CN106008085A - Water-soluble amino acid fertilizer and preparation method thereof - Google Patents
Water-soluble amino acid fertilizer and preparation method thereof Download PDFInfo
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- CN106008085A CN106008085A CN201610330071.7A CN201610330071A CN106008085A CN 106008085 A CN106008085 A CN 106008085A CN 201610330071 A CN201610330071 A CN 201610330071A CN 106008085 A CN106008085 A CN 106008085A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B17/00—Other phosphatic fertilisers, e.g. soft rock phosphates, bone meal
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
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- Life Sciences & Earth Sciences (AREA)
- Soil Sciences (AREA)
- Pest Control & Pesticides (AREA)
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Abstract
The invention provides water-soluble amino acid fertilizer and a preparation method thereof. Raw materials of the water-soluble amino acid fertilizer comprise one or a mixture of bone meal, soybean cakes, rice bran, wheat bran, fish and shrimps. According to the water-soluble amino acid fertilizer, protein waste is used sufficiently, waste is changed into wealth, reaction conditions in a preparation process are mild, amino acid deterioration is avoided, and a racemization effect is not produced. Meanwhile, by the aid of a microbial fermentation technology, soil is conditioned, microorganisms in the soil are activated, soil hardening is avoided, and the air permeability of the soil is improved. Drought pressure of the soil can be relieved, use of chemical fertilizer can be reduced, damage of salt and alkali to the soil can be reduced, and the soil fertility can be improved. Meanwhile, the yield of food crops, cash crops, vegetables, melons and fruits can be increased greatly.
Description
Technical field
The present invention relates to a kind of fertilizer, be more particularly to a kind of aminoacid Water soluble fertilizer and system thereof
Preparation Method.
Background technology
Aminoacid is the class organic compound containing amino and carboxyl, is constitutive protein matter
Ultimate unit, there is complexing power, metastable cooperation can be formed with metal complex
Thing, is to prepare medicine, health product and many animals feed additive and amino acids fertilizer
Important source material.And China has substantial amounts of albumen garbage not to be fully utilized at present, profit
Producing amino acid fertilizer with albumen garbage is one of approach of turning waste into wealth.
Mostly the amino acid fertilizer that existing enterprise produces is to utilize acidolysis protein to prepare amino
Acid, the aminoacid produced with concentrated sulphuric acid hydrolysis such as vegetable protein bean dregs, oil foot, hair, (Shen
Please number: 03111654.X), or in hair keratin through hydrochloric acid hydrolysis preparing ammonia base acid (Shen
Please numbers 201010183263.2).At 105～115 DEG C, obtain aminoacid with acid, basic hydrolysis
(application number: 201010191126.3).Amino is prepared with multiple acid hydrolysis animal protein
Acid liquid fertilizer (application number: 201210432607.8).Ammonia prepared by acidolysis utilized above
Containing substantial amounts of acid in base aqueous acid, the acid removal process that follow-up needs are complex, warp
Help relatively costly.And that the aminoacid that basic hydrolysis protein prepares can suffer in various degree is broken
Go bad and produce racemization phenomenon, and the percent hydrolysis of protein is relatively low, follow-up also need neutralisation treatment
The alkali of excess, increases Financial cost.
Summary of the invention
In view of this, the invention provides a kind of aminoacid Water soluble fertilizer, raw material include bone meal,
One or more mixture in soybean cake, Testa oryzae, Testa Tritici, fish, shrimp.
Preferably, a great number of elements N, P and K are also included；Described a great number of elements N composition
Source includes that carbamide, described a great number of elements P ingredient origin include calcium superphosphate, described greatly
Secondary element K ingredient origin includes potassium nitrate or potassium carbonate.
Preferably, moderate-element Ca and Mg, described moderate-element Ca composition are also included
Source includes that Gypsum Fibrosum, described moderate-element Mg ingredient origin include magnesium sulfate.
Preferably, also including trace element B and Zn, described trace element B component is originated
Including Borax, described trace elements zn ingredient origin includes zinc sulfate.
Preferably, also include that auxiliary agent, described auxiliary agent include dispersant, wetting agent, anticorrosion
One or more in agent.
Present invention also offers the preparation method of a kind of aminoacid Water soluble fertilizer, including following step
Rapid:
(1) prepared by masterbatch: take bone meal, soybean cake, Testa oryzae, Testa Tritici, ammonium sulfate, molasses,
Bacillus subtilis mycopowder, lactic acid bacteria mycopowder, yeast mycopowder, protease enzyme powder, fibre
Dimension enzyme enzyme powder, Lipase Powder prepare masterbatch after adding water by fermentation；
(2) chelatropic reaction one: take fish protein, prawn head shrimp tail, MAP, potassium nitrate
Or potassium carbonate, calcium superphosphate, Gypsum Fibrosum, bacillus cereus mycopowder, Bacillus licheniformis powder,
The masterbatch prepared in photosynthetic bacteria mycopowder, protease enzyme powder, sugar slag, molasses and step (1)
Adding water, the after fermentation that stirs prepares chelate；
(3) chelatropic reaction two: water-soluble carbamide, potassium sulfate or potassium oxide, magnesium sulfate,
The chelate prepared in Borax, zinc sulfate and step (2) stands after stirring, filters
Prepare aminoacid Water soluble fertilizer.
