abstract description 48
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 37
- 239000010439 graphite Substances 0.000 claims abstract description 37
- 239000011259 mixed solution Substances 0.000 claims abstract description 19
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 18
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000007864 aqueous solution Substances 0.000 claims abstract description 11
- 238000001035 drying Methods 0.000 claims abstract description 4
- 238000005406 washing Methods 0.000 claims abstract description 4
- 238000002360 preparation method Methods 0.000 claims description 25
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 14
- 239000003990 capacitor Substances 0.000 claims description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- 244000061458 Solanum melongena Species 0.000 claims description 7
- -1 graphite alkene Chemical class 0.000 claims description 7
- 239000000178 monomer Substances 0.000 claims description 6
- 239000008118 PEG 6000 Substances 0.000 claims description 3
- 229920002565 Polyethylene Glycol 400 Polymers 0.000 claims description 3
- 229920002584 Polyethylene Glycol 6000 Polymers 0.000 claims description 3
- 230000002776 aggregation Effects 0.000 claims description 3
- 238000004220 aggregation Methods 0.000 claims description 3
- JLFNLZLINWHATN-UHFFFAOYSA-N pentaethylene glycol Chemical compound OCCOCCOCCOCCOCCO JLFNLZLINWHATN-UHFFFAOYSA-N 0.000 claims description 3
- 239000013049 sediment Substances 0.000 claims description 3
- 230000008901 benefit Effects 0.000 abstract description 5
- 240000007108 Fuchsia magellanica Species 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000003801 milling Methods 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 10
- 238000012360 testing method Methods 0.000 description 10
- 238000000034 method Methods 0.000 description 7
- 239000008367 deionised water Substances 0.000 description 6
- 229910021641 deionized water Inorganic materials 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 239000012286 potassium permanganate Substances 0.000 description 6
- 239000000843 powder Substances 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 239000002356 single layer Substances 0.000 description 4
- 239000003643 water by type Substances 0.000 description 4
- 239000003575 carbonaceous material Substances 0.000 description 3
- 238000002484 cyclic voltammetry Methods 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 3
- 239000004810 polytetrafluoroethylene Substances 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 239000004966 Carbon aerogel Substances 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 239000004917 carbon fiber Substances 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 229910000428 cobalt oxide Inorganic materials 0.000 description 1
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical class Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 229910000480 nickel oxide Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000006479 redox reaction Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 229910001925 ruthenium oxide Inorganic materials 0.000 description 1
- WOCIAKWEIIZHES-UHFFFAOYSA-N ruthenium(iv) oxide Chemical compound O=[Ru]=O WOCIAKWEIIZHES-UHFFFAOYSA-N 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 238000010532 solid phase synthesis reaction Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 229910000314 transition metal oxide Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/32—Carbon-based
- H01G11/36—Nanostructures, e.g. nanofibres, nanotubes or fullerenes
