CN105105083A - Suaeda salsa biological salt preparation method - Google Patents
Suaeda salsa biological salt preparation method Download PDFInfo
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- CN105105083A CN105105083A CN201510452647.2A CN201510452647A CN105105083A CN 105105083 A CN105105083 A CN 105105083A CN 201510452647 A CN201510452647 A CN 201510452647A CN 105105083 A CN105105083 A CN 105105083A
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Abstract
The invention belongs to the technical field of biological salt preparation and relates to a preparation method of a Suaeda salsa biological salt. The preparation method comprises 1, cleaning, 2, juicing, 3, extraction, 4, impurity removal and 5, condensation and crystallization. The Suaeda salsa biological salt preparation method has simple processes and can be operated easily. The prepared Suaeda salsa biological salt has high potassium salt content higher than sodium salt content, belongs to a low-sodium salt, contains a lot of vitamins and amino acids, is rich in nutrients and has a good health value and high economic value added.
Description
Technical field
The invention belongs to biological salt making technology field, particularly relate to a kind of preparation method of Suaeda salsa biogenic salt.
Background technology
Suaeda salsa (Suaedasalsa) is also called " wolf tail bar ", " HAIYINGCAI ", " alkali wormwood artemisia ", annual herb, stem is upright, cylindrical, up to 30-100 centimetre, Hua Dansheng or 2-3 has handle to cluster on the short handle of axil, and in group's umbrella, perianth is Five-pointed star in the fruit phase, be grown on the beach of near shore more, also can plant, its cultivation technique is more extensive, is mainly distributed in northeast, northwest, North China, Henan, Shandong, Jiangsu and zhejiang and other places.
Suaeda salsa is a kind of typical halophytes, be commonly called as " salt wormwood artemisia ", " seafood dish ", new culturing vegetable kind can be become through domestication, and can cultivate on desalination soil, be born in beach, wasteland, canal bank, river valley, roadside, Tian Bian etc. containing on saline and alkaline soil.
Suaeda salsa happiness high humidity, Salt And Alkali Tolerance, impoverishment tolerant, few disease and pest are a kind of natural pollution-free green food, are suitable for coastal area sandy soil or sandy loam plantation.Suaeda salsa requires that soil has good moisture condition, but due to cauline leaf meat, the moisture that in leaf, contain is a large amount of, therefore temporary transient arid can be stood.The rest period of seed is very short, and meeting suitable condition just can germination and emergence growth rapidly.But most seed germination and emergence rapidly after summer rain.Being scattered about like the stars around alkali lake and on saline-alkaline spot soil or growth of trooping more, can forming pure group, is also the companion species of other haophitic vegetations.
The commodity of Suaeda salsa is good, and plant type is attractive in appearance, and have the refined title of " emerald coral ", fresh and tender cauline leaf is nutritious, has special seafood taste, and mouthfeel is good, and can be used as medicine and cure mainly dyspepsia and stagnate and heating etc.Suaeda salsa has the function absorbing and store salinity, inorganic salts in soil, by root absorption, purify by Suaeda salsa, and selective absorbing, store its stem, Ye Zhong, the amount of saliferous is very high, with sodium chloride, potassium chloride, magnesium chloride for main component, in addition, also containing Ca, P, Fe, Zn, Se, I, Cu, Mn trace element, be the source of rare nutrients biological salt, there is important production development and be worth, but still do not produced and utilize at present.
Summary of the invention
The object of the invention is to: the deficiency existed for prior art, provides the preparation method of simple, the lower-cost Suaeda salsa biogenic salt of a kind of technique.
For solving the problems of the technologies described above, technical scheme of the present invention is:
A preparation method for Suaeda salsa biogenic salt, described preparation method comprises the following steps:
(1) clean: with water by fresh Suaeda salsa rinsed clean repeatedly;
(2) press juice: stem and the leaf of getting the Suaeda salsa after rinsed clean, segment, carries out pressure juice, obtains stoste and solid slag;
(3) lixiviate: be placed in container by described solid slag, adds described solid slag weight 10-15 water soaking 30-40 minute doubly, heats 10-15 minute, while hot suction filtration at 70-80 DEG C, collect extract, be cooled to room temperature, for subsequent use;
(4) removal of impurities: merge described stoste and extract, adding mass concentration is 70% ethanol, at 35-40 DEG C, soak 1-2 hour, leaves standstill, and removing upper solution, obtains lower floor's solution;
(5) concentrated, crystallization: at 50-60 DEG C, described lower floor solution is concentrated, dry, obtain crystalline particle.