Preferably, in described step (1), sweat includes the following two stage:
In the stage one, fermentation temperature is 45～60 degree, and fermentation time is 10～30 days；
Stage two, turning after fermenting 20 days, then ferment 20～45 days.
Preferably, in described step (2), fermentation time is 40～80 days.
Preferably, in described step (3), time of repose is 0.5～3 hour.
Preferably, amino is prepared after described step (3) using 100 mesh filter screen filtration
Acid Water soluble fertilizer.
The aminoacid Water soluble fertilizer that the present invention provides compared with prior art, has the advantage that
(1) use compound protein as the raw material of aminoacid Water soluble fertilizer, make full use of shrimp
The substantial amounts of albumen garbages such as head shrimp tail, turn waste into wealth.Multiple compound protein phase interworking
Closing, hydrolysis prepares rich amino acids in aminoacid water solublity fertilizer, and collocation is rationally.
(2) combinative enzyme hydrolysis protein, its mild condition are used, it is to avoid high temperature, height
Pressure, strong acid and strong base, destroys protein, causes aminoacid to go bad, and do not produce racemization
Effect.Avoid manufacturing machine equipment by corrosion and damage.Reduce Financial cost, be suitable to wide
General popularization and application.
(3) by means of microbial fermentation technology, utilize the protease that microorganism produces by egg
White matter is hydrolyzed into aminoacid.The aminoacid Water soluble fertilizer that this kind of method is made is biological organic fertilizer,
Have conditioning soil, activation Soil Microorganism enlivens rate, overcomes soil compaction, increase
The functions such as soil air permeability.And it is possible to reduce water loss and evaporation, alleviate
Arid pressure, reduce chemical fertilizer use, alleviate saline and alkaline infringement.Soil can be improved simultaneously
Fertility, makes cereal crops, industrial crops, greengrocery, melon and fruit class significantly increase production, right
The quality tool effect of improving of agricultural product: fruit is bright in colour, head is neat,
Ripe concentration, melon agricultural product sugar content, vitamin content are by being improved, and mouthfeel is relatively
Good.
Detailed description of the invention
The claim of the present invention is done further by the mode below in conjunction with specific embodiment
Describing in detail, but be not intended that any limitation of the invention, anyone weighs in the present invention
The amendment of the limited number of time made in profit claimed range, still in scope of the presently claimed invention
Within.
The invention provides a kind of aminoacid Water soluble fertilizer, raw material includes bone meal, soybean cake, rice
One or more mixture in bran, Testa Tritici, fish, shrimp.
Above-mentioned, containing abundant mineral, predominantly hydroxyapatite crystals and nothing in bone meal
Sizing calcium hydrogen phosphate, Ca has also been adsorbed on its surface2+、Mg2+、Na+、Cl-、HCO-、
F-And citrate plasma.What is more important, Ca element abundant in bone meal and P
Element is the macro minerals element of needed by human.Bone meal is usually pale powder, insoluble
Yu Shui, plant utilizes very slow, especially in calacareous soil, but in acid ground then
Comparatively fast.Base manure can be made.Use after being mixed in compost or barnyard manure fermentation, fertilizer efficiency can be improved.
It also is used as animal feed and toothpaste phosphor-included additive.
Soybean cake is a kind of side-product obtained after Semen sojae atricolor extracting bean oil, and protein content is higher.
Oryza glutinosa is China the 1st generalized grain kind, produces about 2.06 hundred million tons per year at present.Account for complete
The 42% of state's total output of grain.Rice yield accounts for the 37% of total output of grain in the world.Rice
Paddy during being processed into polished rice shell to be removed and account for gross weight about 10% peel,
Seed coat, perisperm, mush layer and embryo, traditional Testa oryzae i.e. existing national standards rice
Bran is mainly processed into by peel, seed coat, perisperm, aleurone and embryo, therefore
A small amount of rice husk and a certain amount of dust and microorganism can be infiltrated in the course of processing, but
Rich in various nutrients and biological active substances in Testa oryzae.
Testa Tritici i.e. Testa Tritici, wheat processing milling by products, wheat yellow, lamellar or powdery.
Rich cellulose and vitamin, be preferable organic fertilizer, decomposes compared with slow but effect is lasting.
When Testa Tritici is as fertilizer, it usually needs by fermentation, the Testa Tritici fermented loosens, ventilative
Property good, the root system for crops has preferable protective effect, be difficult to occur " rotten "
Phenomenon.
