CN102093741A - 颜料黄138的制备方法 - Google Patents
颜料黄138的制备方法 Download PDFInfo
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- CN102093741A CN102093741A CN2011100255933A CN201110025593A CN102093741A CN 102093741 A CN102093741 A CN 102093741A CN 2011100255933 A CN2011100255933 A CN 2011100255933A CN 201110025593 A CN201110025593 A CN 201110025593A CN 102093741 A CN102093741 A CN 102093741A
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- Prior art keywords
- pigment yellow
- acid
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- warming
- Prior art date
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- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 229940067265 pigment yellow 138 Drugs 0.000 title abstract description 6
- 239000000049 pigment Substances 0.000 claims abstract description 60
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 27
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 claims abstract description 26
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000006243 chemical reaction Methods 0.000 claims abstract description 20
- AUHHYELHRWCWEZ-UHFFFAOYSA-N tetrachlorophthalic anhydride Chemical compound ClC1=C(Cl)C(Cl)=C2C(=O)OC(=O)C2=C1Cl AUHHYELHRWCWEZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 15
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 15
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 15
- 239000002253 acid Substances 0.000 claims abstract description 12
- 239000000126 substance Substances 0.000 claims abstract description 12
- 238000005406 washing Methods 0.000 claims abstract description 11
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 239000002002 slurry Substances 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 8
- 239000003960 organic solvent Substances 0.000 claims abstract description 7
- 238000010792 warming Methods 0.000 claims description 24
- 239000012043 crude product Substances 0.000 claims description 22
- 230000000485 pigmenting effect Effects 0.000 claims description 16
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 12
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- -1 polyoxyethylene octylphenol Polymers 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- RFFLAFLAYFXFSW-UHFFFAOYSA-N 1,2-dichlorobenzene Chemical compound ClC1=CC=CC=C1Cl RFFLAFLAYFXFSW-UHFFFAOYSA-N 0.000 claims description 6
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 235000019253 formic acid Nutrition 0.000 claims description 6
- 239000000376 reactant Substances 0.000 claims description 6
- 238000010992 reflux Methods 0.000 claims description 6
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 5
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims description 5
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Natural products C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- 239000004952 Polyamide Substances 0.000 claims description 4
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 4
- 229920002647 polyamide Polymers 0.000 claims description 4
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 4
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 3
- GSNUFIFRDBKVIE-UHFFFAOYSA-N DMF Natural products CC1=CC=C(C)O1 GSNUFIFRDBKVIE-UHFFFAOYSA-N 0.000 claims description 2
- 238000006386 neutralization reaction Methods 0.000 claims description 2
- 239000000047 product Substances 0.000 abstract description 10
- 238000003912 environmental pollution Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 238000010438 heat treatment Methods 0.000 abstract 4
- JHIAOWGCGNMQKA-UHFFFAOYSA-N 2-methyl-8-quinolinamine Chemical compound C1=CC=C(N)C2=NC(C)=CC=C21 JHIAOWGCGNMQKA-UHFFFAOYSA-N 0.000 abstract 1
- 239000005711 Benzoic acid Substances 0.000 abstract 1
- 235000010233 benzoic acid Nutrition 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 238000010298 pulverizing process Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 description 7
- 238000011084 recovery Methods 0.000 description 4
- 230000019612 pigmentation Effects 0.000 description 3
- 238000004040 coloring Methods 0.000 description 2
- 238000006482 condensation reaction Methods 0.000 description 2
- 239000012442 inert solvent Substances 0.000 description 2
- IZMJMCDDWKSTTK-UHFFFAOYSA-N quinoline yellow Chemical class C1=CC=CC2=NC(C3C(C4=CC=CC=C4C3=O)=O)=CC=C21 IZMJMCDDWKSTTK-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 2
- 239000003513 alkali Substances 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000012860 organic pigment Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
