CN102186772B - 具有可调的多孔性和表面形态的硅质材料及其合成方法 - Google Patents

具有可调的多孔性和表面形态的硅质材料及其合成方法 Download PDF

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CN102186772B
CN102186772B CN200980142127.4A CN200980142127A CN102186772B CN 102186772 B CN102186772 B CN 102186772B CN 200980142127 A CN200980142127 A CN 200980142127A CN 102186772 B CN102186772 B CN 102186772B
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particles
solution
additive
mixture
silica
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CN102186772A (zh
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布赖恩.T.霍兰
萨斯查.韦尔兹
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ChampionX LLC
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Ondeo Nalco Co
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/126—Preparation of silica of undetermined type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/141—Preparation of hydrosols or aqueous dispersions
    • C01B33/142—Preparation of hydrosols or aqueous dispersions by acidic treatment of silicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/02—Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991—Coated

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Dispersion Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Silicon Compounds (AREA)
  • Catalysts (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
CN200980142127.4A 2008-09-12 2009-09-11 具有可调的多孔性和表面形态的硅质材料及其合成方法 Active CN102186772B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/209,790 2008-09-12
US12/209,790 US8790608B2 (en) 2008-09-12 2008-09-12 Siliceous materials having tunable porosity and surface morphology and methods of synthesizing same
PCT/US2009/056659 WO2010030878A2 (en) 2008-09-12 2009-09-11 Siliceous materials having tunable porosity and surface morphology and methods of synthesizing same

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CN102186772A CN102186772A (zh) 2011-09-14
CN102186772B true CN102186772B (zh) 2015-07-22

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Country Status (8)

Country Link
US (1) US8790608B2 (enExample)
EP (1) EP2346782A2 (enExample)
JP (1) JP5615281B2 (enExample)
KR (1) KR101682254B1 (enExample)
CN (1) CN102186772B (enExample)
MY (1) MY155398A (enExample)
TW (1) TWI527758B (enExample)
WO (1) WO2010030878A2 (enExample)

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US10227238B2 (en) * 2006-04-04 2019-03-12 Ecolab Usa Inc. Production and use of polysilicate particulate materials
US8764974B2 (en) 2010-04-16 2014-07-01 Nalco Company Processing aids to improve the bitumen recovery and froth quality in oil sands extraction processes
US10087081B2 (en) 2013-03-08 2018-10-02 Ecolab Usa Inc. Process for producing high solids colloidal silica
WO2015191962A1 (en) 2014-06-12 2015-12-17 Arizona Board Of Regents On Behalf Of Arizona State University Carbon dioxide adsorbents
CA2992720C (en) 2015-07-18 2025-04-22 Ecolab Usa Inc. Chemical additives for improving oil removal in distillation residue treatment operations
CN105251446B (zh) * 2015-11-11 2018-02-02 中国电建集团中南勘测设计研究院有限公司 一种地下水复合重金属污染修复材料
CN105329906B (zh) * 2015-11-30 2017-06-23 中海油天津化工研究设计院有限公司 一种丙烯腈催化剂用硅溶胶的制备方法
WO2018136695A1 (en) 2017-01-20 2018-07-26 Seo Dong Kyun Aluminosilicate nanorods
CN106823850B (zh) * 2017-03-08 2019-05-24 常州大学 一种桥架有机硅膜孔径的调控方法
JP7034435B2 (ja) * 2017-11-29 2022-03-14 東洋製罐グループホールディングス株式会社 複合体及びその製造方法。
KR102252313B1 (ko) * 2019-01-23 2021-05-14 청주대학교 산학협력단 중공의 다공성 실리카 나노구 및 그 제조방법
US12006439B2 (en) * 2019-03-27 2024-06-11 Canon Kabushiki Kaisha Optical member, optical device and coating liquid
CN120137436B (zh) * 2025-04-22 2025-11-11 中国科学院宁波材料技术与工程研究所 一种硅钛复合防雾涂层及其制备方法与应用

Citations (3)

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CN1241952A (zh) * 1996-11-26 2000-01-19 卡伯特公司 有机改性气凝胶、通过在没有在先溶剂交换的情况下表面改性水凝胶,然后干燥而制备有机改性气凝胶的方法、及其用途
US6680013B1 (en) * 1999-04-15 2004-01-20 Regents Of The University Of Minnesota Synthesis of macroporous structures

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US4451388A (en) 1981-11-02 1984-05-29 Nalco Chemical Company Preparation of aluminum oxide coated silica sols using ultrafiltration
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CN1241952A (zh) * 1996-11-26 2000-01-19 卡伯特公司 有机改性气凝胶、通过在没有在先溶剂交换的情况下表面改性水凝胶,然后干燥而制备有机改性气凝胶的方法、及其用途
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Also Published As

Publication number Publication date
CN102186772A (zh) 2011-09-14
WO2010030878A2 (en) 2010-03-18
US8790608B2 (en) 2014-07-29
EP2346782A2 (en) 2011-07-27
KR20110073443A (ko) 2011-06-29
KR101682254B1 (ko) 2016-12-02
JP2012501958A (ja) 2012-01-26
WO2010030878A3 (en) 2010-05-06
MY155398A (en) 2015-10-15
TWI527758B (zh) 2016-04-01
TW201010942A (en) 2010-03-16
US20100068519A1 (en) 2010-03-18
JP5615281B2 (ja) 2014-10-29

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