CN105029347A - High-nutrient plant salt with various flavoring functions and preparation method thereof - Google Patents
High-nutrient plant salt with various flavoring functions and preparation method thereof Download PDFInfo
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- CN105029347A CN105029347A CN201510458550.2A CN201510458550A CN105029347A CN 105029347 A CN105029347 A CN 105029347A CN 201510458550 A CN201510458550 A CN 201510458550A CN 105029347 A CN105029347 A CN 105029347A
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Abstract
The invention discloses high-nutrient plant salt with various flavoring functions and a preparation method thereof. The high-nutrient plant salt is prepared through the following steps: taking suaeda salsa and Chinese parsley as raw materials, scalding, grinding, mixing, extracting by using an organic solvent under the ultrasonic vibration condition, concentrating and purifying the extracting solution, removing the solvent, and then, performing vacuum spray-drying. The high-nutrient plant salt contains sodium chloride, potassium chloride, chlorophyll, amino acid, vitamins, carotene, microelements including calcium, phosphor, iron, zinc and selenium, as well as various nutrient substances such as mannitol, decanal and coriandrol, has the functions of various condiments, and can replace table salt and monosodium glutamate for use. The method facilitates the implementation of industrialized production, realizes the maximized development and utilization of the suaeda salsa, and has quite high research value.
Description
Technical field
The present invention relates to plant salt technical field, be specifically related to a kind of pure plant extract, have concurrently the technology of high nutrient plant salt of multi-condiment effect.
Background technology
The salt that the mankind eat for a long time is inorganic matter substantially, the demand of human body self to inorganic salts can only be met, be difficult to adapt to because living standard promotes the mankind that cause to the demand of several functions food, particularly salt is in the market sodium chloride, be generally and in sea salt, add KI and the iodizedsalt obtained, too high Na
+take in and all have obvious negative effect to the blood pressure, blood fat etc. of human body.Current people there has been darker understanding to this problem, embody the demand of Cardia Salt more and more stronger.And plant salt extracts, meets the requirement of Cardia Salt and has several mineral materials trace element group from plant organism simultaneously, various element ratio meets the one balance salt of human body requirement, regulates and metabolism and health have the Novel edible salt of certain promotion to the Equilibrium of Trace Elements of human body, function.
Suaeda salsa growth, at wilderness beach, away from pollution, substantially belongs to wild, does not use chemical fertilizer and agricultural chemicals, therefore environmental protection in growth course.Its young stem and leaf rich in nutrition content, delicious flavour is the pollution-free pollution-free food enjoying favor.Analysis of experiments find, stem and leaf of S. salsa (L.) Pall nutritional labeling is complete, total salt quantity up to 4.54%, in anion, Cl
-account for 47.14% of total salt, in cation, Mg
2+account for 20.04% of total salt, except being rich in fat, protein, the content of mineral matter, trace element and vitamin is also very abundant.In its fresh and tender cauline leaf, protein content accounts for 40% of dry, suitable with soybean; Containing abundant amino acid, the fresh taper of every 100g divides containing carrotene 1.75mg, vitamin B2 20.10mg, vitamin C 78mg; Also containing other trace element, as calcium, phosphorus, iron, zinc, selenium etc., wherein many indexs are all higher than spirulina.In Suaeda salsa, calcium, phosphorus, iron and riboflavin content are all higher than vegetables such as spinach, tomato and carrots; Vitamin C content higher than or be equivalent to general vegetables; Vitamin B2 content is 5-8 times of general vegetables; More general food is measured high about 10 times containing Se.The analysis of wild Suaeda salsa is found, the trace element containing 9 kinds of needed by human in Suaeda salsa juice, wherein calcium, magnesium, zinc, iron, nickel rich content, and be rich in chlorophyll.
Suaeda salsa is as the raw industrial crops of a kind of novel salt, and not only at saline and alkaline beach large area self-sow, the Coastal beach establishing in large scale that also should not be able to grow at common plant, raw material sources are extensive, with low cost.Little to the deep processing research of Suaeda salsa at present, eat mainly as vegetables, come out as extracting the report preparing plant salt although have at present, such as number of patent application is the patent of invention of 200610013360.0, disclose with Suaeda salsa is the technology that plant salt prepared by raw material, its method is roughly: by Suaeda salsa wash clean, squeeze out juice, juice filter after get supernatant, supernatant is obtained Suaeda salsa juice stoste through ultrafiltration membrance filter, namely the vacuum drying of Suaeda salsa juice stoste is obtained Suaeda salsa plant salt.The extraction of the method to plant salt still comes with some shortcomings, and does not fully extract and utilize the idiotrophic element of Suaeda salsa.
