CN102178614A - Compound Chinese herbal medicine toothpaste and preparation method of same - Google Patents
Compound Chinese herbal medicine toothpaste and preparation method of same Download PDFInfo
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- CN102178614A CN102178614A CN 201110086550 CN201110086550A CN102178614A CN 102178614 A CN102178614 A CN 102178614A CN 201110086550 CN201110086550 CN 201110086550 CN 201110086550 A CN201110086550 A CN 201110086550A CN 102178614 A CN102178614 A CN 102178614A
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Abstract
A compound Chinese herbal medicine toothpaste comprises baicalin with the mass percent content of 0.05-0.4%, chlorophyll or the copper or sodium salt of the same with the mass percent content of 0.01-0.05%, Paeonol with the mass percent content of 0.014-0.075%, and the balance of basic ingredients of toothpaste. The compound Chinese herbal medicine toothpaste solves the technical problem that the prior art has slight effect of treating gingival bleeding and gingivitis, being a toothpaste especially applicable to cleaning the oral cavity, removing ozostomia and eliminating mouth disease.
Description
Technical field
The present invention relates to a kind of toothpaste, specifically a kind of toothpaste that contains multiple herbal component.
Background technology
Toothpaste is a kind of daily living article, can take care of one's teeth cleaning oral cavity.Many pointed toothpaste have also appearred in the problem at people's tooth often occurs, and as hypo-allergenic toothpaste, alleviate the toothpaste of gingival hemorrhage.A kind of the tooth gingivitis there is inhibiting compound recipe toothpaste as disclosing among the Chinese patent literature CN100525742C, forms for 25 parts by by weight ratio each 0.2 part of 3 parts of 20 parts of 0 part of 20 parts of 1 part of 5 parts of 5 parts of 10 parts of 0.4 part of 0.4 part of 0.2 part of Flos Lonicerae extract, Herba portulacae extract, Folium perillae extract, glycerol, sorbitol, propylene glycol, xanthan gum, abrasivus calcium carbonate, silica 1, titanium dioxides, sodium lauryl sulfates, Oleum Menthae Rotundifoliae, Oleum menthae, Fructus Citri Limoniae oil, citrus oils, 0.3 part of aspartame, 0.3 part of sodium pyrosulfate, 0.05 part of sodium benzoate and water.In this technical scheme, in toothpaste, added Chinese herbal medicine extract such as Flos Lonicerae, Herba Portulacae, Folium Perillae, be used to suppress the tooth gingivitis.But because its active constituent content that plays a role is lower in such Chinese herbal medicine, the ratio that described Chinese herbal medicine is added in the toothpaste is very low again, causes described toothpaste drug effect poor, again owing to the each consumption of toothpaste is limited, thereby be difficult to play corresponding effect, have little effect.
Summary of the invention
For this reason, technical problem to be solved by this invention is compound recipe toothpaste of the prior art, and its medicinal herb components drug effect is relatively poor, the technical problem of DeGrain, thereby proposes a kind of compound Chinese herb toothpaste with good efficacy.
For solving the problems of the technologies described above, a kind of compound Chinese herb toothpaste of the present invention, comprise that the quality percentage composition is that the baicalin of 0.05%-0.4%, chlorophyll that the quality percentage composition is 0.01%-0.05% or its copper sodium and quality percentage composition are the paeonol of 0.014%-0.075%, all the other are the toothpaste base furnish.
The quality percentage composition of described baicalin is 0.1%, and the quality percentage composition of described chlorophyll or its copper sodium is 0.02%, and the quality percentage composition of described paeonol is 0.0455%.
Described toothpaste base furnish comprises that the quality percentage composition is the glycerol of 10%-15%, the quality percentage composition is the deionized water of 20%-35%, the quality percentage composition is the composite binding agent of 0.81%-1.3%, the quality percentage composition is the foaming agent of 1.5%-3%, the quality percentage composition is the sweeting agent of 0.1%-0.25%, the quality percentage composition is the natural calcite powder of 20%-60%, the quality percentage composition is the carbamide of 0-3%, the quality percentage composition is the essence of 0.7-1.5%, the quality percentage composition is that silicon dioxide and the quality percentage composition of 0-10% is the sodium silicate of 0-0.8%.
A kind of compound Chinese herb toothpaste, comprise that the quality percentage composition is that the baicalin of 0.05%-0.4%, chlorophyll that the quality percentage composition is 0.01%-0.05% or its copper sodium, quality percentage composition are the paeonol of 0.014%-0.075%, comprise that also the quality percentage composition is that 0.014%-0.09% Oleum Caryophylli, quality percentage composition are one or more in the Borneolum Syntheticum of 0.0007%-0.0135% and the thymol that the quality percentage composition is 0.007%-0.045%, all the other are basic toothpaste batching.
