CN101947655A - 三角形银纳米片的制备方法 - Google Patents
三角形银纳米片的制备方法 Download PDFInfo
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- CN101947655A CN101947655A CN 201010518174 CN201010518174A CN101947655A CN 101947655 A CN101947655 A CN 101947655A CN 201010518174 CN201010518174 CN 201010518174 CN 201010518174 A CN201010518174 A CN 201010518174A CN 101947655 A CN101947655 A CN 101947655A
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- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title claims abstract description 67
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- 229910052709 silver Inorganic materials 0.000 title claims abstract description 13
- 239000004332 silver Substances 0.000 title claims abstract description 13
- 239000002135 nanosheet Substances 0.000 title abstract 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 74
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims abstract description 52
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims abstract description 52
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims abstract description 52
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 26
- 239000012279 sodium borohydride Substances 0.000 claims abstract description 23
- 229910000033 sodium borohydride Inorganic materials 0.000 claims abstract description 23
- 238000003756 stirring Methods 0.000 claims abstract description 14
- 239000001509 sodium citrate Substances 0.000 claims abstract description 13
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 claims abstract description 13
- 229940038773 trisodium citrate Drugs 0.000 claims abstract description 13
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical group [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 26
- 229910001961 silver nitrate Inorganic materials 0.000 claims description 13
- 101710134784 Agnoprotein Proteins 0.000 claims description 12
- 239000011734 sodium Substances 0.000 claims description 11
- 238000002156 mixing Methods 0.000 claims description 9
- YPNVIBVEFVRZPJ-UHFFFAOYSA-L silver sulfate Chemical compound [Ag+].[Ag+].[O-]S([O-])(=O)=O YPNVIBVEFVRZPJ-UHFFFAOYSA-L 0.000 claims description 8
- 238000006722 reduction reaction Methods 0.000 claims description 6
- 230000000694 effects Effects 0.000 claims description 5
- YDHABVNRCBNRNZ-UHFFFAOYSA-M silver perchlorate Chemical compound [Ag+].[O-]Cl(=O)(=O)=O YDHABVNRCBNRNZ-UHFFFAOYSA-M 0.000 claims description 5
- 238000000034 method Methods 0.000 abstract description 7
- XLYOFNOQVPJJNP-ZSJDYOACSA-N heavy water Substances [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 5
