CN111281836A - Multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines and preparation method thereof - Google Patents

Multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines and preparation method thereof Download PDF

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CN111281836A
CN111281836A CN201811502102.8A CN201811502102A CN111281836A CN 111281836 A CN111281836 A CN 111281836A CN 201811502102 A CN201811502102 A CN 201811502102A CN 111281836 A CN111281836 A CN 111281836A
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powder
dried
grinding
long pepper
tooth
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贺云祥
何美英
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Hunan Hanfang Shennong Chinese Medical Clinic Co ltd
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Hunan Hanfang Shennong Chinese Medical Clinic Co ltd
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
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Abstract

A tooth powder for protecting teeth in various aspects is prepared from Chinese-medicinal materials including achyranthes root, long pepper, ovate leaf holly bark and dendrobium bark through low-temp pressurizing, baking and drying, grinding, and preparing tooth powder. The formula of the invention combines cold and heat, combines elevation and subsidence, and has the effects of tonifying kidney and strengthening teeth, clearing heat and purging fire, and relieving swelling and pain. Effectively solves the problems of toothache, loose teeth, soft teeth, gingival bleeding, gingival swelling and pain, gingival atrophy, tooth decay, decayed teeth, wind-fire toothache, fear of cold and heat, oral ulcer, halitosis, tartar and tartar accumulation, black and yellow teeth and the like.

Description

Multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines and preparation method thereof
Technical Field
The invention relates to a dentifrice and a preparation method thereof, in particular to a dentifrice which can protect various tooth and gum problems, such as toothache, loose teeth, soft teeth, gingival bleeding, gingival swelling and pain, gingival atrophy, dental caries, decayed teeth, wind-fire toothache, fear of cold and heat, oral ulcer, halitosis, tartar and tartar accumulation, black and yellow teeth and the like, and a preparation method thereof; belongs to the technical field of daily nursing articles and manufacturing methods thereof.
Background art:
prior to the advent of toothpaste, dentifrice was the most commonly used dental cleanser for people. In ancient times, various tools were used to wipe teeth for tooth brushing, and various dentifrices were added, most commonly salt, i.e., the precursor of dentifrice. In Song Dynasty, the "tooth powder line" appeared, and the tooth powder prepared by traditional Chinese medicines is specially sold, and the tooth powder has become social commodity. However, the tooth powder has the defect that the use is not very convenient, so people invent the toothpaste; the toothpaste and the tooth powder are different mainly in form, one is powder and the other is paste, and the main effective components are basically the same. However, recently, it has been found that the toothpaste in the form of paste greatly reduces the effect of the effective components due to the addition of a large amount of water and humectant, and particularly the whitening effect is greatly affected, and the dentifrice is improved and then displayed again in the life of people; with the progress of the technology, the formula and the process of the tooth powder are more mature, and the tooth powder is less and less different from the toothpaste. Toothpowders also have the following characteristics relative to toothpastes:
1. the dentifrice is coarser than toothpaste, and the friction of the dentifrice to teeth is larger, so that the dentifrice has advantages in removing tartar, dental plaque, tartar and the like.
2. Dentifrices generally contain little or no artificial pigment; the toothpaste is prepared by chemical process colloidal paste and contains artificial pigment and perfume.
3. The tooth powder has stronger dispelling power than toothpaste by gargling, and the toothpaste mainly removes bacteria, and generally can not dispel dental plaque, tartar and tartar.
At present, although the formula of the conventional dentifrice produced by different manufacturers is different and the ingredients of the dentifrice are different, the main components of the dentifrice are not separated from abradants (calcium carbonate, hydrated silica, calcium hydrogen phosphate and the like), surfactants (SLS), sweeteners (saccharin sodium) and essences. The above components constitute the main body of the dentifrice, and in order to impart more efficacy to the dentifrice, many manufacturers add some active ingredients such as natural antibacterial polyphenols, vitamin D, chlorophyll, zinc citrate, anti-caries fluoride, etc. on the basis of the main body. In order to prevent floating dust from being generated in the using process of the dentifrice, some manufacturers add part of water and a humectant (generally sorbitol) into the formula, so that the powder is more exquisite and the mouthfeel is smoother when the dentifrice is used. Although the conventional tooth powder can clean teeth and whiten teeth in a short time, the tooth powder also has some places needing improvement, mainly the existing tooth powder generally has a defect of tooth protection, and when teeth have certain diseases, the proper tooth powder is used, so that some defects exist; although some traditional Chinese medicines are used for preparing the dentifrice at present, the problems of wide application range and unobvious curative effect generally exist, so that the popularization and the application are influenced, and particularly, the example of how to develop the traditional Chinese medicine dentifrice with various curative effects by adopting pure Chinese medicines according to the traditional Chinese medicines in China is yet to be further researched.
Patent documents in which the same technology as that of the present invention is not found through patent search are reported, and the following patents which have a certain relationship with the present invention are mainly included:
1. the patent number is CN201710694452.83, which is named as 'a Chinese herbal medicine dentifrice process for preventing and treating tonsillitis', and the patent discloses a Chinese herbal medicine dentifrice process for preventing and treating oral tonsillitis, which comprises the following raw materials (by weight):
s100, 60-120g of scabrous elephantfoot herb, 12g of radix bupleuri, 8g of red paeony root, 60-120g of roughhaired holly root, 3g of green salt and 6g of rock candy, wherein the Chinese herbal medicine powder is a mixture, and the rock candy with high purity content can further reduce the taste of the Chinese herbal medicine and has the auxiliary harmonizing effect.