Pool slag can improve soil containing rich in protein and Organic substance as bio-feritlizer
Fertility, increases the sources of nitrogen in soil.It is understood that sugar slag is primverose slag
It can also be glucose sugar slag.
Molasses are brown color thick liquid, and crude protein content is high, and sugar content is high, and price is low
Honest and clean.And live containing abundant vitamin, mineral, tropina, nucleic acid, surface
Property thing and somatomedin etc. composition, and there is antiacid alkali, oxidation resistance.To two
Valency cation has the strongest sequestering power, can form organic chelated trace unit with metal ion
Element, such as Ca2+、Mg2+、Zn2+Deng, promote amino-acid complex various nutrient elements.
Containing a large amount of mucopolysaccharides and abundant collagen protein in fish protein.
The albumen garbage that prawn head shrimp tail is usually abandoned, causes the bigger wasting of resources,
The present invention will make full use of prawn head shrimp tail, turn waste into wealth.
It is understood that the present invention produce by utilizing microorganism amylase, albumen
Enzyme, cellulase and add quantitative amylase, protease, cellulase by protein, shallow lake
The hydrolysis ammonification base acid of powder, fiber, small peptide, polypeptide and some polysaccharide, this kind of method is made
Aminoacid Water soluble fertilizer be biological organic fertilizer, be possible not only to preferably nurse one's health soil, activation
Soil Microorganism enlivens rate, overcomes the merit such as soil compaction, increase soil air permeability
Can, it is also possible to alleviate soil arid pressure, reduce chemical fertilizer use, alleviate saline and alkaline right
In the infringement of soil, the effect increase soil fertility.Cereal crops, warp can be made simultaneously
Ji crop, greengrocery, melon and fruit class are significantly increased production.
Further, a great number of elements N, P and K are also included；Described a great number of elements N becomes
Point source includes carbamide, and described a great number of elements P ingredient origin includes calcium superphosphate, described
A great number of elements K ingredient origin includes potassium nitrate or potassium carbonate.
Above-mentioned, carbamide is a kind of high concentration nitrogenous fertilizer, belong to neutral quick-acting fertilizer it can also be used to
Produce multiple compound fertilizer.In soil, residual harmful substance is less.But carbamide is in pelletize
Middle temperature is too high can produce a small amount of biuret, also known as biuret, crop is had inhibitory action.
Carbamide is organic nitrogenous fertilizer, the urase effect in soil, is hydrolyzed into ammonium carbonate or carbon
After acid hydrogen ammonium, could utilization absorbed by crops.Therefore, carbamide will be in the need fertilizer phase of crop
Within first 4～8 days, use.Carbamide contains abundant N element, can be as nitrogen source.
Calcium superphosphate is the phosphate fertilizer directly prepared with sulfuric acid decomposition phosphorus ore.Main useful constituent
It is the hydrate of dalcium biphosphate and a small amount of free phosphoric acid, possibly together with dead plaster group
Point.Calcium superphosphate can be supplied to the elements such as plant phosphorus, calcium, sulfur, has improvement basic soil
Effect.Can be used as base manure, foliage top dressing, foliage spray.It is used in mixed way with nitrogenous fertilizer, has
Nitrogen fixation, can reduce the loss of nitrogen.Can promote the germination of plant, long root, branch,
Solid and ripe, can be used as producing the raw material of Chemical Mixed Fertilizer.
Potassium nitrate is quite varied in agricultural, commodities market purposes, and potassium nitrate belongs to binary compound fertilizer.
There are good physicochemical properties.Potassium nitrate is applied to Nicotiana tabacum L. and has fertilizer efficiency height, easily inhales
Receive, promote Winter wheat, increase tobacco production, have important work to improving cigarette quality
With.
Further, also include that moderate-element Ca and Mg, described moderate-element Ca become
Point source includes that Gypsum Fibrosum, described moderate-element Mg ingredient origin include magnesium sulfate.
Above-mentioned, Gypsum Fibrosum is monoclinic system mineral, be main chemical compositions be the water of calcium sulfate
Compound.After Gypsum Fibrosum is manured into soil, dissolve the Ca produced2+Adsorb with the soil liquid or colloid
Na+Effect, the readily soluble neutral salt Na of generation2SO4Discharge soil with rainfall, reduce soil
Earth pH value, thus alleviate Na+Murder by poisoning to crop.Meanwhile, also make grogs by sodium soil
It is changed into calcium soil, beneficially the formation of soil aggregate, improves the physics and chemistry of soil
Shape, accelerates Soil Desalting.
Further, also including trace element B and Zn, described trace element B component is come
Source includes that Borax, described trace elements zn ingredient origin include zinc sulfate.
Above-mentioned, boron fertilizer be applied to Brassica campestris L, Cotton Gossypii, Semen arachidis hypogaeae, Fructus Vitis viniferae, fruit, Semen Castaneae,
Effect of increasing production on the crop such as vegetable, pulse family is the most notable.Prove boron deficiency disease after deliberation,
Use boron fertilizer can effectively prevent and treat.This is China's boron fertilizer research and the important breakthrough of application.
