CN103772038A - Production method of natural organic seaweed fertilizer - Google Patents

Production method of natural organic seaweed fertilizer Download PDF

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CN103772038A
CN103772038A CN201410029082.2A CN201410029082A CN103772038A CN 103772038 A CN103772038 A CN 103772038A CN 201410029082 A CN201410029082 A CN 201410029082A CN 103772038 A CN103772038 A CN 103772038A
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seaweed
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fertilizer
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Abstract

The invention provides a production method of a natural organic seaweed fertilizer. The method comprises the following steps: treating seaweeds by using a method of combining mechanical crushing centrifugation with chemical alkali digestion, washing the digested slurry material with water and performing filtration and concentration so as to obtain a corresponding semi-solid filter material; compounding the dried filter material; and producing the compounded filter material by using a granulating process so as to obtain the organic seaweed fertilizer. According to the method, a relatively small amount of alkali is added and an enzyme agent is not used, i.e., and the increasing of the additional cost is avoided, so that the requirement on the working environment of a reaction kettle is relatively low. The produced organic seaweed fertilizer contains a large quantity of organic substances without containing nitrogen and multiple mineral nutrients such as potassium, magnesium and zinc, and particularly contains seaweed polysaccharides and highly unsaturated fatty acids which are specifically contained in the seaweeds and is rich in multiple plant growth regulators such as cytokinins and auxins, thereby having the high biological activity. Thus, the absorption and the growth of plants are promoted by the beneficial substances from the seaweed plants. As a result, the stress resistance of crops is improved; the yield of the crops is increased.

