CN111281838A

CN111281838A - Analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines and preparation method thereof

Info

Publication number: CN111281838A
Application number: CN201811502509.0A
Authority: CN
Inventors: 贺云祥; 何美英
Original assignee: Hunan Hanfang Shennong Chinese Medical Clinic Co ltd
Current assignee: Hunan Hanfang Shennong Chinese Medical Clinic Co ltd
Priority date: 2018-12-10
Filing date: 2018-12-10
Publication date: 2020-06-16

Abstract

A tooth powder with analgesic and tooth protecting effects prepared from pure Chinese herbal medicines is prepared from Halitum as main material, folium Ilicis Purpureae, fructus Piperis Longi and herba Dendrobii by respectively baking at low temperature under pressure and drying, grinding the dried raw materials to obtain powder, and making into tooth powder. The Chinese holly leaf in the formula of the invention has the effects of clearing away heat and toxic materials, relieving swelling and removing blood stasis; the long pepper promotes qi circulation to relieve pain; the dendrobium officinale can nourish stomach yin, promote the production of body fluid and quench thirst; the pepper kills the parasites with acrid heat and is good at removing dental caries and toothache; radix Saposhnikoviae has effects in expelling pathogenic wind and relieving pain; herba asari has effects in relieving exterior syndrome, dispelling cold, expelling pathogenic wind, relieving pain, warming lung, and promoting fluid retention; gypsum Fibrosum has effects of clearing away stomach fire, and can be used for treating toothache due to stomach fire and gingival swelling and pain; radix Angelicae Dahuricae has effects of relieving exterior syndrome, dispelling cold, dispelling pathogenic wind, relieving pain, relieving swelling, expelling pus, clearing away heat and toxic materials; cimicifuga foetida introduces gypsum to treat headache and toothache at vertex of yangming; qing Yan warms middle energizer and dissipates nodulation, detoxifies and relieves pain. The medicines are combined to play the effects of dispelling wind, clearing heat, reducing swelling and relieving pain. Can be used for relieving toothache caused by pathogenic wind-fire, wind-cold, stomach heat, deficiency fire, and dental caries.

Description

Analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines and preparation method thereof

Technical Field

The invention relates to a dentifrice and a preparation method thereof, in particular to a dentifrice for relieving pain and protecting various tooth and gum problems, such as toothache, loose teeth, soft teeth, gingival bleeding, gingival swelling and pain, gingival atrophy, tooth decay, dental caries, toothache caused by wind fire, fear of cold and heat, oral ulcer, halitosis, tartar and tartar accumulation, black and yellow teeth and the like and a preparation method thereof; belongs to the technical field of daily nursing articles and manufacturing methods thereof.

Background art:

prior to the advent of toothpaste, dentifrice was the most commonly used dental cleanser for people. In ancient times, various tools were used to wipe teeth for tooth brushing, and various dentifrices were added, most commonly salt, i.e., the precursor of dentifrice. In Song Dynasty, the "tooth powder line" appeared, and the tooth powder prepared by traditional Chinese medicines is specially sold, and the tooth powder has become social commodity. However, the tooth powder has the defect that the use is not very convenient, so people invent the toothpaste; the toothpaste and the tooth powder are different mainly in form, one is powder and the other is paste, and the main effective components are basically the same. However, recently, it has been found that the toothpaste in the form of paste greatly reduces the effect of the effective components due to the addition of a large amount of water and humectant, and particularly the whitening effect is greatly affected, and the dentifrice is improved and then displayed again in the life of people; with the progress of the technology, the formula and the process of the tooth powder are more mature, and the tooth powder is less and less different from the toothpaste. Toothpowders also have the following characteristics relative to toothpastes:

1. the dentifrice is coarser than toothpaste, and the friction of the dentifrice to teeth is larger, so that the dentifrice has advantages in removing tartar, dental plaque, tartar and the like.

2. Dentifrices generally contain little or no artificial pigment; the toothpaste is prepared by chemical process colloidal paste and contains artificial pigment and perfume.

3. The tooth powder has stronger dispelling power than toothpaste by gargling, and the toothpaste mainly removes bacteria, and generally can not dispel dental plaque, tartar and tartar.

