CN101941872A - Pesticidal foliage fertilizer mixed with plant growth factors and preparation method thereof - Google Patents
Pesticidal foliage fertilizer mixed with plant growth factors and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a pesticidal foliage fertilizer, which is prepared by grinding and uniformly mixing gibberellin 3, heteroauxin, brassinolide, abscisic acid, jasmonic acid, zeatin, salicylic acid, 1-aminocyclopropane-carboxylic acid. The fertilizer is a novel phytosterol foliage fertilizer with advantages of high efficiency, no toxicity and environmental friendliness, can promote the growth of plants by over 10 percent, and has no environmental pollution.
Description
Technical field
The present invention relates to a kind of Pesticidal foliage fertilizer, Pesticidal foliage fertilizer of the long factor of particularly a kind of mixed plant symphysis and preparation method thereof.
Background technology
Because characteristics such as foliage fertilizer has instant effect, utilization ratio height, consumption is few, using method is easy and effect of increasing production is obvious, and be widely used in the agriculture production.In recent years, all take much count of the production and the application of foliage fertilizer both at home and abroad, only hundreds of is arranged at the Chinese commodity foliage fertilizer.But, still do not have preferably, have nutrition, coordinate plant growth, desinsection and multi-functional composite foliage fertilizer such as antibacterial.So we have researched and developed a series of multi-functional composite foliage fertilizer, farming No. 1 foliage fertilizer in north is wherein a kind of, and the research and development application of this kind has been enriched the kind of foliage fertilizer and offered the multiple possible selection of peasant.
Summary of the invention
The object of the present invention is to provide the Pesticidal foliage fertilizer of the long factor of a kind of mixed plant symphysis; The present invention also aims to provide the preparation method of this medicine fertilizer.
Pesticidal foliage fertilizer composition of the present invention, its raw material consists of (weight part):
Plant hormones regulators,gibberellins (3) 7-11 part
Indolylacetic acid 0.01-0.1 part
Brassinolide 0.01-0.1 part
Dormin 0.01-0.1 part
Jasmonic acid 0.01-0.1
Zeatin 0.01-0.1
Whitfield's ointment 0.02-0.1 part
1-amino-cyclopropane-1-carboxylic acid 0.01-0.1 part.
Pesticidal foliage fertilizer composition of the present invention, its raw material consists of (weight part):
Plant hormones regulators,gibberellins 38-9.9 part
Indolylacetic acid 0.01-0.05 part
Brassinolide 0.01-0.04 part
Dormin 0.01-0.03 part
Jasmonic acid 0.01-0.04 part
Zeatin 0.01-0.04 part
Whitfield's ointment 0.02-0.04 part
1-amino-cyclopropane-1-carboxylic acid 0.01-0.03 part.
Pesticidal foliage fertilizer composition of the present invention, its raw material composition is preferably following weight part:
Plant hormones regulators,gibberellins 39.5-9.9 part
Indolylacetic acid 0.04-0.05 part
Brassinolide 0.02-0.03 part
Dormin 0.01-0.02 part
Jasmonic acid 0.01-0.02 part
Zeatin 0.01-0.02 part
Whitfield's ointment 0.02-0.03 part
1-amino-cyclopropane-1-carboxylic acid 0.01-0.02.
Pesticidal foliage fertilizer preparation of compositions method of the present invention is, it is even that said components is pressed the prescription ground and mixed, promptly gets the growth hormone mixture.
Said mixture is prepared as optional one of the face technology of taking off of water dispersant:
A gets this growth hormone mixture 0.5-2.5 weight part (preferred 1-2 weight part), adds dispersion agent 0.1-0.2 weight part (preferred 0.12-0.16) again, and wetting agent 0.05-0.1 weight part (preferred 0.06-0.08) is filled to 10 weight parts.It is 1 that above each component is dissolved in volume ratio: ground and mixed is even in the organic solvent (preferred alcohol) of 1-3 (preferred 1: 2), in 40-70 ℃ (preferred 50 ℃) oven dry, grind evenly, and drying, packing promptly obtains growth hormone mixture water dispersant.