The quality percentage composition of described Oleum Caryophylli is 0.052%, and the quality percentage composition of described Borneolum Syntheticum is 0.0065%, and the quality percentage composition of described thymol is 0.026%.
Described toothpaste base furnish comprises that the quality percentage composition is the glycerol of 10%-15%, the quality percentage composition is the deionized water of 20%-35%, the quality percentage composition is the composite binding agent of 0.81%-1.3%, the quality percentage composition is the foaming agent of 1.5%-3%, the quality percentage composition is the sweeting agent of 0.1%-0.25%, the quality percentage composition is the natural calcite powder of 20%-60%, the quality percentage composition is the carbamide of 0-3%, the quality percentage composition is the essence of 0.7-1.5%, the quality percentage composition is that silicon dioxide and the quality percentage composition of 0-10% is the sodium silicate of 0-0.8%.
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.1% baicalin, the quality percentage composition is 0.02% sodium copper chlorophllin, the quality percentage composition is 0.0455% paeonol, the quality percentage composition is 0.0065% Borneolum Syntheticum, the quality percentage composition is 0.052% Oleum Caryophylli, the quality percentage composition is 0.026% thymol, the quality percentage composition is 12% glycerol, the quality percentage composition is 31.18% deionized water, the quality percentage composition is the cellulose gum of 1.05 %, the quality percentage composition is 0.1% xanthan gum, the quality percentage composition is 2.2% sodium lauryl sulphate, the quality percentage composition is 0.25% glucide, the quality percentage composition is 45% natural calcite powder, the quality percentage composition is 4% silicon dioxide, the quality percentage composition is 0.8% sodium silicate, the quality percentage composition is that 2% carbamide and quality percentage composition are 1.3% essence.
A kind of method for preparing compound Chinese herb toothpaste is characterized in that, comprises the steps:
(1) composite binding agent, foaming agent are added in the glycerol, be uniformly dispersed, form glycerite by high-speed stirred;
(2) sweeting agent, carbamide, chlorophyll or its copper sodium, baicalin are dissolved in the deionized water, form aqueous solution;
(3) the paeonol dissolving is made an addition in the essence;
(4) aqueous solution in the described step (2) is mixed with glycerite in the described step (1), leave standstill and add natural calcite, silicon dioxide and described essence after 5-10 hour, the high-speed stirred homogenizing forms mastic, fill then under vacuum 0.092-0.1MPa degassing phase.
In described step (3), with the quality percentage composition that accounts for described toothpaste be the Borneolum Syntheticum of 0.0007%-0.0135%, Oleum Caryophylli that the quality percentage composition is 0.014%-0.09% and quality percentage composition be 0.007%-0.045% thymol in one or more dissolvings make an addition in the described essence.
In described step (4), time of repose is 8 hours, carries out high-speed stirred under the degassing phase of vacuum 0.96Mpa.
Technique scheme of the present invention has the following advantages compared to existing technology,
(1) compound Chinese herb toothpaste of the present invention; comprise that the quality percentage composition is the baicalin of 0.05%-0.4%; the quality percentage composition is that the chlorophyll of 0.01%-0.05% or its copper sodium and quality percentage composition are the paeonol of 0.014%-0.075%; the effect that not only has cleaning oral cavity; also have auxiliary hemostasis; the effect that suppresses the tooth bacterium; chlorophyll and derivant thereof and baicalin use the effect with good anti-inflammation hemostasia and counteract oral malodour simultaneously; and paeonol has good antianaphylactic effect; make that not only oral environment is effectively purified; and make tooth be protected, gingival hemorrhage; the symptom of hemodia is effectively alleviated.Effective percentage to gingivitis reaches 91%, effective percentage to gingival hemorrhage reaches 81%, and in the experiment general toothpaste to the effective percentage of gingivitis only 76%, effective percentage to gingival hemorrhage is 62%, this shows, its curative effect of compound Chinese herb toothpaste of the present invention makes that far above general toothpaste symptoms such as oral disease such as gingivitis, gingival hemorrhage, halitosis and tooth body allergy are effectively alleviated.
(2) compound Chinese herb toothpaste of the present invention, the quality percentage composition of described baicalin is 0.1%, the quality percentage composition of described chlorophyll or its copper sodium is 0.02%, the quality percentage composition of described paeonol is 0.0455%, this optimum ratio not only can be so that the curative effect of toothpaste be preferable, and make that the color and luster of toothpaste is attractive in appearance, can not make to have good result of use by the toothpaste its colour changed into yellow owing to the too high levels of baicalin.