Avoid the occurrence of situations such as " flower buds and do not spend ".
Further, also include that auxiliary agent, described auxiliary agent include dispersant, wetting agent, prevent
One or more in rotten agent.
Above-mentioned, the effect of dispersant is to use wetting dispersing agent to reduce dispersive process institute
The time needed and energy, stabilising dispersions, shorten jitter time, prevent flocculation, anti-
Only sedimentation.
Wetting agent has anionic and nonionic surfactant.Live in anionic surface
Property agent includes alkyl sulfate, sulfonate, fatty acid or fatty acid ester sulfate, carboxylic acid
Soaps, phosphate ester etc..Nonionic surfactant includes polyoxyethylated alkyl phenol,
Polyoxyethylene aliphatic alcohol ether, polyoxyethylene polyoxypropylene block copolymer etc..
Preservative is prevented from aminoacid Water soluble fertilizer and goes bad after fermentation, has preferably
Fungistatic effect.
Present invention also offers the preparation method of a kind of aminoacid Water soluble fertilizer, including following step
Rapid:
(1) prepared by masterbatch: take bone meal, bean cake, Testa oryzae, rapeseed cake, ammonium sulfate, sugar
Honey, bacillus subtilis mycopowder, lactic acid bacteria mycopowder, yeast mycopowder, protease enzyme powder,
Cellulase enzyme powder, Lipase Powder prepare masterbatch after adding water by fermentation；
Above-mentioned, above material is loaded in container, uniform stirring 10～60 minutes.
The masterbatch mixture that will stir remove, stack with a fixed area lucifuge, protection against the tide,
Lee piles 3 meters high 2 meters wide rectangular-shaped.After inserting thermometer, cover waterproof
Cloth, cloth against sunshine, thermometer temperature must not exceed 60 degree, the turning immediately more than 60 degree.
(2) chelatropic reaction one: take fish, shrimp, MAP, potassium nitrate or potassium carbonate,
Calcium superphosphate, Gypsum Fibrosum, bacillus cereus mycopowder, Bacillus licheniformis powder, photosynthetic bacteria bacterium
The masterbatch prepared in powder, protease enzyme powder, sugar slag, molasses and step (1) adds water,
The after fermentation that stirs prepares chelate；
Above-mentioned, all chelatropic reactions are carried out the most at normal temperatures, and chelation percent can reach 90%
Above, it is not necessary to increase heating equipment, greatly reduce production cost.
(3) chelatropic reaction two: water-soluble carbamide, potassium sulfate or potassium oxide, magnesium sulfate,
The chelate prepared in Borax, zinc sulfate and step (2) stands after stirring, filters
Prepare aminoacid Water soluble fertilizer.
Above-mentioned, by adjusting the sequencing of chelatropic reaction so that each element has preferably
Chelate effect.
Further, in described step (1), sweat includes the following two stage:
In the stage one, fermentation temperature is 45～60 degree, and fermentation time is 10～30 days；
Stage two, turning after fermenting 20 days, then ferment 20～45 days.
Further, in described step (2), fermentation time is 40～80 days.
Further, in described step (3), time of repose is 0.5～3 hour.
Further, ammonia is prepared after described step (3) using 100 mesh filter screen filtration
Base acid Water soluble fertilizer.
For the ease of understanding the present invention, further illustrate the present invention below in conjunction with embodiment
Technical scheme.Applicant states, the present invention illustrates the present invention by above-described embodiment
Detailed process equipment and technological process, but the invention is not limited in above-mentioned detailed process
Equipment and technological process, i.e. do not mean that the present invention has to rely on above-mentioned detailed process equipment
Could implement with technological process.Person of ordinary skill in the field it will be clearly understood that to this
Any improvement of invention, the equivalence of raw material each to product of the present invention is replaced and auxiliary element
Interpolation, concrete way choice etc., all fall within protection scope of the present invention and open scope
Within.
