CN102092979A - 一种氨基磺酸盐减水剂及其制备方法 - Google Patents
一种氨基磺酸盐减水剂及其制备方法 Download PDFInfo
- Publication number
- CN102092979A CN102092979A CN 201010583995 CN201010583995A CN102092979A CN 102092979 A CN102092979 A CN 102092979A CN 201010583995 CN201010583995 CN 201010583995 CN 201010583995 A CN201010583995 A CN 201010583995A CN 102092979 A CN102092979 A CN 102092979A
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- China
- Prior art keywords
- parts
- formaldehyde
- add
- reaction
- phenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003638 chemical reducing agent Substances 0.000 title claims abstract description 37
- IIACRCGMVDHOTQ-UHFFFAOYSA-M sulfamate Chemical compound NS([O-])(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-M 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 42
- 238000006243 chemical reaction Methods 0.000 claims abstract description 36
- HVBSAKJJOYLTQU-UHFFFAOYSA-N 4-aminobenzenesulfonic acid Chemical compound NC1=CC=C(S(O)(=O)=O)C=C1 HVBSAKJJOYLTQU-UHFFFAOYSA-N 0.000 claims abstract description 15
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229950000244 sulfanilic acid Drugs 0.000 claims abstract description 14
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 claims abstract description 6
- 238000000034 method Methods 0.000 claims abstract 7
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 81
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 40
- 239000002253 acid Substances 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 16
- 238000004519 manufacturing process Methods 0.000 claims description 8
- 239000012263 liquid product Substances 0.000 claims description 5
- 150000007513 acids Chemical class 0.000 claims description 4
- 238000005304 joining Methods 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 239000007787 solid Substances 0.000 claims description 2
- 238000003912 environmental pollution Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 abstract 1
- 239000004568 cement Substances 0.000 description 7
- 239000007859 condensation product Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- PKIRNMPSENTWJX-UHFFFAOYSA-N 4-aminobenzenesulfonic acid Chemical compound NC1=CC=C(S(O)(=O)=O)C=C1.NC1=CC=C(S(O)(=O)=O)C=C1 PKIRNMPSENTWJX-UHFFFAOYSA-N 0.000 description 1
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 description 1
- 229920001732 Lignosulfonate Polymers 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001912 cyanamides Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 235000019357 lignosulphonate Nutrition 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 229920005552 sodium lignosulfonate Polymers 0.000 description 1
- ITCAUAYQCALGGV-XTICBAGASA-M sodium;(1r,4ar,4br,10ar)-1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylate Chemical compound [Na+].C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C([O-])=O ITCAUAYQCALGGV-XTICBAGASA-M 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B40/00—Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
- C04B40/0028—Aspects relating to the mixing step of the mortar preparation
- C04B40/0039—Premixtures of ingredients
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201010583995 CN102092979B (zh) | 2010-12-10 | 2010-12-10 | 一种氨基磺酸盐减水剂及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201010583995 CN102092979B (zh) | 2010-12-10 | 2010-12-10 | 一种氨基磺酸盐减水剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102092979A true CN102092979A (zh) | 2011-06-15 |
CN102092979B CN102092979B (zh) | 2012-11-14 |
Family
ID=44126267
