CN102272250A - 光致变色油墨的制备 - Google Patents

光致变色油墨的制备 Download PDF

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Publication number
CN102272250A
CN102272250A CN2009801541524A CN200980154152A CN102272250A CN 102272250 A CN102272250 A CN 102272250A CN 2009801541524 A CN2009801541524 A CN 2009801541524A CN 200980154152 A CN200980154152 A CN 200980154152A CN 102272250 A CN102272250 A CN 102272250A
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CN
China
Prior art keywords
hydrogen
alkyl
spiropyran
phenyl
alkoxy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2009801541524A
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English (en)
Chinese (zh)
Inventor
M·毛雷尔
M·许金
T·莱曼
L·费勒
B·因德比兹恩
A·富赫斯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CN102272250A publication Critical patent/CN102272250A/zh
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K9/00Tenebrescent materials, i.e. materials for which the range of wavelengths for energy absorption is changed as a result of excitation by some form of energy
    • C09K9/02Organic tenebrescent materials
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D471/00Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00
    • C07D471/02Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00 in which the condensed system contains two hetero rings
    • C07D471/10Spiro-condensed systems
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D491/00Heterocyclic compounds containing in the condensed ring system both one or more rings having oxygen atoms as the only ring hetero atoms and one or more rings having nitrogen atoms as the only ring hetero atoms, not provided for by groups C07D451/00 - C07D459/00, C07D463/00, C07D477/00 or C07D489/00
    • C07D491/02Heterocyclic compounds containing in the condensed ring system both one or more rings having oxygen atoms as the only ring hetero atoms and one or more rings having nitrogen atoms as the only ring hetero atoms, not provided for by groups C07D451/00 - C07D459/00, C07D463/00, C07D477/00 or C07D489/00 in which the condensed system contains two hetero rings
    • C07D491/10Spiro-condensed systems
    • C07D491/107Spiro-condensed systems with only one oxygen atom as ring hetero atom in the oxygen-containing ring
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B57/00Other synthetic dyes of known constitution
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/02Printing inks
    • C09D11/03Printing inks characterised by features other than the chemical nature of the binder
    • C09D11/037Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/50Sympathetic, colour changing or similar inks
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2211/00Chemical nature of organic luminescent or tenebrescent compounds
    • C09K2211/10Non-macromolecular compounds
    • C09K2211/1018Heterocyclic compounds
    • C09K2211/1025Heterocyclic compounds characterised by ligands
    • C09K2211/1029Heterocyclic compounds characterised by ligands containing one nitrogen atom as the heteroatom
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2211/00Chemical nature of organic luminescent or tenebrescent compounds
    • C09K2211/10Non-macromolecular compounds
    • C09K2211/1018Heterocyclic compounds
    • C09K2211/1025Heterocyclic compounds characterised by ligands
    • C09K2211/1088Heterocyclic compounds characterised by ligands containing oxygen as the only heteroatom
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00Chemistry: analytical and immunological testing
    • Y10T436/14Heterocyclic carbon compound [i.e., O, S, N, Se, Te, as only ring hetero atom]
    • Y10T436/141111Diverse hetero atoms in same or different rings [e.g., alkaloids, opiates, etc.]

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)
  • Non-Silver Salt Photosensitive Materials And Non-Silver Salt Photography (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
CN2009801541524A 2009-01-08 2009-12-23 光致变色油墨的制备 Pending CN102272250A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09150214 2009-01-08
EP09150214.6 2009-01-08
PCT/EP2009/067825 WO2010079098A1 (en) 2009-01-08 2009-12-23 Preparation of a photochromic ink

Publications (1)

Publication Number Publication Date
CN102272250A true CN102272250A (zh) 2011-12-07

Family

ID=40429960

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2009801541524A Pending CN102272250A (zh) 2009-01-08 2009-12-23 光致变色油墨的制备

Country Status (10)

Country Link
US (2) US8287776B2 (https=)
EP (1) EP2385972A1 (https=)
JP (1) JP2012514671A (https=)
KR (1) KR20110106434A (https=)
CN (1) CN102272250A (https=)
AU (1) AU2009336680A1 (https=)
BR (1) BRPI0923937A2 (https=)
IL (1) IL213815A0 (https=)
MX (1) MX2011007275A (https=)
WO (1) WO2010079098A1 (https=)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107075287A (zh) * 2014-09-12 2017-08-18 多米诺英国有限公司 油墨组合物
CN107828283A (zh) * 2017-12-21 2018-03-23 宝艺新材料股份有限公司 纸板印刷用水性防伪油墨及其制备方法
CN116891480A (zh) * 2023-07-05 2023-10-17 浙江理工大学嵊州创新研究院有限公司 一种多重刺激响应螺吡喃类光致变色材料的制备方法和应用