Description

A kind of production method of natural seaweed fertilizer
Technical field
The present invention relates to extract the production technique of slurry production seaweed fertilizer from phycophyta, more specifically point out, the present invention relates to use mechanical process in conjunction with chemical Treatment algae from one, therefrom extracting effective components is prepared the production method of seaweed fertilizer.
Background technology
The use of chemical fertilizer plays an important role to agriculture volume increase, but since early 1980s, use single chemical fertilizer because without stint is a large amount of, make ecotope, edaphon be subject to destruction in various degree, cause crops quality to reduce, " dish is tasteless, and melon is sweetless; fruit is not fragrant ", has a strong impact on agriculture Sustainable development.The pollution bringing to agricultural along with single chemical fertilizer becomes increasingly conspicuous; and people are to life quality, the attention of agricultural sustainable development and environment protection, many countries have reduced the amount of application of chemical fertilizer; advocate energetically application of organic fertilizers, bio-fertilizer, develop eco-agriculture, green agriculture.
At present, domestic and international many scholars have confirmed the vital role of seaweed fertilizer in agriculture production, as article " The effect of a seaweed concentrate on the in vitro growth and acclimatization of potato plantlets " etc., seaweed organism fertilizer is described as the Jinin good wine that people unique in the world today and plant can " drink ", there is significant biological effect, possessed the feature of current most advanced fertilizer.
In marine alga, comprise the nutritive ingredient such as abundant mineral substance and trace element, also contain the polyphenolic substance of some amount simultaneously, laminarin, fucoidin and a large amount of growth regulators, as phytokinin (" The effect of hydrolysed seaweed on certain plant pests and diseases "), growth hormone (" Plant growth regulatory substances in commercial seaweed extracts "), the class cytokinin factor, cytokinin (" Enhanced leaf chlorophyll levels in plants treated with seaweed extract "), dormin, Plant hormones regulators,gibberellins, ethene, trimethyl-glycine, polyamines (" active ingredient in seaweed plants growth regulator "), trans-N6-isopentennyladenine and derivative thereof, the acid of amino-cyclopropane shuttle, ethene precursor, indolylacetic acid, benzazolyl compounds etc.Seaweed organic fertilizer integrates nutritive ingredient, antibiotics, plant hormone, and these organic active factor pair stimulating plant growths play an important role.Polyphenolic substance has extremely strong oxidation-resistance, and growth that can Antifungi, is convenient to farm crop and preserves for a long time; Plant hormone, dormin can be controlled photosynthetic process, simultaneously the balance of the generation of non-specific regulatory factor and adjusting endogenous hormone in stimulating plant body.
The seaweed fertilizer obtaining by the advanced composting technology such as chemical, biological, composite can improve the output of farm crop significantly, improve the quality of agricultural-food, strengthen the biologos of soil, strengthen the ability of farm crop opposings poor environment, promote absorption and the transfer of nutrient, promote the thick of the growth of root system and stem, improve percentage of germination, suppress disease and pest, improve quality, the prolongation preservation term of fruit, extend the cutflower preservation phase etc.This seaweed fertilizer environmental protection, has important effect to agriculture Sustainable development.Along with the development of Modern Agriculture in China, and the gradually attention of people to agricultural product quality and environmental protection, to the demand of seaweed manure, by increasing, the future market of seaweed organism fertilizer has a extensive future.
Chinese patent CN200810238683.9 directly uses potassium hydroxide configuration solution to carry out marine alga to clear up, use alkali lye single, and relating generally to algae is sea-tangle, sargassun, bladder wrack; Chinese patent CN102276326A has used marine alga to pulverize liquid in conjunction with biological enzyme agent, ferment and obtain organic liquid fertilizer, relating generally to algae is sea-tangle, sargassun, bulk kelp, but owing to using fermented by biological enzyme technology, it needs strict the control factors such as pH value, temperature and other microbial contamination, the use of expensive enzymes agent on the other hand for fermented extracted environmental requirement harshness, the problems such as liquid fertilizer is filling, storage and transport, have increased the cost that extracts seaweed fertilizer too; Chinese patent CN102491798A has used the mode of supersonic wave wall breaking to extract seaweed fertilizer; Chinese patent CN102503707A uses potassium hydroxide to clear up marine alga, relate generally to bulk kelp and Enteromorpha, in the course of processing, relate to the melting of urea, and urea itself is unstable, be heated and easily decompose, 132.7 degrees Celsius of decomposition temperatures, just in the preparation temperature range of its patent, therefore, exist effective fertilizer composition to decompose the risk reducing; Chinese patent CN102584440A utilizes cryogenic high pressure technology to decompose marine alga, relates to sargassun, and cryogenic high pressure equipment complexity, energy consumption is also higher.
Summary of the invention
Seaweed fertilizer production method is introduced:
Concentrated filtrate-the > of clean-> mechanical disintegration-> alkaline purification-> of marine alga is dry-and > is composite, and be uniformly mixed-> screening-> pressurization granulation-> detections-> packs puts in storage
(1) algae is cleaned and pulverizes mechanically homogenate, can use sonioation method, grind, pulverize method, the mode such as high-pressure homogenization method, freezing and pulverizing method;
(2) in reactor, add to pressurize to heat up in the solution such as sodium carbonate, calcium carbonate, potassium hydroxide, sodium hydroxide of certain volume and clear up, remove insoluble component;
(3) postdigestive slurry is washed, filtering and concentrating, obtains corresponding semi-solid state filtrate;
(4) semi-solid state filtrate water ratio is higher, can reach 60% to 70%, need to be dried, dried material can be chosen the materials such as humic acid, urea, potassium sulfate, potassium primary phosphate, monoammonium phosphate and trace element and carry out composite, close on the basis of the indexs such as GB organic-inorganic complex fertilizer (GB18877-2009) satisfied, adjust corresponding component content for applicable object;