(3) compound Chinese herb toothpaste of the present invention, also comprise the quality percentage composition and be 0.014%-0.09% Oleum Caryophylli, quality percentage composition and be the Borneolum Syntheticum of 0.0007%-0.0135%, in the thymol that the quality percentage composition is 0.007%-0.045% one or more, described Oleum Caryophylli, Borneolum Syntheticum and thymol make the effect of described toothpaste anti-inflammation hemostasia, inhibition oral cavity bacterium further improve, be used with baicalin and have better therapeutic, can reduce simultaneously the component of baicalin, make that the color and luster of toothpaste is better, effect is strengthened.
(4) compound Chinese herb toothpaste of the present invention, preferred described Oleum Caryophylli accounts for 0.052% of quality percentage composition, described Borneolum Syntheticum accounts for 0.0065% of quality percentage composition, described thymol accounts for 0.026% of quality percentage composition, this preferred component has not only guaranteed the toothpaste favorable effects, and strengthened the effect of its anti-inflammation hemostasia, and also further save cost, have good cost performance.
(5) compound Chinese herb toothpaste of the present invention, described chlorophyll or its copper sodium are sodium copper chlorophllin, described sodium copper chlorophllin not only is easy to extract and add, and has the effect in good alleviation halitosis, pure and fresh oral cavity, further improves the whole structure of toothpaste.
(6) preparation method of compound Chinese herb toothpaste of the present invention, at first make aqueous solution, then with sweeting agent, carbamide, chlorophyll or its copper sodium, baicalin is dissolved in the deionized water, form aqueous solution, again described aqueous solution is mixed with described glycerite, after leaving standstill 5-10 hour, preferred herein 8 hours, can reach good mixed effect, add natural calcite then, silicon dioxide and the essence that has added paeonol, at vacuum 0.092-0.1Mpa, the high-speed stirred homogenizing forms mastic under the degassing phase of preferred 0.096Mpa, fill then, in this technical scheme, paeonol etc. is difficult for water-soluble material adds in the essence, make its easier dissolving, guarantee the effect that it is good, simultaneously, this preparation method step is simple, and has guaranteed that each component can well bring into play its effect, adopt natural plant extract, make the safety of toothpaste improve.
(7) preparation method of compound Chinese herb toothpaste of the present invention, described Borneolum Syntheticum, Oleum Caryophylli and thymol all add in the essence earlier, again described essence is added in the described toothpaste, make these be difficult for the well dissolving in essence of water-soluble material like this, give full play to its effect, by the mode of adding essence it is added in the toothpaste, not only method is simple but also effective, simultaneously the component of natural essence oil not only makes toothpaste have good mouthfeel but also has guaranteed the safety of toothpaste more than 90% in described essence.
The specific embodiment
Provide the specific embodiment of the described compound Chinese herb toothpaste of present embodiment below:
Embodiment 1:
A kind of compound Chinese herb toothpaste, comprise that the quality percentage composition is 0.05% baicalin, the quality percentage composition is that 0.02% sodium copper chlorophllin (being CHLOROPHYLLINE-copper complex CI 75810 herein) and quality percentage composition are 0.05% paeonol, all the other are the toothpaste base furnish, and toothpaste base furnish in the present embodiment is: the quality percentage composition is 12% glycerol, the quality percentage composition is 29% deionized water, the quality percentage composition is 1% cellulose gum (as composite binding agent), the quality percentage composition is 2% lauryl sulphate acid fat sodium (foaming agent), the quality percentage composition is 0.2% glucide (sweeting agent), the quality percentage composition is 54.6% natural calcite powder, the quality percentage composition is 1.08% essence.
A kind of method for preparing the compound Chinese herb toothpaste in the foregoing description 1 comprises the steps:
(1) cellulose gum, lauryl sulphate acid fat sodium are added in the glycerol, be uniformly dispersed, form glycerite by high-speed stirred;
(2) glucide, sodium copper chlorophllin, baicalin are dissolved in the deionized water, form aqueous solution;
(3) the paeonol dissolving is made an addition in the essence;
(4) described aqueous solution is mixed with described glycerite, leave standstill adding natural calcite and described essence after 8 hours, the high-speed stirred homogenizing forms mastic, fill then under vacuum 0.096MPa degassing phase.
Embodiment 2:
A kind of compound Chinese herb toothpaste, comprise that the quality percentage composition is 0.4% baicalin, the quality percentage composition is that 0.03% chlorophyll and quality percentage composition are 0.06% paeonol, all the other are the toothpaste base furnish, and toothpaste base furnish in the present embodiment is: the quality percentage composition is 15% glycerol, the quality percentage composition is 31% deionized water, the quality percentage composition is 0.9% cellulose gum (as composite binding agent), the quality percentage composition is 1.5% lauryl sulphate acid fat sodium (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 45% natural calcite powder, the quality percentage composition is 1% carbamide, the quality percentage composition is 0.81% essence, the quality percentage composition is that 4% silicon dioxide and quality percentage composition are 0.2% sodium silicate.