S200, the dentifrice process is simple in manufacturing process, environment-friendly and healthy, and can obtain a finished product after green salt, crystal sugar and Chinese herbal medicines which are mixed and proportioned are ground into powder, sieved, processed and packaged.
S300, the scabrous elephantfoot herb, the Chinese thorowax root, the red paeony root, the roughhaired holly root, the green salt and the rock sugar are used as raw materials of the medicament with the dentin resisting effect, and the six Chinese herbal medicines are safe to use and have obvious effects of resisting dentin and preventing and treating the oral tonsillitis in the process of nursing the oral cavity and the teeth.
S400, the scabrous elephantfoot herb and the roughhaired holly root are bitter and cold and are good medicines for clearing heat and removing toxicity. The two medicines have the effect of clearing heat and removing toxicity and are multiplied. It can be used for treating swelling and pain of throat, carbuncle, sore, tonsillitis, pulmonary abscess, and intestinal abscess. Bupleurum root, radix Paeoniae Rubra and the two herbs are good anti-inflammatory herbs, because they are one-cold in nature. The two medicines have multiplied anti-inflammatory effect, and can be used for relieving depression, easing pain, promoting blood circulation to remove blood stasis, treating carbuncle and swelling sores, resisting bacteria and viruses and regulating immunity, and the dentifrice has the effect of preventing and treating the oral tonsillitis.
S500, the Chinese herbal medicine dentifrice has the advantages that the Chinese herbal medicine dentifrice is not used when being carelessly eaten in the belly during tooth brushing, and is beneficial to oral cavity teeth.
2. The patent number is CN201810376999 entitled "a Haimaishi Chinese herbal medicine dentifrice", which has the following characters: the patent of Shanxi university of science and technology discloses a Haimaishi Chinese herbal medicine dentifrice which comprises the raw materials of active Haimaishi powder, cattail pollen, folium artemisiae argyi, eclipta, ramie root, liquorice, borneol, etamsylate, sodium dodecyl sulfate and water. Adding the active hyphen stone powder obtained by activating the hyphen stone powder and other raw materials into a ball mill for wet grinding, drying and grinding to obtain the hyphen stone Chinese herbal medicine dentifrice.
3. The patent number is CN201711456055, which is named as 'a traditional Chinese medicine dentifrice for treating kidney deficiency type loose and loose teeth and exfoliation and a preparation method thereof', and the application is as follows: the invention discloses an invention patent of Fujian Guangshengtang pharmaceutical industry Co., Ltd, and discloses a traditional Chinese medicine dentifrice for treating kidney deficiency type loose and loose teeth and falling and a preparation method thereof. The traditional Chinese medicine dentifrice for treating the deficiency of the kidney type loose and loose teeth and the falling comprises the following components in parts by weight: 10-100 parts of radix aconiti praeparata, 10-100 parts of halitum, 10-80 parts of fructus psoraleae, 10-100 parts of gypsum and 10-40 parts of mint leaves. The composition is extracted by related technologies, and then is mixed with auxiliary materials to prepare the traditional Chinese medicine dentifrice for clinical use.
Through careful analysis of the above patents, although the patents relate to some tooth powders and manufacturing methods thereof, specific tooth powder improvement technical solutions are also provided, through careful analysis, the proposed tooth powders can only perform local single efficacy, and have a narrow adaptation range, so that the problem of difficult popularization and application still exists, and further research and improvement are needed.
Disclosure of Invention
The invention aims to provide a novel multifunctional dentifrice prepared from pure Chinese herbal medicines and a preparation method thereof, aiming at the defects of single effect, poor efficacy and difficulty in general popularization and adoption of the existing dentifrice.
In order to achieve the purpose, the invention provides a multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines, which is characterized in that: the tooth powder is prepared by taking green salt as a main material, adding achyranthes root, long pepper, ovate leaf holly bark, eucalyptus leaf and dendrobium officinale and auxiliary materials.
Furthermore, the weight ratio of the green salt to achyranthes root, long pepper, ovate leaf holly bark, eucalyptus leaf and dendrobium officinale is as follows: 15-25g of green salt, 4-10g of achyranthes root, 3-5g of long pepper, 4-10g of ovate leaf holly bark, 4-10g of dendrobium officinale and 4-10g of eucalyptus leaf.
Furthermore, the auxiliary materials in the formula comprise wild chrysanthemum, dandelion, mint, eucommia, dried alum, gypsum, fructus psoraleae, radix angelicae, radix saposhnikoviae, eclipta alba, asarum, cimicifugae foetidae, rhizoma drynariae, pseudo-ginseng and pepper, more than two of the wild chrysanthemum, the dandelion, the mint, the eucommia, the achyranthes, the dried alum, the gypsum, the fructus psoraleae, the radix angelicae, the radix saposhnikoviae, the eclipta alba, the asarum, the cimicifugae foetidae, the rhizoma drynariae, the pseudo-ginseng and the pepper are prepared, the drying treatment and the drying treatment are carried out by respectively pressurizing at low temperature, then the raw materials which are.
Furthermore, the auxiliary materials comprise wild chrysanthemum flower, dandelion, mint, eucommia bark, achyranthes root, dried alum, gypsum, fructus psoraleae, angelica dahurica, divaricate saposhnikovia root, eclipta alba, asarum, cimicifuga foetida, rhizoma drynariae, pseudo-ginseng and pepper in the following proportion: 8-15g of wild chrysanthemum flower, 8-15g of dandelion, 8-15g of mint, 4-10g of eucommia bark, 3-8g of dried alum, 4-10g of gypsum, 4-10g of fructus psoraleae, 4-10g of radix angelicae, 4-10g of radix saposhnikoviae, 6-12g of eclipta alba, 3-5g of asarum, 4-10g of cimicifugae foetidae, 4-10g of rhizoma drynariae, 2-5g of pseudo-ginseng and 4-10g of pepper.