(5) use Squeezinggranulator granulation, can use flat-die type powdered extruder grain, produce cylindrical particle, then by throw twice throwing of circular knitting machine circle, vibratory screening apparatus screening laggard enter water cooler, testing product index, finally weighs pack.
For the problem of above-mentioned prior art feature and existence, the present invention has used the more technique of science, has adjusted flow process, has obtained effective seaweed fertilizer product.To achieve these goals, the technical solution used in the present invention is:
In the present invention, use the method that the centrifugal combination chemical bases of mechanical disintegration is cleared up to process marine alga, because used in advance mechanical disintegration, so further the usage quantity of the required alkali of fracture cell walls reduces relatively, and do not use enzyme agent additionally to increase cost, require also relatively low to the Working environment of reactor.
In the present invention, recommend but be not limited to several algae, as Sha Caizao, kylin algae and sargassun etc., its main component is as shown in table 1, in the seaweed fertilizer of producing, contain a large amount of non-itrogenous organic substances, potassium, magnesium, the multiple mineral nutrient such as zinc, particularly contain peculiar Sargassum polysaccharides in marine alga, highly unsaturated fatty acids, be rich in phytokinin simultaneously, growth hormone, the class cytokinin factor, cytokinin, Plant hormones regulators,gibberellins, ethene, the various plants growth regulators such as indolylacetic acid, there is very high biological activity, these benefit materials that come from seaweed plants itself can promote absorption and the growth of plant, improve crop anti-adversity, increase output.
The chemical composition (g/100g dry weight) of table 1 marine alga.
Figure 897381DEST_PATH_IMAGE001
In the present invention, use multiple alkaline solution or the alkaline salt solution of proportioning to carry out corresponding alkaline purification, as KOH and NaOH etc., give full play to the advantage of different alkali lye processing marine algas, thereby reach the usage quantity of less alkali lye, reduce costs.
In the present invention, use composite mode in conjunction with agglomeration technique, make solid-state seaweed fertilizer, can reduce packing, storage and transportation cost, also can facilitate field fertilization.Can produce organic seaweed fertilizer, the organic and inorganic seaweed fertilizer etc. with bioactive ingredients by choosing different complex materials, can, according to different plant nutrition demands, adjust compound proportion, exploitation becomes extraordinary seaweed fertilizer with strong points.
Embodiment
Operational path of the present invention is as follows:
Concentrated filtrate-the > of clean-> mechanical disintegration-> alkaline purification-> of marine alga is dry-and > is composite, and be uniformly mixed-> screening-> pressurization granulation-> detections-> packs puts in storage
Below in conjunction with concrete embodiment, the present invention is described in further detail.Should understand embodiment below and only be not used in the restriction scope of the invention for the present invention is described.
embodiment 1
Getting the kylin algae (calculating with dry vegetalbe) of 300 kilograms cleans, pulverize homogenate, pour in the reactor that volume is 5000L, use the alkali lye processing that solution KOH:NaOH proportioning is 0.4, through 4 hours, then the PH that adjusts marine alga slurries can reach and approach neutrality, add again 10-60 boiling water doubly, stir 7 to 10 hours at about 70-98 ℃, marine alga is boiled molten, then filter concentrating under reduced pressure, until become semi solid slurry, now water ratio is about 80%, carries out dryness in the sun, obtains water ratio and is about 25% Seaweed Extract.Be Seaweed Extract according to mass ratio: urea: phosphoric acid diamines: potassium sulfate=11:522:85:81, compositely become organic seaweed fertilizer, use 900 eye mesh screen screenings, use flat-die type powdered extruder grain, produce cylindrical particle, then by throw circular knitting machine twice throwing circle, vibratory screening apparatus screening laggard enter water cooler, testing product index, finally weighs pack.
embodiment 2
The Sha Caizao (calculating with dry vegetalbe) that gets 300 kilograms cleans, pulverize homogenate, pour in the reactor that volume is 5000L, use the alkali lye processing that solution KOH:NaOH proportioning is 0.5, through 3 hours, then the PH that adjusts marine alga slurries can reach and approach neutrality, add again 10-60 boiling water doubly, stir 7 to 10 hours at about 70-98 ℃, marine alga is boiled molten, then filter concentrating under reduced pressure, until become semi solid slurry, now water ratio is about 80%, carries out dryness in the sun, obtains water ratio and is about 25% Seaweed Extract.Be Seaweed Extract according to mass ratio: urea: MAP: potassium sulfate=12:479:122:75, compositely become organic seaweed fertilizer, use 900 eye mesh screen screenings, use flat-die type powdered extruder grain, produce cylindrical particle, then by throw circular knitting machine twice throwing circle, vibratory screening apparatus screening laggard enter water cooler, testing product index, finally weighs pack.
embodiment 3
Experiment Nanjing County, Zhangzhou City, Shi Fujian Province, place, is red soil for examination soil, contains the soil organism 1.82%, available N 60.6mg/kg, available P 12.1mg/kg.Vegetable variety is cucumber, is divided into 15 trial plots, and each community area is 22m 2, by the plantation of 0.4m*1.1m space between plants, 50 strains of every community.
Fertilizing method:
(1) according to locality custom, conventional fertilizer application is base fertilizer farm manure 4500kg/ mu, urea 25kg/ mu, diammonium phosphate 25kg/ mu, and potassium sulfate 10kg/ mu, topdresses three times, executes urea 20kg/ mu at every turn;
(2) example 1 seaweed fertilizer, base fertilizer farm manure 4500kg/ mu, seaweed fertilizer 60kg/ mu, topdresses three times, executes seaweed fertilizer 15kg/ mu at every turn;
(3) blank test, base fertilizer is farm manure 4500kg/ mu, etc. weight clear water.
Table 2 field experiment (g/100g dry weight).
Figure 643882DEST_PATH_IMAGE002
The output of use-case 1 seaweed fertilizer is obviously high about 14.7% than the output of conventional fertilizer application, and soluble sugar and vitamins C are also significantly increased.Promoting the use of of seaweed fertilizer can effectively make crop yield, make increasing peasant income, can effectively promote the development of the ecological agriculture, green agriculture.

