CN102381910B - Microorganism probiotic implanted nutrient liquid and preparation method of microorganism probiotic implanted nutrient liquid as well as microorganism fertilizer and application of microorganism fertilizer in agriculture and forestry production - Google Patents
Microorganism probiotic implanted nutrient liquid and preparation method of microorganism probiotic implanted nutrient liquid as well as microorganism fertilizer and application of microorganism fertilizer in agriculture and forestry production Download PDFInfo
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- CN102381910B CN102381910B CN201110210426.6A CN201110210426A CN102381910B CN 102381910 B CN102381910 B CN 102381910B CN 201110210426 A CN201110210426 A CN 201110210426A CN 102381910 B CN102381910 B CN 102381910B
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Abstract
The invention discloses a microorganism probiotic implanted nutrient liquid and a preparation method of the microorganism probiotic implanted nutrient liquid as well as a microorganism fertilizer and application of the microorganism fertilizer in agriculture and forestry production, belonging to the fields of agriculture and forestry. The microorganism probiotic implanted nutrient liquid comprises the following components by weight percent: 20-50wt% of organic matters, 1-5wt% of nitrogen, 1-5wt% of potassium and the balance of oxygen and other oxygen-containing compounds. Compared with the prior art, the microorganism probiotic implanted nutrient liquid disclosed by the invention meets the requirement of implanting microorganism probiotics in various fertilizers and is capable of improving the survival rate of a microorganism bactericide in various fertilizers so as to form a multifunctional controlled-release fertilizer.
Description
Technical field
The present invention relates to a kind of microorganism probiotic and implant nutritive medium and preparation method, microbial fertilizer and the application in agricultural and forestry production thereof.
Background technology
Existing market is admixed in chemical fertilizer microbiobacterial agent, is all to take organic-inorganic compound mixed fertilizer as base fertilizer, and more the production of domestic organic-inorganic compound mixed fertilizer adopts bird or domestic animal, straw, municipal wastes etc. to be equipped with nitrogen phosphorus potassium and make.Its nutrient low (15～25%), harmful germ content is high, heavy metal content exceeds standard simultaneously, when implanting plants probiotics, and its surviving rate lower (60～75%).In agricultural production practice, effect is not remarkable, because of fertilizer efficiency not high, need use in addition chemical fertilizer, and affect the quality of agricultural-food: the objectionable impuritiess such as agricultural-food nitrite, harmful germ, heavy metal, pesticide residue exceed standard, the mouthfeel of agricultural-food is poor, agricultural product security is unstable.
Summary of the invention
In present specification, as nothing particularly points out, component ratio is weight ratio.
In present specification, fixed nitrogen series bacillus, Bacillus licheniformis can obtain from the Chinese Academy of Sciences.
One of object of the present invention is to provide a kind of microorganism probiotic and implants nutritive medium, this microorganism probiotic is implanted nutritive medium can meet the needs that various fertilizer is implanted microorganism probiotic, and can improve the surviving rate of microbiobacterial agent in various fertilizer, form Multifunctional controlling release fertilizer.
Microorganism probiotic is implanted a nutritive medium, comprises following component: organic 20～50 wt %, and nitrogen 1～5wt %,
potassium1～5wt %, surplus is oxygen and other oxygenatedchemicals.
As preferably, described organic matter is containing yellow humic acid 5～10 wt %, hymatomalenic acid 14～35 wt % and amino acid/11～5wt %.
As preferably, described organic matter is containing yellow humic acid 8 wt %, hymatomalenic acid 25 wt % and amino acid 3wt %.
Another object of the present invention is to provide the preparation method that a kind of mentioned microorganism probiotic bacterium is implanted nutritive medium, and the method comprises the following steps:
Activation solution A produces: brown coal pulverized, with alkali lye boiling, extracted, and press filtration, then oxygen solution activator oxygen solution activates into activation solution A;
Pulvis B produces: the concentrated concentrate of monosodium glutamate waste liquid heating, filter, and after filtration cakes torrefaction, be ground into pulvis B;
Admixture activation liquid A and pulvis B.