B gets this growth hormone mixture 0.5-2.5 weight part (preferred 1-2 weight part), adds dispersion agent 0.1-0.2 weight part (preferred 0.12-0.16) again, and wetting agent 0.05-0.1 weight part (preferred 0.06-0.08) is filled to 10 weight parts.It is 1 that above each component is dissolved in volume ratio: ground and mixed is even in the organic solvent (preferred alcohol) of 1-3 (preferred 1: 1), in 40-70 ℃ (preferred 50 ℃) oven dry, grind evenly, and drying, packing promptly obtains growth hormone mixture water dispersant.
Used organic solvent can also be selected to indefiniteness a kind of in chloroform, 40-90 ℃ sherwood oil, ether, ethyl acetate, normal hexane, hexanaphthene, benzene, ethyl acetate, methyl alcohol, acetone, the pimelinketone etc. except that ethanol.
Used dispersion agent can be a kind of in the alkaline sodium lignosulfonate A of improvement, improvement alkaline sodium lignosulfonate B, desugar sodium lignosulfonate (M-9), desugar condensation sodium lignosulfonate (M series), the methanonaphthalene sulfonic acid class dispersion agent (as dispersion agent NNO, Dispersant MF, dispersing agent C NF, super dispersion agent 550S, Di Sier economic benefits and social benefits); Wetting agent is how sodium sulfonate, succsinic acid alkyl sodium sulfonate a kind of of Saponin/TSM, animal protein factor digest, lipid acid vitriol, this sulfonate of alkyl, single two sodium alkyl benzene sulfonates, polymerization of carboxylic acid sodium, sodium lignosulfonate, petroleum sodium sulfonate, alkyl biphenyl ether sulfonic acid sodium, dipropyl benzene sulfonic acid sodium salt, butyl; Permeate agent is any one or a few among Fatty Alcohol(C12-C14 and C12-C18) polyoxy ether alkene, permeate agent BA, penetrant m, the penetrant t H; Filler is: a kind of in potter's clay, clay, kaolin, diatomite, talcum powder, pyrophyllite, the white carbon black.
Novel many growth hormone foliage fertilizer is made (weight part) by following raw material:
Growth hormone mixture water dispersant 0.1-0.3 part
Nutritive element mixture 2-6 part
Plant sterol mixture 2-3.5 part
Weighting agent adds to 10 parts
Novel many growth hormone foliage fertilizer is preferably made (weight part) by following raw material:
0.11 part of growth hormone mixture water dispersant
5 parts in nutritive element mixture
2.5 parts in plant sterol mixture
Weighting agent adds to 10 parts
Novel many growth hormone foliage fertilizer is preferably made (weight part) by following raw material:
0.12 part of growth hormone mixture water dispersant
4 parts in nutritive element mixture
3.5 parts in plant sterol mixture
Weighting agent adds to 10 parts
Novel many growth hormone foliage fertilizer is preferably made (weight part) by following raw material:
0.13 part of growth hormone mixture water dispersant
6 parts in nutritive element mixture
3 parts in plant sterol mixture
Weighting agent adds to 10 parts
Growth hormone mixture water dispersant of the present invention (0.1-0.3 part) nutritive element mixture (2-6 part) and plant sterol mixture (2-3.5 part), more than all be weight part, add a certain amount of filler to 10 part again, abundant mixing, dry, packing gets final product.
Above-mentioned nutritive element mixture among the present invention (is example with 20 weight parts) comprises urea 5 weight parts, potassium primary phosphate 2 weight parts, boric acid 2 weight parts; Disodium ethylene diamine tetraacetate 1.8 weight parts, Manganous chloride tetrahydrate 2 weight parts, calcium chloride 1 weight part, sal epsom 2 weight parts, ferrous sulfate 2 weight parts, zinc sulfate 1 weight part, copper sulfate 0.2 weight part, (above-mentioned raw materials mixing, be dissolved in an amount of water, spraying drying gets final product).