Further, taking green salt as a main material, adding achyranthes root, long pepper, rotundine, folium eucalypti globueli and dendrobium officinale into the main material, and adding the green salt, the achyranthes root, the long pepper, the rotundine, the folium eucalypti globueli and the dendrobium officinale into the main material, and auxiliary materials; respectively drying the raw materials by low-temperature pressurization, grinding the dried raw materials to form powder, and making the powder into tooth powder; the preparation of the dentifrice comprises the following steps:
1) placing the main material green salt in an oven, baking at 50-70 deg.C for 60-120 min, taking out, naturally cooling to normal temperature, placing in a wall breaking pulverizer, grinding into powder, sieving with 800 mesh sieve, and retaining the sieved powder;
2) baking and drying the achyranthes bidentata, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale according to the characteristics of the materials, grinding the dried achyranthes bidentata thumb, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
3) drying other auxiliary materials according to the self characteristics of various auxiliary material materials, grinding the dried auxiliary materials into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
4) mixing the powdered green salt, achyranthes root, long pepper, ovate leaf holly bark, eucalyptus leaf, dendrobium officinale and other auxiliary materials according to the proportion of 1:1:1 to form the tooth powder.
Further, the long pepper drying treatment is to put long pepper prepared into traditional Chinese medicinal materials into a baking box, bake the long pepper at the low temperature of 50-70 ℃ and under the pressure of 0.5-1 MPa for 60-120 minutes to completely remove moisture in the long pepper to form dried long pepper, take the dried long pepper out of the baking box, pour the dried long pepper into grinding equipment for grinding, sieve the long pepper after grinding, sieve the long pepper by 800 meshes, leave sieved powder, mix the powder with other powder materials and prepare tooth powder.
Further, the dried ovate leaf holly bark is obtained by putting the ovate leaf holly bark prepared into the traditional Chinese medicinal materials into a baking box, baking at the low temperature of 50-70 ℃ and under the pressure of 0.5-1 MPa for 60-120 minutes to completely remove moisture in the ovate leaf holly bark to form the dried ovate leaf holly bark, taking out the dried ovate leaf holly bark from the baking box, pouring the dried ovate leaf holly bark into grinding equipment for grinding, sieving the ground ovate leaf holly bark by a sieve of 800 meshes, remaining sieved powder, and mixing the sieved powder with other powder materials to prepare the tooth powder.
Further, the drying treatment of the dendrobium officinale comprises the steps of putting the dendrobium officinale made into the traditional Chinese medicinal materials into a baking box, baking the dendrobium officinale at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 80-150 minutes to completely remove moisture in the dendrobium officinale to form dried dendrobium officinale, taking the dried dendrobium officinale out of the baking box, pouring the dried dendrobium officinale into grinding equipment for grinding, sieving the ground dendrobium officinale after grinding, sieving the dendrobium officinale through 800 meshes, reserving sieved powder, and mixing the powder with other powder materials to prepare the tooth powder.
Further, the drying treatment of the eucalyptus leaves comprises the steps of putting the eucalyptus leaves prepared into the traditional Chinese medicinal materials into a baking box, baking the eucalyptus leaves at the low temperature of 50-70 ℃ and under the pressure of 0.5-1 MPa for 60-120 minutes to completely remove moisture in the eucalyptus leaves to form dried eucalyptus leaves, taking the dried long pepper out of the baking box, pouring the long pepper into a grinding device for grinding, sieving the long pepper after grinding, sieving the long pepper with 800 meshes, remaining sieved powder, mixing the powder with other powder materials, and preparing the tooth powder
Further, the drying treatment of the achyranthes bidentata is to put the achyranthes bidentata which is prepared into the traditional Chinese medicinal materials into a baking box, bake the achyranthes bidentata at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 80-150 minutes to completely remove the moisture in the achyranthes bidentata and form dried achyranthes bidentata, take the dried piper longum out of the baking box, pour the piper longum into grinding equipment for grinding, sieve the piper longum after grinding, sieve the piper longum through 800 meshes, leave sieved powder, mix the powder with other powder materials and prepare the dentifrice.
The invention has the advantages that:
the invention takes green salt as a main material, and is added with achyranthes root, long pepper, ovate leaf holly bark and dendrobium officinale, the achyranthes root, the long pepper, the ovate leaf holly bark and the dendrobium officinale are respectively baked and dried under low temperature and pressure, and then the dried raw materials are ground to form powder material, so as to prepare the tooth powder. The formula of the invention combines cold and heat, combines elevation and subsidence, and has the effects of tonifying kidney and strengthening teeth, clearing heat and purging fire, and relieving swelling and pain. Effectively solves the problems of toothache, loose teeth, soft teeth, gingival bleeding, gingival swelling and pain, gingival atrophy, tooth decay, decayed teeth, wind-fire toothache, fear of cold and heat, oral ulcer, halitosis, tartar and tartar accumulation, black and yellow teeth and the like.
Detailed Description
The invention is further illustrated with reference to the following figures and specific examples.
Example one
A tooth powder for protecting teeth in various aspects is prepared from Chinese-medicinal materials including achyranthes root, long pepper, ovate leaf of holly bark, eucalyptus leaf and dendrobium officinale through preparing green salt, adding achyranthes root, long pepper, ovate leaf of holly bark, eucalyptus leaf and dendrobium officinale, low-temp pressurizing, baking and drying, grinding to obtain powder, and preparing tooth powder.