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 201010583995 Expired - Fee Related CN102092979B (zh) | 2010-12-10 | 2010-12-10 | 一种氨基磺酸盐减水剂及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN102092979B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103113037A (zh) * | 2013-01-22 | 2013-05-22 | 科之杰新材料集团有限公司 | 一种低成本低泌水氨基磺酸盐高效减水剂及其制备方法 |
CN103265204A (zh) * | 2013-05-10 | 2013-08-28 | 济南融祺建材有限公司 | 一种氨基磺酸盐高效减水剂的制作方法 |
CN106117482A (zh) * | 2016-06-29 | 2016-11-16 | 南京瑞迪高新技术有限公司 | 一种改性高保坍萘系减水剂及其制备方法 |
CN107759756A (zh) * | 2017-10-17 | 2018-03-06 | 江苏苏博特新材料股份有限公司 | 一种氨基磺酸盐减水剂及其制备方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS52111893A (en) * | 1976-03-17 | 1977-09-19 | Taki Chem Co Ltd | Water treating agent |
JP2000191739A (ja) * | 1998-10-23 | 2000-07-11 | Nissan Chem Ind Ltd | スルファニル酸変性メラミンホルムアルデヒド樹脂水溶液の製造方法 |
CN1274696A (zh) * | 1999-05-19 | 2000-11-29 | 四川大学 | 固态混凝土减水剂及其制造方法 |
CN1559963A (zh) * | 2004-02-26 | 2005-01-05 | 同济大学 | 建筑用氨基磺酸盐高性能减水剂及其制备方法 |
CN101224958A (zh) * | 2008-02-01 | 2008-07-23 | 福州大学 | 磺化碱木素改性氨基磺酸系高效减水剂及其制备方法 |
CN101289291A (zh) * | 2007-04-17 | 2008-10-22 | 中国石油集团工程技术研究院 | 一种水下不分散混凝土用快凝絮凝剂 |
-
2010
- 2010-12-10 CN CN 201010583995 patent/CN102092979B/zh not_active Expired - Fee Related
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS52111893A (en) * | 1976-03-17 | 1977-09-19 | Taki Chem Co Ltd | Water treating agent |
JP2000191739A (ja) * | 1998-10-23 | 2000-07-11 | Nissan Chem Ind Ltd | スルファニル酸変性メラミンホルムアルデヒド樹脂水溶液の製造方法 |
CN1274696A (zh) * | 1999-05-19 | 2000-11-29 | 四川大学 | 固态混凝土减水剂及其制造方法 |
CN1559963A (zh) * | 2004-02-26 | 2005-01-05 | 同济大学 | 建筑用氨基磺酸盐高性能减水剂及其制备方法 |
CN101289291A (zh) * | 2007-04-17 | 2008-10-22 | 中国石油集团工程技术研究院 | 一种水下不分散混凝土用快凝絮凝剂 |
CN101224958A (zh) * | 2008-02-01 | 2008-07-23 | 福州大学 | 磺化碱木素改性氨基磺酸系高效减水剂及其制备方法 |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103113037A (zh) * | 2013-01-22 | 2013-05-22 | 科之杰新材料集团有限公司 | 一种低成本低泌水氨基磺酸盐高效减水剂及其制备方法 |
CN103113037B (zh) * | 2013-01-22 | 2015-03-11 | 科之杰新材料集团有限公司 | 一种低成本低泌水氨基磺酸盐高效减水剂及其制备方法 |
CN103265204A (zh) * | 2013-05-10 | 2013-08-28 | 济南融祺建材有限公司 | 一种氨基磺酸盐高效减水剂的制作方法 |
CN103265204B (zh) * | 2013-05-10 | 2015-07-29 | 济南融祺建材有限公司 | 一种氨基磺酸盐高效减水剂的制作方法 |
CN106117482A (zh) * | 2016-06-29 | 2016-11-16 | 南京瑞迪高新技术有限公司 | 一种改性高保坍萘系减水剂及其制备方法 |
CN106117482B (zh) * | 2016-06-29 | 2018-05-18 | 南京瑞迪高新技术有限公司 | 一种改性高保坍萘系减水剂及其制备方法 |
CN107759756A (zh) * | 2017-10-17 | 2018-03-06 | 江苏苏博特新材料股份有限公司 | 一种氨基磺酸盐减水剂及其制备方法 |
CN107759756B (zh) * | 2017-10-17 | 2020-08-11 | 江苏苏博特新材料股份有限公司 | 一种氨基磺酸盐减水剂及其制备方法 |
Also Published As
Publication number | Publication date |
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CN102092979B (zh) | 2012-11-14 |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: TIANZHU SCIENCE AND TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: MA QINGHAO Effective date: 20130417 |
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C41 | Transfer of patent application or patent right or utility model | ||
COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 101408 HUAIROU, BEIJING TO: 401220 CHANGSHOU, CHONGQING |
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TR01 | Transfer of patent right |
Effective date of registration: 20130417 Address after: 401220, longevity zone, Chongqing Yan Street Chemical Park Management Committee, four floor, science and Technology Building Patentee after: CHONGQING TIANZHU SCIENCE AND TECHNOLOGY CO., LTD. Address before: 101408 Beijing city Huairou District Huai Beizhen Hefangkou village 543 Mu lake company Patentee before: Ma Qinghao |
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C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20121114 Termination date: 20131210 |