The present invention plants the plant sterol of another functional additive for directly extracting from leguminous plants, comprise that β-Gu Zaichun, Stigmasterol, campesterol, brassicasterol, avenasterol, ergosterol, this sterol of standing grain, citrostadienol, Lip river fly enol, ring jackfruit alcohol, cycloartenol, 2,4-methylene basic ring jackfruit alcohol waits any one or a few.Directly from plant, extract with organic solvent and to obtain.Used organic solvent can also be selected to indefiniteness a kind of in chloroform, 40-90 ℃ sherwood oil, ether, ethyl acetate, normal hexane, hexanaphthene, benzene, ethyl acetate, methyl alcohol, acetone, the cyclohexanone etc. except that ethanol.
Among the present invention, also optionally added auxiliary materials such as synergistic agent, permeate agent and stablizer, its usage ratio is 0.1-2%, and synergistic agent is any in tea saponin, root of langdu chromone, methylenedioxy benzene derivative, the 6-vinyl capraldehyde; Permeate agent is any in emulsifier BP, azone, the triphen phosphorus.Stablizer is a kind of in sodium alkyl benzene sulfonate, the Soxylat A 25-7.
Characteristic of the present invention is to collect coordinate plant growth, desinsection, multiple function such as antibacterial in foliage fertilizer, the technical process maturation, cheap for manufacturing cost, its various components are nontoxic composition, environmentally safe, can significantly improve the output of farm crop, the Sustainable Production of useful agricultural.
The present invention is based on Plant hormones regulators,gibberellins, and science other plant hormone of arranging in pairs or groups is made water dispersant, in the water dispersant, and dispersion agent, wetting agent, convenient agricultural is used.Functional additive trace element mixture, plant sterol mixture can promote the growth of plant, can reach the effect of killing pests and suppressing bacteria again.
The invention provides a kind of efficient, nontoxic, environment amenable new plant growth regulator, the growth that it not only can promote plant is more than 10%, and do not have any problem of environmental pollution, is a kind of very outstanding plant-growth regulator foliage fertilizer.
Following enforcement or experimental example are used to further specify, but are not limited to the present invention.
Experimental example 1 pharmacodynamic study data
By pot experiment, studied of the influence of northern agricultural No. 1 (embodiment 1) foliage fertilizer to spinach growth characteristic in seedling stage.4 processing are established in test, handle 1: contrast (clear water); Handle 2: 100 times of liquid of No. 1 nutritive medium dilution of north farming; Handle 3: 200 times of liquid of No. 1 nutritive medium dilution of north farming; Handle 4: 400 times of liquid of No. 1 nutritive medium dilution of north farming.Adopt pot experiment: the basin alms bowl is black plastic keg (internal diameter 10cm, high 10cm), and soil is to adorn basin behind flower nutrition soil and the sole of the foot stone 1:1 mixing, adds water, sowing, and every basin sowing 3-5 grain, the back thinning of emerging keeps 1 strain, and each handles the water and fertilizer management unanimity.The spring sowing rape was emerged on November 20th, 2009, and on January 20th, 2010 gathered.Foliage-spray 3 times, each 10 days at interval, the solution amount that each every basin sprays was 150mL, made the positive and negative blade face of plant moistening evenly.Spray the 1st time on December 20th, 2009 (rape 4 leaves 1 heart), spray respectively on December 30, January 10 the 2nd time, the 3rd time.During results, every basin plant is all gathered.
Gather behind the seedling, measure leaf area, gross weight, over-ground part weight, root weight respectively, relatively the clear water control group calculates the per-cent that each position of plant increases.Calculation formula is as follows:
Increase the observed value of percentage=(sample measurement value-control group observed value) * 100%/sample
Experimental result is as follows:
1. the leaf of spinach area:
North No. 1 100,200,400 times of diluents of farming have the effect that obvious promotion the leaf of spinach area increases, and reduce with concentration, and increasing amount also reduces.