The weight ratio of the green salt to the achyranthes root, the long pepper, the ovate leaf holly bark, the eucalyptus leaf and the dendrobium officinale is as follows: 60-120-25g of green salt, 4-10g of achyranthes bidentata, 3-5g of long pepper, 4-10g of ovate leaf holly bark, 4-10g of dendrobium officinale and 4-10g of eucalyptus leaves.
The tooth powder can be prepared by adding some auxiliary materials according to the needs, wherein the auxiliary materials comprise more than two of wild chrysanthemum flower, dandelion, mint, eucommia bark, dried alum, gypsum, malaytea scurfpea fruit, angelica dahurica, divaricate saposhnikovia root, eclipta, asarum, rhizoma drynariae, pseudo-ginseng and pepper, the wild chrysanthemum flower, the dandelion, the mint, the eucommia bark, the dried alum, the gypsum, the malaytea scurfpea fruit, the angelica dahurica, the divaricate saposhnikovia root, the eclipta, the asarum, the cimicifuga foetida, the rhizoma drynariae, the pseudo-ginseng and the pepper are respectively baked and dried, and then the dried raw materials.
The auxiliary materials comprise 8-15g of wild chrysanthemum flower, 8-60-120g of dandelion, 8-15g of mint, 4-10g of eucommia bark, 3-8g of dried alum, 4-10g of gypsum, 4-10g of fructus psoraleae, 4-10g of radix angelicae, 4-10g of radix saposhnikoviae, 6-12g of eclipta alba, 3-5g of asarum, 4-10g of rhizoma cimicifugae, 4-10g of rhizoma drynariae, 2-5g of pseudo-ginseng and 4-10g of pepper.
The preparation of the dentifrice comprises the following steps:
1) selecting medicinal materials according to the ratio of the dentifrice, placing main material green salt in an oven, baking at 50-70 deg.C for 60-120 min, taking out, naturally cooling to room temperature, grinding in a wall-breaking pulverizer, grinding into powder, sieving with 800 mesh sieve, and retaining the sieved powder;
2) baking and drying the achyranthes bidentata, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale according to the characteristics of the materials, grinding the dried achyranthes bidentata thumb, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
3) respectively carrying out drying treatment on other auxiliary materials according to the characteristics of the materials, grinding the dried auxiliary materials into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
4) mixing the powdered green salt, achyranthes root, long pepper, ovate leaf holly bark, eucalyptus leaf, dendrobium officinale and other auxiliary materials according to the proportion of 1:1:1 to form the tooth powder.
The drying treatment of the long pepper is to put the long pepper prepared into traditional Chinese medicinal materials into a baking box, bake the long pepper at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the long pepper to form dried long pepper, take the dried long pepper out of the baking box, pour the dried long pepper into grinding equipment for grinding, sieve the long pepper after grinding, sieve the long pepper by 800 meshes, leave sieved powder, mix the powder with other powder materials and prepare tooth powder.
The dried ovate leaf holly bark is prepared by putting the ovate leaf holly bark prepared into the traditional Chinese medicinal materials into a baking box, baking at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the ovate leaf holly bark to form dried ovate leaf holly bark, taking out the dried ovate leaf holly bark from the baking box, pouring the dried ovate leaf holly bark into grinding equipment for grinding, sieving after grinding, sieving through 800 meshes, remaining sieved powder, and mixing with other powder materials to prepare the tooth powder.
The drying treatment of the dendrobium officinale is to put the dendrobium officinale made into traditional Chinese medicinal materials into a baking box, bake the dendrobium officinale in the baking box at a low temperature of 50-70 ℃ and under a pressure of 0.5MPa-1MPa for 80-150 minutes so that the moisture in the dendrobium officinale is completely removed to form dried dendrobium officinale, take the dried dendrobium officinale out of the baking box, pour the dried dendrobium officinale into grinding equipment for grinding, sieve the dried dendrobium officinale after grinding, sieve the dendrobium officinale through 800 meshes, retain sieved powder, and mix the powder with other powder materials to prepare tooth powder.
The drying treatment of the eucalyptus leaves comprises the steps of putting the eucalyptus leaves which are made into traditional Chinese medicinal materials into a baking box, baking the eucalyptus leaves at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the eucalyptus leaves to form dried eucalyptus leaves, taking the dried long pepper out of the baking box, pouring the long pepper into grinding equipment for grinding, sieving the long pepper after grinding, sieving the long pepper through a 800-mesh sieve, remaining sieved powder, and mixing the powder with other powder materials to prepare the tooth powder.
The drying treatment of the achyranthes bidentata is to put the achyranthes bidentata which is made into traditional Chinese medicinal materials into a baking box, bake the achyranthes bidentata for 80-150 minutes by pressurizing at low temperature of 50-70 ℃ under 0.5-1 MPa so as to completely remove moisture in the achyranthes bidentata and form dried achyranthes bidentata, take the dried long pepper out of the baking box, pour the long pepper into grinding equipment for grinding, sieve the long pepper after grinding through 800 meshes, leave and sieve powder, and mix the powder with other powder materials to prepare tooth powder.