Embodiment 1
The preparation method of aminoacid Water soluble fertilizer, comprises the following steps:
(1) prepared by masterbatch: take following raw material by weight:
Bone meal 150 parts
Bean cake 300 parts
100 parts of Testa oryzae
Rapeseed cake 200 parts
50 parts of ammonium sulfate
200 parts of molasses
Bacillus subtilis mycopowder, lactic acid bacteria mycopowder, yeast mycopowder totally 5 parts, wherein
Weight part ratio is, bacillus subtilis mycopowder: lactic acid bacteria mycopowder: yeast mycopowder=1:2:1
Protease enzyme powder 0.4 part
Cellulase enzyme powder 0.3 part
Lipase Powder 0.3 part
Add 500 parts of uniform stirrings of water 20 minutes, the turning in 20 days of 57 DEG C of bottom fermentations, then
Masterbatch is prepared after fermenting 35 days；
(2) chelatropic reaction one: take following dispensing by weight:
Take fish protein 500 parts
500 parts of prawn head shrimp tail
MAP 50 parts
Potassium nitrate or potassium carbonate 50 parts
Calcium superphosphate 50 parts
50 parts of Gypsum Fibrosum
Bacillus cereus mycopowder, Bacillus licheniformis powder, photosynthetic bacteria mycopowder totally 5 parts, its
Middle weight part ratio is, bacillus cereus mycopowder: Bacillus licheniformis powder: photosynthetic bacteria mycopowder
=1:2:1
Protease enzyme powder 3 parts
Sugar slag 200 parts
100 parts of molasses
And the masterbatch 500 parts prepared in step (1)
Adding the stirring in every two days of 1500 parts of water once, the after fermentation that stirs prepares for 60 days
Chelate；
(3) chelatropic reaction two: take following dispensing by weight:
300 parts of water-soluble carbamide
Potassium sulfate or potassium oxide 300 parts
300 parts of magnesium sulfate
Borax 50 parts
30 parts of zinc sulfate
1 hour is stood after stirring with the chelate 10000 parts prepared in step (2),
Aminoacid Water soluble fertilizer is prepared after 100 mesh filter screen filtration.
Embodiment 2
The preparation method of aminoacid Water soluble fertilizer, comprises the following steps:
(1) prepared by masterbatch: take following raw material by weight:
Bone meal 100 parts
Soybean cake 200 parts
300 parts of Testa oryzae
300 parts of Testa Tritici
60 parts of ammonium sulfate
300 parts of molasses
Bacillus subtilis mycopowder, lactic acid bacteria mycopowder, yeast mycopowder totally 5 parts, wherein
Weight part ratio is, bacillus subtilis mycopowder: lactic acid bacteria mycopowder: yeast mycopowder=1:2:1
Protease enzyme powder 1 part
Cellulase enzyme powder 1 part
Lipase Powder 1 part
Add 400 parts of uniform stirrings of water 20 minutes, the turning in 30 days of 45 DEG C of bottom fermentations, then
Masterbatch is prepared after fermenting 45 days；
(2) chelatropic reaction one: take following dispensing by weight:
Take fish protein 600 parts
700 parts of prawn head shrimp tail
MAP 80 parts
Potassium nitrate or potassium carbonate 80 parts
Calcium superphosphate 80 parts
80 parts of Gypsum Fibrosum
Bacillus cereus mycopowder, Bacillus licheniformis powder, photosynthetic bacteria mycopowder totally 6 parts, its
Middle weight part ratio is, bacillus cereus mycopowder: Bacillus licheniformis powder: photosynthetic bacteria mycopowder
=1:1:1
Protease enzyme powder 5 parts
Sugar slag 100 parts
200 parts of molasses
And the masterbatch 600 parts prepared in step (1)
Adding the stirring in every two days of 1200 parts of water once, the after fermentation that stirs prepares for 60 days
Chelate；
(3) chelatropic reaction two: take following dispensing by weight:
200 parts of water-soluble carbamide
Potassium sulfate or potassium oxide 200 parts
200 parts of magnesium sulfate
Borax 80 parts
50 parts of zinc sulfate
3 hours are stood after stirring with the chelate 8000 parts prepared in step (2),
Aminoacid Water soluble fertilizer is prepared after 100 mesh filter screen filtration.
Embodiment 3
The preparation method of aminoacid Water soluble fertilizer, comprises the following steps:
(1) prepared by masterbatch: take following raw material by weight:
Bone meal 200 parts
Soybean cake 400 parts
400 parts of Testa oryzae
100 parts of Testa Tritici
30 parts of ammonium sulfate
50 parts of molasses
Bacillus subtilis mycopowder, lactic acid bacteria mycopowder, yeast mycopowder totally 8 parts, wherein
Weight part ratio is, bacillus subtilis mycopowder: lactic acid bacteria mycopowder: yeast mycopowder=2:3:3
Protease enzyme powder 0.2 part
Cellulase enzyme powder 0.2 part
Lipase Powder 0.2 part
Add 800 parts of uniform stirrings of water 30 minutes, the turning in 10 days of 60 DEG C of bottom fermentations, then
Masterbatch is prepared after fermenting 45 days；
(2) chelatropic reaction one: take following dispensing by weight:
Take fish protein 300 parts
800 parts of prawn head shrimp tail
MAP 30 parts
Potassium nitrate or potassium carbonate 30 parts
Calcium superphosphate 30 parts
30 parts of Gypsum Fibrosum
Bacillus cereus mycopowder, Bacillus licheniformis powder, photosynthetic bacteria mycopowder totally 10 parts, its
Middle weight part ratio is, bacillus cereus mycopowder: Bacillus licheniformis powder: photosynthetic bacteria mycopowder
=3:3:4
Protease enzyme powder 8 parts
Sugar slag 400 parts
400 parts of molasses
And the masterbatch 800 parts prepared in step (1)
Adding the stirring in every two days of 1800 parts of water once, the after fermentation that stirs prepares for 60 days
Chelate；
(3) chelatropic reaction two: take following dispensing by weight:
200 parts of water-soluble carbamide
Potassium sulfate or potassium oxide 600 parts
600 parts of magnesium sulfate
Borax 100 parts
80 parts of zinc sulfate
0.5 is stood little after stirring with the chelate 12000 parts prepared in step (2)
Time, after 100 mesh filter screen filtration, prepare aminoacid Water soluble fertilizer.