Improve as one, in step (2), by described stoste centrifugal 10-15 minute under 5000rpm, get supernatant.
Improve as one, in step (4), be 70% ethanol washing 3-5 time, obtain cleaning mixture by described lower floor solution mass concentration, by described cleaning mixture stratification, removing upper strata cleaning solution, obtains lower floor's cleaning solution.
As improving further, by described lower floor cleaning solution through 0.45 μm of filtering with microporous membrane.
Improve as one, in step (5), described drying is spraying dry.
Owing to have employed technique scheme, the invention has the beneficial effects as follows:
The preparation method of Suaeda salsa biogenic salt provided by the invention, it comprises cleaning, pressure juice, lixiviate, removal of impurities, concentrated and crystallization, its step is simple, raw materials usedly to be easy to get, the solvent used is cheap, thus makes its production cost lower, by the Suaeda salsa biogenic salt that the method is obtained, its nutritional labeling is high, is rich in trace element, the V such as Ca, P, Fe, Zn, Se, I, Cu, Mn
c, V
b1, V
b2, V
b5, V
b12deng several amino acids such as vitamin and serine, lysine, phenylalanines, and its good absorbing, Trace Elements in Human Body, vitamin and amino acid whose deficiency can be supplemented, leaching process just goes out chlorophyll in Suaeda salsa plant and flavone component, to improve the one-tenth colourity of final products, the nutritional labeling in Suaeda salsa plant is not almost destroyed, without any side effects, the method salt manufacturing productive rate, at 2.5-3%, takes full advantage of coastal resources.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
Embodiment one
A preparation method for Suaeda salsa biogenic salt, described preparation method comprises the following steps:
(1) clean: with water by the rinsing repeatedly of fresh Suaeda salsa, until by Suaeda salsa rinsed clean, not containing impurity such as silts;
(2) press juice: stem and the leaf of getting the Suaeda salsa after rinsed clean, segment, utilizes squeezer to carry out pressure juice, obtains stoste and solid slag;
(3) lixiviate: be placed in container by above-mentioned solid slag, adds the water soaking 30 minutes of solid slag weight 10 times, heats 15 minutes, suction filtration while hot at 70 DEG C, collects extract, is cooled to room temperature, for subsequent use;
(4) removal of impurities: merge above-mentioned stoste and extract, adding mass concentration is 70% ethanol, soaks 2 hours at 35 DEG C, leaves standstill, and removing upper solution, obtains lower floor's solution;
(5) concentrated, crystallization: concentrated by above-mentioned lower floor solution at 50 DEG C, spraying dry, obtains crystalline particle.
Embodiment two
A preparation method for Suaeda salsa biogenic salt, described preparation method comprises the following steps:
(1) clean: with water by the rinsing repeatedly of fresh Suaeda salsa, until by Suaeda salsa rinsed clean, not containing impurity such as silts;
(2) press juice: stem and the leaf of getting the Suaeda salsa after rinsed clean, segment, utilizes squeezer to carry out pressure juice, obtains stoste and solid slag;
(3) lixiviate: be placed in container by above-mentioned solid slag, adds the water soaking 40 minutes of solid slag weight 15 times, heats 10 minutes, suction filtration while hot at 80 DEG C, collects extract, is cooled to room temperature, for subsequent use;
(4) removal of impurities: merge above-mentioned stoste and extract, adding mass concentration is 70% ethanol, soaks 1 hour at 40 DEG C, leaves standstill, and removing upper solution, obtains lower floor's solution;
(5) concentrated, crystallization: concentrated by above-mentioned lower floor solution at 60 DEG C, spraying dry, obtains crystalline particle.