2. spinach gross weight
North No. 1 100,200,400 times of diluents of farming have the effect that obvious promotion spinach gross weight increases, and reduce with concentration, and increasing amount also reduces.
3. spinach over-ground part
North No. 1 100,200,400 times of diluents of farming have the effect that obvious promotion spinach over-ground part weight increases, and reduce with concentration, and increasing amount also reduces.
4. Radix spinach is heavy
North No. 1 100,200,400 times of diluents of farming have the effect that obviously alleviates Radix spinach weight, and change in concentration is little to the reduction influence.
Experimental result shows, the leaf area of spinach, gross weight, over-ground part weight and clear water are relatively, increment all reaches more than 19%, the weight of root reduces more than 30% approximately, illustrate that the oriented over-ground part of nutritive substance shifts obviously on the root, for the greengrocery crop, demonstration is a kind of reasonable plant-growth regulator foliage fertilizer.
Embodiment
Embodiment 1: with CA3 (Gibberellins, Plant hormones regulators,gibberellins 3) 1200mg, IAA (Indole-3-acetic acid, indolylacetic acid) 5.6mg, BR (Bressinosteroids, brassinolide) 2.5mg, ABA (Abscisic acid, dormin), 1.2mg, JA (Jasmonic acid jasmonic acid) 1.2mg, Z (Zeatin, zeatin) 2.8mg, SA (Salicylic acid Whitfield's ointment) 1.2mg mixing, add dispersing agent C NF150mg, wetting agent sodium laurylsulfonate 80mg, be dissolved in 95% ethanol, grind, use disk granulation, promptly obtain the water dispersant of growth hormone mixture.Add 4g trace element mixture, 3.5g plant sterol mixture again, add weighting agent to 10g, mixing, vacuum packaging promptly obtains No. 1 foliage fertilizer of north farming.
Embodiment 2: with CA3 (Gibberellins, Plant hormones regulators,gibberellins 3) 1200mg, IAA (Indole-3-acetic acid, indolylacetic acid) 5.6mg, BR (Bressinosteroids, brassinolide) 2.5mg, ABA (Abscisic acid, dormin), 1.2mg, JA (Jasmonic acid jasmonic acid) 1.2mg, Z (Zeatin, zeatin) 2.8mg, SA (Salicylic acid Whitfield's ointment) 1.2mg mixing, add dispersing agent C NF180mg, wetting agent sodium laurylsulfonate 100mg, be dissolved in 70% ethanol spraying drying, 110 ℃ of control drying temperatures, make granularity at 0.1-0.5mm, promptly obtain the water dispersant of growth hormone mixture.Add 6g trace element mixture, 2g plant sterol mixture again, add weighting agent to 10g, mixing, vacuum packaging promptly obtains No. 1 foliage fertilizer of north farming.
Embodiment 3: with CA3 (Gibberellins; Plant hormones regulators,gibberellins 3) 1200mg; IAA (Indole-3-acetic acid; indolylacetic acid) 5.6mg; BR (Bressinosteroids; brassinolide) 2.5mg; ABA (Abscisic acid; dormin); 1.2mg; JA (Jasmonic acid jasmonic acid) 1.2mg; Z (Zeatin; zeatin) 2.8mg; SA (Salicylic acid Whitfield's ointment) 1.2mg mixing; add dispersing agent C NF180mg; wetting agent sodium laurylsulfonate 90mg; grind mixing; water spray is granulated in the rotation nodulizer, and drying promptly obtains the water dispersant of growth hormone mixture.Add 3g trace element mixture, 3g plant sterol mixture again, add weighting agent to 10g, mixing, vacuum packaging promptly obtains No. 1 foliage fertilizer of north farming.