As everyone knows, containing a large amount of chlorophyll in Suaeda salsa, chlorophyll is a kind of fat-soluble pigment extensively existed in green plants, is the natural colouring matter that China and most countries allow to use.Modern study shows, chlorophyll have hematopoiesis, anti-inflammatory, antiulcer, anti-cholesterol, provide accumulate in vitamin, removing body toxin, opposing radiation, regulate blood sugar concentration, disease-resistantly the effect such as to keep fit, it is the large health-care good product in modern people life, chlorophyllous molecule and the haemoglobin molecule of human body are very structurally similar, unique differences be exactly respective core is magnesium atom and iron atom.Therefore, drink chlorophyll can be very helpful to puerpera and because of the unexpected person of losing blood.But chlorophyll is a kind of organic matter, water insoluble, therefore, number of patent application is that most of chlorophyll is not fully extracted utilization only containing less free chlorophyll in the plant salt prepared in the patent of invention of 200610013360.0.
The nutriment such as a large amount of vitamins, trace element that Suaeda salsa plant salt contains because of Suaeda salsa self, to compare inorganic salts and other plant salt, there is more abundant nutritive value, and because growth is at Coastal beach, there is special seafood mouthfeel.Therefore, to the exploitation of Suaeda salsa plant salt, there is boundless future and value.
Summary of the invention
First technical problem to be solved by this invention is: the deficiency existed for prior art, a kind of high nutrient plant salt having multi-condiment effect concurrently is provided, the primary raw material Suaeda salsa wide material sources, with low cost used, add the distinctive fragrance of caraway, be mixed with the plant salt obtained not only to be of high nutritive value, containing multivitamin and trace element, and have multi-condiment effect concurrently, improve the value of exploiting and utilizing of Suaeda salsa.
Second technical problem to be solved by this invention is: the deficiency existed for prior art, a kind of preparation method having the high nutrient plant salt of multi-condiment effect concurrently is provided, the primary raw material Suaeda salsa wide material sources, with low cost that the method uses, add the distinctive fragrance of caraway, the plant salt be mixed with not only is of high nutritive value, containing multivitamin and trace element, and have multi-condiment effect concurrently, improve the value of exploiting and utilizing of Suaeda salsa.
For solving above-mentioned first technical problem, technical scheme of the present invention is:
A kind of high nutrient plant salt having multi-condiment effect concurrently, described high nutrient plant salt is that raw material prepares by Suaeda salsa and caraway, containing sodium chloride, potassium chloride, chlorophyll, amino acid, vitamin, carrotene in described high nutrient plant salt, and microelements of calcium, phosphorus, iron, zinc, selenium; Also containing mannitol, positive certain herbaceous plants with big flowers aldehyde and coriandrol.
For solving above-mentioned second technical problem, technical scheme of the present invention is:
A kind of high nutrient plant salt having multi-condiment effect concurrently and preparation method thereof, is characterized in that comprising the following steps:
(1) get the raw materials ready: the Suaeda salsa choosing growth animated period, get tender stem and blade, first use the brewed in hot water 2 ~ 5 minutes of 75 ~ 80 DEG C, then with warm water washing once, remove surface moisture with centrifuge; Choose fresh caraway, get stem and leaf part, first use the brewed in hot water 2 ~ 5 minutes of 75 ~ 80 DEG C, then with warm water washing once, remove surface moisture with centrifuge.
(2) batch mixing: the stem and leaf of S. salsa (L.) Pall after dehydration and caraway cauline leaf are shredded respectively, and be milled to pulpous state with grater respectively, is that 7 ~ 9:3 ~ 1 mixes according to the weight ratio of Suaeda salsa slurry and caraway slurry, and stirs.
(3) alcohol extracting: add Extraction solvent in slurry upon mixing, addition is 2 ~ 5 times of slurry, extraction is shaken 0.5 ~ 1 hour under ultrasonic vibration condition, Separation of Solid and Liquid, the solid material that separation obtains is added again the Extraction solvent of 2 ~ 5 times of described solid material, again under ultrasonic vibration condition, shake extraction 0.5 ~ 1 hour, Separation of Solid and Liquid, the liquid material that twice separation obtains is mixed to get extract.
(4) concentrated purification: use filter press to filter described extract, filtrate is carried out rectification under vacuum, reclaim Extraction solvent, and then Vacuum Concentration is to 1/3 ~ 1/4 of original volume, obtains concentrate.