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Crystallography & Structural Chemistry (AREA)
- Nanotechnology (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
- Battery Electrode And Active Subsutance (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/CN2010/078142 WO2012055095A1 (fr) | 2010-10-27 | 2010-10-27 | Matériau électrode composite, procédé de fabrication et application associée |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103098162A true CN103098162A (zh) | 2013-05-08 |
Family
ID=45993055
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010800688115A Pending CN103098162A (zh) | 2010-10-27 | 2010-10-27 | 复合电极材料及其制备方法和应用 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US20130168611A1 (fr) |
| EP (1) | EP2634783A4 (fr) |
| JP (1) | JP2014501028A (fr) |
| CN (1) | CN103098162A (fr) |
| WO (1) | WO2012055095A1 (fr) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114512353A (zh) * | 2022-03-06 | 2022-05-17 | 桂林理工大学 | 一种三维石墨烯/导电聚吡咯/导电mof复合电极材料及其制备方法 |
| CN114976062A (zh) * | 2020-10-15 | 2022-08-30 | 昆明理工大学 | 氮掺杂rGO负载MnO纳米颗粒催化剂的制备方法 |
Families Citing this family (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DK2794475T3 (da) | 2011-12-21 | 2020-04-27 | Univ California | Forbundet korrugeret carbonbaseret netværk |
| KR101371288B1 (ko) * | 2011-12-22 | 2014-03-07 | 이화여자대학교 산학협력단 | 망간 산화물/그래핀 나노복합체 및 이의 제조 방법 |
| WO2013134207A1 (fr) | 2012-03-05 | 2013-09-12 | The Regents Of The University Of California | Condensateur avec des électrodes faites d'un réseau interconnecté à base de carbone ondulé |
| CN103663572A (zh) * | 2012-09-11 | 2014-03-26 | 中国科学院上海硅酸盐研究所 | 具有超高比容量的氧化镍材料的制备方法 |
| WO2014158970A1 (fr) | 2013-03-14 | 2014-10-02 | Saudi Basic Industries Corporation | Condensateur d'ordre fractionnel basé sur un diélectrique polymère dopé aux nano-charges conductrices |
| CN103811718B (zh) * | 2014-02-20 | 2016-08-17 | 深圳市贝特瑞新能源材料股份有限公司 | 一种石墨烯基复合负极材料的制备方法及制得的负极材料和锂离子电池 |
| KR102443607B1 (ko) | 2014-06-16 | 2022-09-16 | 더 리전트 오브 더 유니버시티 오브 캘리포니아 | 하이브리드 전기화학 전지 |
| JP2018501644A (ja) | 2014-11-18 | 2018-01-18 | ザ リージェンツ オブ ザ ユニバーシティ オブ カリフォルニア | 多孔性の相互接続された波状カーボンベースネットワーク（ｉｃｃｎ）複合材料 |
| CN105448530A (zh) * | 2015-11-30 | 2016-03-30 | 广东工业大学 | 一种钼酸镍/石墨烯复合材料的制备方法 |
| CN105355893B (zh) * | 2015-12-16 | 2017-11-17 | 西北工业大学 | 柔性锂离子电池负极材料的制备方法 |
| CA3006997A1 (fr) | 2015-12-22 | 2017-06-29 | The Regents Of The University Of California | Films de graphene cellulaire |
| CA3009208A1 (fr) | 2016-01-22 | 2017-07-27 | The Regents Of The University Of California | Dispositifs haute tension |
| KR102361374B1 (ko) | 2016-03-23 | 2022-02-09 | 나노테크 에너지, 인크. | 고전압 및 태양 응용분야를 위한 디바이스 및 방법 |
| AU2017245151B2 (en) | 2016-04-01 | 2022-03-17 | The Regents Of The University Of California | Direct growth of polyaniline nanotubes on carbon cloth for flexible and high-performance supercapacitors |
| CN107359054B (zh) * | 2016-05-09 | 2019-12-03 | 国家纳米科学中心 | 一种复合电极材料、其制备方法及应用 |
| US11097951B2 (en) | 2016-06-24 | 2021-08-24 | The Regents Of The University Of California | Production of carbon-based oxide and reduced carbon-based oxide on a large scale |
| EA201990587A1 (ru) | 2016-08-31 | 2019-07-31 | Дзе Риджентс Оф Дзе Юнивёрсити Оф Калифорния | Устройства, содержащие материалы на основе углерода, и их производство |
| CN106920700B (zh) * | 2017-01-24 | 2019-01-15 | 中国科学院宁波材料技术与工程研究所 | 一种功能化的氧化石墨烯/细菌纤维素/碳纳米管复合膜制备方法及其应用 |
| JP7358719B2 (ja) * | 2017-05-09 | 2023-10-11 | 株式会社Flosfia | サーミスタ膜およびその成膜方法 |
| US11133134B2 (en) | 2017-07-14 | 2021-09-28 | The Regents Of The University Of California | Simple route to highly conductive porous graphene from carbon nanodots for supercapacitor applications |