As preferably,
describedbrown coal: alkali=1:1～7, the potassium hydroxide solution that described alkali lye is 5～15%, described boiling is extracted in 80～100 ℃, 1～2h;
The hydrogen peroxide that described oxygen solution activator is 10%, weight ratio is 50:3～5,50～69 ℃ of oxygen solution activation temperatures, oxygen solution soak time 3～4 hours;
Described being dried at 100～120 ℃, 10～60 minutes time of drying;
Described activation solution A and pulvis B ratio of mixture are 1000 parts: 150～300 parts, mixing adds under 35～40 parts of ammonium molybdates and 10 parts of synergy methyl catechol and 5 parts of molasses and completes at 40～60 ℃.
As preferably, described brown coal pulverize after particle diameter be less than or equal to 100 orders, pulvis B particle diameter is less than or equal to 100 orders.
As preferably, described brown coal pulverize after particle diameter be less than or equal to 100 orders, pulvis B particle diameter is less than or equal to 100 orders.
Another object of the present invention is to provide a kind of microbial fertilizer, this microbial fertilizer can be according to the difference of crop different growing stages nutrient demand, for crop is long-acting, equilibrium provides multiple nutrient, in Different Crop special product sensitivity, the generation of the nutritional deficiency diseases such as the interpolation of trace element and control plant and vegetables.
A microbial fertilizer, this microbial fertilizer contains above-mentioned microorganism probiotic implants nutritive medium.
As preferably, described microbial fertilizer also contains nitrogenous fertilizer, phosphate fertilizer, potash fertilizer.
A further object of the present invention is that above-mentioned microbial fertilizer is applied in agricultural, production of forestry.
A kind of application in agricultural, production of forestry by the microbial fertilizer of above-mentioned microbial fertilizer.
As preferably, described in be applied to wheat, corn, paddy rice or vegetable melon and fruit and spread manuer in holes, spread fertilizer over the fields as base manure or topdress.
Inventive principle and beneficial effect:
1, this nutritive medium is the special use implantation carrier that microorganism probiotic is implanted chemical fertilizer, can meet the needs that various fertilizer is implanted microorganism probiotics, and can improve the surviving rate of microbiobacterial agent in various fertilizer, forms Multifunctional controlling release fertilizer.
2, this nutritive medium is to take brown coal as organic nutrients such as the main and auxiliary waste liquid of producing with sucrose and monosodium glutamate etc. and waste residue refinement humic acids (HAc, FA), carbohydrate and amino acid.The invention solves the difficult problem that microorganism probiotic is implanted at compound fertilizer of high concentration, the broad-spectrum micro-organisms probiotic bacterium that is applicable to high, medium and low various Chemical Mixed Fertilizer (composite fertilizer) is implanted nutritive medium, improved microorganism probiotic and implanted the surviving rate in fertilizer: reached more than 80%, expanded the kind of microorganism probiotic implantation fertilizer.
Accompanying drawing explanation
Fig. 1 is that microorganism probiotic of the present invention is implanted nutritive medium preparation technology schema.
Embodiment
Below in conjunction with accompanying drawing, the invention will be further described.
Press described in Fig. 1, it is as follows that microorganism probiotic is implanted nutritive medium preparation technology:
Brown coal (humic acids) are pulverized to (≤100 order), by brown coal: the weight ratio of alkali=1:1～7 adds 5～15% potassium hydroxide solution, at 80～100 ℃, in boiling extractor, 1～2h is extracted in boiling, extracting solution is after the separated slagging-off of pressure filter, by the weight ratio of 50:3～5 to the hydrogen peroxide that adds 10% in filtrate, in 50～69 ℃ of oxygen solution activation 3～4 hours in activated bath, make activation solution A;
By the concentrated concentrate of glutamate production high-concentration waste liquid heating, filtering separation in strainer, gets filter cake and be dried 10～60 minutes at 100～120 ℃, pulverizes in (≤150 order), makes pulvis B;
The activation solution A obtaining in 1000 parts of steps 1 is added in mixing tank, at 40～60 ℃, add 35～40 parts of ammonium molybdates, add again 150～300 parts of pulvis B after to be dissolved, be uniformly mixed, add 10 parts of synergy methyl catechol and 5 parts of molasses, both obtained microorganism probiotic and implanted nutritive medium, measure canned.