Claims (7)
1. Pesticidal foliage fertilizer is characterized in that mainly being made by the raw material of following weight part:
Plant hormones regulators,gibberellins (3) 7-11 part
Indolylacetic acid 0.01-0.1 part
Brassinolide 0.01-0.1 part
Dormin 0.01-0.1 part
Jasmonic acid 0.01-0.1 part
Zeatin 0.01-0.1 part
Whitfield's ointment 0.02-0.1 part
1-amino-cyclopropane-1-carboxylic acid 0.01-0.1 part.
2. Pesticidal foliage fertilizer as claimed in claim 1 is characterized in that mainly being made by the raw material of following weight part:
Plant hormones regulators,gibberellins 38-9.9 part
Indolylacetic acid 0.01-0.05 part
Brassinolide 0.01-0.04 part
Dormin 0.01-0.03 part
Jasmonic acid 0.01-0.04 part
Zeatin 0.01-0.04 part
Whitfield's ointment 0.02-0.04 part
1-amino-cyclopropane-1-carboxylic acid 0.01-0.03 part.
3. Pesticidal foliage fertilizer as claimed in claim 1 is characterized in that mainly being made by the raw material of following weight part:
Plant hormones regulators,gibberellins 39.5-9.9 part
Indolylacetic acid 0.04-0.05 part
Brassinolide 0.02-0.03 part
Dormin 0.01-0.02 part
Jasmonic acid 0.01-0.02 part
Zeatin 0.01-0.02 part
Whitfield's ointment 0.02-0.03 part
1-amino-cyclopropane-1-carboxylic acid 0.01-0.02 part.
4. as the preparation method of any one Pesticidal foliage fertilizer water dispersant as described in the claim 1-3, it is characterized in that this preparation method is:
Plant hormones regulators,gibberellins 3, indolylacetic acid, brassinolide, dormin, jasmonic acid, zeatin, Whitfield's ointment,
It is even that 1-amino-cyclopropane-1-carboxylic acid is pressed the prescription ground and mixed, the growth hormone mixture; Mixture is prepared as water dispersant chooses one of following method:
A gets this growth hormone mixture 0.5-2.5 part, dispersion agent 0.1-0.2 part, wetting agent 0.05-0.1 part is filled to 10 parts; It is 1 that above each component is dissolved in volume ratio: ground and mixed is even in the organic solvent of 1-3,40-70 ℃ of oven dry, grind evenly, and drying, packing promptly obtains growth hormone mixture water dispersant;
B gets this growth hormone mixture 0.5-2.5 part, adds dispersion agent 0.1-0.2 part again, and wetting agent 0.05-0.1 part is filled to 10 parts; It is 1 that above each component is dissolved in volume ratio: ground and mixed is even in the organic solvent of 1-3,40-70 ℃ of oven dry, grind evenly, and drying, packing promptly obtains growth hormone mixture water dispersant; Described dispersion agent can be a kind of in the alkaline sodium lignosulfonate A of improvement, improvement alkaline sodium lignosulfonate B, desugar sodium lignosulfonate, desugar condensation sodium lignosulfonate, the methanonaphthalene sulfonic acid class dispersion agent;
Described wetting agent is how a kind of among sodium sulfonate, succsinic acid alkyl sodium sulfonate, Fatty Alcohol(C12-C14 and C12-C18) polyoxy ether alkene, permeate agent BA, penetrant m, the penetrant t H of dipropyl benzene sulfonic acid sodium salt, butyl; Filler is: a kind of in potter's clay, clay, kaolin, diatomite, talcum powder, pyrophyllite, the white carbon black, tamanori is: a kind of in vegetable and animals oils, starch paste, natural gum, bean powder, animal gelatine, carboxymethyl cellulose, polyvinyl alcohol, polyethylene butyl ether, the polyvinyl acetate, disintegrating agent is a kind of in starch, low-substituted hydroxypropyl cellulose, calcium carboxymethylcellulose, croscarmellose sodium, polyvinylpolypyrrolidone, sodium alginate, the Lalgine.
