CN102443494B - Washing agent specially used for female underpants and its preparation method - Google Patents
Washing agent specially used for female underpants and its preparation method Download PDFInfo
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- CN102443494B CN102443494B CN 201010502445 CN201010502445A CN102443494B CN 102443494 B CN102443494 B CN 102443494B CN 201010502445 CN201010502445 CN 201010502445 CN 201010502445 A CN201010502445 A CN 201010502445A CN 102443494 B CN102443494 B CN 102443494B
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Abstract
The invention belongs to a washing agent, concretely relates to the washing agent specially used for female underpants with the characteristics of stable product performance, long storage life, strong multienzyme decomposition capability on organic matter, good effect for cleaning the contaminants on the female underpants, bacteriostasis and disinfection, and its preparation method. The washing agent comprises the following raw materials by weight part: 50-118 parts of surfactant, 10-34 parts of propylene glycol, 10-34 parts of triethanolamine, 1 part of ethylparaben, 12-40 parts of enzyme stabilizing agent, 1-26 parts of sodium hydrosulphite, 0.04-2 parts of calcium chloride, 2-25 parts of sodium citrate, 4-20 parts of citric acid, 2-15 parts of protease, 3-10 parts of biological enzyme used for compound and 11-238 parts of deionized water; has the advantages of good hard water resistance, nontoxicity and innocuousness, flexibility, antistatic property and shrink resistance, and is capable of obviously increasing the softness of the washed cotton fabric, so that the fabric is soft and the color is white, the washing agent has inhibition effects for a plurality of bacteria and mildew, and the cleanness and sanitation of the underpants can be ensured.
Description
Technical field
The invention belongs to washing composition, be specifically related to that a kind of product performance are stable, the shelf lives long, multienzyme decomposing organic matter ability is strong, clean underpants for women special purpose detergent of the effective and antibacterial disinfection of dirt on the underpants for women and preparation method thereof.
Background technology
The application of enzyme in Betengent product is one of Important Techmical Progress in the detergent industry evolution.What the initial stage used is single proteolytic enzyme, has developed successively later on amylase, cellulase, fatty application of enzymes, and the synergistic application of two or more enzyme.These development make washing composition over-all properties be improved significantly, quality product has had large increase.But enzyme itself is protein structure, enzyme is in active condition in liquid washing agent, proteolytic enzyme can decompose other enzymes of destruction, even decomposition of protein enzyme self, therefore other enzymes can not be composite in same system with proteolytic enzyme, even it is also shorter to contain the liquid washing agent storage life of single proteolytic enzyme.And with the multienzyme detergent that solid particulate exists, do not interfere with each other between the multiple prozyme, be beneficial to storage, but will first the solid particulate dissolving that contains multienzyme be scattered in the water when using, discharge enzyme, produce actively, give like this to operate and bring a lot of inconvenience.
The cleaning of underpants for women has brought a lot of troubles to numerous women compatriot in the daily life, the bloodstain that particularly is stained with between holiday and usually be attached to secretory product such as leukorrhea on the underpants, these spots are difficult to clean up, and as easy as rolling off a logly stay yellow vestige, and are particularly evident on the cotton underpants.Usually wash underpants for women with washing powder, tend to cause spot residual, and because harmful chemicals such as the phosphorus that washing powder contains, benzene, lead are difficult for thoroughly removing, the clothing of residual these nuisances of long-time dress, can cause pachylosis, peel, itch, seriously then can cause the diseases such as contact dermatitis.And residual sodium alkyl benzene sulfonate easily causes the women to suffer from vaginitis, mammary cancer after the washing powder cleaning, is hysteromyoma, Infertility, gynopathic arch-criminal occur.
Summary of the invention
The object of the invention is to overcome defective of the prior art and provide that a kind of product performance are stable, the shelf lives long, multienzyme decomposing organic matter ability is strong, clean underpants for women special purpose detergent of the effective and antibacterial disinfection of dirt on the underpants for women and preparation method thereof.
