CN101939286B - 己二胺的纯化方法 - Google Patents

己二胺的纯化方法 Download PDF

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Publication number
CN101939286B
CN101939286B CN200880110853.3A CN200880110853A CN101939286B CN 101939286 B CN101939286 B CN 101939286B CN 200880110853 A CN200880110853 A CN 200880110853A CN 101939286 B CN101939286 B CN 101939286B
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CN
China
Prior art keywords
hexamethylenediamine
distillation
column
tha
hmd
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN200880110853.3A
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English (en)
Chinese (zh)
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CN101939286A (zh
Inventor
M·I·布罗格里奥
D·阿莫罗
J·范尼尔
D·勒图尔纳
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Polyamide High Performance GmbH
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Rhodia Operations SAS
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/86—Separation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/84—Purification

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyamides (AREA)
CN200880110853.3A 2007-10-11 2008-10-03 己二胺的纯化方法 Active CN101939286B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR07/07134 2007-10-11
FR0707134A FR2922207B1 (fr) 2007-10-11 2007-10-11 Procede de purification d'hexamethylene diamine
PCT/EP2008/063288 WO2009047219A1 (fr) 2007-10-11 2008-10-03 Procede de purification d'hexamethylene diamine

Publications (2)

Publication Number Publication Date
CN101939286A CN101939286A (zh) 2011-01-05
CN101939286B true CN101939286B (zh) 2014-12-10

Family

ID=39345177

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200880110853.3A Active CN101939286B (zh) 2007-10-11 2008-10-03 己二胺的纯化方法

Country Status (12)

Country Link
US (1) US8436212B2 (enExample)
EP (1) EP2195283B1 (enExample)
JP (2) JP2011500526A (enExample)
KR (1) KR101196691B1 (enExample)
CN (1) CN101939286B (enExample)
AT (1) ATE524430T1 (enExample)
BR (1) BRPI0816604B1 (enExample)
FR (1) FR2922207B1 (enExample)
IN (1) IN2010CN01933A (enExample)
RU (1) RU2495021C2 (enExample)
TW (1) TWI346654B (enExample)
WO (1) WO2009047219A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101624567B1 (ko) * 2013-02-22 2016-05-26 주식회사 삼양사 박막증류에 이은 컬럼증류를 채택한 단일 증류단계를 포함하는 고순도 무수당 알코올의 제조방법
CN103936595B (zh) * 2014-04-30 2015-12-02 中国天辰工程有限公司 一种粗己二胺的精制方法

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1246843A (zh) * 1997-02-07 2000-03-08 Basf公司 从含有胺和亚胺的混合物中分离亚胺的方法
CN1306514A (zh) * 1998-03-20 2001-08-01 Basf公司 从含胺及吖庚因衍生物的混合物中脱除吖庚因衍生物
WO2001064624A1 (de) * 2000-02-29 2001-09-07 Basf Aktiengesellschaft Verfahren zur reduzierung des gehalts an einem ungesättigten imin in einer mischung enthaltend ein imin und ein amin
CN1416418A (zh) * 2000-03-08 2003-05-07 巴斯福股份公司 从含胺和吖庚因衍生物的混合物中除去吖庚因衍生物的方法
CN1829680A (zh) * 2003-06-27 2006-09-06 罗狄亚聚酰胺中间体公司 二胺的纯化方法
CN101018763A (zh) * 2004-09-10 2007-08-15 因维斯塔技术有限公司 从包含六亚甲基二胺、6－氨基己腈和四氢氮杂的混合物中分离6－氨基己腈和六亚甲基二胺
CN1758942B (zh) * 2003-03-07 2010-04-28 因维斯塔技术有限公司 从包含己二胺、6-氨基己腈和四氢氮杂的混合物中分离己二胺的蒸馏方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3017331A (en) * 1959-04-15 1962-01-16 Chemstrand Corp Method for the purification of hexamethylenediamine
US3121671A (en) * 1961-04-26 1964-02-18 Du Pont Production of highly refined hexamethylenediamine
US5192399A (en) * 1991-01-30 1993-03-09 E. I. Du Pont De Nemours And Company Purification of aminonitriles or diamines
DE19704612A1 (de) * 1997-02-07 1998-08-13 Basf Ag Verfahren zur Gewinnung von Hexamethylendiamin aus Hexamethylendiamin enthaltenden Mischungen
FR2777562B1 (fr) * 1998-04-16 2002-07-19 Rhone Poulenc Fibres Procede de purification d'aminonitriles aliphatiques
DE19830598A1 (de) * 1998-07-09 2000-01-13 Basf Ag Verfahren zur Reduzierung des Gehalts an einem ungesättigten cyclischen Imin in einer Mischung enthaltend Hexamethylendiamin und dieses Imin
US5961788A (en) * 1998-10-09 1999-10-05 E. I. Du Pont De Nemours And Company Sequential distillation process for removing tetrahydroazepine from aminocapronitrile and/or hexamethylenediamine
US7060819B2 (en) * 2003-09-15 2006-06-13 Invista North America S.A.R.L. Process for producing hexamethylenediamine and aminocapronitrile from adiponitrile, wherein the hexamethylenediamine contains less than 100 ppm tetrahydroazepine
FR2892118B1 (fr) * 2005-10-18 2010-12-10 Rhodia Recherches & Tech Procede de fabrication d'hexamethylene diamine et d'aminocapronitrile.