The solution of the invention is: tooth cleaning and prevention are usually combined, and toothache is a common symptom, which is caused by dental diseases and periodontal diseases. Kidney deficiency is the root cause of periodontal disease, and wind-fire, wind-cold, stomach-fire, and deficient-fire are the signs. In the formula, the achyranthes root is used for tonifying liver and kidney, strengthening bones and muscles, breaking blood and removing stasis, guiding blood to descend and reducing inflammation fire, so that the toothache is mainly treated; eucommia bark has the effects of tonifying liver and kidney and strengthening tendons and bones; rhizoma Drynariae has the effect of lowering blood pressure, tonifying kidney to recover floating yang, especially for toothache; fructus Psoraleae is effective for invigorating kidney yang; herba Ecliptae has effects in nourishing liver, invigorating kidney, cooling blood, and stopping bleeding; it is a root cause treatment product. In the formula, the eucalyptus leaves can disperse wind and heat, clear away heat and toxic materials, kill parasites and relieve itching; cortex Ilicis Rotundae is effective in clearing away heat and relieving pain; dendrobium officinale is good at nourishing stomach yin, promoting the production of body fluid to quench thirst, clearing stomach heat and treating gum swelling and pain, mouth and tongue sores due to stomach heat and yin deficiency; cimicifugae foetidae, which is pungent and cool, can relieve yang-heat toxicity; the combination of the medicines can strengthen the effect of dispelling wind, clearing heat and reducing fire. The asarum, the angelica dahurica and the divaricate saposhnikovia root are pungent and warm and can achieve the effects of dispelling wind, relieving pain, activating blood and expelling pus; the long pepper is pungent and hot, can promote qi circulation and relieve pain, and is used for treating toothache and red and swollen gum caused by swelling and pain due to cold pathogen coagulation and fire stagnation; gypsum is used as an auxiliary material, and has sweet and pungent taste and cold and cool property, and the main effect of clearing stomach fire is achieved; the wild chrysanthemum and the dandelion clear away heat and toxic materials, and relieve swelling and pain; the mint leaves can disperse wind and heat; the pepper kills the parasites with acrid heat and is good at removing dental caries and toothache; notoginseng dispels blood stasis to stop bleeding, detumescence and relieve pain; dried alum promotes tissue regeneration, stops bleeding, detoxifies, kills parasites, and treats mouth and tongue sores and gingival bleeding; qing Yan warms the middle energizer and dissipates nodulation, detoxifies and relieves pain, and is used for gargling as early as ancient times.
The formula combines cold and heat, combines elevation and subsidence, and has the effects of tonifying kidney and strengthening teeth, clearing heat and purging fire, and relieving swelling and pain. Effectively solves the problems of toothache, loose teeth, soft teeth, gingival bleeding, gingival swelling and pain, gingival atrophy, tooth decay, decayed teeth, wind-fire toothache, fear of cold and heat, oral ulcer, halitosis, tartar and tartar accumulation, black and yellow teeth and the like.
The using method comprises the following steps:
1. selecting a soft toothbrush
2. Soaking in water, drying, and soaking the powder
3. Lightly applying the dentifrice to the periphery of the teeth with a toothbrush
4. It is preferable to penetrate the dentifrice into the crevices of teeth to the greatest extent so that the crevices of teeth are slightly filled with the dentifrice
5. After the tooth is fully coated, the time for protecting and curing the tooth by the dentifrice is fully ensured after the tooth is waited for 1 to 3 minutes or more
6. Gargling, and lightly brushing off the dentifrice with a toothbrush.
The method is general in daily life: the product can be used as toothpaste companion, and toothpaste and dentifrice can be used for brushing teeth for 2-3 min, and rinsing mouth with clear water once in the morning and evening. Or dissolving the medicinal powder in water as collutory. For long-term use, the aged teeth are firm and do not shake.
Example two
The principle of the second embodiment is the same as that of the first embodiment, but the formulation and the preparation method are slightly different, and the second embodiment is a multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines and the preparation method thereof.
The formula also comprises auxiliary materials, wherein the auxiliary materials comprise wild chrysanthemum flower, dandelion, mint, eucommia bark, dried alum, gypsum, fructus psoraleae, radix angelicae, radix saposhnikoviae, eclipta alba, asarum, cimicifuga foetida, rhizoma drynariae, pseudo-ginseng and pepper, the wild chrysanthemum flower, the dandelion, the mint, the eucommia bark, the achyranthes root, the dried alum, the gypsum, the fructus psoraleae, the radix angelicae, the radix saposhnikoviae, the eclipta alba, the asarum, the cimicifuga foetida, the rhizoma drynariae, the pseudo-ginseng and the pepper are subjected to baking and drying treatment, and the dried raw materials are.
The formula comprises the following components in percentage by weight:
the weight ratio of the green salt to the achyranthes root, the long pepper, the ovate leaf holly bark, the eucalyptus leaf and the dendrobium officinale is as follows: 18-23g of green salt, 6-8g of achyranthes root, 4-5g of long pepper, 6-8g of ovate leaf holly bark, 6-8g of dendrobium officinale and 6-8g of eucalyptus leaf.
The auxiliary materials are as follows: 10-15g of wild chrysanthemum flower, 10-12g of dandelion, 10-12g of mint, 5-10g of eucommia bark, 4-6g of dried alum, 6-8g of gypsum, 6-8g of fructus psoraleae, 6-8g of radix angelicae, 6-8g of radix saposhnikoviae, 8-10g of eclipta alba, 3-5g of asarum, 6-8g of rhizoma cimicifugae, 6-8g of rhizoma drynariae, 2-4g of pseudo-ginseng and 6-8g of pepper.