The object of the present invention is achieved like this: formulated according to parts by weight by following raw material: tensio-active agent 50-118 part, propylene glycol 10-34 part, trolamine 10-34 part, 1 part of ethyl p-hydroxybenzoate, enzyme stabilizers 12-40 part, S-WAT 1-26 part, calcium chloride 0.04-2 part, Trisodium Citrate 2-25 part, citric acid 4-20 part, proteolytic enzyme 2-15 part are composite with biological enzyme 3-10 part and deionized water 11-238 part.Described tensio-active agent is selected from fatty alcohol-polyoxyethylene ether, alkylsulfonate and alkyl glycoside and their mixture.Described enzyme stabilizers is selected from borax and sodium acetate and their mixture.Describedly compositely be selected from amylase with biological enzyme, cellulase and lipase and their mixture.
The preparation method of underpants for women special purpose detergent of the present invention comprises the steps:
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added tensio-active agent mix;
C, deionized water is heated to 30 ℃-40 ℃;
D, will the deionized water after the heating among the step c add fully dissolving in the mixture that adds among the step b behind the tensio-active agent;
E, the mixture that adds in the steps d behind the deionized water dissolving is added enzyme stabilizers, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, add proteolytic enzyme and compositely stir with biological enzyme being adjusted to neutral solution in the step g, finished product.
The present invention and Business Name are: the Doraemon woman pants washing composition that Shanghai Doraemon makeup company limited produces compares.
1, kapillary identification method
The first step: get 1mL the present invention and 1mL contrast product and be positioned over respectively in two beakers, in two beakers, add respectively ordinary tap water and be diluted to 500 times; Second step: the fresh rabbit blood of kapillary absorption equivalent of getting altogether 100 is for subsequent use; The 3rd step: 100 among the step b kapillaries of drawing fresh rabbit blood are divided into identical two groups of quantity put into respectively described two beakers of step a; The 4th step: described two beakers of step c were used respectively ultrasonic cleaning 10 minutes.
Wash result is: it is 38 that the present invention cleans the pipe number, and contrast product is cleaned several 9 of pipe.
2, standard soiled cloth method
The first step: get 1mL the present invention and 1mL contrast product and be positioned over respectively in two beakers, in two beakers, add ordinary tap water and be diluted to 400 times; Second step: the cotton calico is cut into the rectangle calico of a wide 5cm of long 10cm, rectangle cotton calico is immersed in the fresh rabbit blood, take out after 5 minutes and dry; The 3rd step: the rectangle cotton calico after drying among the step b is cut into the square of the wide 5cm of two block length 5cm, puts into respectively described two beakers of step a; The 4th step: described two beakers of step c were used respectively ultrasonic cleaning 10 minutes; The 5th step: compare after the cotton calico of the wide 5cm of two block length 5cm dried.
Cleaning performance: thoroughly to clean be 3 minutes to bloodstain on the cotton, and to clean fully be 2 minutes to bloodstain on the cotton, on the cotton bloodstain with clean before not too big difference be 1 minute
Wash result is: the present invention must be divided into 3 minutes, and contrast product must be divided into 1 minute.
3, washing method in kind
The first step: collect 20 of underpants speckling with women's menstrual blood; Second step: get 20mL the present invention and 20mL contrast product and be positioned over respectively in two small washing machines, add respectively ordinary tap water in two small washing machines and be diluted to 400 times; The 3rd step: with 20 of the underpants of the women's menstrual blood among the step a, be divided into two groups of equal amts, put into respectively described two small washing machines of step b; The 4th step: the women's menstrual blood underpants in described two small washing machines of step c were cleaned respectively 10 minutes; The 5th step: 20 women's menstrual blood underpants are dried compare.
Cleaning performance: thoroughly to clean be 3 minutes to bloodstain on the underpants, and to clean fully be 2 minutes to bloodstain on the underpants, on the underpants bloodstain with clean before not too big difference be 1 minute
Wash result is: the present invention must be divided into 26 minutes, and contrast product must be divided into 14 minutes.