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2011132941A (ru) * 2009-01-08 2013-02-20 Басф Се Временно-температурный индикатор, содержащий спиро-пираны на основе индоленина
US8772184B2 (en) 2009-03-31 2014-07-08 Illinois Tool Works Inc. Reversible color-changing sanitizer-indicating nonwoven wipe
US8772185B2 (en) 2010-10-15 2014-07-08 Illinois Tool Works Inc. Reversible color-changing ink formulations and nonwoven wipes
CN103288841B (zh) * 2013-05-28 2015-03-04 中国科学技术大学 一种螺吡喃取代二乙炔及其制备方法和应用
CN103524517A (zh) * 2013-10-25 2014-01-22 苏州大学 一种螺氮、氧-缩醛类化合物及其制备方法
CN113637020A (zh) * 2021-08-18 2021-11-12 江南大学 水溶性光致变色化合物及其制备方法与应用
CN114940844A (zh) * 2022-06-16 2022-08-26 西北工业大学 一种基于光响应的液晶型防伪油墨及其制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3964911A (en) * 1972-12-22 1976-06-22 La Cellophane Photographic reproduction processes using diazonium salts and substituted spiro[benzopyrane]
CN1180708A (zh) * 1997-11-12 1998-05-06 南开大学戈德防伪技术公司 光化学基因识别材料及其制备方法和用途
US20030002132A1 (en) * 2001-05-24 2003-01-02 Xerox Corporation Photochromic electrophoretic ink display

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4913354B1 (https=) 1970-12-19 1974-03-30
GB2214191B (en) * 1988-01-12 1990-10-31 Sicpa Holding Sa Reversibly photochromic printing inks
US5633109A (en) 1995-12-05 1997-05-27 Xerox Corporation Ink compositions with liposomes containing photochromic compounds
KR101173524B1 (ko) * 2004-02-02 2012-08-14 프레쉬포인트 홀딩스 에스아 원자가 이성체화를 기초로 하는 시간-온도 지시약
WO2008049755A2 (en) 2006-10-26 2008-05-02 Ciba Holding Inc. Light absorbing layer for photo-chromic systems
CN101611115A (zh) 2007-01-11 2009-12-23 弗雷什波因特控股有限公司 光稳定化的时间温度指示器
ATE489445T1 (de) 2007-01-11 2010-12-15 Basf Se Tti-indikator mit balancierten photochemischen prozessen
KR20100014829A (ko) 2007-01-22 2010-02-11 프레쉬포인트 홀딩스 에스아 올리고머성 스피로방향족 화합물을 기재로 한 시간-온도 지시계
CN101646940A (zh) 2007-02-27 2010-02-10 巴斯夫欧洲公司 变色指示剂
US7718325B2 (en) * 2007-06-13 2010-05-18 Xerox Corporation Photochromic material, inkless reimageable printing paper, and methods
EP2291382B1 (en) 2008-05-21 2011-12-14 Basf Se Time temperature indicator comprising indolenin based spiropyrans containing a n-acetylamido or n- acetylester side chain

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3964911A (en) * 1972-12-22 1976-06-22 La Cellophane Photographic reproduction processes using diazonium salts and substituted spiro[benzopyrane]
CN1180708A (zh) * 1997-11-12 1998-05-06 南开大学戈德防伪技术公司 光化学基因识别材料及其制备方法和用途
US20030002132A1 (en) * 2001-05-24 2003-01-02 Xerox Corporation Photochromic electrophoretic ink display

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107075287A (zh) * 2014-09-12 2017-08-18 多米诺英国有限公司 油墨组合物
CN107828283A (zh) * 2017-12-21 2018-03-23 宝艺新材料股份有限公司 纸板印刷用水性防伪油墨及其制备方法
CN116891480A (zh) * 2023-07-05 2023-10-17 浙江理工大学嵊州创新研究院有限公司 一种多重刺激响应螺吡喃类光致变色材料的制备方法和应用

Also Published As

Publication number Publication date
US20130026428A1 (en) 2013-01-31
JP2012514671A (ja) 2012-06-28
WO2010079098A1 (en) 2010-07-15
US8287776B2 (en) 2012-10-16
US20110297898A1 (en) 2011-12-08
IL213815A0 (en) 2011-07-31
BRPI0923937A2 (pt) 2016-01-12
AU2009336680A1 (en) 2011-07-28
EP2385972A1 (en) 2011-11-16
MX2011007275A (es) 2011-08-12
KR20110106434A (ko) 2011-09-28

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Application publication date: 20111207