(5) plant salt preparation: described concentrate is 60 ~ 80 DEG C in temperature and carries out vacuum spray drying, have the high nutrient plant salt of multi-condiment effect described in obtaining concurrently.
As the preferred technical scheme of one, described Extraction solvent is ethanol, acetone or dimethyl formamide.
As one preferred technical scheme further, the mass concentration of described ethanol is 70 ~ 80%, and the mass concentration of described acetone is 40 ~ 70%, and the mass concentration of described dimethyl formamide is 30 ~ 60%.
As the preferred technical scheme of one, filtering accuracy when using filter press to filter described extract is greater than 200 orders.
As the preferred technical scheme of one, the temperature in described step (4) during Vacuum Concentration is 40 ~ 80 DEG C, and vacuum during described Vacuum Concentration is 0.02 ~ 0.05Mpa.
As the preferred technical scheme of one, the temperature in described step (4) during rectification under vacuum is 40 ~ 80 DEG C.
Owing to have employed technique scheme, the invention has the beneficial effects as follows:
The high nutrient plant salt having multi-condiment effect concurrently of the present invention, described high nutrient plant salt is that raw material prepares by Suaeda salsa and caraway, containing sodium chloride, potassium chloride, chlorophyll, amino acid, vitamin, carrotene in described high nutrient plant salt, and microelements of calcium, phosphorus, iron, zinc, selenium; Also containing mannitol, positive certain herbaceous plants with big flowers aldehyde and coriandrol, the primary raw material Suaeda salsa wide material sources, with low cost used, add the distinctive fragrance of caraway, be mixed with the plant salt obtained not only to be of high nutritive value, common table salt and monosodium glutamate can be substituted simultaneously, improve the value of exploiting and utilizing of Suaeda salsa.
The present invention chooses the Suaeda salsa of growth animated period when getting the raw materials ready, the content of Suaeda salsa Determination of Chlorophyll and salt is the highest, extract the chlorophyll that obtains and plant salt yield high, Suaeda salsa and caraway are first used the brewed in hot water 2 ~ 5 minutes of 75 ~ 80 DEG C, again with warm water washing once, remove surface moisture with centrifuge, the hot water of 75 ~ 80 DEG C not only can make softening of the cell wall be easier to the extraction of back, and can not destroy chlorophyll wherein; Therefore being milled to pulpous state when using alcohol extract with grater, extracting under being extracted in ultrasonic vibration condition simultaneously, improve the dissolution rate of chlorophyll, salinity and other nutriments, and the chlorophyll in Suaeda salsa and caraway can not be destroyed; Temperature when concentrated purification and vacuum spray drying is all no more than 80 DEG C, all can not destroy chlorophyllous structure.
The present invention with Suaeda salsa and caraway for raw material extracts the plant salt obtained containing chlorophyllous high nutritive value simultaneously, raw material sources are extensive, low production cost, the plant salt prepared is rich in chlorophyll, amino acid, multivitamin, and be rich in calcium, phosphorus, iron, zinc, selenium and other trace elements, not only low sodium but also rich in nutrition content, especially contain mannitol specific to caraway, positive certain herbaceous plants with big flowers aldehyde and coriandrol, therefore there is the effect of multi-condiment material, salt and monosodium glutamate can be substituted simultaneously.The inventive method is easy to realize suitability for industrialized production, achieves and develops the maximization of Suaeda salsa, very have researching value.
Detailed description of the invention
Below in conjunction with specific embodiment, set forth the present invention further.Should be understood that these embodiments are only not used in for illustration of the present invention to limit the scope of the invention.In addition should be understood that those skilled in the art can make various changes or modifications the present invention, and these equivalent form of values fall within the application's appended claims limited range equally after the content of having read the present invention's instruction.
Embodiment 1
Have a high nutrient plant salt for multi-condiment effect concurrently, described high nutrient plant salt is that raw material prepares by Suaeda salsa and caraway, containing the sodium chloride of 32.88wt%, the potassium chloride of 22.5wt% in described high nutrient plant salt; Chlorophyllous content is 4.3g/Kg, and the total content of amino acid and vitamin, carrotene is 39.63wt%, and the content of mannitol, positive certain herbaceous plants with big flowers aldehyde and coriandrol is 1.58g/Kg, and the content of microelements of calcium, phosphorus, iron, zinc, selenium is 0.47g/Kg.