5. Pesticidal foliage fertilizer is characterized in that mainly being made by the raw material of following weight part:
Growth hormone mixture water dispersant 0.1-0.3 part
Nutritive element mixture 2-6 part
Plant sterol mixture 2-3.5 part
Weighting agent adds to 10 parts
Described growth hormone mixture water dispersant is Plant hormones regulators,gibberellins (3) 7-11 part, indolylacetic acid 0.01-0.1 part, brassinolide 0.01-0.1 part, dormin 0.01-0.1 part, jasmonic acid 0.01-0.1, zeatin 0.01-0.1, Whitfield's ointment 0.02-0.1 part, 1-amino-cyclopropane-1-carboxylic acid 0.01-0.1 part; Ground and mixed is even, gets the growth hormone mixture; Get this growth hormone mixture 0.5-2.5 part, dispersion agent 0.1-0.2 part, wetting agent 0.05-0.1 part is filled to 10 parts; It is 1 that above each component is dissolved in volume ratio: ground and mixed is even in the organic solvent of 1-3,40-70 ℃ of oven dry, grind evenly, and drying, packing promptly obtains growth hormone mixture water dispersant; Or get this growth hormone mixture 0.5-2.5 part, add dispersion agent 0.1-0.2 part again, wetting agent 0.05-0.1 part is filled to 10 parts; It is 1 that above each component is dissolved in volume ratio: ground and mixed is even in the organic solvent of 1-3,40-70 ℃ of oven dry, grind evenly, and drying, packing promptly obtains growth hormone mixture water dispersant; Described dispersion agent can be a kind of in the alkaline sodium lignosulfonate A of improvement, improvement alkaline sodium lignosulfonate B, desugar sodium lignosulfonate, desugar condensation sodium lignosulfonate, the methanonaphthalene sulfonic acid class dispersion agent; Described wetting agent is how a kind of among sodium sulfonate, succsinic acid alkyl sodium sulfonate, Fatty Alcohol(C12-C14 and C12-C18) polyoxy ether alkene, permeate agent BA, penetrant m, the penetrant t H of dipropyl benzene sulfonic acid sodium salt, butyl; Filler is: a kind of in potter's clay, clay, kaolin, diatomite, talcum powder, pyrophyllite, the white carbon black, tamanori is: a kind of in vegetable and animals oils, starch paste, natural gum, bean powder, animal gelatine, carboxymethyl cellulose, polyvinyl alcohol, polyethylene butyl ether, the polyvinyl acetate, and disintegrating agent is a kind of in starch, low-substituted hydroxypropyl cellulose, calcium carboxymethylcellulose, croscarmellose sodium, polyvinylpolypyrrolidone, sodium alginate, the Lalgine;
Described nutritive element mixture is by 5 parts in urea, 2 parts of potassium primary phosphates, 2 parts of boric acid; 1.8 parts of disodium ethylene diamine tetraacetate, 2 parts of Manganous chloride tetrahydrates, 1 part in calcium chloride, 2 parts in sal epsom, 2 parts in ferrous sulfate, 1 part in zinc sulfate, 0.2 part in copper sulfate are dissolved in an amount of water, and spraying drying gets final product;
Described plant sterol mixture comprises that β-Gu Zaichun, Stigmasterol, campesterol, brassicasterol, avenasterol, ergosterol, this sterol of standing grain, citrostadienol, Lip river fly enol, ring jackfruit alcohol, cycloartenol, 2, in the 4-methylene basic ring jackfruit alcohol.
6. Pesticidal foliage fertilizer as claimed in claim 5 is characterized in that mainly being made by the raw material of following weight part:
0.11 part of growth hormone mixture water dispersant
5 parts in nutritive element mixture
2.5 parts in plant sterol mixture
Weighting agent adds to 10 parts.
7. Pesticidal foliage fertilizer as claimed in claim 5 is characterized in that mainly being made by the raw material of following weight part:
0.12 part of growth hormone mixture water dispersant
4 parts in nutritive element mixture
3.5 parts in plant sterol mixture
Weighting agent adds to 10 parts.
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