CN102951638B - 中空碳纳米材料的水热合成方法 - Google Patents
中空碳纳米材料的水热合成方法 Download PDFInfo
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- CN102951638B CN102951638B CN201210499894.4A CN201210499894A CN102951638B CN 102951638 B CN102951638 B CN 102951638B CN 201210499894 A CN201210499894 A CN 201210499894A CN 102951638 B CN102951638 B CN 102951638B
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- Prior art keywords
- hollow carbon
- carbon nanomaterials
- synthesis method
- hydrothermal synthesis
- hollow
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 43
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 42
- 239000002086 nanomaterial Substances 0.000 title claims abstract description 35
- 238000000034 method Methods 0.000 title claims abstract description 27
- 238000001027 hydrothermal synthesis Methods 0.000 title claims abstract description 11
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims abstract description 14
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 9
- 239000008103 glucose Substances 0.000 claims abstract description 9
- 229920000428 triblock copolymer Polymers 0.000 claims abstract description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 5
- 229930006000 Sucrose Natural products 0.000 claims description 5
- 239000005720 sucrose Substances 0.000 claims description 5
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 3
- 238000006555 catalytic reaction Methods 0.000 abstract description 3
- 239000004094 surface-active agent Substances 0.000 abstract 2
- 230000007613 environmental effect Effects 0.000 abstract 1
- 239000002245 particle Substances 0.000 description 7
- 239000003575 carbonaceous material Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000013543 active substance Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 238000002441 X-ray diffraction Methods 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 229910021392 nanocarbon Inorganic materials 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000001241 arc-discharge method Methods 0.000 description 2
- 238000005137 deposition process Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- XMWRBQBLMFGWIX-UHFFFAOYSA-N C60 fullerene Chemical compound C12=C3C(C4=C56)=C7C8=C5C5=C9C%10=C6C6=C4C1=C1C4=C6C6=C%10C%10=C9C9=C%11C5=C8C5=C8C7=C3C3=C7C2=C1C1=C2C4=C6C4=C%10C6=C9C9=C%11C5=C5C8=C3C3=C7C1=C1C2=C4C6=C2C9=C5C3=C12 XMWRBQBLMFGWIX-UHFFFAOYSA-N 0.000 description 1
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 241000143432 Daldinia concentrica Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000004917 carbon fiber Substances 0.000 description 1
- 229910021393 carbon nanotube Inorganic materials 0.000 description 1
- 239000002041 carbon nanotube Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 230000003252 repetitive effect Effects 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
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- Carbon And Carbon Compounds (AREA)
Abstract
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CN201210499894.4A CN102951638B (zh) | 2012-11-30 | 2012-11-30 | 中空碳纳米材料的水热合成方法 |
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CN201210499894.4A CN102951638B (zh) | 2012-11-30 | 2012-11-30 | 中空碳纳米材料的水热合成方法 |
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CN102951638A CN102951638A (zh) | 2013-03-06 |
CN102951638B true CN102951638B (zh) | 2014-12-31 |
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Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104591176B (zh) * | 2015-02-04 | 2017-03-29 | 中国科学院宁波材料技术与工程研究所 | 一种石墨烯的制备方法 |
CN104805682A (zh) * | 2015-04-17 | 2015-07-29 | 浙江冶金环境保护设计研究有限公司 | 应用于电Fenton体系的碳纤维材料及其制备方法 |
CN105712317B (zh) * | 2016-01-30 | 2017-10-17 | 山西大学 | 一种含纳米中空碳材料的制备方法 |
CN106082160B (zh) * | 2016-06-02 | 2018-04-27 | 浙江大学 | 中空炭材料的制备方法及其产品 |
CN107014931B (zh) * | 2017-03-07 | 2019-11-08 | 浙江省立同德医院 | 一种细胞膜修饰纳米碳球材料及其制备方法和应用 |
CN108529692B (zh) * | 2018-06-01 | 2020-06-30 | 南京理工大学 | 空心球形氧化镍的制备方法 |
CN110975812B (zh) * | 2019-12-18 | 2022-03-01 | 西北农林科技大学 | 一种茶皂素空心碳球及其制备方法和在重金属吸附中的应用 |
CN113104836B (zh) * | 2021-03-04 | 2022-12-23 | 上海大学 | 烧瓶结构的碳纳米材料及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1356265A (zh) * | 2001-08-20 | 2002-07-03 | 复旦大学 | 形貌可控的大孔径介孔分子筛的制备方法 |
CN101348254A (zh) * | 2007-07-18 | 2009-01-21 | 中国科学院大连化学物理研究所 | 一种中空纳米氧化硅球的制备方法 |
CN101625919A (zh) * | 2009-04-30 | 2010-01-13 | 中国计量学院 | 一种新型结构的介孔纳米磁性材料的制备方法 |
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- 2012-11-30 CN CN201210499894.4A patent/CN102951638B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1356265A (zh) * | 2001-08-20 | 2002-07-03 | 复旦大学 | 形貌可控的大孔径介孔分子筛的制备方法 |
CN101348254A (zh) * | 2007-07-18 | 2009-01-21 | 中国科学院大连化学物理研究所 | 一种中空纳米氧化硅球的制备方法 |
CN101625919A (zh) * | 2009-04-30 | 2010-01-13 | 中国计量学院 | 一种新型结构的介孔纳米磁性材料的制备方法 |
Non-Patent Citations (1)
Title |
---|
尺寸可控空心碳球的水热合成;靳秀芝 等;《稀有金属材料与工程》;20110630;第40卷;第101页1.2纳米碳空心球的制备,第103页3结论 * |
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