At present, although the formula of the conventional dentifrice produced by different manufacturers is different and the ingredients of the dentifrice are different, the main components of the dentifrice are not separated from abradants (calcium carbonate, hydrated silica, calcium hydrogen phosphate and the like), surfactants (SLS), sweeteners (saccharin sodium) and essences. The above components constitute the main body of the dentifrice, and in order to impart more efficacy to the dentifrice, many manufacturers add some active ingredients such as natural antibacterial polyphenols, vitamin D, chlorophyll, zinc citrate, anti-caries fluoride, etc. on the basis of the main body. In order to prevent floating dust from being generated in the using process of the dentifrice, some manufacturers add part of water and a humectant (generally sorbitol) into the formula, so that the powder is more exquisite and the mouthfeel is smoother when the dentifrice is used. Although the conventional tooth powder can clean teeth and whiten teeth in a short time, the tooth powder also has some places needing improvement, mainly the existing tooth powder generally has a defect of tooth protection, and when teeth have certain diseases, the proper tooth powder is used, so that some defects exist; although some traditional Chinese medicines are used for preparing the dentifrice at present, the problems of wide application range and unobvious curative effect generally exist, so that the popularization and the application are influenced, and particularly, the example of how to develop the traditional Chinese medicine dentifrice with various curative effects by adopting pure Chinese medicines according to the traditional Chinese medicines in China is yet to be further researched.

Patent documents in which the same technology as that of the present invention is not found through patent search are reported, and the following patents which have a certain relationship with the present invention are mainly included:

1. the patent number is CN201710694452.83, which is named as 'a Chinese herbal medicine dentifrice process for preventing and treating tonsillitis', and the patent discloses a Chinese herbal medicine dentifrice process for preventing and treating oral tonsillitis, which comprises the following raw materials (by weight):

s100, 60-120g of scabrous elephantfoot herb, 12g of radix bupleuri, 8g of red paeony root, 60-120g of roughhaired holly root, 3g of green salt and 6g of rock candy, wherein the Chinese herbal medicine powder is a mixture, and the rock candy with high purity content can further reduce the taste of the Chinese herbal medicine and has the auxiliary harmonizing effect.

S200, the dentifrice process is simple in manufacturing process, environment-friendly and healthy, and can obtain a finished product after green salt, crystal sugar and Chinese herbal medicines which are mixed and proportioned are ground into powder, sieved, processed and packaged.

S300, the scabrous elephantfoot herb, the Chinese thorowax root, the red paeony root, the roughhaired holly root, the green salt and the rock sugar are used as raw materials of the medicament with the dentin resisting effect, and the six Chinese herbal medicines are safe to use and have obvious effects of resisting dentin and preventing and treating the oral tonsillitis in the process of nursing the oral cavity and the teeth.

S400, the scabrous elephantfoot herb and the roughhaired holly root are bitter and cold and are good medicines for clearing heat and removing toxicity. The two medicines have the effect of clearing heat and removing toxicity and are multiplied. It can be used for treating swelling and pain of throat, carbuncle, sore, tonsillitis, pulmonary abscess, and intestinal abscess. Bupleurum root, radix Paeoniae Rubra and the two herbs are good anti-inflammatory herbs, because they are one-cold in nature. The two medicines have multiplied anti-inflammatory effect, and can be used for relieving depression, easing pain, promoting blood circulation to remove blood stasis, treating carbuncle and swelling sores, resisting bacteria and viruses and regulating immunity, and the dentifrice has the effect of preventing and treating the oral tonsillitis.

S500, the Chinese herbal medicine dentifrice has the advantages that the Chinese herbal medicine dentifrice is not used when being carelessly eaten in the belly during tooth brushing, and is beneficial to oral cavity teeth.

2. The patent number is CN201810376999 entitled "a Haimaishi Chinese herbal medicine dentifrice", which has the following characters: the patent of Shanxi university of science and technology discloses a Haimaishi Chinese herbal medicine dentifrice which comprises the raw materials of active Haimaishi powder, cattail pollen, folium artemisiae argyi, eclipta, ramie root, liquorice, borneol, etamsylate, sodium dodecyl sulfate and water. Adding the active hyphen stone powder obtained by activating the hyphen stone powder and other raw materials into a ball mill for wet grinding, drying and grinding to obtain the hyphen stone Chinese herbal medicine dentifrice.