Embodiment 4
The preparation method of aminoacid Water soluble fertilizer, comprises the following steps:
(1) prepared by masterbatch: take following raw material by weight:
Bone meal 500 parts
Soybean cake 500 parts
500 parts of Testa oryzae
500 parts of Testa Tritici
10 parts of ammonium sulfate
100 parts of molasses
Bacillus subtilis mycopowder, lactic acid bacteria mycopowder, yeast mycopowder totally 10 parts, wherein
Weight part ratio is, bacillus subtilis mycopowder: lactic acid bacteria mycopowder: yeast mycopowder=4:4:2
Protease enzyme powder 1.5 parts
Cellulase enzyme powder 1.5 parts
Lipase Powder 1.5 parts
Add 1000 parts of uniform stirrings of water 60 minutes, the turning in 25 days of 53 DEG C of bottom fermentations, then
Masterbatch is prepared after fermenting 40 days；
(2) chelatropic reaction one: take following dispensing by weight:
Take fish protein 100 parts
100 parts of prawn head shrimp tail
MAP 50 parts
Potassium nitrate or potassium carbonate 50 parts
Calcium superphosphate 50 parts
50 parts of Gypsum Fibrosum
Bacillus cereus mycopowder, Bacillus licheniformis powder, photosynthetic bacteria mycopowder totally 3 parts, its
Middle weight part ratio is, bacillus cereus mycopowder: Bacillus licheniformis powder: photosynthetic bacteria mycopowder
=1:1:1
Protease enzyme powder 2 parts
Sugar slag 600 parts
600 parts of molasses
And the masterbatch 1200 parts prepared in step (1)
Adding the stirring in every two days of 1500 parts of water once, the after fermentation that stirs prepares for 60 days
Chelate；
(3) chelatropic reaction two: take following dispensing by weight:
100 parts of water-soluble carbamide
Potassium sulfate or potassium oxide 200 parts
600 parts of magnesium sulfate
Borax 100 parts
80 parts of zinc sulfate
0.5 is stood little after stirring with the chelate 12000 parts prepared in step (2)
Time, after 100 mesh filter screen filtration, prepare aminoacid Water soluble fertilizer.
Claims (10)
1. an aminoacid Water soluble fertilizer, it is characterised in that raw material include bone meal, soybean cake,
One or more mixture in Testa oryzae, Testa Tritici, fish, shrimp.
2. aminoacid Water soluble fertilizer as claimed in claim 1, it is characterised in that also include
A great number of elements N, P and K；Described a great number of elements N ingredient origin includes carbamide, described
A great number of elements P ingredient origin includes calcium superphosphate, described a great number of elements K ingredient origin bag
Include potassium nitrate or potassium carbonate.
3. aminoacid Water soluble fertilizer as claimed in claim 1, it is characterised in that also include
Moderate-element Ca and Mg, described moderate-element Ca ingredient origin includes Gypsum Fibrosum, described
Moderate-element Mg ingredient origin includes magnesium sulfate.
4. aminoacid Water soluble fertilizer as claimed in claim 1, it is characterised in that also include
Trace element B and Zn, described trace element B component source includes Borax, described trace
Element Zn ingredient origin includes zinc sulfate.
5. aminoacid Water soluble fertilizer as claimed in claim 1, it is characterised in that also include
Auxiliary agent, described auxiliary agent includes one or more in dispersant, wetting agent, preservative.
6. the preparation method of aminoacid Water soluble fertilizer as claimed in claim 1, its feature exists
In, comprise the following steps:
(1) prepared by masterbatch: take bone meal, soybean cake, Testa oryzae, Testa Tritici, ammonium sulfate, molasses,
Bacillus subtilis mycopowder, lactic acid bacteria mycopowder, yeast mycopowder, protease enzyme powder, fibre
Dimension enzyme enzyme powder, Lipase Powder prepare masterbatch after adding water by fermentation；
(2) chelatropic reaction one: take fish, shrimp, MAP, potassium nitrate or potassium carbonate,
Calcium superphosphate, Gypsum Fibrosum, bacillus cereus mycopowder, Bacillus licheniformis powder, photosynthetic bacteria bacterium
The masterbatch prepared in powder, protease enzyme powder, sugar slag, molasses and step (1) adds water,
The after fermentation that stirs prepares chelate；
(3) chelatropic reaction two: water-soluble carbamide, potassium sulfate or potassium oxide, magnesium sulfate,
The chelate prepared in Borax, zinc sulfate and step (2) stands after stirring, filters
Prepare aminoacid Water soluble fertilizer.