The present invention uses propylene glycol, trolamine, S-WAT and enzyme stabilizers can effectively protect the activity of multiple biological enzyme, prevent from decomposing each other destroying, cooperate again the composite cleanup action of kinds of surface promoting agent and the preservative activity of ethyl p-hydroxybenzoate to make the present invention; Product performance of the present invention are stable, the shelf lives is long, and multienzyme decomposing organic matter ability is strong, clean the respond well of dirt on the underpants, the effect of antibacterial sterilization arranged, and bloodstain is had the clean effect of mystery.Neutral pH of the present invention, composition is natural, character is gentle, does not hinder skin and is fit to hand washing.The anti-hard water of the present invention is good, nontoxic and have the performances such as flexibility, static resistance and shrink resistance concurrently, can increase obviously that to wash having of rear cotton fabric soft, and fabric sofetening and color and luster are brightened.The present invention contains disinfection sanitizer, and various bacteria, mould are all had restraining effect, can guarantee the underpants sanitation and hygiene.The without phosphorus prescription of the present invention, the height environmental protection, biological degradability surpasses 90%.Using only needs when of the present invention the washing composition dilution is got final product, easy to operate, is easy to rinsing.
The present invention is fit to the cleaning of underpants for women, particularly speckles with the underpants of menstruation bloodstain, can increase obviously that to wash having of rear cotton fabric soft, and fabric sofetening, color and luster are brightened.The cleaning that fabric and the medicine equipment of bloodstain are infected with by the applicable equally hospital of the present invention, the cleaning of article such as scalpel, mosquito forceps, medical endoscope.The medical endoscope passage is narrow, use rear owing to be infected with the organism such as blood, mucous membrane tissue, human excrement and urine, and cause obstruction, very difficult when so the washing composition that uses common washing composition or contain single enzyme cleans this type of apparatus, and cleaning performance is bad, and the residual things such as bacterium easily cause infection when reusing.The present invention contains highly active biological enzyme, and plurality of enzymes acts synergistically, and can effectively decompose human secretion, has both reduced the high maintenance service of instruments, reaches better effect in the time of can making again sterilization, avoids occurring superinfection.
Embodiment
The present invention is formulated according to parts by weight by following raw material: tensio-active agent 50-118 part, propylene glycol 10-34 part, trolamine 10-34 part, 1 part of ethyl p-hydroxybenzoate, enzyme stabilizers 12-40 part, S-WAT 1-26 part, calcium chloride 0.04-2 part, Trisodium Citrate 2-25 part, citric acid 4-20 part, proteolytic enzyme 2-15 part are composite with biological enzyme 3-10 part and deionized water 11-238 part.Described tensio-active agent is selected from fatty alcohol-polyoxyethylene ether, alkylsulfonate and alkyl glycoside and their mixture.Described enzyme stabilizers is selected from borax and sodium acetate and their mixture.Describedly compositely be selected from amylase with biological enzyme, cellulase and lipase and their mixture.
The preparation method of underpants for women special purpose detergent of the present invention comprises the steps:
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added tensio-active agent mix;
C, deionized water is heated to 30 ℃-40 ℃;
D, will the deionized water after the heating among the step c add fully dissolving in the mixture that adds among the step b behind the tensio-active agent;
E, the mixture that adds in the steps d behind the deionized water dissolving is added enzyme stabilizers, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, add proteolytic enzyme and compositely stir with biological enzyme being adjusted to neutral solution in the step g, finished product.
Below in conjunction with specific embodiment, further specify the present invention:
Embodiment 1
Fatty alcohol-polyoxyethylene ether 50 grams, propylene glycol 10 grams, trolamine 10 grams, ethyl p-hydroxybenzoate 1 gram, borax 12 grams, S-WAT 1 gram, calcium chloride 0.04 gram, Trisodium Citrate 2 grams, citric acid 4 grams, proteolytic enzyme 2 grams, amylase 3 grams and deionized water 11 grams.
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added fatty alcohol-polyoxyethylene ether mix;
C, deionized water is heated to 30 ℃;
D, will the deionized water after the heating among the step c add fully dissolving in the mixture that adds among the step b after the fatty alcohol-polyoxyethylene ether;
E, the mixture that adds in the steps d behind the deionized water dissolving is added borax, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, neutral solution adds proteolytic enzyme and amylase stirs with being adjusted in the step g, finished product.
Embodiment 2
Alkylsulfonate 84 grams, propylene glycol 22 grams, trolamine 22 grams, 1 part of ethyl p-hydroxybenzoate, sodium acetate 26 grams, S-WAT 13.5 grams, calcium chloride 1.02 grams, Trisodium Citrate 13.5 grams, citric acid 12 grams, proteinase 8 .5 gram, cellulase 6.5 grams and deionized water 124.5 grams.
