CN102551028B - Method for preparing suaeda salsa biogenetic salt - Google Patents
Method for preparing suaeda salsa biogenetic salt Download PDFInfo
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- CN102551028B CN102551028B CN2012100512655A CN201210051265A CN102551028B CN 102551028 B CN102551028 B CN 102551028B CN 2012100512655 A CN2012100512655 A CN 2012100512655A CN 201210051265 A CN201210051265 A CN 201210051265A CN 102551028 B CN102551028 B CN 102551028B
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Abstract
The invention discloses a method for preparing a suaeda salsa biogenetic salt. The method comprises the following steps of: taking parts, such as stems and leaves, above roots of fresh suaedasalsa; juicing; adding water into residual solid parts and extracting once; mixing the two liquids; and performing enzymolysis, boiling, decoloration, heavy metal removal, concentration and crystallization onthe mixed liquid, thus obtaining a finished product. The yield of the product is 1.2-2.1%. The product comprises inorganic salts serving as major ingredients and natural organic matters serving as minor ingredients. The inorganic salts mainly comprise sodium chloride, potassium chloride and magnesium sulfate as well as a trace amount of trace elements (Ca, P, Fe, Zn, Se, I, Cu and Mn) and the organic matters in the product mainly comprises vitamins, amino acid and polysaccharide. During preparation, any chemical substances are not required; furthermore, the raw materials are abundant, readilyavailable and low in cost, and have extremely high economic additional value; and moreover, the preparation method is simple and feasible, is easy to produce and operate, and is wide in market prospect.
Description
Technical field
The present invention relates to the preparation method of the fluffy biogenic salt of a kind of alkali of beach plant extract chemical field.
Background technology
Alkali fluffy (Suaedasalsa) is called " wolf tail bar " again, " HAIYINGCAI ", " alkali wormwood artemisia ", because of certain emperor once treats use, " emperor's seat dish " is otherwise known as, " Huang Xucai " and " gold zone dish " etc., annual herb, stem is upright, cylindrical, up to 30-100 centimetre, Hua Dansheng or 2-3 has handle to cluster on the short handle of axil, is a umbrella, perianth is the five-pointed star shape in the fruit phase, be typical halophytes, grow near the beach of seashore more, also can plant, its cultivation technique is more extensive, mainly is distributed in northeast, the northwest, North China, Henan, Shandong, Jiangsu and zhejiang and other places.The fluffy commodity of alkali is good, and plant type is attractive in appearance, and the refined title of " emerald coral " is arranged, and fresh and tender cauline leaf is nutritious, has special seafood flavor, and mouthfeel is good, and can be used as medicine and cure mainly that dyspepsia is stagnated and heating etc.The fluffy function that has absorption and store salinity of alkali, alkali is fluffy to be absorbed by root, the inorganic salts in the soil are purified, and selective the absorption, store in its stem, the leaf, the amount of saliferous is very high, is main component with sodium chloride, potassium chloride, magnesium chloride, in addition, also contain Ca, P, Fe, Zn, Se, I, Cu, Mn trace element, be the source of rare nutrients biological salt, have important production exploitation and be worth, but still do not obtain at present producing and utilizing.
Summary of the invention
For the fluffy this biogenic salt with nutritive value of alkali is applied to healthy food, remedy the existing deficiency of utilizing halophytes exploitation biogenic salt technology to lack, and the preparation method of the fluffy biogenic salt of a kind of alkali that proposes.
Its technical scheme is to get the fluffy stem of fresh soda and leaf, press extracting juice after, juice carries out enzymolysis, boils, decolouring, removing heavy-metal, condensing crystallizing, makes the fluffy biogenic salt of alkali.
Such scheme further improves: the stem that fresh soda is fluffy and leaf, after pressing extracting juice, remaining solid partly expects admittedly that by alkali is fluffy 0.1-3 times of weight ratio interpolation water extracts once, merge twice liquid, the juice that merges is added biology enzyme to be handled, cool 70-75 ℃ after heating is boiled then, add the food-grade active carbon, the addition of active carbon is the 1%-3% of liquid weight, stirs insulation 30-50 minute, removes by filter active carbon, obtain the stillness of night, deviate from heavy metal ion, condensing crystallizing under temperature 60-70 ℃ of vacuum 0.8-09mpa condition makes the fluffy biogenic salt of alkali.
Biology enzyme used in the biology enzyme processing procedure refers to protease, comprise single enzyme or complex enzyme in alkali protease, neutral proteinase, bromelain or the papain, the consumption of described protease is every kilogram of liquid 10-100 ten thousand unit of activity, be incubated 30 ℃-45 ℃ after adding protease, stir 30-50 rev/min, kept 30-60 minute; The method of deviating from heavy metal ion comprises to be used the pellicle method or uses flucculation process, wherein, the selected flocculant of flucculation process is shitosan and algin, and the ratio of shitosan and algin is weight ratio 1:1, consumption is the 0.01%-0.1% of treat liquid weight, processing method is that elder generation is distributed to algin in the treatment fluid, stirs 25-35 minute, then chitosan solution is added, continue to stir 25-30 minute, staticly settle, filter.