3. The patent number is CN201711456055, which is named as 'a traditional Chinese medicine dentifrice for treating kidney deficiency type loose and loose teeth and exfoliation and a preparation method thereof', and the application is as follows: the invention discloses an invention patent of Fujian Guangshengtang pharmaceutical industry Co., Ltd, and discloses a traditional Chinese medicine dentifrice for treating kidney deficiency type loose and loose teeth and falling and a preparation method thereof. The traditional Chinese medicine dentifrice for treating the deficiency of the kidney type loose and loose teeth and the falling comprises the following components in parts by weight: 10-100 parts of radix aconiti praeparata, 10-100 parts of halitum, 10-80 parts of fructus psoraleae, 10-100 parts of gypsum and 10-40 parts of mint leaves. The composition is extracted by related technologies, and then is mixed with auxiliary materials to prepare the traditional Chinese medicine dentifrice for clinical use.

Through careful analysis of the above patents, although the patents relate to some tooth powders and manufacturing methods thereof, specific tooth powder improvement technical solutions are also provided, through careful analysis, the proposed tooth powders can only perform local single efficacy, and have a narrow adaptation range, so that the problem of difficult popularization and application still exists, and further research and improvement are needed.

Disclosure of Invention

The invention aims to provide a novel multifunctional dentifrice prepared from pure Chinese herbal medicines and a preparation method thereof, aiming at the defects of single effect, poor efficacy and difficulty in general popularization and adoption of the existing dentifrice.

In order to achieve the purpose, the invention provides pain-relieving tooth-protecting dentifrice prepared from Chinese herbal medicines, comprising green Chinese holly, long pepper and dendrobium officinale.

Further, the weight ratio of the green salt to the Chinese holly, the long pepper and the dendrobium officinale is as follows: 15-25g of green salt, 6-10g of Chinese holly, 3-8g of long pepper and 4-10g of dendrobium officinale.

Furthermore, the auxiliary materials in the formula comprise gypsum, angelica dahurica, radix sileris, asarum, cimicifuga foetida and pepper, more than two components of the gypsum, the angelica dahurica, the radix sileris, the asarum, the cimicifuga foetida and the pepper are prepared into the auxiliary materials, the auxiliary materials are dried by respectively carrying out low-temperature pressure baking and drying treatment, then the dried raw materials are ground and processed to form powder materials, and the powder materials are prepared into the tooth powder auxiliary materials.

Furthermore, the auxiliary materials comprise gypsum, angelica dahurica, radix sileris, asarum, cimicifuga foetida and pepper in the following proportion: 4-10g of gypsum, 4-10g of angelica dahurica, 4-10g of divaricate saposhnikovia root, 3-8g of asarum, 4-10g of cimicifuga foetida and 4-10g of pepper.

A method for preparing analgesic tooth protecting dentifrice from Chinese herbal medicine comprises taking Halitum as main material, adding folium Ilicis Purpureae, fructus Piperis Longi and herba Dendrobii, mixing folium Ilicis Purpureae, fructus Piperis Longi and herba Dendrobii, and adjuvant; respectively carrying out low-temperature pressurizing baking and drying treatment, and then grinding the dried raw materials to form powder to prepare the dentifrice; the preparation of the dentifrice comprises the following steps:

1) placing main material green salt in an oven, pressurizing at 50-70 deg.C under 0.5-1 MPa, baking at low temperature under pressure for 60-120 min, taking out, naturally cooling to normal temperature, grinding in a wall-breaking pulverizer, grinding into powder, sieving with 800 mesh sieve, and retaining the sieved powder;

2) baking and drying the Chinese holly leaf, the long pepper and the dendrobium officinale according to the characteristics of the materials respectively, grinding the dried Chinese holly leaf, the long pepper and the dendrobium officinale into powder by using grinding equipment, screening by using a 800-mesh sieve, and leaving screened powder;

3) drying other auxiliary materials according to the self characteristics of various auxiliary material materials, grinding the dried auxiliary materials into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;

4) mixing the green salt, fructus Ilicis Purpureae, fructus Piperis Longi and herba Dendrobii, and other adjuvants at a ratio of 1:1:1 to obtain dentifrice.

Further, the drying treatment of the long pepper is that the long pepper prepared into traditional Chinese medicinal materials is put into a baking box, the long pepper is pressurized at the temperature of 50-70 ℃ and 0.5MPa-1MPa for low-temperature pressurized baking for 60-120 minutes, so that the moisture in the long pepper is completely removed to form dried long pepper, the dried long pepper is taken out from the baking box and poured into grinding equipment for grinding, the ground long pepper is sieved after being ground, screened by an 800-mesh sieve, sieved powder is remained, and the dried long pepper and other powder materials are mixed and prepared to prepare the tooth powder.