- 239000003638 chemical reducing agent Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- VLTRZXGMWDSKGL-UHFFFAOYSA-M perchlorate Inorganic materials [O-]Cl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-M 0.000 description 3
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 3
- UORVGPXVDQYIDP-UHFFFAOYSA-N borane Chemical compound B UORVGPXVDQYIDP-UHFFFAOYSA-N 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 239000003223 protective agent Substances 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 241000792859 Enema Species 0.000 description 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 239000000090 biomarker Substances 0.000 description 1
- 229910000085 borane Inorganic materials 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000013872 defecation Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000007920 enema Substances 0.000 description 1
- 229940095399 enema Drugs 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 229910001410 inorganic ion Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002082 metal nanoparticle Substances 0.000 description 1
- 238000000593 microemulsion method Methods 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 229910000104 sodium hydride Inorganic materials 0.000 description 1
- 239000012312 sodium hydride Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000829 suppository Substances 0.000 description 1
- 238000004416 surface enhanced Raman spectroscopy Methods 0.000 description 1
- 238000002198 surface plasmon resonance spectroscopy Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
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Cited By (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102351887A (zh) * | 2011-06-27 | 2012-02-15 | 江南大学 | 用于高灵敏、高选择性检测硫脲的贵金属纳米光学探针的合成方法 |
CN102371357A (zh) * | 2011-09-14 | 2012-03-14 | 王利兵 | 一种液相制备树枝状微米银的方法 |
CN102507710A (zh) * | 2011-10-11 | 2012-06-20 | 中国科学院合肥物质科学研究院 | 一种痕量、快速检测多氯联苯的电化学方法 |
CN102554258A (zh) * | 2012-02-03 | 2012-07-11 | 济南大学 | 一种在水溶液里制备金属银纳米结构的方法 |
CN102672167A (zh) * | 2011-03-16 | 2012-09-19 | 首都师范大学 | 一种新型三角形银-硫化银纳米复合颗粒的制备及其应用 |
CN103817346A (zh) * | 2014-03-11 | 2014-05-28 | 上海交通大学 | 一种形貌可控的三角形片状纳米银粉制备方法 |
CN103820826A (zh) * | 2012-11-19 | 2014-05-28 | 中国科学院合肥物质科学研究院 | 形貌可控的银纳米片组装结构阵列的制备方法及其产物的用途 |
CN104259482A (zh) * | 2014-10-27 | 2015-01-07 | 山东大学 | 单分散银纳米片的宏量制备方法 |
CN104422688A (zh) * | 2013-08-21 | 2015-03-18 | 中国科学院宁波材料技术与工程研究所 | 一种半胱氨酸的检测试剂及检测方法 |
CN105127448A (zh) * | 2015-09-25 | 2015-12-09 | 合肥工业大学 | 一种超大面积纳米银片的室温制备方法 |
CN105149613A (zh) * | 2015-09-24 | 2015-12-16 | 厦门大学 | 一种片状银纳米材料的制备方法 |
CN105290420A (zh) * | 2012-11-29 | 2016-02-03 | 江苏理工学院 | 制备片状纳米银粉的方法 |
CN106248633A (zh) * | 2016-07-25 | 2016-12-21 | 兰州大学 | 一种原位高通量检测芯片的制备方法 |