Effect of the present invention is mainly reflected in: the yield of product is 1.2-2.1%, main component in the product is inorganic salts, less important part is natural organic matter, mainly contain sodium chloride (21%-23%), potassium chloride (23%-25%) and magnesium sulfate (18%-20%) in the product in the inorganic salts, also contain Ca, P, Fe, Zn, Se, I, Cu, the Mn trace element of trace, the main component in the organic matter in the product is vitamin, amino acid and polysaccharide.The present invention prepares the process of the fluffy biogenic salt of alkali need not add any chemical substance, and pure natural components is nutritious, the constant salt is abundant, trace element is complete, the healthy nutritive value with high-quality, in addition, the used abundant raw material of the present invention is easy to get, with low cost, have very high economic value added, and preparation technology's simple possible of the present invention, be easy to production operation, market prospects are very wide.
The specific embodiment
Embodiment 1
Get fluffy cauline leaf 100 grams of fresh alkali, press extracting juice, remaining solid part adding distil water 10 grams, extract once again, merge twice liquid, add alkali protease 50,000 units, handled 30 minutes for 37 ℃, boil, cool to 70 ℃, add active carbon 1 gram, stir insulation 30 minutes, suction filtration is handled with membrane filtration, condensing crystallizing obtains finished product 1.5 grams.
Embodiment 2
Get fluffy cauline leaf 100 grams of fresh alkali, press extracting juice, remaining solid part adding distil water 300 grams, extract once again, merge twice liquid, add each 10,000 unit of neutral proteinase and bromelain, handled 30 minutes for 37 ℃, boil, cool to 75 ℃, add active carbon 3 grams, stir insulation 50 minutes, suction filtration is handled with membrane filtration, condensing crystallizing obtains finished product 2.1 grams.
Embodiment 3
Get fluffy cauline leaf 100 grams of fresh alkali, press extracting juice, remaining solid part adding distil water 100 grams extract once again, merge twice liquid, add papain 30,000 units, handled 30 minutes for 37 ℃, boil, cool to 73 ℃, add active carbon 2 grams, stir insulation 40 minutes, suction filtration adds 80 milligrams of algins, stirred 30 minutes, and added the solution that contains 80 milligrams of shitosans, stirred 30 minutes, leave standstill the back and filter, the filtrate condensing crystallizing obtains finished product 1.4 grams.
Claims (1)
1. the preparation method of the fluffy biogenic salt of alkali, it is characterized in that: the stem that fresh soda is fluffy and leaf, after pressing extracting juice, remaining solid partly expects admittedly that by alkali is fluffy 0.1-3 times of weight ratio interpolation water extracts once, merge twice liquid, the juice that merges is added biology enzyme to be handled, cool 70-75 ℃ after heating is boiled then, add the food-grade active carbon, the addition of active carbon is the 1%-3% of liquid weight, stir insulation 30-50 minute, remove by filter active carbon, obtain the stillness of night, deviate from heavy metal ion, condensing crystallizing under temperature 60-70 ℃ of vacuum 0.8-09mpa condition makes the fluffy biogenic salt of alkali; Biology enzyme used in the biology enzyme processing procedure refers to protease, comprise single enzyme or complex enzyme in alkali protease, neutral proteinase, bromelain or the papain, the consumption of described protease is every kilogram of liquid 10-100 ten thousand unit of activity, be incubated 30 ℃-45 ℃ after adding protease, stir 30-50 rev/min, kept 30-60 minute; Deviate from heavy metal ion and adopt flucculation process, wherein, the selected flocculant of flucculation process is shitosan and algin, and the ratio of shitosan and algin is weight ratio 1:1, consumption is the 0.01%-0.1% of treat liquid weight, processing method is that elder generation is distributed to algin in the treatment fluid, stirs 25-35 minute, then chitosan solution is added, continue to stir 25-30 minute, staticly settle, filter.
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| CN2012100512655A CN102551028B (en) | 2012-03-01 | 2012-03-01 | Method for preparing suaeda salsa biogenetic salt |
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| CN2012100512655A CN102551028B (en) | 2012-03-01 | 2012-03-01 | Method for preparing suaeda salsa biogenetic salt |
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| KR100448672B1 (en) * | 2000-02-22 | 2004-09-18 | 홍영표 | A liquefied plant salt of preparation method and liquefied plant salt |
| KR100448673B1 (en) * | 2000-02-22 | 2004-09-16 | 홍영표 | Plant salt of preparation method and Plant salt |
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| CN101668436A (en) * | 2007-05-17 | 2010-03-10 | 植物盐有限公司 | Salicornia spp.-derived salt and its production process |
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