Further, the drying treatment of the green Chinese holly comprises the steps of putting the green Chinese holly prepared into the traditional Chinese medicinal materials into a baking box, pressurizing at the temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa, baking for 60-120 minutes to completely remove moisture in the green Chinese holly to form dried green Chinese holly, taking the dried green Chinese holly out of the baking box, pouring the dried green Chinese holly into grinding equipment for grinding, sieving after grinding, sieving through 800 meshes, reserving sieved powder, mixing with other powder materials, and preparing the mixture to prepare the tooth powder.

Further, the drying treatment of the dendrobium officinale comprises the steps of putting the dendrobium officinale made into the traditional Chinese medicinal materials into a baking box, pressurizing at 50-70 ℃ and 0.5-1 MPa for low-temperature pressurizing baking for 80-150 minutes to completely remove moisture in the dendrobium officinale to form dried dendrobium officinale, taking the dried dendrobium officinale out of the baking box, pouring the dried dendrobium officinale into grinding equipment for grinding, sieving after grinding, sieving through 800 meshes, reserving sieved powder, mixing with other powder materials, and preparing to prepare the tooth powder.

Further, the drying treatment of the gypsum, the angelica dahurica, the radix sileris, the asarum, the cimicifuga foetida and the pepper in the auxiliary materials is that the prepared various traditional Chinese medicinal materials are respectively put into a baking box, the low-temperature pressure baking is carried out for 80-150 minutes at the temperature of 50-70 ℃ under the pressure of 0.5MPa-1MPa, so that the moisture in the various traditional Chinese medicinal materials is completely removed to form dried raw materials, the dried gypsum, the angelica dahurica, the radix sileris, the asarum, the cimicifuga foetida and the pepper are respectively taken out from the baking box to be respectively poured into grinding equipment to be ground, the ground raw materials are sieved after being sieved, the sieved powder is left after 800 meshes of screening, and then the powder is.

Furthermore, the Chinese holly leaf, the long pepper, the radix angelicae, the radix sileris, the asarum, the cimicifugae foetidae and the pepper are dried in a closed environment, vacuumized and dried by filling inert gas and pressurizing, so that volatile gas in the Chinese holly leaf, the long pepper, the radix angelicae, the radix sileris, the asarum, the cimicifugae foetidae and the pepper is prevented from overflowing in the drying process.

The invention has the advantages that:

the Chinese holly leaf in the formula of the invention has the effects of clearing away heat and toxic materials, relieving swelling and removing blood stasis; the long pepper is pungent and hot, can promote qi circulation and relieve pain, and is used for treating toothache and red and swollen gum caused by swelling and pain due to cold pathogen coagulation and fire stagnation; dendrobium officinale is good at nourishing stomach yin, promoting the production of body fluid to quench thirst, clearing stomach heat and treating gum swelling and pain, mouth and tongue sores due to stomach heat and yin deficiency; the pepper kills the parasites with acrid heat and is good at removing dental caries and toothache; radix Saposhnikoviae has effects in expelling pathogenic wind and relieving pain; the asarum enters lung, liver, spleen and other channels, has the effects of relieving exterior syndrome, dispelling cold, expelling wind, relieving pain, warming lung, resolving fluid retention and dredging orifices; gypsum Fibrosum is sweet and pungent in flavor, cold in nature, enters lung and stomach channels, and is mainly used for clearing stomach fire, treating toothache due to stomach fire and gingival swelling and pain, and mainly treating wind-cold headache, nasosinusitis, toothache, phlegm and fluid retention cough, rheumatic arthralgia, etc.; radix Angelicae Dahuricae is warm in nature and pungent in flavor, and enters lung, spleen and stomach meridians; has effects in relieving exterior syndrome, dispelling cold, dispelling pathogenic wind, relieving pain, relieving swelling, promoting pus discharge, and clearing away heat and toxic materials, and can be used for treating headache, toothache, odontoptosis hemorrhage, nasosinusitis, intestinal wind, hemorrhoid, carbuncle, skin ulcer, etc.; cimicifuga rhizome, rhizoma cimicifugae, is pungent, sweet and slightly bitter, and gypsum can be introduced to treat headache and toothache at the vertex of yangming meridians; qing Yan warms middle energizer and dissipates nodulation, detoxifies and relieves pain. The medicines are combined to play the effects of dispelling wind, clearing heat, reducing swelling and relieving pain. Can be used for relieving toothache caused by pathogenic wind-fire, wind-cold, stomach heat, deficiency fire, and dental caries.