7. the preparation method of aminoacid Water soluble fertilizer as described in claim 6, its feature
Being, in described step (1), sweat includes the following two stage:
In the stage one, fermentation temperature is 45～60 degree, and fermentation time is 10～30 days；
Stage two, turning after fermenting 20 days, then ferment 20～45 days.
8. the preparation method of aminoacid Water soluble fertilizer as described in claim 6, its feature
Being, in described step (2), fermentation time is 40～80 days.
9. the preparation method of aminoacid Water soluble fertilizer as described in claim 6, its feature
Being, in described step (3), time of repose is 0.5～3 hour.
10. the preparation method of aminoacid Water soluble fertilizer as described in claim 6, it is special
Levy and be, after described step (3) uses 100 mesh filter screen filtration, prepare amino sour water
Molten fertilizer.
Priority Applications (1)
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106478271A (en) * | 2016-11-10 | 2017-03-08 | 云南农业大学 | A kind of water-soluble fertilizer of aminoacid containing enzymatic isolation method and preparation method thereof |
| CN107245013A (en) * | 2017-06-22 | 2017-10-13 | 贵州祥驰农业开发有限公司 | A kind of special amino-acid state nitrogenous fertilizer of oil tea grafting and preparation method thereof |
| CN107353054A (en) * | 2017-06-21 | 2017-11-17 | 威海温喜生物科技有限公司 | A kind of preparation method of the small-peptide chelated middle trace element water-soluble fertilizer of Fish protein |
| CN108178667A (en) * | 2017-09-11 | 2018-06-19 | 农法自然（上海）农业科技有限公司 | The high nitrogen organic water-soluble fertilizer of fruit tree and its application process |
| CN108440129A (en) * | 2018-05-21 | 2018-08-24 | 烟台泓源生物肥料有限公司 | It is a kind of that edaphon can be promoted to expand numerous water soluble fertilizer and preparation method thereof |
| CN108947658A (en) * | 2018-07-26 | 2018-12-07 | 陈云 | Amino acid Water soluble fertilizer and preparation method thereof |
| CN109265227A (en) * | 2018-11-30 | 2019-01-25 | 湖南袁禾农业科技有限公司 | A kind of drop cadmium fertilizer and its application method |
| CN109503234A (en) * | 2018-12-06 | 2019-03-22 | 中国热带农业科学院农产品加工研究所 | A kind of ammino acid liquid fertilizer and preparation method thereof comprehensively utilizing discarded marine product preparation |
| CN110683882A (en) * | 2019-11-13 | 2020-01-14 | 湛江市绿海生物工程有限公司 | Process method for preparing amino acid water-soluble fertilizer from feather meal |
| CN112159288A (en) * | 2020-08-31 | 2021-01-01 | 东北农业大学 | Biologically fermented feed-grade organic fertilizer and preparation method thereof |
| CN115087351A (en) * | 2020-02-14 | 2022-09-20 | 禾大国际股份公开有限公司 | Seed coating additive |
| CN115403429A (en) * | 2022-08-20 | 2022-11-29 | 海南农佳佳科技发展有限公司 | Amino acid water-soluble fertilizer and preparation method thereof |
| CN116514581A (en) * | 2023-02-20 | 2023-08-01 | 馆陶县三绿农业高科技有限公司 | Amino acid fertilizer with low salt and low proline content and preparation method thereof |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101092311A (en) * | 2006-06-21 | 2007-12-26 | 王荣辉 | Method for producing rinsing fertilization of amino acid |
| CN101786931A (en) * | 2010-02-08 | 2010-07-28 | 徐贵阁 | Green bioactive organic fertilizer |
| CN102964175A (en) * | 2012-11-12 | 2013-03-13 | 北京依科曼生物技术有限公司 | Composite amino-acid-containing water-soluble fertilizer and preparation method thereof |
| CN103073348A (en) * | 2012-11-12 | 2013-05-01 | 北京依科曼生物技术有限公司 | Compound water soluble fertilizer used for citrus crops, preparation method and application method |
| CN104098363A (en) * | 2014-06-25 | 2014-10-15 | 覃柏鸿 | Fertilizer formula for tea trees |
| CN104710241A (en) * | 2015-03-14 | 2015-06-17 | 武鸣县红鹰肥业有限公司 | Special slow release fertilizer for eucalyptus and preparation method for fertilizer |
| CN105218262A (en) * | 2015-08-25 | 2016-01-06 | 广西喷施宝股份有限公司 | A kind of containing oligochitosan amino acid water-soluble fertilizer and preparation method thereof |