A kind of method for preparing the compound Chinese herb toothpaste in the foregoing description 2 comprises the steps:
(1) cellulose gum, lauryl sulphate acid fat sodium are added in the glycerol, be uniformly dispersed, form glycerite by high-speed stirred;
(2) glucide, carbamide, sodium silicate, sodium copper chlorophllin, baicalin are dissolved in the deionized water, form aqueous solution;
(3) the paeonol dissolving is made an addition in the essence;
(4) described aqueous solution is mixed with described glycerite, leave standstill and add natural calcite, silicon dioxide and described essence after 8 hours, the high-speed stirred homogenizing forms mastic, fill then under vacuum 0.096MPa degassing phase.
Embodiment 3:
A kind of compound Chinese herb toothpaste, comprise that the quality percentage composition is 0.1% baicalin, the quality percentage composition is that 0.01% sodium copper chlorophllin and quality percentage composition are 0.04% paeonol, all the other are the toothpaste base furnish, and toothpaste base furnish in the present embodiment is: the quality percentage composition is 12% glycerol, the quality percentage composition is 29% deionized water, the quality percentage composition is 1% cellulose gum (as composite binding agent), the quality percentage composition is 2% lauryl sulphate acid fat sodium (foaming agent), the quality percentage composition is 0.2% glucide (sweeting agent), the quality percentage composition is 49% natural calcite powder, the quality percentage composition is 1% carbamide, the quality percentage composition is 1.05% essence, the quality percentage composition is that 4% silicon dioxide and quality percentage composition are 0.6% sodium silicate.
Embodiment 4:
A kind of compound Chinese herb toothpaste, comprise that percentage composition is 0.3% baicalin, percentage composition is that 0.05% chlorophyll and quality percentage composition are 0.035% paeonol, all the other are the toothpaste base furnish, and the toothpaste base furnish comprises that the quality percentage composition is 15% glycerol, the quality percentage composition is 35.005% deionized water, the quality percentage composition is 1.3% cellulose gum (as composite binding agent), the quality percentage composition is 3% lauryl sulphate acid fat sodium (foaming agent), the quality percentage composition is 0.25% glucide (sweeting agent), the quality percentage composition is 30% natural calcite powder, the quality percentage composition is 3% carbamide, the quality percentage composition is 1.26% essence, the quality percentage composition is that 10% silicon dioxide and quality percentage composition are 0.8% sodium silicate.
Embodiment 5:
A kind of compound Chinese herb toothpaste, comprise that the quality percentage composition is 0.08% baicalin, the quality percentage composition is that 0.04% sodium copper chlorophllin and quality percentage composition are 0.014% paeonol, all the other are the toothpaste base furnish, and the toothpaste base furnish comprises that the quality percentage composition is 13% glycerol, the quality percentage composition is 30% deionized water, the quality percentage composition is 1.1% cellulose gum (as composite binding agent), the quality percentage composition is 2.5% lauryl sulphate acid fat sodium (foaming agent), the quality percentage composition is 0.2% glucide (sweeting agent), the quality percentage composition is 52% natural calcite powder, the quality percentage composition is 1.066% essence.
Embodiment 6:
A kind of compound Chinese herb toothpaste, comprise that the quality percentage composition is 0.2% baicalin, the quality percentage composition is that 0.02% chlorophyll and quality percentage composition are 0.075% paeonol, all the other are the toothpaste base furnish, and described toothpaste base furnish comprises that the quality percentage composition is 10% glycerol, the quality percentage composition is 20% deionized water, the quality percentage composition is 0.81% cellulose gum (as composite binding agent), the quality percentage composition is 1.5% lauryl sulphate acid fat sodium (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 52% natural calcite powder, the quality percentage composition is the essence of 1.495 %, the quality percentage composition is 3% carbamide, the quality percentage composition is that 10% silicon dioxide and quality percentage composition are 0.8% sodium silicate.
Embodiment 7:
A kind of compound Chinese herb toothpaste, comprise that the quality percentage composition is 0.1% baicalin, the quality percentage composition is that 0.02% sodium copper chlorophllin and quality percentage composition are 0.0455% paeonol, all the other are the toothpaste base furnish, and described toothpaste base furnish comprises that the quality percentage composition is 12% glycerol, the quality percentage composition is 31.12% deionized water, the quality percentage composition is 1.15% cellulose gum (as composite binding agent), the quality percentage composition is 2.2% lauryl sulphate acid fat sodium (foaming agent), the quality percentage composition is 0.25% glucide (sweeting agent), the quality percentage composition is 45% natural calcite powder, the quality percentage composition is 2% carbamide, the quality percentage composition is 1.3145% essence, the quality percentage composition is that 4% silicon dioxide and quality percentage composition are 0.8% sodium silicate.