Claims (5)

1. a production method for natural seaweed fertilizer, is characterized in that, comprises the following steps:
Concentrated filtrate-the > of clean-> mechanical disintegration-> alkaline purification-> of marine alga is dry-and > is composite, and be uniformly mixed-> screening-> pressurization granulation-> detections-> packs puts in storage
(1) algae is cleaned and pulverizes mechanically homogenate; (2) in reactor, add to pressurize to heat up in the basic solution of certain volume and clear up, remove insoluble component; (3) postdigestive slurry is washed, filtering and concentrating, obtains corresponding semi-solid state filtrate; (4) semi-solid state filtrate is dried, and dried material can be chosen other organic and inorganic raw materials and carry out composite; (5) use Squeezinggranulator granulation, testing product index, finally weighs pack.
2. the production method of a kind of seaweed organic fertilizer according to claim 1, is characterized in that: for the production of marine alga can be red algae or brown alga, can be also the mixing of the two, as Sha Caizao, kylin algae and sargassun etc.
3. the production method of a kind of seaweed organic fertilizer according to claim 1, is characterized in that: the mode such as mechanical disintegration homogenate can be used sonioation method, grinds, pulverizes method, high-pressure homogenization method, freezing and pulverizing method.
4. the production method of a kind of seaweed organic fertilizer according to claim 1, it is characterized in that: alkaline purification liquid can multiple alkaline solution or alkaline salt solution carry out corresponding alkaline purification and clear up, the solution such as such as sodium carbonate, calcium carbonate, potassium hydroxide, sodium hydroxide, can bring into play so different alkali lye and process the advantage of different sorts marine alga, thereby reach the usage quantity of less alkali lye, reduce cost, as KOH and NaOH mixing, its solution KOH:NaOH proportioning is 0.1 to 0.9.
5. the production method of a kind of seaweed organic fertilizer according to claim 1, carrying out composite organic and inorganic material can be humic acid, urea, potassium sulfate, potassium primary phosphate, monoammonium phosphate and trace element etc.
CN201410029082.2A 2014-01-22 2014-01-22 Production method of natural organic seaweed fertilizer Pending CN103772038A (en)

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Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104447008A (en) * 2014-12-05 2015-03-25 中国科学院烟台海岸带研究所 Method for preparing liquid seaweed fertilizer
CN104817398A (en) * 2015-04-28 2015-08-05 众德肥料(烟台)有限公司 Basic-protein bio-organic fertilizer production technology
CN104877044A (en) * 2015-06-16 2015-09-02 中国水产科学研究院黄海水产研究所 Chitin cleaning production technique
CN104892250A (en) * 2015-06-18 2015-09-09 张家港市五湖新材料技术开发有限公司 Algae-containing special fertilizer for flowers
CN104892157A (en) * 2015-05-29 2015-09-09 领先生物农业股份有限公司 Active seaweed fertilizer and production method thereof
CN106008094A (en) * 2016-05-23 2016-10-12 青岛海大生物集团有限公司 Seaweed potassium fertilizer and preparation method thereof
CN106416761A (en) * 2016-10-17 2017-02-22 连云港市林业技术指导站 Method for grafting seedling culture of new horse chestnut variety
CN108975962A (en) * 2018-09-13 2018-12-11 滁州职业技术学院 A kind of preparation method of liquid fertilizer
CN109081740A (en) * 2018-10-19 2018-12-25 广东海洋大学 A kind of nitrogen-phosphorus-potassium compound fertilizer and preparation method thereof containing alginic acid
CN110396012A (en) * 2018-11-27 2019-11-01 湖北新洋丰肥业股份有限公司 A kind of preparation method of nitro high tower seaweed compound fertilizer
CN110819659A (en) * 2019-11-15 2020-02-21 斯蒂芬·Y·周 Preparation method of seaweed organic polymer
CN111908982A (en) * 2020-08-10 2020-11-10 济南航晨生物科技有限公司 Method for extracting seaweed by electromagnetic radiation
CN113906951A (en) * 2021-10-27 2022-01-11 罗甸天纯农旅开发有限公司 High-yield cultivation technology of bee sugar plums
GB2582522B (en) * 2017-11-17 2023-02-22 Bernard Port Louis Seaweed composition
CN116730775A (en) * 2023-05-06 2023-09-12 新洋丰农业科技股份有限公司 Drought-resistant synergistic corn fertilizer and preparation method thereof