Detailed Description

The invention will be further illustrated with reference to specific examples.

Example one

A Chinese medicinal dentifrice with analgesic and teeth protecting effects is prepared from Halitum as main material, folium Ilicis Purpureae, fructus Piperis Longi and herba Dendrobii by baking at low temperature and drying, grinding, and making into dentifrice.

The weight ratio of the green salt to the Chinese holly, the long pepper and the dendrobium officinale is as follows: 15-25g of green salt, 6-10g of Chinese holly, 3-8g of long pepper and 4-10g of dendrobium officinale.

The auxiliary materials in the formula comprise gypsum, angelica dahurica, radix sileris, asarum, cimicifuga foetida and pepper, more than two components of the gypsum, the angelica dahurica, the radix sileris, the asarum, the cimicifuga foetida and the pepper are prepared into the auxiliary materials, the auxiliary materials are respectively baked, dried and dried under low temperature and pressure, then the dried raw materials are ground and processed to form powder, and the powder is prepared into the tooth powder auxiliary materials.

The auxiliary materials comprise gypsum, angelica dahurica, radix sileris, asarum, cimicifuga foetida and pepper in the following proportion: 4-10g of gypsum, 4-10g of angelica dahurica, 4-10g of divaricate saposhnikovia root, 3-8g of asarum, 4-10g of cimicifuga foetida and 4-10g of pepper.

The preparation of the dentifrice comprises the following steps:

1) selecting medicinal materials according to the ratio of the dentifrice, putting main material green salt in an oven, pressurizing at 50-70 ℃ and 0.5-1 MPa, baking at low temperature under pressure for 60-120 min, taking out, naturally cooling to normal temperature, grinding in a wall breaking pulverizer, grinding into powder, sieving with 800 mesh sieve, and retaining the sieved powder;

2) respectively baking and drying the Chinese holly leaf, the long pepper and the dendrobium officinale according to the characteristics of the materials, grinding the dried Chinese holly leaf, the long pepper and the dendrobium officinale into powder by using grinding equipment, screening by using a 800-mesh screen, and reserving screened powder;

3) respectively carrying out drying treatment on other auxiliary materials according to the characteristics of the materials, grinding the dried auxiliary materials into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;

4) mixing the powdered green salt, fructus Ilicis Purpureae, fructus Piperis Longi and herba Dendrobii, and other adjuvants at a ratio of 1:1:1 to obtain dentifrice.

The drying treatment of the long pepper is to put the long pepper prepared into traditional Chinese medicinal materials into a baking box, pressurize the long pepper at the temperature of 50-70 ℃ and 0.5MPa-1MPa, bake the long pepper at low temperature and pressure for 60-120 minutes to completely remove moisture in the long pepper to form dried long pepper, take the dried long pepper out of the baking box, pour the dried long pepper into grinding equipment for grinding, sieve the long pepper after grinding, sieve the long pepper by 800 meshes, leave and sieve powder, and mix the powder with other powder to prepare tooth powder.

The dried Chinese holly leaves are put into a baking box, the Chinese holly leaves which are prepared into traditional Chinese medicinal materials are pressurized at the temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for low-temperature pressurized baking for 60-120 minutes, so that the moisture in the Chinese holly leaves is completely removed to form dried Chinese holly leaves, the dried Chinese holly leaves are taken out from the baking box, poured into grinding equipment for grinding, sieved after grinding, sieved through 800 meshes, sieved powder is remained, and the dried Chinese holly leaves and other powder materials are mixed together to prepare the tooth powder.

The drying treatment of the dendrobium officinale is to put the dendrobium officinale made into traditional Chinese medicinal materials into a baking box, perform low-temperature pressure baking at the temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for 80-150 minutes to completely remove the moisture in the dendrobium officinale to form dried dendrobium officinale, take out the dried dendrobium officinale from the baking box, pour the dried dendrobium officinale into grinding equipment for grinding, sieve the dried dendrobium officinale after grinding, sieve the dried dendrobium officinale through 800 meshes, retain sieved powder, and mix the powder with other powder to prepare tooth powder.