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- Paints Or Removers (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
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CN 201110025593 CN102093741B (zh) | 2011-01-24 | 2011-01-24 | 颜料黄138的制备方法 |
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CN 201110025593 CN102093741B (zh) | 2011-01-24 | 2011-01-24 | 颜料黄138的制备方法 |
Publications (2)
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CN102093741A true CN102093741A (zh) | 2011-06-15 |
CN102093741B CN102093741B (zh) | 2013-05-08 |
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CN 201110025593 Expired - Fee Related CN102093741B (zh) | 2011-01-24 | 2011-01-24 | 颜料黄138的制备方法 |
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CN (1) | CN102093741B (zh) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102965506A (zh) * | 2012-12-14 | 2013-03-13 | 葛新芳 | 苯甲酸盐沉淀法从稀土溶液中除铝方法 |
CN102993171A (zh) * | 2012-12-11 | 2013-03-27 | 百合花集团有限公司 | 合成喹酞酮黄的方法 |
CN108864730A (zh) * | 2018-08-10 | 2018-11-23 | 滨海明昇化工有限公司 | 一种颜料黄py138生产的新工艺 |
CN109061931A (zh) * | 2018-08-10 | 2018-12-21 | 滨海明昇化工有限公司 | 一种液晶显示器用py138衍生物的制备方法 |
CN110790982A (zh) * | 2019-10-30 | 2020-02-14 | 东莞理工学院 | 颜料黄138或其衍生物的高分子材料包裹物、其制备方法及其下游产品 |
CN113462188A (zh) * | 2021-06-16 | 2021-10-01 | 潍坊泰兴生物化工有限责任公司 | 一种弱溶剂中易分散颜料黄138及其制备方法 |
CN113881242A (zh) * | 2021-07-29 | 2022-01-04 | 潍坊泰兴生物化工有限责任公司 | 一种印铁油墨用低屈服值颜料黄py138产品制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5106980A (en) * | 1990-06-27 | 1992-04-21 | Basf Aktiengesellschaft | Preparation of quinophthalones |
CN1918244A (zh) * | 2003-12-31 | 2007-02-21 | 太阳化学公司 | 黄色颜料的制备 |
US20070119345A1 (en) * | 2004-02-20 | 2007-05-31 | Mca Technologies, Gmbh | Process for the preparation of organic materials |
-
2011
- 2011-01-24 CN CN 201110025593 patent/CN102093741B/zh not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5106980A (en) * | 1990-06-27 | 1992-04-21 | Basf Aktiengesellschaft | Preparation of quinophthalones |
CN1918244A (zh) * | 2003-12-31 | 2007-02-21 | 太阳化学公司 | 黄色颜料的制备 |
US20070119345A1 (en) * | 2004-02-20 | 2007-05-31 | Mca Technologies, Gmbh | Process for the preparation of organic materials |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102993171A (zh) * | 2012-12-11 | 2013-03-27 | 百合花集团有限公司 | 合成喹酞酮黄的方法 |
CN102993171B (zh) * | 2012-12-11 | 2015-04-15 | 百合花集团股份有限公司 | 合成喹酞酮黄的方法 |
CN102965506B (zh) * | 2012-12-14 | 2015-07-22 | 葛新芳 | 苯甲酸盐沉淀法从稀土溶液中除铝方法 |
CN102965506A (zh) * | 2012-12-14 | 2013-03-13 | 葛新芳 | 苯甲酸盐沉淀法从稀土溶液中除铝方法 |
CN109061931B (zh) * | 2018-08-10 | 2021-03-09 | 山东盛宏安华化学有限公司 | 一种液晶显示器用py138衍生物的制备方法 |
CN108864730A (zh) * | 2018-08-10 | 2018-11-23 | 滨海明昇化工有限公司 | 一种颜料黄py138生产的新工艺 |
CN109061931A (zh) * | 2018-08-10 | 2018-12-21 | 滨海明昇化工有限公司 | 一种液晶显示器用py138衍生物的制备方法 |
CN110790982A (zh) * | 2019-10-30 | 2020-02-14 | 东莞理工学院 | 颜料黄138或其衍生物的高分子材料包裹物、其制备方法及其下游产品 |
CN110790982B (zh) * | 2019-10-30 | 2021-02-09 | 东莞理工学院 | 颜料黄138或其衍生物的高分子材料包裹物、其制备方法及其下游产品 |
CN113462188A (zh) * | 2021-06-16 | 2021-10-01 | 潍坊泰兴生物化工有限责任公司 | 一种弱溶剂中易分散颜料黄138及其制备方法 |
CN113462188B (zh) * | 2021-06-16 | 2023-12-01 | 潍坊泰兴生物化工有限责任公司 | 一种弱溶剂中易分散颜料黄138及其制备方法 |
CN113881242A (zh) * | 2021-07-29 | 2022-01-04 | 潍坊泰兴生物化工有限责任公司 | 一种印铁油墨用低屈服值颜料黄py138产品制备方法 |
CN113881242B (zh) * | 2021-07-29 | 2023-07-18 | 潍坊泰兴生物化工有限责任公司 | 一种印铁油墨用低屈服值颜料黄py138产品制备方法 |
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CN102093741B (zh) | 2013-05-08 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CP03 | Change of name, title or address | ||
CP03 | Change of name, title or address |
Address after: 226100 Nantong, Haimen City, Jiangsu Province, the new area of the Yangtze River Road, No. 88 Patentee after: NANTONG LONGXIANG NEW MATERIALS TECHNOLOGY Co.,Ltd. Address before: 226103 Jiangsu city of Nantong Province Haimen Development Zone, Haimen port Patentee before: Nantong Longxiang Chemical Co.,Ltd. |
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TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20220629 Address after: 226100 room 508, building 8, Guidu Zhixing, Haimen street, Haimen District, Nantong City, Jiangsu Province Patentee after: Nantong Longyi New Material Technology Co.,Ltd. Address before: 226100 No. 88, Yangzijiang Road, Linjiang new area, Haimen City, Nantong City, Jiangsu Province Patentee before: NANTONG LONGXIANG NEW MATERIALS TECHNOLOGY Co.,Ltd. |
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CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130508 |