Embodiment three
A preparation method for Suaeda salsa biogenic salt, described preparation method comprises the following steps:
(1) clean: with water by the rinsing repeatedly of fresh Suaeda salsa, until by Suaeda salsa rinsed clean, not containing impurity such as silts;
(2) press juice: stem and the leaf of getting the Suaeda salsa after rinsed clean, segment, utilizes squeezer to carry out pressure juice, obtains stoste and solid slag, by stoste under 5000rpm centrifugal 10 minutes, gets supernatant;
(3) lixiviate: be placed in container by above-mentioned solid slag, adds the water soaking 35 minutes of solid slag weight 12 times, heats 12 minutes, suction filtration while hot at 75 DEG C, collects extract, is cooled to room temperature, for subsequent use;
(4) removal of impurities: merge above-mentioned stoste and extract, adding mass concentration is 70% ethanol, soaks 1.5 hours at 38 DEG C, leaves standstill, and removing upper solution, obtains lower floor's solution;
(5) concentrated, crystallization: concentrated by above-mentioned lower floor solution at 55 DEG C, spraying dry, obtains crystalline particle.
Embodiment four
A preparation method for Suaeda salsa biogenic salt, described preparation method comprises the following steps:
(1) clean: with water by the rinsing repeatedly of fresh Suaeda salsa, until by Suaeda salsa rinsed clean, not containing impurity such as silts;
(2) press juice: stem and the leaf of getting the Suaeda salsa after rinsed clean, segment, utilizes squeezer to carry out pressure juice, obtains stoste and solid slag, by stoste under 5000rpm centrifugal 15 minutes, gets supernatant;
(3) lixiviate: be placed in container by above-mentioned solid slag, adds the water soaking 40 minutes of solid slag weight 15 times, heats 10 minutes, suction filtration while hot at 80 DEG C, collects extract, is cooled to room temperature, for subsequent use;
(4) removal of impurities: merge above-mentioned stoste and extract, adding mass concentration is 70% ethanol, soak 1 hour at 40 DEG C, leave standstill, removing upper solution, obtain lower floor's solution, be 70% ethanol washing 3-5 time by lower floor's solution mass concentration, obtain cleaning mixture, by cleaning mixture stratification, removing upper strata cleaning solution, obtains lower floor's cleaning solution;
(5) concentrated, crystallization: concentrated by above-mentioned lower floor solution at 60 DEG C, spraying dry, obtains crystalline particle.
Embodiment five
A preparation method for Suaeda salsa biogenic salt, described preparation method comprises the following steps:
(1) clean: with water by the rinsing repeatedly of fresh Suaeda salsa, until by Suaeda salsa rinsed clean, not containing impurity such as silts;
(2) press juice: stem and the leaf of getting the Suaeda salsa after rinsed clean, segment, utilizes squeezer to carry out pressure juice, obtains stoste and solid slag, by stoste under 5000rpm centrifugal 15 minutes, gets supernatant;
(3) lixiviate: be placed in container by above-mentioned solid slag, adds the water soaking 40 minutes of solid slag weight 15 times, heats 10 minutes, suction filtration while hot at 80 DEG C, collects extract, is cooled to room temperature, for subsequent use;
(4) removal of impurities: merge above-mentioned stoste and extract, adding mass concentration is 70% ethanol, soaks 1 hour at 40 DEG C, leaves standstill, removing upper solution, obtain lower floor's solution, be 70% ethanol washing 3-5 time by lower floor's solution mass concentration, obtain cleaning mixture, by cleaning mixture stratification, removing upper strata cleaning solution, obtains lower floor's cleaning solution, by lower floor's cleaning solution through 0.45 μm of filtering with microporous membrane;
(5) concentrated, crystallization: concentrated by above-mentioned lower floor solution at 60 DEG C, spraying dry, obtains crystalline particle.