The preparation of the dentifrice comprises the following steps:
1) selecting medicinal materials according to the ratio of the dentifrice, placing main material green salt in an oven, baking at 50-70 deg.C for 60-120 min, taking out, naturally cooling to room temperature, grinding in a wall-breaking pulverizer, grinding into powder, sieving with 800 mesh sieve, and retaining the sieved powder;
2) baking and drying the achyranthes bidentata, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale according to the characteristics of the materials, grinding the dried achyranthes bidentata thumb, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
3) respectively carrying out drying treatment on other auxiliary materials according to the characteristics of the materials, grinding the dried auxiliary materials into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
4) mixing the powdered green salt, achyranthes root, long pepper, ovate leaf holly bark, eucalyptus leaf, dendrobium officinale and other auxiliary materials according to the proportion of 1:1:1 to form the tooth powder.
The drying treatment of the long pepper is to put the long pepper prepared into traditional Chinese medicinal materials into a baking box, bake the long pepper at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the long pepper to form dried long pepper, take the dried long pepper out of the baking box, pour the dried long pepper into grinding equipment for grinding, sieve the long pepper after grinding, sieve the long pepper by 800 meshes, leave sieved powder, mix the powder with other powder materials and prepare tooth powder.
The dried ovate leaf holly bark is prepared by putting the ovate leaf holly bark prepared into the traditional Chinese medicinal materials into a baking box, baking at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the ovate leaf holly bark to form dried ovate leaf holly bark, taking out the dried ovate leaf holly bark from the baking box, pouring the dried ovate leaf holly bark into grinding equipment for grinding, sieving after grinding, sieving through 800 meshes, remaining sieved powder, and mixing with other powder materials to prepare the tooth powder.
The drying treatment of the dendrobium officinale is to put the dendrobium officinale made into traditional Chinese medicinal materials into a baking box, bake the dendrobium officinale for 25-40 minutes by pressurizing at a low temperature of 50-70 ℃ for 0.5-1 MPa, so that the moisture in the dendrobium officinale is completely removed to form dried dendrobium officinale, take out the dried dendrobium officinale from the baking box, pour the dried dendrobium officinale into grinding equipment for grinding, sieve the dried dendrobium officinale after grinding, sieve the dried dendrobium officinale through 800 meshes, retain sieved powder, and mix the powder with other powder materials to prepare tooth powder.
The drying treatment of the eucalyptus leaves comprises the steps of putting the eucalyptus leaves which are made into traditional Chinese medicinal materials into a baking box, baking the eucalyptus leaves at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the eucalyptus leaves to form dried eucalyptus leaves, taking the dried long pepper out of the baking box, pouring the long pepper into grinding equipment for grinding, sieving the long pepper after grinding, sieving the long pepper through a 800-mesh sieve, remaining sieved powder, and mixing the powder with other powder materials to prepare the tooth powder.
The drying treatment of the achyranthes bidentata is to put the achyranthes bidentata which is made into traditional Chinese medicinal materials into a baking box, bake the achyranthes bidentata for 80-150 minutes by pressurizing at low temperature of 50-70 ℃ under 0.5-1 MPa so as to completely remove moisture in the achyranthes bidentata and form dried achyranthes bidentata, take the dried long pepper out of the baking box, pour the long pepper into grinding equipment for grinding, sieve the long pepper after grinding through 800 meshes, leave and sieve powder, and mix the powder with other powder materials to prepare tooth powder.
EXAMPLE III
The principle of the third embodiment is the same as that of the first embodiment, but the formulation and the preparation method are slightly different, and the third embodiment is a multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines and the preparation method thereof.
The formula also comprises auxiliary materials, the auxiliary materials comprise wild chrysanthemum flower, dandelion, mint, eucommia bark, achyranthes root, dried alum, gypsum, malaytea scurfpea fruit, angelica dahurica, divaricate saposhnikovia root, eclipta alba, asarum, rhizoma cimicifugae, rhizoma drynariae, pseudo-ginseng and pepper, the wild chrysanthemum flower, the dandelion, the mint, the eucommia bark, the achyranthes root, the dried alum, the gypsum, the malaytea scurfpea fruit, the angelica dahurica, the divaricate saposhnikovia root, the yerbadetajo herb, asarum, cimicifuga foetida, the rhizoma drynariae, the pseudo-ginseng and the pepper are subjected.
The weight ratio of the green salt to the achyranthes root, the long pepper, the ovate leaf holly bark, the eucalyptus leaf and the dendrobium officinale is as follows: 15-25g of green salt, 10g of achyranthes root, 5g of long pepper, 10g of ovate leaf holly bark, 10g of dendrobium officinale and 10g of eucalyptus leaf.
The auxiliary materials are as follows: 10g of wild chrysanthemum flower, 10g of dandelion, 10g of mint, 5g of eucommia bark, 5g of dried alum, 5g of gypsum, 5g of fructus psoraleae, 5g of radix angelicae, 5g of divaricate saposhnikovia root, 10g of eclipta alba, 5g of asarum, 5g of cimicifuga foetida, 5g of rhizoma drynariae, 5g of pseudo-ginseng and 5g of pepper.
The preparation of the dentifrice comprises the following steps:
1) selecting medicinal materials according to the ratio of the dentifrice, placing main material green salt in an oven, baking at 50-70 deg.C for 60-120 min, taking out, naturally cooling to room temperature, grinding in a wall-breaking pulverizer, grinding into powder, sieving with 800 mesh sieve, and retaining the sieved powder;
2) baking and drying the achyranthes bidentata, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale according to the characteristics of the materials, grinding the dried achyranthes bidentata thumb, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
3) respectively carrying out drying treatment on other auxiliary materials according to the characteristics of the materials, grinding the dried auxiliary materials into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
4) mixing the powdered green salt, achyranthes root, long pepper, ovate leaf holly bark, eucalyptus leaf, dendrobium officinale and other auxiliary materials according to the proportion of 1:1:1 to form the tooth powder.