The drying treatment of the gypsum, the angelica dahurica, the radix sileris, the asarum, the cimicifuga foetida and the pepper in the auxiliary materials is that the prepared various traditional Chinese medicinal materials are respectively put into a baking box, the low-temperature pressure baking is carried out for 80-150 minutes under the pressure of 0.5MPa-1MPa at the temperature of 50-70 ℃, the moisture in the various traditional Chinese medicinal materials is completely removed, the dried raw materials are formed, the dried gypsum, the angelica dahurica, the radix sileris, the asarum, the cimicifuga foetida and the pepper are respectively taken out from the baking box and put into grinding equipment for grinding, the ground raw materials are sieved, screened by a 800-mesh sieve, powder is remained, and then the dried gypsum, the angelica dahuri.

The Chinese holly leaf, the long pepper, the angelica dahurica, the divaricate saposhnikovia root, the asarum, the cimicifuga foetida and the pepper are dried in a closed environment, and are vacuumized and then filled with inert gas to be pressurized for drying treatment, so that volatile gas in the Chinese holly leaf, the long pepper, the angelica dahurica, the divaricate saposhnikovia root, the asarum, the cimicifuga foetida and the pepper is prevented from overflowing in the drying process.

The solution of the invention is: the Chinese holly leaf in the formula of the invention has the effects of clearing away heat and toxic materials, relieving swelling and removing blood stasis; the long pepper is pungent and hot, can promote qi circulation and relieve pain, and is used for treating toothache and red and swollen gum caused by swelling and pain due to cold pathogen coagulation and fire stagnation; dendrobium officinale is good at nourishing stomach yin, promoting the production of body fluid to quench thirst, clearing stomach heat and treating gum swelling and pain, mouth and tongue sores due to stomach heat and yin deficiency; the pepper kills the parasites with acrid heat and is good at removing dental caries and toothache; radix Saposhnikoviae has effects in expelling pathogenic wind and relieving pain; the asarum enters lung, liver, spleen and other channels, has the effects of relieving exterior syndrome, dispelling cold, expelling wind, relieving pain, warming lung, resolving fluid retention and dredging orifices; gypsum Fibrosum is sweet and pungent in flavor, cold in nature, enters lung and stomach channels, and is mainly used for clearing stomach fire, treating toothache due to stomach fire and gingival swelling and pain, and mainly treating wind-cold headache, nasosinusitis, toothache, phlegm and fluid retention cough, rheumatic arthralgia, etc.; radix Angelicae Dahuricae is warm in nature and pungent in flavor, and enters lung, spleen and stomach meridians; has effects in relieving exterior syndrome, dispelling cold, dispelling pathogenic wind, relieving pain, relieving swelling, promoting pus discharge, and clearing away heat and toxic materials, and can be used for treating headache, toothache, odontoptosis hemorrhage, nasosinusitis, intestinal wind, hemorrhoid, carbuncle, skin ulcer, etc.; cimicifuga rhizome, rhizoma cimicifugae, is pungent, sweet and slightly bitter, and gypsum can be introduced to treat headache and toothache at the vertex of yangming meridians; qing Yan warms middle energizer and dissipates nodulation, detoxifies and relieves pain. The medicines are combined to play the effects of dispelling wind, clearing heat, reducing swelling and relieving pain. Can be used for relieving toothache caused by pathogenic wind-fire, wind-cold, stomach heat, deficiency fire, and dental caries.

The using method comprises the following steps:

1. selecting a soft toothbrush

2. Soaking in water, drying, and soaking the powder

3. Lightly applying the dentifrice to the periphery of the teeth with a toothbrush

4. It is preferable to penetrate the dentifrice into the crevices of teeth to the greatest extent so that the crevices of teeth are slightly filled with the dentifrice

5. After the tooth is fully coated, the time for protecting and curing the tooth by the dentifrice is fully ensured after the tooth is waited for 1 to 3 minutes or more

6. Gargling, and lightly brushing off the dentifrice with a toothbrush.

The method is general in daily life: the product can be used as toothpaste companion, and toothpaste and dentifrice can be used for brushing teeth for 2-3 min, and rinsing mouth with clear water once in the morning and evening. Or dissolving the medicinal powder in water as collutory. For long-term use, the aged teeth are firm and do not shake.