| CN105367262A (en) * | 2015-12-01 | 2016-03-02 | 王德和 | Cucumber zinc-calcium-rich efficient compound fertilizer |
| CN105399474A (en) * | 2015-12-08 | 2016-03-16 | 广东省农业科学院农业资源与环境研究所 | Method for preparing liquid fertilizer by utilizing fish waste |
-
2016
- 2016-05-18 CN CN201610330071.7A patent/CN106008085A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101092311A (en) * | 2006-06-21 | 2007-12-26 | 王荣辉 | Method for producing rinsing fertilization of amino acid |
| CN101786931A (en) * | 2010-02-08 | 2010-07-28 | 徐贵阁 | Green bioactive organic fertilizer |
| CN102964175A (en) * | 2012-11-12 | 2013-03-13 | 北京依科曼生物技术有限公司 | Composite amino-acid-containing water-soluble fertilizer and preparation method thereof |
| CN103073348A (en) * | 2012-11-12 | 2013-05-01 | 北京依科曼生物技术有限公司 | Compound water soluble fertilizer used for citrus crops, preparation method and application method |
| CN104098363A (en) * | 2014-06-25 | 2014-10-15 | 覃柏鸿 | Fertilizer formula for tea trees |
| CN104710241A (en) * | 2015-03-14 | 2015-06-17 | 武鸣县红鹰肥业有限公司 | Special slow release fertilizer for eucalyptus and preparation method for fertilizer |
| CN105218262A (en) * | 2015-08-25 | 2016-01-06 | 广西喷施宝股份有限公司 | A kind of containing oligochitosan amino acid water-soluble fertilizer and preparation method thereof |
| CN105367262A (en) * | 2015-12-01 | 2016-03-02 | 王德和 | Cucumber zinc-calcium-rich efficient compound fertilizer |
| CN105399474A (en) * | 2015-12-08 | 2016-03-16 | 广东省农业科学院农业资源与环境研究所 | Method for preparing liquid fertilizer by utilizing fish waste |
Non-Patent Citations (1)
| Title |
|---|
| （美）国家研究委员会: "《温水鱼类和甲壳类的营养需要（修订版）》", 31 May 1990, 农业出版社 * |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106478271A (en) * | 2016-11-10 | 2017-03-08 | 云南农业大学 | A kind of water-soluble fertilizer of aminoacid containing enzymatic isolation method and preparation method thereof |
| CN107353054A (en) * | 2017-06-21 | 2017-11-17 | 威海温喜生物科技有限公司 | A kind of preparation method of the small-peptide chelated middle trace element water-soluble fertilizer of Fish protein |
| CN107245013A (en) * | 2017-06-22 | 2017-10-13 | 贵州祥驰农业开发有限公司 | A kind of special amino-acid state nitrogenous fertilizer of oil tea grafting and preparation method thereof |
| CN108178667A (en) * | 2017-09-11 | 2018-06-19 | 农法自然（上海）农业科技有限公司 | The high nitrogen organic water-soluble fertilizer of fruit tree and its application process |
| CN108440129A (en) * | 2018-05-21 | 2018-08-24 | 烟台泓源生物肥料有限公司 | It is a kind of that edaphon can be promoted to expand numerous water soluble fertilizer and preparation method thereof |
| CN108947658A (en) * | 2018-07-26 | 2018-12-07 | 陈云 | Amino acid Water soluble fertilizer and preparation method thereof |
| CN109265227A (en) * | 2018-11-30 | 2019-01-25 | 湖南袁禾农业科技有限公司 | A kind of drop cadmium fertilizer and its application method |
| CN109265227B (en) * | 2018-11-30 | 2021-08-27 | 湖南袁禾农业科技有限公司 | Cadmium-reducing fertilizer and use method thereof |
| CN109503234A (en) * | 2018-12-06 | 2019-03-22 | 中国热带农业科学院农产品加工研究所 | A kind of ammino acid liquid fertilizer and preparation method thereof comprehensively utilizing discarded marine product preparation |
| CN110683882A (en) * | 2019-11-13 | 2020-01-14 | 湛江市绿海生物工程有限公司 | Process method for preparing amino acid water-soluble fertilizer from feather meal |
| CN115087351A (en) * | 2020-02-14 | 2022-09-20 | 禾大国际股份公开有限公司 | Seed coating additive |
| CN112159288A (en) * | 2020-08-31 | 2021-01-01 | 东北农业大学 | Biologically fermented feed-grade organic fertilizer and preparation method thereof |
| CN115403429A (en) * | 2022-08-20 | 2022-11-29 | 海南农佳佳科技发展有限公司 | Amino acid water-soluble fertilizer and preparation method thereof |
| CN116514581A (en) * | 2023-02-20 | 2023-08-01 | 馆陶县三绿农业高科技有限公司 | Amino acid fertilizer with low salt and low proline content and preparation method thereof |
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