Test 1 microorganism probiotic and implant the preparation of nutritive medium
Brown coal (humic acids) are pulverized to (≤100 order), by the weight ratio of brown coal: alkali=1:4, add 10% potassium hydroxide solution, at 80～100 ℃, in boiling extractor, 1～2h is extracted in boiling, extracting solution is after the separated slagging-off of pressure filter, by the weight ratio of 50:4 to the hydrogen peroxide that adds 10% in filtrate, in 50～69 ℃ of oxygen solution activation 3～4 hours in activated bath, make activation solution A;
By the concentrated concentrate of glutamate production high-concentration waste liquid heating, filtering separation in strainer, gets filter cake and be dried 10～60 minutes at 100～120 ℃, pulverizes in (≤150 order), makes pulvis B;
The activation solution A obtaining in 1000 parts of steps 1 is added in mixing tank, at 40～60 ℃, add 38 parts of ammonium molybdates, add again 280 parts of pulvis B after to be dissolved, be uniformly mixed, add 10 parts of synergy methyl catechol and 5 parts of molasses, both obtained microorganism probiotic and implanted nutritive medium.This microorganism probiotic is implanted nutritive medium probiotic bacterium surviving rate when Chemical Mixed Fertilizer is implanted plants probiotics and is reached 80～85%, and harmful mushroom of ecological slow-release carbamide is lower than 1% simultaneously, and harmful element (heavy metal) meets GB/T2339-2009 standard-required.
Test producing of 2 microbial fertilizers
Phosphogypsum, 130～200 ℃ of dehydrations, grinds with Raymond mill.Semi-hydrated gypsum after dehydration and urea, in urea: semi-hydrated gypsum weight part 70:28 ratio is mixed into mixture C.At 25～60 ℃, the water atomization of 1～8 wt % is sprayed into mixture C, hydration reaction, makes urea surface form the film D of one deck dihydrate gypsum and semi-hydrated gypsum.By 3 parts of fixed nitrogen series bacillus, Bacillus licheniformis, joining 15 parts has the microorganism probiotic that experiment 1 makes to implant in nutritive medium, after being uniformly mixed, add 3 parts of magnesium sulfate, 15 parts of zinc sulfate, 6 parts of manganous sulfates, 3 parts of Sodium Tetraboratees, through being uniformly mixed, by the weight ratio of 10:90, spray on film D again.
Experiment 3: microbial fertilizer application
The microbial fertilizer that experiment 2 is prepared is planted for vegetables, melon and fruit, experiment shows: the field crops such as wheat, corn, paddy rice: implant the microbial fertilizer of nutritive medium and compare with implanting plants probiotics but do not add microorganism probiotic of the present invention, the microbial fertilizer in the present invention generally has following effect:
The field crops such as wheat, corn, paddy rice: shift to an earlier date 3～10 days maturations, full seed, amount of increase in production 8%～20%.
Vegetable melon and fruit: blade is generous, single fruit weight increases, pulp thickens, mouthfeel is good, amount of increase in production 15%～30%, ripen in advance listing 3～10 days.
Above the preferred embodiment for the present invention is explained in detail; but the present invention is also confined to above-mentioned embodiment incessantly; in most of every ken possessing those of ordinary skills, under the prerequisite that does not depart from aim of the present invention, make various variations all within the scope of protection of the invention.