Embodiment 2
(1) get the raw materials ready: the Suaeda salsa choosing growth animated period, get tender stem and blade, first use the brewed in hot water 2 minutes of 78 DEG C, then with warm water washing once, remove surface moisture with centrifuge; Choose fresh caraway, get stem and leaf part, first use the brewed in hot water 2 minutes of 78 DEG C, then with warm water washing once, remove surface moisture with centrifuge.
(2) batch mixing: the stem and leaf of S. salsa (L.) Pall after dehydration and caraway cauline leaf are shredded respectively, and be milled to pulpous state with grater respectively, is 7:3 mixing according to the weight ratio of Suaeda salsa slurry and caraway slurry, and stirs.
(3) alcohol extracting: add Extraction solvent in slurry upon mixing, addition is 3 times of slurry, extraction is shaken 0.5 hour under ultrasonic vibration condition, Separation of Solid and Liquid, the solid material that separation obtains is added again the Extraction solvent of 3 times of described solid material, again under ultrasonic vibration condition, shake extraction 0.5 hour, Separation of Solid and Liquid, the liquid material that twice separation obtains is mixed to get extract.
(4) concentrated purification: use filter press to filter described extract, filtrate is carried out rectification under vacuum, reclaim Extraction solvent, and then Vacuum Concentration is to 1/3 of original volume, obtains concentrate.
(5) plant salt preparation: described concentrate is 70 DEG C in temperature and carries out vacuum spray drying, have the high nutrient plant salt of multi-condiment effect described in obtaining concurrently.
Embodiment 3
(1) get the raw materials ready: the Suaeda salsa choosing growth animated period, get tender stem and blade, first use the brewed in hot water 3 minutes of 75 DEG C, then with warm water washing once, remove surface moisture with centrifuge; Choose fresh caraway, get stem and leaf part, first use the brewed in hot water 3 minutes of 75 DEG C, then with warm water washing once, remove surface moisture with centrifuge.
(2) batch mixing: the stem and leaf of S. salsa (L.) Pall after dehydration and caraway cauline leaf are shredded respectively, and be milled to pulpous state with grater respectively, is 9:1 mixing according to the weight ratio of Suaeda salsa slurry and caraway slurry, and stirs.
(3) alcohol extracting: add the ethanol that mass concentration is 75% in slurry upon mixing, addition is 4 times of slurry, extraction is shaken 0.5 hour under ultrasonic vibration condition, Separation of Solid and Liquid, the solid material that separation obtains is added again the ethanol of 75% of 3.5 times of described solid material, again under ultrasonic vibration condition, shake extraction 0.5 hour, Separation of Solid and Liquid, the liquid material that twice separation obtains is mixed to get extract.
(4) concentrated purification: use filter press to filter described extract, filtering accuracy 220 order, filtrate is carried out rectification under vacuum, reclaim ethanol, and then Vacuum Concentration is to 1/4 of original volume, obtains concentrate, temperature during rectification under vacuum is 75 DEG C, temperature during Vacuum Concentration is 70 DEG C, and vacuum during described Vacuum Concentration is 0.05Mpa.
(5) plant salt preparation: described concentrate is 70 DEG C in temperature and carries out vacuum spray drying, have the high nutrient plant salt of multi-condiment effect described in obtaining concurrently.
Embodiment 4
(1) get the raw materials ready: the Suaeda salsa choosing growth animated period, get tender stem and blade, first use the brewed in hot water 2 minutes of 76 DEG C, then with warm water washing once, remove surface moisture with centrifuge; Choose fresh caraway, get stem and leaf part, first use the brewed in hot water 2 minutes of 76 DEG C, then with warm water washing once, remove surface moisture with centrifuge.
(2) batch mixing: the stem and leaf of S. salsa (L.) Pall after dehydration and caraway cauline leaf are shredded respectively, and be milled to pulpous state with grater respectively, is 8:2 mixing according to the weight ratio of Suaeda salsa slurry and caraway slurry, and stirs.
(3) alcohol extracting: add the acetone that mass concentration is 60% in slurry upon mixing, addition is 3 times of slurry, extraction is shaken 0.6 hour under ultrasonic vibration condition, Separation of Solid and Liquid, the solid material that separation obtains is added again the acetone of 60% of 3 times of described solid material, again under ultrasonic vibration condition, shake extraction 0.6 hour, Separation of Solid and Liquid, the liquid material that twice separation obtains is mixed to get extract.