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added alkylsulfonate mix;
C, deionized water is heated to 35 ℃;
D, will the deionized water after the heating among the step c add fully dissolving in the mixture that adds among the step b behind the alkylsulfonate;
E, the mixture that adds in the steps d behind the deionized water dissolving is added sodium acetate, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, neutral solution adds proteolytic enzyme and cellulase stirs with being adjusted in the step g, finished product.
Embodiment 3
Alkyl glycoside 118 grams, propylene glycol 34 grams, trolamine 34 grams, ethyl p-hydroxybenzoate 1 gram, borax 10 grams, sodium acetate 30 grams, S-WAT 26 grams, calcium chloride 2 grams, Trisodium Citrate 25 grams, citric acid 20 grams, proteolytic enzyme 15 grams, lipase 10 grams and deionized water 238 grams.
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added alkyl glycoside mix;
C, deionized water is heated to 40 ℃;
D, will the deionized water after the heating among the step c add fully dissolving in the mixture that adds among the step b after the alkyl glycoside;
E, the mixture that adds in the steps d behind the deionized water dissolving is added borax, sodium acetate, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, neutral solution adds proteolytic enzyme and lipase stirs with being adjusted in the step g, finished product.
Embodiment 4
Fatty alcohol-polyoxyethylene ether 40 grams, alkylsulfonate 20 grams, alkyl glycoside 110 grams, propylene glycol 60 grams, trolamine 60 grams, ethyl p-hydroxybenzoate 3 grams, borax 30 grams, sodium acetate 10 grams, S-WAT 35 grams, calcium chloride 4 grams, Trisodium Citrate 50 grams, citric acid 40 grams, protease 30 gram, amylase 5 grams, cellulase 4 grams, lipase 11 grams and deionized water 488 grams.
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added fatty alcohol-polyoxyethylene ether, alkylsulfonate and alkyl glycoside mix;
C, deionized water is heated to 32 ℃;
D, will the deionized water after the heating among the step c add among the step b and add fatty alcohol-polyoxyethylene ether, fully dissolving in the mixture after alkylsulfonate and the alkyl glycoside;
E, the mixture that adds in the steps d behind the deionized water dissolving is added borax, sodium acetate, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, will be adjusted in the step g neutral solution add proteolytic enzyme, amylase, and cellulase and lipase stir, finished product.
Embodiment 5
Fatty alcohol-polyoxyethylene ether 1360 grams and alkylsulfonate 1000 grams, propylene glycol 680 grams, trolamine 680 grams, ethyl p-hydroxybenzoate 30 grams, borax 600 grams, sodium acetate 200 grams, S-WAT 520 grams, calcium chloride 40 grams, Trisodium Citrate 500 grams, citric acid 400 grams, protease 3 00 gram, amylase 120 grams, cellulase 70 grams and deionized water 3500 grams.
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added fatty alcohol-polyoxyethylene ether and alkylsulfonate mixes;
C, deionized water is heated to 38 ℃;
D, will the deionized water after the heating among the step c add fully dissolving in the mixture that adds among the step b behind fatty alcohol-polyoxyethylene ether and the alkylsulfonate;
E, the mixture that adds in the steps d behind the deionized water dissolving is added borax, sodium acetate, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, add proteolytic enzyme, amylase and cellulase and stir being adjusted to neutral solution in the step g, finished product.
Embodiment 6
Fatty alcohol-polyoxyethylene ether 50 grams, alkyl glycoside 115 grams, propylene glycol 68 grams, trolamine 60 grams, ethyl p-hydroxybenzoate 3 grams, borax 50 grams, S-WAT 52 grams, calcium chloride 4 grams, Trisodium Citrate 50 grams, citric acid 40 grams, protease 30 gram, amylase 15 grams, lipase 5 grams and deionized water 458 grams.
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added fatty alcohol-polyoxyethylene ether and alkyl glycoside mixes;
C, deionized water is heated to 32 ℃;
D, will the deionized water after the heating among the step c add fully dissolving in the mixture that adds among the step b after fatty alcohol-polyoxyethylene ether and the alkyl glycoside;
E, the mixture that adds in the steps d behind the deionized water dissolving is added borax, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, will be adjusted in the step g neutral solution add proteolytic enzyme, and amylase and lipase stir, finished product.