Divide the inorganic salts in the Suaeda salsa biogenic salt of above-described embodiment one to embodiment five preparation and measure, its measurement result is as follows:
Table 1
As can be seen from the table, the Suaeda salsa biogenic salt that the present invention obtains, its potassium salts content is a little more than sodium salt content, belong to Cardia Salt, and wherein containing a large amount of vitamin and amino acid, it is nutritious, has good health value and higher economic value added, and its technique is simple, be easy to operation.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. a preparation method for Suaeda salsa biogenic salt, is characterized in that, described preparation method comprises the following steps:
(1) clean: with water by fresh Suaeda salsa rinsed clean repeatedly;
(2) press juice: stem and the leaf of getting the Suaeda salsa after rinsed clean, segment, carries out pressure juice, obtains stoste and solid slag;
(3) lixiviate: be placed in container by described solid slag, adds described solid slag weight 10-15 water soaking 30-40 minute doubly, heats 10-15 minute, while hot suction filtration at 70-80 DEG C, collect extract, be cooled to room temperature, for subsequent use;
(4) removal of impurities: merge described stoste and extract, adding mass concentration is 70% ethanol, at 35-40 DEG C, soak 1-2 hour, leaves standstill, and removing upper solution, obtains lower floor's solution;
(5) concentrated, crystallization: at 50-60 DEG C, described lower floor solution is concentrated, dry, obtain crystalline particle.
2. the preparation method of a kind of Suaeda salsa biogenic salt as claimed in claim 1, is characterized in that: in step (2), by described stoste centrifugal 10-15 minute under 5000rpm, gets supernatant.
3. the preparation method of a kind of Suaeda salsa biogenic salt as claimed in claim 1, it is characterized in that: in step (4), be 70% ethanol washing 3-5 time by described lower floor solution mass concentration, obtain cleaning mixture, by described cleaning mixture stratification, removing upper strata cleaning solution, obtains lower floor's cleaning solution.
4. the preparation method of a kind of Suaeda salsa biogenic salt as claimed in claim 3, is characterized in that: by described lower floor cleaning solution through 0.45 μm of filtering with microporous membrane.
5. the preparation method of a kind of Suaeda salsa biogenic salt as claimed in claim 1, it is characterized in that: in step (5), described drying is spraying dry.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105876738A (en) * | 2016-04-19 | 2016-08-24 | 王胜 | Vegetable salt and method for preparing suaeda salsa vegetable salt by adopting air-drying crystallization technology |
| CN105876739A (en) * | 2016-04-19 | 2016-08-24 | 王胜 | Vegetable salt and method for preparing suaeda salsa vegetable salt by adopting biological heavy-metal-removing technology utilizing chitosan |
| CN105901649A (en) * | 2016-05-03 | 2016-08-31 | 王胜 | Plant salt containing ginkgo extracts and preparation method thereof |
| CN105901639A (en) * | 2016-04-19 | 2016-08-31 | 王胜 | A plant salt and a method of extracting the plant salt from suaeda salsa by adopting an ultrasonic-assisted hot extraction process |
| CN105901642A (en) * | 2016-04-19 | 2016-08-31 | 王胜 | An alkaline plant salt and a method of extracting the alkaline plant salt from suaeda salsa by adopting cellulase and compound proteases |
| CN105901643A (en) * | 2016-04-19 | 2016-08-31 | 王胜 | A plant salt and a method of extracting the plant salt high in amino acids from suaeda salsa by adopting compound proteases |
| CN106722772A (en) * | 2016-12-28 | 2017-05-31 | 山东博华高效生态农业科技有限公司 | A kind of frost flower plant salt and its preparation technology |
| CN107997110A (en) * | 2017-10-25 | 2018-05-08 | 山东胜景旅游发展有限公司 | A kind of Suaeda salsa biology salt production process |
| CN111772157A (en) * | 2020-07-14 | 2020-10-16 | 中科蓬辉(北京)环境科技有限公司 | Biological salt and preparation method thereof |
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| CN106722772A (en) * | 2016-12-28 | 2017-05-31 | 山东博华高效生态农业科技有限公司 | A kind of frost flower plant salt and its preparation technology |
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| CN111772157A (en) * | 2020-07-14 | 2020-10-16 | 中科蓬辉(北京)环境科技有限公司 | Biological salt and preparation method thereof |
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