The drying treatment of the long pepper is to put the long pepper prepared into traditional Chinese medicinal materials into a baking box, bake the long pepper at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the long pepper to form dried long pepper, take the dried long pepper out of the baking box, pour the dried long pepper into grinding equipment for grinding, sieve the long pepper after grinding, sieve the long pepper by 800 meshes, leave sieved powder, mix the powder with other powder materials and prepare tooth powder.
The dried ovate leaf holly bark is prepared by putting the ovate leaf holly bark prepared into the traditional Chinese medicinal materials into a baking box, baking at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the ovate leaf holly bark to form dried ovate leaf holly bark, taking out the dried ovate leaf holly bark from the baking box, pouring the dried ovate leaf holly bark into grinding equipment for grinding, sieving after grinding, sieving through 800 meshes, remaining sieved powder, and mixing with other powder materials to prepare the tooth powder.
The drying treatment of the dendrobium officinale is to put the dendrobium officinale made into traditional Chinese medicinal materials into a baking box, bake the dendrobium officinale for 60-130 minutes by pressurizing at a low temperature of 50-70 ℃ for 0.5-1 MPa, so that the moisture in the dendrobium officinale is completely removed to form dried dendrobium officinale, take out the dried dendrobium officinale from the baking box, pour the dried dendrobium officinale into grinding equipment for grinding, sieve the dried dendrobium officinale after grinding, sieve the dried dendrobium officinale through 800 meshes, retain sieved powder, and mix the powder with other powder materials to prepare tooth powder.
The drying treatment of the eucalyptus leaves comprises the steps of putting the eucalyptus leaves which are made into traditional Chinese medicinal materials into a baking box, baking the eucalyptus leaves at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the eucalyptus leaves to form dried eucalyptus leaves, taking the dried long pepper out of the baking box, pouring the long pepper into grinding equipment for grinding, sieving the long pepper after grinding, sieving the long pepper through a 800-mesh sieve, remaining sieved powder, and mixing the powder with other powder materials to prepare the tooth powder.
The drying treatment of the achyranthes bidentata is to put the achyranthes bidentata which is made into traditional Chinese medicinal materials into a baking box, bake the achyranthes bidentata for 80-150 minutes by pressurizing at low temperature of 50-70 ℃ under 0.5-1 MPa so as to completely remove moisture in the achyranthes bidentata and form dried achyranthes bidentata, take the dried long pepper out of the baking box, pour the long pepper into grinding equipment for grinding, sieve the long pepper after grinding through 800 meshes, leave and sieve powder, and mix the powder with other powder materials to prepare tooth powder.
The above listed embodiments are only for clear and complete description of the technical solution of the present invention; it is to be understood that the described embodiments are merely a few embodiments of the invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention has the advantages that:
according to the invention, the raw materials including the halite serving as a main material and the achyranthes root, the long pepper, the ovate leaf holly bark and the dendrobium officinale are added, the achyranthes root, the long pepper, the ovate leaf holly bark and the dendrobium officinale are respectively baked and dried at low temperature under pressure, so that the effective ingredients in the raw materials are favorably kept, and then the dried raw materials are ground to form powder so as to prepare the tooth powder. The formula of the invention combines cold and heat, combines elevation and subsidence, and has the effects of tonifying kidney and strengthening teeth, clearing heat and purging fire, and relieving swelling and pain. Effectively solves the problems of toothache, loose teeth, soft teeth, gingival bleeding, gingival swelling and pain, gingival atrophy, tooth decay, decayed teeth, wind-fire toothache, fear of cold and heat, oral ulcer, halitosis, tartar and tartar accumulation, black and yellow teeth and the like.

Claims (10)

1. A multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines is characterized in that: the method comprises the steps of taking green salt as a main material, adding achyranthes bidentata, long pepper, ovate leaf holly bark, folium eucalypti and dendrobium officinale into the green salt, and auxiliary materials to prepare tooth powder, respectively drying the achyranthes bidentata, the long pepper, the ovate leaf holly bark and the dendrobium officinale under low temperature and pressure, grinding the dried raw materials to form powder, and preparing the tooth powder.
2. The multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines and the preparation method thereof as claimed in claim 1, wherein: the weight ratio of the green salt to the achyranthes root, the long pepper, the ovate leaf holly bark, the eucalyptus leaf and the dendrobium officinale is as follows: 15-25g of green salt, 4-10g of achyranthes root, 3-5g of long pepper, 4-10g of ovate leaf holly bark, 4-10g of dendrobium officinale and 4-10g of eucalyptus leaf.
3. The multi-aspect tooth care dentifrice prepared from pure Chinese herbal medicines according to claim 1, wherein: the auxiliary materials in the formula comprise wild chrysanthemum flower, dandelion, mint, eucommia bark, dried alum, gypsum, malaytea scurfpea fruit, angelica dahurica, divaricate saposhnikovia root, eclipta alba, asarum, rhizoma cimicifugae, rhizoma drynariae, pseudo-ginseng and pepper, more than two components of wild chrysanthemum flower, dandelion, mint, eucommia bark, achyranthes root, dried alum, gypsum, malaytea scurfpea fruit, angelica dahurica, divaricate saposhnikovia root, eclipta alba, asarum, cimicifuga foetida, rhizoma drynariae, pseudo-ginseng and pepper are prepared, drying is carried out by respectively carrying out low-temperature pressure baking and drying treatment, then the dried raw materials.