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CN101585723A (en) * 2008-06-20 2009-11-25 青岛聚大洋海藻工业有限公司 Preparation method of seaweed biological long-acting fertilizer
CN102584448A (en) * 2012-02-17 2012-07-18 南京工业大学 Compound fertilizer
CN102898245A (en) * 2012-11-09 2013-01-30 中国农业科学院农业资源与农业区划研究所 Seaweed synergia compound fertilizer and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN101585723A (en) * 2008-06-20 2009-11-25 青岛聚大洋海藻工业有限公司 Preparation method of seaweed biological long-acting fertilizer
CN102584448A (en) * 2012-02-17 2012-07-18 南京工业大学 Compound fertilizer
CN102898245A (en) * 2012-11-09 2013-01-30 中国农业科学院农业资源与农业区划研究所 Seaweed synergia compound fertilizer and preparation method thereof

Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104447008A (en) * 2014-12-05 2015-03-25 中国科学院烟台海岸带研究所 Method for preparing liquid seaweed fertilizer
CN104817398B (en) * 2015-04-28 2017-10-17 众德肥料(烟台)有限公司 A kind of basic protein biological organic fertilizer production technology
CN104817398A (en) * 2015-04-28 2015-08-05 众德肥料(烟台)有限公司 Basic-protein bio-organic fertilizer production technology
CN104892157B (en) * 2015-05-29 2017-10-17 领先生物农业股份有限公司 A kind of active alga fertilizer and its production method
CN104892157A (en) * 2015-05-29 2015-09-09 领先生物农业股份有限公司 Active seaweed fertilizer and production method thereof
CN104877044A (en) * 2015-06-16 2015-09-02 中国水产科学研究院黄海水产研究所 Chitin cleaning production technique
CN104892250A (en) * 2015-06-18 2015-09-09 张家港市五湖新材料技术开发有限公司 Algae-containing special fertilizer for flowers
CN106008094A (en) * 2016-05-23 2016-10-12 青岛海大生物集团有限公司 Seaweed potassium fertilizer and preparation method thereof
CN106416761A (en) * 2016-10-17 2017-02-22 连云港市林业技术指导站 Method for grafting seedling culture of new horse chestnut variety
GB2582522B (en) * 2017-11-17 2023-02-22 Bernard Port Louis Seaweed composition
US11751573B2 (en) 2017-11-17 2023-09-12 Bernard PORT-LOUIS Seaweed composition
CN108975962A (en) * 2018-09-13 2018-12-11 滁州职业技术学院 A kind of preparation method of liquid fertilizer
CN109081740A (en) * 2018-10-19 2018-12-25 广东海洋大学 A kind of nitrogen-phosphorus-potassium compound fertilizer and preparation method thereof containing alginic acid
CN110396012A (en) * 2018-11-27 2019-11-01 湖北新洋丰肥业股份有限公司 A kind of preparation method of nitro high tower seaweed compound fertilizer
CN110819659A (en) * 2019-11-15 2020-02-21 斯蒂芬·Y·周 Preparation method of seaweed organic polymer
CN111908982A (en) * 2020-08-10 2020-11-10 济南航晨生物科技有限公司 Method for extracting seaweed by electromagnetic radiation
CN113906951A (en) * 2021-10-27 2022-01-11 罗甸天纯农旅开发有限公司 High-yield cultivation technology of bee sugar plums
CN116730775A (en) * 2023-05-06 2023-09-12 新洋丰农业科技股份有限公司 Drought-resistant synergistic corn fertilizer and preparation method thereof

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