In the foregoing description 3-7, the preparation method of embodiment 3-7 is identical with the preparation method of embodiment 2.
Embodiment 8
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.02% chlorophyll, the quality percentage composition is a baicalin 0.1%, the quality percentage composition is 0.0455% paeonol, the quality percentage composition is 0.0065% Borneolum Syntheticum, the quality percentage composition is 0.052% Oleum Caryophylli, 0.026% thymol, the quality percentage composition is 12% glycerol, the quality percentage composition is 31.05% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 1.05 %, the quality percentage composition is 0.1% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 2.2% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.25% glucide, the quality percentage composition is 45% natural calcite powder, the quality percentage composition is 4% silicon dioxide, the quality percentage composition is 0.8% sodium silicate, the quality percentage composition is that 2% carbamide and quality percentage composition are 1.3% essence.
During the described compound Chinese herb toothpaste of a kind of preparation the foregoing description 8, it comprises the steps:
(1) cellulose gum, xanthan gum, lauryl sulphate acid fat sodium are added in the glycerol, be uniformly dispersed, form glycerite by high-speed stirred;
(2) glucide, carbamide, sodium silicate, chlorophyll, baicalin are dissolved in the deionized water, form aqueous solution;
(3) paeonol, Oleum Caryophylli, Borneolum Syntheticum, thymol dissolving are made an addition in the essence;
(4) described aqueous solution is mixed with described glycerite, leave standstill and add natural calcite, silicon dioxide and described essence after 10 hours, the high-speed stirred homogenizing forms mastic, fill then under vacuum 0.092MPa degassing phase.
Embodiment 9
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.02% chlorophyll, the quality percentage composition is a baicalin 0.1%, the quality percentage composition is 0.0443% paeonol, the quality percentage composition is 0.09% Oleum Caryophylli, the quality percentage composition is 0.0007% Borneolum Syntheticum, the quality percentage composition is 0.045% thymol, the quality percentage composition is 12% glycerol, the quality percentage composition is 31% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 1.05 %, the quality percentage composition is 0.1% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 2.2% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.25% glucide (sweeting agent), the quality percentage composition is 45% natural calcite powder, the quality percentage composition is 4% silicon dioxide, the quality percentage composition is 0.8% sodium silicate, the quality percentage composition is that 2% carbamide and quality percentage composition are 1.3% essence.
During the described compound Chinese herb toothpaste of a kind of preparation the foregoing description 9, it comprises the steps:
(1) cellulose gum, xanthan gum, lauryl sulphate acid fat sodium are added in the glycerol, be uniformly dispersed, form glycerite by high-speed stirred;
(2) glucide, carbamide, sodium silicate, chlorophyll, baicalin are dissolved in the deionized water, form aqueous solution;
(3) paeonol, Oleum Caryophylli, Borneolum Syntheticum, thymol dissolving are made an addition in the essence;
(4) described aqueous solution is mixed with described glycerite, leave standstill and add natural calcite, silicon dioxide and described essence after 5 hours, the high-speed stirred homogenizing forms mastic, fill then under vacuum 0.1MPa degassing phase.
Embodiment 10
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.03% chlorophyll, the quality percentage composition is a baicalin 0.2%, the quality percentage composition is 0.0395% paeonol, the quality percentage composition is 0.01% Oleum Caryophylli, the quality percentage composition is 0.0135% Borneolum Syntheticum, the quality percentage composition is 0.007% thymol, the quality percentage composition is 12% glycerol, the quality percentage composition is 35% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 1 %, the quality percentage composition is 0.3% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 3% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.2% glucide (sweeting agent), the quality percentage composition is 35.7% natural calcite powder, the quality percentage composition is 8% silicon dioxide, the quality percentage composition is 0.5% sodium silicate, the quality percentage composition is that 3% carbamide and quality percentage composition are 1% essence.
Embodiment 11
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.04% chlorophyll, the quality percentage composition is a baicalin 0.4%, the quality percentage composition is 0.07% paeonol, the quality percentage composition is 0.052% Oleum Caryophylli, the quality percentage composition is 0.0065% Borneolum Syntheticum, the quality percentage composition is 0.026% thymol, the quality percentage composition is 10% glycerol, the quality percentage composition is 30% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 0.5 %, the quality percentage composition is 0.31% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 1.5% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 53.4955% natural calcite powder, the quality percentage composition is 1% silicon dioxide, the quality percentage composition is 0.5% sodium silicate, the quality percentage composition is that 1% carbamide and quality percentage composition are 1% essence.