4. The multi-aspect tooth care dentifrice prepared from pure Chinese herbal medicines as claimed in claim 3, wherein: the auxiliary materials comprise wild chrysanthemum flower, dandelion, mint, eucommia bark, achyranthes root, dried alum, gypsum, malaytea scurfpea fruit, angelica dahurica, divaricate saposhnikovia root, eclipta alba, asarum, cimicifuga foetida, rhizoma drynariae, pseudo-ginseng and pepper in the following proportion: 8-15g of wild chrysanthemum flower, 8-15g of dandelion, 8-15g of mint, 4-10g of eucommia bark, 3-8g of dried alum, 4-10g of gypsum, 4-10g of fructus psoraleae, 4-10g of radix angelicae, 4-10g of radix saposhnikoviae, 6-12g of eclipta alba, 3-5g of asarum, 4-10g of cimicifugae foetidae, 4-10g of rhizoma drynariae, 2-5g of pseudo-ginseng and 4-10g of pepper.
5. A method for preparing multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines according to claim 1, which is characterized in that: taking green salt as main material, adding Achyranthis radix, fructus Piperis Longi, cortex Ilicis Rotundae, folium Eucalypti Globueli and herba Dendrobii, mixing green salt, Achyranthis radix, fructus Piperis Longi, cortex Ilicis Rotundae, folium Eucalypti Globueli and herba Dendrobii, and adjuvants; respectively drying the raw materials by low-temperature pressurization, grinding the dried raw materials to form powder, and making the powder into tooth powder; the preparation of the dentifrice comprises the following steps:
1) placing the main material green salt in an oven, baking at 50-70 deg.C for 60-120 min, taking out, naturally cooling to normal temperature, placing in a wall breaking pulverizer, grinding into powder, sieving with 800 mesh sieve, and retaining the sieved powder;
2) baking and drying the achyranthes bidentata, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale according to the characteristics of the materials, grinding the dried achyranthes bidentata thumb, the long pepper, the rotundifolia thumb, the eucalyptus leaves and the dendrobium officinale into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
3) drying other auxiliary materials according to the self characteristics of various auxiliary material materials, grinding the dried auxiliary materials into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;
4) mixing the powdered green salt, achyranthes root, long pepper, ovate leaf holly bark, eucalyptus leaf, dendrobium officinale and other auxiliary materials according to the proportion of 1:1:1 to form the tooth powder.
6. The method for preparing multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines according to claim 5, wherein the method comprises the following steps: the long pepper drying treatment is to put long pepper prepared into traditional Chinese medicinal materials into a baking box, bake the long pepper at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the long pepper to form dried long pepper, take the dried long pepper out of the baking box, pour the dried long pepper into grinding equipment for grinding, sieve the long pepper after grinding, sieve the long pepper by 800 meshes, leave sieved powder, mix the powder with other powder materials and prepare tooth powder.
7. The method for preparing multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines according to claim 5, wherein the method comprises the following steps: the dried ovate leaf holly bark is prepared by putting the ovate leaf holly bark prepared into the traditional Chinese medicinal materials into a baking box, baking at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the ovate leaf holly bark to form dried ovate leaf holly bark, taking out the dried ovate leaf holly bark from the baking box, pouring the dried ovate leaf holly bark into grinding equipment for grinding, sieving after grinding, sieving through 800 meshes, remaining sieved powder, and mixing with other powder materials to prepare the tooth powder.
8. The method for preparing multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines according to claim 5, wherein the method comprises the following steps: the drying treatment of the dendrobium officinale comprises the steps of putting the dendrobium officinale made into traditional Chinese medicinal materials into a baking box, baking the dendrobium officinale in the baking box at the low temperature of 120-50-70 ℃ and under the pressure of 0.5MPa-1MPa for 25-40 minutes to completely remove water in the dendrobium officinale and form dried dendrobium officinale, taking the dried dendrobium officinale out of the baking box, pouring the dried dendrobium officinale into grinding equipment for grinding, sieving the ground dendrobium officinale after grinding, sieving the dendrobium officinale through 800 meshes, reserving sieved powder, and mixing the powder with other powder materials to prepare tooth powder.
9. The method for preparing multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines according to claim 5, wherein the method comprises the following steps: the drying treatment of the eucalyptus leaves comprises the steps of putting the eucalyptus leaves which are made into traditional Chinese medicinal materials into a baking box, baking the eucalyptus leaves at the low temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 60-120 minutes to completely remove moisture in the eucalyptus leaves to form dried eucalyptus leaves, taking the dried long pepper out of the baking box, pouring the long pepper into grinding equipment for grinding, sieving the long pepper after grinding, sieving the long pepper through a 800-mesh sieve, remaining sieved powder, and mixing the powder with other powder materials to prepare the tooth powder.
10. The method for preparing multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines according to claim 5, wherein the method comprises the following steps: the drying treatment of the achyranthes bidentata is to put the achyranthes bidentata which is made into traditional Chinese medicinal materials into a baking box, bake the achyranthes bidentata for 80-150 minutes by pressurizing at low temperature of 50-70 ℃ under 0.5-1 MPa so as to completely remove moisture in the achyranthes bidentata and form dried achyranthes bidentata, take the dried long pepper out of the baking box, pour the long pepper into grinding equipment for grinding, sieve the long pepper after grinding through 800 meshes, leave and sieve powder, and mix the powder with other powder materials to prepare tooth powder.
CN201811502102.8A 2018-12-10 2018-12-10 Multi-aspect tooth-protecting dentifrice prepared from pure Chinese herbal medicines and preparation method thereof Pending CN111281836A (en)

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Application publication date: 20200616