Embodiment 7
Alkylsulfonate 15 grams, alkyl glycoside 36 grams, propylene glycol 16 grams, trolamine 18 grams, ethyl p-hydroxybenzoate 0.9 gram, borax 10 grams, S-WAT 16 grams, calcium chloride 1.6 grams, Trisodium Citrate 18 grams, citric acid 16 grams, proteolytic enzyme 12.5 grams, cellulase 4 grams, lipase 6 grams and deionized water 130 grams.
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added alkylsulfonate and alkyl glycoside mixes;
C, deionized water is heated to 34 ℃;
D, will the deionized water after the heating among the step c add fully dissolving in the mixture that adds among the step b after alkylsulfonate and the alkyl glycoside;
E, the mixture that adds in the steps d behind the deionized water dissolving is added borax, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, will be adjusted in the step g neutral solution add proteolytic enzyme, and cellulase and lipase stir, finished product.
The present invention is not limited to above-described embodiment.
Claims (2)
1. underpants for women special purpose detergent, it is characterized in that: formulated according to parts by weight by following raw material: tensio-active agent 50-118 part, propylene glycol 10-34 part, trolamine 10-34 part, 1 part of ethyl p-hydroxybenzoate, enzyme stabilizers 12-40 part, S-WAT 1-26 part, calcium chloride 0.04-2 part, Trisodium Citrate 2-25 part, citric acid 4-20 part, proteolytic enzyme 2-15 part are composite with biological enzyme 3-10 part and deionized water 11-238 part;
Described tensio-active agent is selected from fatty alcohol-polyoxyethylene ether, alkylsulfonate and alkyl glycoside and their mixture;
Described enzyme stabilizers is selected from borax and sodium acetate and their mixture;
Describedly compositely be selected from amylase with biological enzyme, cellulase and lipase and their mixture.
2. the method for the preparation of underpants for women special purpose detergent claimed in claim 1 is characterized in that: comprise the steps:
A, be dissolved in ethyl p-hydroxybenzoate in the propylene glycol after;
B, the mixing solutions among the step a is added tensio-active agent mix;
C, deionized water is heated to 30 ℃-40 ℃;
D, will the deionized water after the heating among the step c add fully dissolving in the mixture that adds among the step b behind the tensio-active agent;
E, the mixture that adds in the steps d behind the deionized water dissolving is added enzyme stabilizers, S-WAT successively, evenly mix behind calcium chloride and the Trisodium Citrate;
F, the mixing solutions that obtains among the step e is added trolamine, evenly mix;
G, the mixing solutions behind the adding trolamine among the step f is extremely neutral with the lemon acid for adjusting pH;
H, add proteolytic enzyme and compositely stir with biological enzyme being adjusted to neutral solution in the step g, finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN 201010502445 CN102443494B (en) | 2010-10-11 | 2010-10-11 | Washing agent specially used for female underpants and its preparation method |
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| CN 201010502445 CN102443494B (en) | 2010-10-11 | 2010-10-11 | Washing agent specially used for female underpants and its preparation method |
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| CN102443494B true CN102443494B (en) | 2013-01-23 |
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| CN106590975A (en) * | 2016-12-07 | 2017-04-26 | 四川昂迈维商贸有限公司 | Novel cloth washing water and preparation method thereof |
| CN106753825A (en) * | 2016-12-30 | 2017-05-31 | 江阴市本特塞缪森生命科学研究院有限公司 | A kind of composition for cleaning underwear |
| CN110408481A (en) * | 2019-08-16 | 2019-11-05 | 浙江芬尼奇工贸有限公司 | A kind of clothing stain removal agent and its preparation process |
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| CN1322802A (en) * | 2001-06-04 | 2001-11-21 | 贾发颂 | Phosphate-free liquid detergent and its compounding process |
| CN101096619A (en) * | 2006-06-30 | 2008-01-02 | 天津晶岭电子材料科技有限公司 | Ceramic cleaning fluid |
| CN101041793A (en) * | 2007-04-23 | 2007-09-26 | 北京交通大学 | Automobile windscreen cleaning agent |
| JP5349792B2 (en) * | 2007-12-04 | 2013-11-20 | 花王株式会社 | Liquid detergent composition |
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Granted publication date: 20130123 Termination date: 20161011 |