CN106563814A (zh) * | 2016-11-11 | 2017-04-19 | 广州大学 | 一种光诱导法对银纳米三角片的可控制备方法及其应用 |
CN107486026A (zh) * | 2017-08-18 | 2017-12-19 | 清华大学 | 抗生物污染的分离膜及其制备方法 |
CN108405880A (zh) * | 2018-04-20 | 2018-08-17 | 河南大学 | 利用旋涂法制备黄原胶网络结构辅助均匀分散三角形纳米银复合材料的方法 |
CN109128216A (zh) * | 2018-10-26 | 2019-01-04 | 启东科赛尔纳米科技有限公司 | 常温下金纳米粒子的合成方法 |
CN109500405A (zh) * | 2019-01-17 | 2019-03-22 | 鲁东大学 | 一种三角银纳米片的制备方法 |
CN109781697A (zh) * | 2018-12-27 | 2019-05-21 | 西安交通大学 | 一种柔性sers基底及其制备方法和双氧水sers光谱检测的应用 |
CN110039066A (zh) * | 2019-04-04 | 2019-07-23 | 连云港职业技术学院 | 一种以pvp为导向和组装的纳米金岛状结构的制备方法 |
CN111151767A (zh) * | 2020-01-16 | 2020-05-15 | 江苏镭明新材料科技有限公司 | 一种复合纳米银喷墨导电墨水的制备方法 |
CN111250729A (zh) * | 2020-04-02 | 2020-06-09 | 海泰纳鑫科技(成都)有限公司 | 调节银纳米片尺寸的方法 |
CN111691003A (zh) * | 2020-05-27 | 2020-09-22 | 南通纺织丝绸产业技术研究院 | 基于片状银纳米粒子的物理色纤维及其制备方法 |
CN112299936A (zh) * | 2020-11-06 | 2021-02-02 | 西南科技大学 | 用于炸药激光引爆的光热材料的制备方法及应用 |
CN112870221A (zh) * | 2021-01-05 | 2021-06-01 | 中山大学附属第五医院 | 一种壳聚糖纳米铑材料及其应用 |
CN115570144A (zh) * | 2022-09-20 | 2023-01-06 | 天津理工大学 | 厚度可控的银纳米片的制备方法 |
CN115805316A (zh) * | 2021-09-14 | 2023-03-17 | 中国科学院化学研究所 | 片状银纳米颗粒及其制备方法以及导电银浆组合物和导电银浆 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1935422A (zh) * | 2006-09-30 | 2007-03-28 | 南京大学 | 单分散三角纳米银片的制备方法 |
CN101731272A (zh) * | 2009-12-24 | 2010-06-16 | 中国人民解放军军事医学科学院基础医学研究所 | 一种抗菌纳米银溶胶的制备方法 |
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2010
- 2010-10-25 CN CN2010105181749A patent/CN101947655B/zh not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1935422A (zh) * | 2006-09-30 | 2007-03-28 | 南京大学 | 单分散三角纳米银片的制备方法 |
CN101731272A (zh) * | 2009-12-24 | 2010-06-16 | 中国人民解放军军事医学科学院基础医学研究所 | 一种抗菌纳米银溶胶的制备方法 |
Non-Patent Citations (2)
Title |
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《物理化学学报》 20100430 赖文忠等 用双还原法制备三角形银纳米片及其光学性能 1177-1183 1-5 第26卷, 第4期 2 * |
《贵金属》 20080531 郭斌等 双还原剂法制备的三角形银纳米盘的吸收和发射光谱研究 5-10 1-5 第29卷, 第2期 2 * |
Cited By (36)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102672167A (zh) * | 2011-03-16 | 2012-09-19 | 首都师范大学 | 一种新型三角形银-硫化银纳米复合颗粒的制备及其应用 |
CN102672167B (zh) * | 2011-03-16 | 2014-04-02 | 首都师范大学 | 一种新型三角形银-硫化银纳米复合颗粒的制备及其应用 |
CN102351887A (zh) * | 2011-06-27 | 2012-02-15 | 江南大学 | 用于高灵敏、高选择性检测硫脲的贵金属纳米光学探针的合成方法 |
CN102371357A (zh) * | 2011-09-14 | 2012-03-14 | 王利兵 | 一种液相制备树枝状微米银的方法 |
CN102371357B (zh) * | 2011-09-14 | 2013-06-12 | 王利兵 | 一种液相制备树枝状微米银的方法 |
CN102507710A (zh) * | 2011-10-11 | 2012-06-20 | 中国科学院合肥物质科学研究院 | 一种痕量、快速检测多氯联苯的电化学方法 |
CN102554258A (zh) * | 2012-02-03 | 2012-07-11 | 济南大学 | 一种在水溶液里制备金属银纳米结构的方法 |
CN102554258B (zh) * | 2012-02-03 | 2014-05-28 | 济南大学 | 一种在水溶液里制备金属银纳米结构的方法 |
CN103820826A (zh) * | 2012-11-19 | 2014-05-28 | 中国科学院合肥物质科学研究院 | 形貌可控的银纳米片组装结构阵列的制备方法及其产物的用途 |