| CN107742707B (zh) * | 2017-10-16 | 2020-08-21 | 河源广工大协同创新研究院 | 一种纳米氧化镧/石墨烯/硫复合材料的制备方法 |
| CN108199015B (zh) * | 2017-12-15 | 2020-11-27 | 同济大学 | 黑磷量子点/碳化钛纳米片复合材料的制备方法和应用 |
| CN108428877A (zh) * | 2018-03-28 | 2018-08-21 | 成都理工大学 | 纳米Fe3O4@C原位复合多孔锂离子电池负极材料及其制备方法 |
| CN108565426B (zh) * | 2018-04-16 | 2020-09-15 | 三峡大学 | Li3VO4/LiVO2复合锂离子电池负极材料及其制备方法 |
| CN108615884B (zh) * | 2018-04-25 | 2020-10-23 | 国家纳米科学中心 | 一种中空结构的KFeF3纳米材料及其制备方法和应用 |
| CN108649222B (zh) * | 2018-05-09 | 2020-12-22 | 上海电力学院 | 一种高性能钠离子电池正极材料及其制备方法 |
| CN108711613B (zh) * | 2018-05-18 | 2020-10-30 | 中南大学 | 一种聚苯胺/聚乙二醇共包裹的复合三元正极材料及其制备和应用 |
| CN108806997A (zh) * | 2018-06-30 | 2018-11-13 | 鹿寨鹿康科技有限公司 | 一种改性石墨烯及其在超级电容器复合材料的应用 |
| US10938032B1 (en) | 2019-09-27 | 2021-03-02 | The Regents Of The University Of California | Composite graphene energy storage methods, devices, and systems |
| CN112687476B (zh) * | 2019-10-18 | 2022-06-10 | 昆山科技大学 | 氧化石墨烯碳气凝胶制备与应用 |
| CN113793761B (zh) * | 2021-08-24 | 2022-08-12 | 洛阳理工学院 | 生物发酵二氧化锰/石墨烯电极材料的制备方法及应用 |
| CN114360923B (zh) * | 2022-01-18 | 2023-05-30 | 贵州师范学院 | 一种氧化镍复合电极材料的制备方法 |
| CN114604900B (zh) * | 2022-03-29 | 2023-06-06 | 东北石油大学 | 一种自组装KMn8O16@还原氧化石墨烯二维复合材料的制备方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101527202A (zh) * | 2009-04-24 | 2009-09-09 | 南京理工大学 | 氧化石墨烯/聚苯胺超级电容器复合电极材料及其制备方法、用途 |
| WO2010027337A9 (fr) * | 2008-09-08 | 2010-07-01 | Nanyang Technological University | Matériaux d’électrode pour piles métal-air, piles à combustible et supercondensateurs |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9190667B2 (en) * | 2008-07-28 | 2015-11-17 | Nanotek Instruments, Inc. | Graphene nanocomposites for electrochemical cell electrodes |
-
2010
- 2010-10-27 EP EP10858824.5A patent/EP2634783A4/fr not_active Withdrawn
- 2010-10-27 US US13/821,247 patent/US20130168611A1/en not_active Abandoned
- 2010-10-27 CN CN2010800688115A patent/CN103098162A/zh active Pending
- 2010-10-27 JP JP2013533066A patent/JP2014501028A/ja active Pending
- 2010-10-27 WO PCT/CN2010/078142 patent/WO2012055095A1/fr active Application Filing
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010027337A9 (fr) * | 2008-09-08 | 2010-07-01 | Nanyang Technological University | Matériaux d’électrode pour piles métal-air, piles à combustible et supercondensateurs |
| CN101527202A (zh) * | 2009-04-24 | 2009-09-09 | 南京理工大学 | 氧化石墨烯/聚苯胺超级电容器复合电极材料及其制备方法、用途 |
Non-Patent Citations (4)
| Title |
|---|
| JUN YAN: "Fast and reversible surface redox reaction of graphene–MnO2¬ composites as supercapacitor electrodes", 《CARBON》 * |
| JUN YAN: "Fast and reversible surface redox reaction of graphene–MnO2¬ composites as supercapacitor electrodes", 《CARBON》, vol. 48, 25 June 2010 (2010-06-25), pages 3825 - 3833, XP027189807 * |
| SHENG CHEN: ""Graphene Oxide-MnO2 Nanocomposites for Supercapacitors"", 《ACS NANO》 * |
| 柴兰琴，董文魁: ""相转移催化反应机理及应用"", 《兰州铁道学院学报》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114976062A (zh) * | 2020-10-15 | 2022-08-30 | 昆明理工大学 | 氮掺杂rGO负载MnO纳米颗粒催化剂的制备方法 |
| CN114976062B (zh) * | 2020-10-15 | 2024-01-26 | 昆明理工大学 | 氮掺杂rGO负载MnO纳米颗粒催化剂的制备方法 |
| CN114512353A (zh) * | 2022-03-06 | 2022-05-17 | 桂林理工大学 | 一种三维石墨烯/导电聚吡咯/导电mof复合电极材料及其制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2634783A4 (fr) | 2018-03-28 |
| WO2012055095A1 (fr) | 2012-05-03 |
| EP2634783A1 (fr) | 2013-09-04 |
| JP2014501028A (ja) | 2014-01-16 |
| US20130168611A1 (en) | 2013-07-04 |
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Application publication date: 20130508 |
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| RJ01 | Rejection of invention patent application after publication |