Example two

The principle of the second embodiment is the same as that of the first embodiment, but the formulation and the preparation method are slightly different, and the second embodiment is the pain-relieving tooth-protecting dentifrice prepared from pure Chinese herbal medicines and the preparation method thereof.

The weight ratio of the green salt to the Chinese holly, the long pepper and the dendrobium officinale is as follows: 20-25g of green salt, 8-10g of Chinese holly, 5-8g of long pepper and 5-10g of dendrobium officinale.

The auxiliary materials comprise gypsum, angelica dahurica, radix sileris, asarum, cimicifuga foetida and pepper in the following proportion: 5-10g of gypsum, 5-10g of angelica dahurica, 5-10g of divaricate saposhnikovia root, 5-8g of asarum, 5-10g of rhizoma cimicifugae and 5-10g of pepper.

The preparation of the dentifrice comprises the following steps:

The Chinese holly leaf, the long pepper, the angelica dahurica, the divaricate saposhnikovia root, the asarum, the cimicifuga foetida and the pepper are dried in a closed environment, and are vacuumized and then filled with inert gas to be pressurized for drying treatment, so that volatile gas in the Chinese holly leaf, the long pepper, the angelica dahurica, the divaricate saposhnikovia root, the asarum, the cimicifuga foetida and the pepper is prevented from overflowing in the drying process. The vacuum degree is-10-45 KPa, the injected inert gas is nitrogen, and the pressure of the nitrogen is 0.5-1 KPa.

EXAMPLE III

The third embodiment is the same as the first embodiment in principle, is slightly different in formula and preparation method, is an analgesic tooth-protecting dentifrice prepared from pure Chinese herbal medicines and a preparation method thereof, and is prepared by taking green salt as a main material, adding green Chinese holly, long pepper and dendrobium officinale, respectively performing low-temperature pressure baking and drying treatment on the green Chinese holly, the long pepper and the dendrobium officinale, and then grinding the dried raw materials to form powder and preparing the dentifrice.

The weight ratio of the green salt to the Chinese holly, the long pepper and the dendrobium officinale is as follows: 15-20g of green salt, 6-8g of Chinese holly, 3-5g of long pepper and 4-8g of dendrobium officinale.

The auxiliary materials comprise gypsum, angelica dahurica, radix sileris, asarum, cimicifuga foetida and pepper in the following proportion: 4-5g of gypsum, 4-5g of angelica dahurica, 4-5g of divaricate saposhnikovia root, 3-5g of asarum, 4-5g of cimicifuga foetida and 4-5g of pepper.

The preparation of the dentifrice comprises the following steps:

The above listed embodiments are only for clear and complete description of the technical solution of the present invention; it is to be understood that the described embodiments are merely a few embodiments of the invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The invention has the advantages that:

Claims

1. An analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines is characterized in that: the preparation method comprises the steps of taking green salt as a main material, and performing low-temperature pressure baking and drying treatment on the green salt, the long pepper and the dendrobium officinale respectively, then grinding the dried raw materials to form powder, and preparing the powder into tooth powder.

2. An analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines as claimed in claim 1, characterized in that: the weight ratio of the green salt to the Chinese holly, the long pepper and the dendrobium officinale is as follows: 15-25g of green salt, 6-10g of Chinese holly, 3-8g of long pepper and 4-10g of dendrobium officinale.

3. An analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines as claimed in claim 1, characterized in that: the auxiliary materials in the formula comprise gypsum, angelica dahurica, radix sileris, asarum, cimicifuga foetida and pepper, more than two components of the gypsum, the angelica dahurica, the radix sileris, the asarum, the cimicifuga foetida and the pepper are prepared into the auxiliary materials, the auxiliary materials are respectively baked, dried and dried under low temperature and pressure, then the dried raw materials are ground and processed to form powder, and the powder is prepared into the tooth powder auxiliary materials.

4. An analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines as claimed in claim 3, characterized in that: the auxiliary materials comprise gypsum, angelica dahurica, radix sileris, asarum, cimicifuga foetida and pepper in the following proportion: 4-10g of gypsum, 4-10g of angelica dahurica, 4-10g of divaricate saposhnikovia root, 3-8g of asarum, 4-10g of cimicifuga foetida and 4-10g of pepper.