CN105290420B (zh) * | 2012-11-29 | 2017-11-21 | 江苏理工学院 | 制备片状纳米银粉的方法 |
CN105290420A (zh) * | 2012-11-29 | 2016-02-03 | 江苏理工学院 | 制备片状纳米银粉的方法 |
CN104422688A (zh) * | 2013-08-21 | 2015-03-18 | 中国科学院宁波材料技术与工程研究所 | 一种半胱氨酸的检测试剂及检测方法 |
CN104422688B (zh) * | 2013-08-21 | 2017-06-06 | 中国科学院宁波材料技术与工程研究所 | 一种半胱氨酸的检测试剂及检测方法 |
CN103817346A (zh) * | 2014-03-11 | 2014-05-28 | 上海交通大学 | 一种形貌可控的三角形片状纳米银粉制备方法 |
CN104259482A (zh) * | 2014-10-27 | 2015-01-07 | 山东大学 | 单分散银纳米片的宏量制备方法 |
CN105149613A (zh) * | 2015-09-24 | 2015-12-16 | 厦门大学 | 一种片状银纳米材料的制备方法 |
CN105127448A (zh) * | 2015-09-25 | 2015-12-09 | 合肥工业大学 | 一种超大面积纳米银片的室温制备方法 |
CN106248633A (zh) * | 2016-07-25 | 2016-12-21 | 兰州大学 | 一种原位高通量检测芯片的制备方法 |
CN106563814A (zh) * | 2016-11-11 | 2017-04-19 | 广州大学 | 一种光诱导法对银纳米三角片的可控制备方法及其应用 |
CN106563814B (zh) * | 2016-11-11 | 2018-12-07 | 广州大学 | 一种光诱导法对银纳米三角片的可控制备方法 |
CN107486026A (zh) * | 2017-08-18 | 2017-12-19 | 清华大学 | 抗生物污染的分离膜及其制备方法 |
CN107486026B (zh) * | 2017-08-18 | 2021-04-02 | 清华大学 | 抗生物污染的分离膜及其制备方法 |
CN108405880A (zh) * | 2018-04-20 | 2018-08-17 | 河南大学 | 利用旋涂法制备黄原胶网络结构辅助均匀分散三角形纳米银复合材料的方法 |
CN109128216A (zh) * | 2018-10-26 | 2019-01-04 | 启东科赛尔纳米科技有限公司 | 常温下金纳米粒子的合成方法 |
CN109781697A (zh) * | 2018-12-27 | 2019-05-21 | 西安交通大学 | 一种柔性sers基底及其制备方法和双氧水sers光谱检测的应用 |
CN109500405A (zh) * | 2019-01-17 | 2019-03-22 | 鲁东大学 | 一种三角银纳米片的制备方法 |
CN109500405B (zh) * | 2019-01-17 | 2022-02-22 | 鲁东大学 | 一种三角银纳米片的制备方法 |
CN110039066A (zh) * | 2019-04-04 | 2019-07-23 | 连云港职业技术学院 | 一种以pvp为导向和组装的纳米金岛状结构的制备方法 |
CN111151767A (zh) * | 2020-01-16 | 2020-05-15 | 江苏镭明新材料科技有限公司 | 一种复合纳米银喷墨导电墨水的制备方法 |
CN111250729A (zh) * | 2020-04-02 | 2020-06-09 | 海泰纳鑫科技(成都)有限公司 | 调节银纳米片尺寸的方法 |
CN111691003A (zh) * | 2020-05-27 | 2020-09-22 | 南通纺织丝绸产业技术研究院 | 基于片状银纳米粒子的物理色纤维及其制备方法 |
CN111691003B (zh) * | 2020-05-27 | 2021-09-17 | 南通纺织丝绸产业技术研究院 | 基于片状银纳米粒子的物理色纤维及其制备方法 |
CN112299936A (zh) * | 2020-11-06 | 2021-02-02 | 西南科技大学 | 用于炸药激光引爆的光热材料的制备方法及应用 |
CN112870221A (zh) * | 2021-01-05 | 2021-06-01 | 中山大学附属第五医院 | 一种壳聚糖纳米铑材料及其应用 |
CN115805316A (zh) * | 2021-09-14 | 2023-03-17 | 中国科学院化学研究所 | 片状银纳米颗粒及其制备方法以及导电银浆组合物和导电银浆 |
CN115570144A (zh) * | 2022-09-20 | 2023-01-06 | 天津理工大学 | 厚度可控的银纳米片的制备方法 |
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Effective date of registration: 20130807 Address after: 226600, Haiphong Road, Chengdong Town, Haian County, Jiangsu, Nantong, 33 Patentee after: Nantong Sixiang Silk Co.,Ltd. Patentee after: JIANGSU University OF TECHNOLOGY Address before: 213001 Changzhou Province in the Clock Tower District, Jiangsu, Wu Road, No. 1801 Patentee before: Jiangsu Teachers University of Technology |
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