Embodiment 12
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.02% chlorophyll, the quality percentage composition is a baicalin 0.2%, the quality percentage composition is 0.07% paeonol, the quality percentage composition is 0.09% Oleum Caryophylli, the quality percentage composition is 0.0135% Borneolum Syntheticum, the quality percentage composition is 10% glycerol, the quality percentage composition is 30.22% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 0.5 %, the quality percentage composition is 0.31% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 1.5% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 53.4765% natural calcite powder, the quality percentage composition is 1% silicon dioxide, the quality percentage composition is 0.5% sodium silicate, the quality percentage composition is that 1% carbamide and quality percentage composition are 1% essence.
Embodiment 13
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.02% chlorophyll, the quality percentage composition is a baicalin 0.2%, the quality percentage composition is 0.07% paeonol, the quality percentage composition is 0.0007% Borneolum Syntheticum, the quality percentage composition is 0.045% thymol, the quality percentage composition is 10% glycerol, the quality percentage composition is 30.22% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 0.5 %, the quality percentage composition is 0.31% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 1.5% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 53.5343% natural calcite powder, the quality percentage composition is 1% silicon dioxide, the quality percentage composition is 0.5% sodium silicate, the quality percentage composition is that 1% carbamide and quality percentage composition are 1% essence.
Embodiment 14
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.02% chlorophyll, the quality percentage composition is a baicalin 0.2%, the quality percentage composition is 0.07% paeonol, the quality percentage composition is 0.09% Oleum Caryophylli, the quality percentage composition is 0.007% thymol, the quality percentage composition is 10% glycerol, the quality percentage composition is 30.1687% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 0.5 %, the quality percentage composition is 0.31% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 1.5% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 53.5343% natural calcite powder, the quality percentage composition is 1% silicon dioxide, the quality percentage composition is 0.5% sodium silicate, the quality percentage composition is that 1% carbamide and quality percentage composition are 1% essence.
Embodiment 15
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.02% chlorophyll, the quality percentage composition is a baicalin 0.2%, the quality percentage composition is 0.07% paeonol, the quality percentage composition is 0.052% Oleum Caryophylli, the quality percentage composition is 10% glycerol, the quality percentage composition is 29.468% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 0.5 %, the quality percentage composition is 0.31% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 1.5% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 54.28% natural calcite powder, the quality percentage composition is 1% silicon dioxide, the quality percentage composition is 0.5% sodium silicate, the quality percentage composition is that 1% carbamide and quality percentage composition are 1% essence.
Embodiment 16
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.02% chlorophyll, the quality percentage composition is a baicalin 0.2%, the quality percentage composition is 0.07% paeonol, the quality percentage composition is 0.0065% Borneolum Syntheticum, the quality percentage composition is 10% glycerol, the quality percentage composition is 29.6435% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 0.5 %, the quality percentage composition is 0.31% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 1.5% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 54.15% natural calcite powder, the quality percentage composition is 1% silicon dioxide, the quality percentage composition is 0.5% sodium silicate, the quality percentage composition is that 1% carbamide and quality percentage composition are 1% essence.
Embodiment 17
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.02% chlorophyll, the quality percentage composition is a baicalin 0.2%, the quality percentage composition is 0.07% paeonol, the quality percentage composition is 0.026% thymol, 0.0065% Borneolum Syntheticum, the quality percentage composition is 10% glycerol, the quality percentage composition is 29.6175% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 0.5 %, the quality percentage composition is 0.31% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 1.5% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 54.15% natural calcite powder, the quality percentage composition is 1% silicon dioxide, the quality percentage composition is 0.5% sodium silicate, the quality percentage composition is that 1% carbamide and quality percentage composition are 1% essence.
Embodiment 18
A kind of compound Chinese herb toothpaste comprises that the quality percentage composition is 0.02% chlorophyll, the quality percentage composition is a baicalin 0.2%, the quality percentage composition is 0.07% paeonol, the quality percentage composition is 0.014% Oleum Caryophylli, the quality percentage composition is 0.01% Borneolum Syntheticum, the quality percentage composition is 0.02% thymol, the quality percentage composition is 10% glycerol, the quality percentage composition is 29.606% deionized water, the quality percentage composition is the cellulose gum (composite binding agent a kind of) of 0.5 %, the quality percentage composition is 0.31% xanthan gum (a composite binding agent a kind of), the quality percentage composition is 1.5% sodium lauryl sulphate (foaming agent), the quality percentage composition is 0.1% glucide (sweeting agent), the quality percentage composition is 54.15% natural calcite powder, the quality percentage composition is 1% silicon dioxide, the quality percentage composition is 0.5% sodium silicate, the quality percentage composition is that 1% carbamide and quality percentage composition are 1% essence.