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1246843A (zh) * 1997-02-07 2000-03-08 Basf公司 从含有胺和亚胺的混合物中分离亚胺的方法
CN1306514A (zh) * 1998-03-20 2001-08-01 Basf公司 从含胺及吖庚因衍生物的混合物中脱除吖庚因衍生物
WO2001064624A1 (de) * 2000-02-29 2001-09-07 Basf Aktiengesellschaft Verfahren zur reduzierung des gehalts an einem ungesättigten imin in einer mischung enthaltend ein imin und ein amin
CN1416418A (zh) * 2000-03-08 2003-05-07 巴斯福股份公司 从含胺和吖庚因衍生物的混合物中除去吖庚因衍生物的方法
CN1758942B (zh) * 2003-03-07 2010-04-28 因维斯塔技术有限公司 从包含己二胺、6-氨基己腈和四氢氮杂的混合物中分离己二胺的蒸馏方法
CN1829680A (zh) * 2003-06-27 2006-09-06 罗狄亚聚酰胺中间体公司 二胺的纯化方法
CN101018763A (zh) * 2004-09-10 2007-08-15 因维斯塔技术有限公司 从包含六亚甲基二胺、6－氨基己腈和四氢氮杂的混合物中分离6－氨基己腈和六亚甲基二胺

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
己二胺生产工艺;姜海源 等;《化学工程师》;19971231(第6期);全文 *
己二胺装置精馏工序的模拟及扩产改造研究;李燕 等;《石油化工设计》;20061231;第23卷(第4期);全文 *

Also Published As

Publication number Publication date
IN2010CN01933A (enExample) 2010-09-10
JP2014132011A (ja) 2014-07-17
FR2922207B1 (fr) 2009-12-04
US20100292511A1 (en) 2010-11-18
JP2011500526A (ja) 2011-01-06
EP2195283A1 (fr) 2010-06-16
EP2195283B1 (fr) 2011-09-14
TWI346654B (en) 2011-08-11
BRPI0816604B1 (pt) 2017-11-21
WO2009047219A1 (fr) 2009-04-16
TW200936543A (en) 2009-09-01
FR2922207A1 (fr) 2009-04-17
BRPI0816604A2 (pt) 2015-03-03
JP5863847B2 (ja) 2016-02-17
ATE524430T1 (de) 2011-09-15
US8436212B2 (en) 2013-05-07
KR20100063115A (ko) 2010-06-10
RU2495021C2 (ru) 2013-10-10
RU2010118474A (ru) 2011-11-20
KR101196691B1 (ko) 2012-11-08
CN101939286A (zh) 2011-01-05

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C06 Publication
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SE01 Entry into force of request for substantive examination
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TR01 Transfer of patent right

Effective date of registration: 20200220

Address after: Fa Guobali

Patentee after: POLYAMIDE HIGH PERFORMANCE GmbH

Address before: Obervillier, France

Patentee before: RHODIA OPERATIONS