Claims (3)
1. prepare microorganism probiotic and implant a preparation method for nutritive medium, comprise the following steps:
Activation solution A produces; Brown coal are pulverized, with alkali lye boiling, extracted, press filtration, then oxygen solution activator oxygen solution activates into activation solution A;
Pulvis B produces; The concentrated concentrate of monosodium glutamate waste liquid heating, filters, and is ground into pulvis B after filtration cakes torrefaction;
Admixture activation liquid A and pulvis B;
Described microorganism probiotic is implanted nutritive medium and is comprised of following composition:
Organic 20～50 wt %
Nitrogen 1～5wt %
Potassium 1～5wt %
Surplus is oxygen and other oxygenatedchemicals.
2. microorganism probiotic as claimed in claim 1 is implanted a preparation method for nutritive medium, it is characterized in that:
Described brown coal: alkali=1:1～7, the potassium hydroxide solution that described alkali lye is 5～15%, described boiling is extracted in 80～100 ℃, 1～2h;
The hydrogen peroxide that described oxygen solution activator is 10%, filtrate: hydrogen peroxide weight ratio is 50:3～5,50～69 ℃ of oxygen solution activation temperatures, oxygen solution soak time 3～4 hours;
Described being dried at 100～120 ℃, 10～60 minutes time of drying;
Described activation solution A and pulvis B ratio of mixture are 1000 parts: 150～300 parts, mixing adds 35～40 parts of ammonium molybdates and 10 parts of synergy methyl catechol and 5 parts of molasses to complete at 40～60 ℃.
3. microorganism probiotic according to claim 1 is implanted the preparation method of nutritive medium, it is characterized in that: described brown coal are pulverized rear particle diameter and are less than or equal to 100 orders, and pulvis B particle diameter is less than or equal to 100 orders.
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| CN201110210426.6A CN102381910B (en) | 2011-07-26 | 2011-07-26 | Microorganism probiotic implanted nutrient liquid and preparation method of microorganism probiotic implanted nutrient liquid as well as microorganism fertilizer and application of microorganism fertilizer in agriculture and forestry production |
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| CN201110210426.6A CN102381910B (en) | 2011-07-26 | 2011-07-26 | Microorganism probiotic implanted nutrient liquid and preparation method of microorganism probiotic implanted nutrient liquid as well as microorganism fertilizer and application of microorganism fertilizer in agriculture and forestry production |
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| CN102757262B (en) * | 2012-06-12 | 2013-12-11 | 福建省诏安县绿洲生化有限公司 | Method for producing liquid water-soluble carbon fertilizer with high-concentration organic waste water |
| CN102701868A (en) * | 2012-06-27 | 2012-10-03 | 中国农业科学院农业资源与农业区划研究所 | Modified glutamic acid fertilizer synergist and production method and application thereof |
| CN106888889A (en) * | 2016-12-12 | 2017-06-27 | 广西中议农业开发有限公司 | A kind of Tree Drought Resistance cold-resistant implantation methods |
| CN110172007A (en) * | 2019-07-12 | 2019-08-27 | 惠州护地农科有限公司 | A kind of water solubility refined organic fertilizer and its preparation process |
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| CN1099399C (en) * | 1999-07-14 | 2003-01-22 | 朱晓鸣 | Multi-element organic-inorganic compound liquid fertilizer |
| CN1353101A (en) * | 2001-12-11 | 2002-06-12 | 江东荣 | Multipurpose agricultural liquid nutrient and its preparing process |
| CN101628831B (en) * | 2008-07-14 | 2011-09-21 | 上海温兴生物工程有限公司 | Liquid-state soluble humic acid organic fertilizer and method for manufacturing same |
| CN101423536B (en) * | 2008-12-02 | 2013-12-18 | 昆明理工大学 | Method for preparing humic acid and salt thereof by oxidation and degradation of brown coal |
| CN101844944B (en) * | 2009-03-23 | 2013-04-24 | 北京世纪阿姆斯生物技术股份有限公司 | Total nutrient liquid microbial fertilizer |
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