In the foregoing description 10-18, the preparation method of described compound Chinese herb toothpaste is identical with preparation method among the embodiment 8, just in step (3), one or more substance dissolves in Oleum Caryophylli, Borneolum Syntheticum, the thymol are added in the essence according to the difference of preparing burden.
Provide the one group data of above-mentioned compound Chinese herb toothpaste in Zhejiang Provincial People's Hospital's clinical experiment below, the case source is as shown in table 1:
Table 1
The A group is used compound Chinese herb toothpaste of the present invention, and the B group is used ordinary toothpaste, and through bimestrial clinical experiment, the statistical data that obtains is as shown in table 2 below:
Table 2
In the above-mentioned statistics, it is effectively more than 70% that gingivitis indices reduces, and reducing by 100% is produce effects; It is effectively more than 85% that the bleeding index of gingival hemorrhage reduces, and reducing by 100% is produce effects.
By above-mentioned experiment as seen, A group compound Chinese herb toothpaste is 91.1% to the effective percentage of gingivitis, and the effective percentage of matched group toothpaste B group is 76.7%, both curative effect significant differences (P＜0.01).
A group compound Chinese herb toothpaste is 80.88% to the effective percentage of gingival hemorrhage, and the effective percentage of matched group B group toothpaste is 62.50%, both curative effect significant differences (P＜0.01).
In addition, compound Chinese herb toothpaste of the present invention is to halitosis, dentin hypersensitiveness, and periodontal pain, severe periodontal disease also have better curative effect, and experimental data is as follows:
Table 3
By above-mentioned experimental data as seen, toothpaste of the present invention is compared with ordinary toothpaste other periodontals such as halitosis, tooth body allergy, periodontal pains and is had better curative effect.
Find also that by experiment use present embodiment 1 described compound Chinese herb toothpaste, the effective percentage of gingivitis can reach 91.7%; Present embodiment 8 described compound Chinese herb toothpaste have mouthfeel preferably, use the back that the effective percentage of gingivitis is reached 93.1%, and situations of teeth has good improvement.
Obviously, the foregoing description only is for example clearly is described, and is not the qualification to embodiment.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here need not also can't give exhaustive to all embodiments.And conspicuous variation of being extended out thus or change still are among the protection domain of the invention.
Claims (10)
1. compound Chinese herb toothpaste, comprise that the quality percentage composition is that the baicalin of 0.05%-0.4%, chlorophyll that the quality percentage composition is 0.01%-0.05% or its copper sodium and quality percentage composition are the paeonol of 0.014%-0.075%, all the other are the toothpaste base furnish.
2. compound Chinese herb toothpaste according to claim 1 is characterized in that: the quality percentage composition of described baicalin is 0.1%, and the quality percentage composition of described chlorophyll or its copper sodium is 0.02%, and the quality percentage composition of described paeonol is 0.0455%.
3. compound Chinese herb toothpaste according to claim 1 and 2 is characterized in that: described toothpaste base furnish comprises that the quality percentage composition is the glycerol of 10%-15%, the quality percentage composition is the deionized water of 20%-35%, the quality percentage composition is the composite binding agent of 0.81%-1.3%, the quality percentage composition is the foaming agent of 1.5%-3%, the quality percentage composition is the sweeting agent of 0.1%-0.25%, the quality percentage composition is the natural calcite powder of 20%-60%, the quality percentage composition is the carbamide of 0-3%, the quality percentage composition is the essence of 0.7-1.5%, the quality percentage composition is that silicon dioxide and the quality percentage composition of 0-10% is the sodium silicate of 0-0.8%.
4. compound Chinese herb toothpaste comprises that the quality percentage composition is that the baicalin of 0.05%-0.4%, chlorophyll that the quality percentage composition is 0.01%-0.05% or its copper sodium, quality percentage composition are the paeonol of 0.014%-0.075%; Comprise that also the quality percentage composition is that 0.014%-0.09% Oleum Caryophylli, quality percentage composition are one or more in the Borneolum Syntheticum of 0.0007%-0.0135% and the thymol that the quality percentage composition is 0.007%-0.045%, all the other are basic toothpaste batching.
5. compound Chinese herb toothpaste according to claim 4 is characterized in that: the quality percentage composition of described Oleum Caryophylli is 0.052%, and the quality percentage composition of described Borneolum Syntheticum is 0.0065%, and the quality percentage composition of described thymol is 0.026%.