(4) concentrated purification: use filter press to filter described extract, filtering accuracy 220 order, filtrate is carried out rectification under vacuum, reclaim acetone, and then Vacuum Concentration is to 1/4 of original volume, obtains concentrate, temperature during rectification under vacuum is 60 DEG C, temperature during Vacuum Concentration is 75 DEG C, and vacuum during described Vacuum Concentration is 0.04Mpa.
(5) plant salt preparation: described concentrate is 75 DEG C in temperature and carries out vacuum spray drying, have the high nutrient plant salt of multi-condiment effect described in obtaining concurrently.Containing the sodium chloride of 30.54wt%, the potassium chloride of 22.0wt% in the high nutrient plant salt prepared, chlorophyllous content is 4., 28g/Kg, the total content of amino acid and vitamin, carrotene is 40.35wt%, the content of mannitol, positive certain herbaceous plants with big flowers aldehyde and coriandrol is 1.90g/Kg, and the content of microelements of calcium, phosphorus, iron, zinc, selenium is 0.55g/Kg.
Claims (7)
1. one kind has the high nutrient plant salt of multi-condiment effect concurrently, it is characterized in that: described high nutrient plant salt is that raw material prepares by Suaeda salsa and caraway, containing sodium chloride, potassium chloride, chlorophyll, amino acid, vitamin, carrotene in described high nutrient plant salt, and microelements of calcium, phosphorus, iron, zinc, selenium; Also containing mannitol, positive certain herbaceous plants with big flowers aldehyde and coriandrol.
2. have a preparation method for the high nutrient plant salt of multi-condiment effect concurrently, it is characterized in that comprising the following steps:
(1) get the raw materials ready: the Suaeda salsa choosing growth animated period, get tender stem and blade, first use the brewed in hot water 2 ~ 5 minutes of 75 ~ 80 DEG C, then with warm water washing once, remove surface moisture with centrifuge; Choose fresh caraway, get stem and leaf part, first use the brewed in hot water 2 ~ 5 minutes of 75 ~ 80 DEG C, then with warm water washing once, remove surface moisture with centrifuge;
(2) batch mixing: the stem and leaf of S. salsa (L.) Pall after dehydration and caraway cauline leaf are shredded respectively, and be milled to pulpous state with grater respectively, is that 7 ~ 9:3 ~ 1 mixes according to the weight ratio of Suaeda salsa slurry and caraway slurry, and stirs;
(3) alcohol extracting: add Extraction solvent in slurry upon mixing, addition is 2 ~ 5 times of slurry, extraction is shaken 0.5 ~ 1 hour under ultrasonic vibration condition, Separation of Solid and Liquid, the solid material that separation obtains is added again the Extraction solvent of 2 ~ 5 times of described solid material, again under ultrasonic vibration condition, shake extraction 0.5 ~ 1 hour, Separation of Solid and Liquid, the liquid material that twice separation obtains is mixed to get extract;
(4) concentrated purification: use filter press to filter described extract, filtrate is carried out rectification under vacuum, reclaim Extraction solvent, and then Vacuum Concentration is to 1/3 ~ 1/4 of original volume, obtains concentrate;
(5) plant salt preparation: described concentrate is 60 ~ 80 DEG C in temperature and carries out vacuum spray drying, have the high nutrient plant salt of multi-condiment effect described in obtaining concurrently.
3. a kind of preparation method having the high nutrient plant salt of multi-condiment effect concurrently as claimed in claim 2, is characterized in that: described Extraction solvent is ethanol, acetone or dimethyl formamide.
4. a kind of preparation method having the high nutrient plant salt of multi-condiment effect concurrently as claimed in claim 3, it is characterized in that: the mass concentration of described ethanol is 70 ~ 80%, the mass concentration of described acetone is 40 ~ 70%, and the mass concentration of described dimethyl formamide is 30 ~ 60%.
5. a kind of preparation method having the high nutrient plant salt of multi-condiment effect concurrently as claimed in claim 2, is characterized in that: filtering accuracy when using filter press to filter described extract is greater than 200 orders.
6. a kind of preparation method having the high nutrient plant salt of multi-condiment effect concurrently as claimed in claim 2, it is characterized in that: the temperature in described step (4) during Vacuum Concentration is 40 ~ 80 DEG C, and vacuum during described Vacuum Concentration is 0.02 ~ 0.05Mpa.
7. a kind of preparation method having the high nutrient plant salt of multi-condiment effect concurrently as claimed in claim 2, is characterized in that: the temperature in described step (4) during rectification under vacuum is 40 ~ 80 DEG C.
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