5. A method for preparing an analgesic tooth-protecting dentifrice prepared from the Chinese herbal medicines as claimed in claim 1, which is characterized in that: taking green salt as main material, adding folium Ilicis Purpureae, fructus Piperis Longi and herba Dendrobii, mixing folium Ilicis Purpureae, fructus Piperis Longi and herba Dendrobii, and adjuvant; respectively carrying out low-temperature pressurizing baking and drying treatment, and then grinding the dried raw materials to form powder to prepare the dentifrice; the preparation of the dentifrice comprises the following steps:

2) baking and drying the Chinese holly leaf, the long pepper and the dendrobium officinale according to the characteristics of the materials respectively, grinding the dried Chinese holly leaf, the long pepper and the dendrobium officinale into powder by using grinding equipment, screening by using a 800-mesh sieve, and reserving screened powder;

6. The method for preparing an analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines according to claim 5, wherein the analgesic tooth-protecting dentifrice comprises: the drying treatment of the long pepper is that the long pepper prepared into traditional Chinese medicinal materials is put into a baking box, the pressure is 0.5MPa to 1MPa at the temperature of 50 ℃ to 70 ℃, the low-temperature pressure baking is carried out, the long pepper is baked for 60 minutes to 120 minutes, so that the moisture in the long pepper is completely removed to form dried long pepper, the dried long pepper is taken out from the baking box, the dried long pepper is poured into grinding equipment for grinding, the ground long pepper is sieved after grinding, sieved by 800 meshes, sieved powder is remained, and the powder is mixed with other powder materials to prepare tooth powder.

7. The method for preparing an analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines according to claim 5, wherein the analgesic tooth-protecting dentifrice comprises: the dried Chinese holly leaves are put into a baking box, the Chinese holly leaves which are prepared into traditional Chinese medicinal materials are pressurized at the temperature of 50-70 ℃ and under the pressure of 0.5MPa-1MPa for low-temperature pressurized baking for 60-120 minutes, so that the moisture in the Chinese holly leaves is completely removed to form dried Chinese holly leaves, the dried Chinese holly leaves are taken out from the baking box, poured into grinding equipment for grinding, sieved after grinding, sieved through 800 meshes, sieved powder is remained, and the dried Chinese holly leaves and other powder materials are mixed together to prepare the tooth powder.

8. The method for preparing an analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines according to claim 5, wherein the analgesic tooth-protecting dentifrice comprises: the drying treatment of the dendrobium officinale comprises the steps of putting the dendrobium officinale made into traditional Chinese medicinal materials into a baking box, pressurizing at the temperature of 120-50-70 ℃ and under the pressure of 0.5MPa-1MPa, baking for 25-40 minutes to completely remove moisture in the dendrobium officinale to form dried dendrobium officinale, taking out the dried dendrobium officinale from the baking box, pouring the dried dendrobium officinale into grinding equipment for grinding, sieving after grinding, sieving through 800 meshes, reserving sieved powder, mixing with other powder materials together, and preparing to prepare tooth powder.

9. The method for preparing an analgesic tooth-protecting dentifrice prepared from Chinese herbal medicines according to claim 5, wherein the analgesic tooth-protecting dentifrice comprises: the drying treatment of the gypsum, the angelica dahurica, the radix sileris, the asarum, the cimicifuga foetida and the pepper in the auxiliary materials is that the prepared various traditional Chinese medicinal materials are respectively put into a baking box, the low-temperature pressure baking is carried out for 80-150 minutes under the pressure of 0.5MPa-1MPa at the temperature of 50-70 ℃, the moisture in the various traditional Chinese medicinal materials is completely removed, the dried raw materials are formed, the dried gypsum, the angelica dahurica, the radix sileris, the asarum, the cimicifuga foetida and the pepper are respectively taken out from the baking box and put into grinding equipment for grinding, the ground raw materials are sieved, screened by a 800-mesh sieve, powder is remained, and then the dried gypsum, the angelica dahuri.

10. The method for preparing the Chinese herbal medicine tooth strengthening dentifrice as claimed in claim 5, wherein the method comprises the following steps: the Chinese holly leaf, the long pepper, the angelica dahurica, the divaricate saposhnikovia root, the asarum, the cimicifuga foetida and the pepper are dried in a closed environment, and are vacuumized and then filled with inert gas to be pressurized for drying treatment, so that volatile gas in the Chinese holly leaf, the long pepper, the angelica dahurica, the divaricate saposhnikovia root, the asarum, the cimicifuga foetida and the pepper is prevented from overflowing in the drying process.