6. according to claim 4 or 5 described compound Chinese herb toothpaste, it is characterized in that: described toothpaste base furnish comprises that the quality percentage composition is the glycerol of 10%-15%, the quality percentage composition is the deionized water of 20%-35%, the quality percentage composition is the composite binding agent of 0.81%-1.3%, the quality percentage composition is the foaming agent of 1.5%-3%, the quality percentage composition is the sweeting agent of 0.1%-0.25%, the quality percentage composition is the natural calcite powder of 20%-60%, the quality percentage composition is the carbamide of 0-3%, the quality percentage composition is the essence of 0.7-1.5%, the quality percentage composition is that silicon dioxide and the quality percentage composition of 0-10% is the sodium silicate of 0-0.8%.
7. compound Chinese herb toothpaste according to claim 6 is characterized in that: the quality percentage composition is 0.1% baicalin, the quality percentage composition is 0.02% sodium copper chlorophllin, the quality percentage composition is 0.0455% paeonol, the quality percentage composition is 0.0065% Borneolum Syntheticum, the quality percentage composition is 0.052% Oleum Caryophylli, the quality percentage composition is 0.026% thymol, the quality percentage composition is 12% glycerol, the quality percentage composition is 31.05% deionized water, the quality percentage composition is the cellulose gum of 1.05 %, the quality percentage composition is 0.1% xanthan gum, the quality percentage composition is 2.2% sodium lauryl sulphate, the quality percentage composition is 0.25% glucide, the quality percentage composition is 45% natural calcite powder, the quality percentage composition is 4% silicon dioxide, the quality percentage composition is 0.8% sodium silicate, the quality percentage composition is that 2% carbamide and quality percentage composition are 1.3% essence.
8. a method for preparing compound Chinese herb toothpaste is characterized in that, comprises the steps:
Composite binding agent, foaming agent are added in the glycerol, be uniformly dispersed, form glycerite by high-speed stirred;
Sweeting agent, chlorophyll or its copper sodium, baicalin are dissolved in the deionized water, form aqueous solution;
The paeonol dissolving is made an addition in the essence;
Aqueous solution in the described step (2) is mixed with glycerite in the described step (1), leave standstill and add natural calcite and described essence after 5-10 hour, the high-speed stirred homogenizing forms mastic, fill then under vacuum 0.092-0.1MPa degassing phase.
9. method according to claim 8, it is characterized in that: in described step (3), with the quality percentage composition that accounts for described toothpaste be the Borneolum Syntheticum of 0.0007%-0.0135%, Oleum Caryophylli that the quality percentage composition is 0.014%-0.09% and quality percentage composition be 0.007%-0.045% thymol in one or more dissolvings make an addition in the described essence.
10. method according to claim 9 is characterized in that: in described step (4), time of repose is 8 hours, carries out high-speed stirred under the degassing phase of vacuum 0.096Mpa.
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| CN103445980A (en) * | 2013-08-24 | 2013-12-18 | 上海方木精细化工有限公司 | Paeonol tooth protection toothpaste |
| CN103520012A (en) * | 2013-10-18 | 2014-01-22 | 柳州两面针股份有限公司 | Application of baicalin in preparation of oral care product |
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| CN105943409A (en) * | 2016-05-28 | 2016-09-21 | 养美医药有限责任公司 | Traditional Chinese medicinal toothpaste for alleviating redness-swollenness and bleeding as well as pain of gum |
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| CN103445980A (en) * | 2013-08-24 | 2013-12-18 | 上海方木精细化工有限公司 | Paeonol tooth protection toothpaste |
| CN103445980B (en) * | 2013-08-24 | 2016-03-02 | 上海方木精细化工有限公司 | Paeonol tooth protection toothpaste |
| CN103520012A (en) * | 2013-10-18 | 2014-01-22 | 柳州两面针股份有限公司 | Application of baicalin in preparation of oral care product |
| CN104306268A (en) * | 2014-11-03 | 2015-01-28 | 广州百草堂药业有限公司 | Oral care product and extraction method of composition |
| CN105943409A (en) * | 2016-05-28 | 2016-09-21 | 养美医药有限责任公司 | Traditional Chinese medicinal toothpaste for alleviating redness-swollenness and bleeding as well as pain of gum |
| CN105943409B (en) * | 2016-05-28 | 2019-04-02 | 养美医药有限责任公司 | A kind of Chinese medicinal toothpaste mitigating gum redness bleeding pain |
| CN107412138A (en) * | 2017-09-06 | 2017-12-01 | 南京希元生物医药科技有限公司 | A kind of green bee glue tooth paste of Brazil |
| CN107412138B (en) * | 2017-09-06 | 2020-10-02 | 南京希元生物医药科技有限公司 | Brazil green propolis toothpaste |
| CN112691057A (en) * | 2020-12-23 | 2021-04-23 | 中国热带农业科学院热带作物品种资源研究所 | Compound functional toothpaste and preparation method thereof |
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Application publication date: 20110914 |