CN101810306A - Sugarless mensal sweetening material and production method thereof - Google Patents
Sugarless mensal sweetening material and production method thereof Download PDFInfo
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- CN101810306A CN101810306A CN200910250383A CN200910250383A CN101810306A CN 101810306 A CN101810306 A CN 101810306A CN 200910250383 A CN200910250383 A CN 200910250383A CN 200910250383 A CN200910250383 A CN 200910250383A CN 101810306 A CN101810306 A CN 101810306A
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Abstract
The invention relates to a sugarless mensal sweetening material and a production method thereof. The sugarless mensal sweetening material comprises the following ingredients: 11 to 20 percent of xylitol, 17 to 26 percent of phycite, 55 to 70 percent of oligoisomaltose and 0.07 to 0.16 percent of neotame. The process comprises the following steps: respectively adding 6 percent of oligoisomaltose and neotame into a heating container; respectively adding deionized water for mixing; raising the temperature for dissolution; respectively adding active carbon in the solution; carrying out filtration while the solution is hot; respectively merging the filter liquid into a storage tank; adding mixed materials of the pulverized xylitol, the pulverized phycite and the pulverized oligoisomaltose into a spraying fluidized bed by positive pressure; making the mixed materials flow in a accelerated mode from bottom to top; exerting negative pressure on the upper part of the spraying fluidized bed; carrying out vibration from top to bottom so that the materials boil up and down in the bed; continuously spraying and dispersing the refined neotame solution onto fine sugar alcohol bodies by a multi-point spraying gun at the side part of the fluidized bed; then, pumping the solution into the oligoisomaltose solution; carrying out continuous spraying drying; and obtaining the sugarless mensal sweetening material. The production flow process is simple and convenient, the operation is easy, and the product saccharinity is 5 to 10 times of that of ordinary cane sugar.
Description
Technical field
The present invention relates to a kind of edible dining table sweetener, relate in particular to a kind of Sugarless mensal sweetening material and production method thereof.
Background technology
Along with the increase of people because of too much bringing disease, people's demand safety, healthy Sugarless type dining table sweetener with sugar; In production procedure, reach from raw material and put into the vanguard technology that finished product one step finishes; It is learnt from other's strong points to offset one's weaknesses, has complementary advantages to make between the sugar alcohol sweet taste on the formula for a product, can play during product uses and cover the effect that promotes mouthfeel with synergy, people thirst under the prerequisite that satisfies sugariness height, empty calory, and occupation modeization, with cane-sugar taste safety and Health Sugarless type dining table sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of Sugarless mensal sweetening material and production method thereof are provided, adopt the scientific technology of easy operation control, the molten speed of product, mouthfeel, sugariness all are higher than the prior art optimum value.
Purpose of the present invention is achieved through the following technical solutions:
Sugarless mensal sweetening material, characteristics are to comprise following composition (percentage by weight): xylitol 11～20%, antierythrite 17～26%, oligoisomaltose 55～70%, knob sweet 0.07～0.16%.
Further, above-mentioned Sugarless mensal sweetening material, wherein, xylitol 15%, antierythrite 19.928%, oligoisomaltose 65%, knob sweet 0.072%.
The production method of Sugarless mensal sweetening material comprises following processing step:
1. with 6% sweet the joining respectively in the heating container of oligoisomaltose, knob, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing;
4. with xylitol, oligoisomaltose and antierythrite are put in the spray-fluidized bed apparatus after pulverizing, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the production method of above-mentioned Sugarless mensal sweetening material, the oligoisomaltose with 6%, knob is sweet joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Xylitol, oligoisomaltose and antierythrite reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
Again further, the production method of above-mentioned Sugarless mensal sweetening material, the bed temperature scope of described fluidized bed with spraying is 35～80 ℃, and wherein the bed temperature of the sweet spraying dispersion of phase I knob is 35～50 ℃, and the bed temperature of second stage oligoisomaltose mist projection granulating is 50～80 ℃.
Again further, the production method of above-mentioned Sugarless mensal sweetening material, in the phase I of described spraying mixed fluidized bed, the sweet spraying of knob is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In second stage, the oligoisomaltose spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical solution of the present invention is outstanding are mainly reflected in:
With xylitol, antierythrite, oligoisomaltose, knob is sweet is primary raw material, modifies uniformly and coats by preparation method to sugariness, makes product sweetness reach 5～10 times of common sucrose.The negative pressure fluid bed fluidization technique that adopts scientific formula, uses advanced is in conjunction with the multi-point atomizing method, and time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.Products obtained therefrom does not have smell, do not have color, and is soluble in water, and this fluffy granular composite sugar-free table sweetener is easy to use, and its production process science is simple and easy to operate, is fit to very much large-scale production.
Description of drawings
Below in conjunction with accompanying drawing technical solution of the present invention is described further:
Fig. 1: process chart of the present invention.
The specific embodiment
Sugarless mensal sweetening material, its composition is: xylitol 11～20%, antierythrite 17～26%, oligoisomaltose 55～70%, knob sweet 0.07～0.16%.Ideal formulations is: xylitol 15%, antierythrite 19.928%, oligoisomaltose 65%, knob sweet 0.072%.
As shown in Figure 1, the production technology of Sugarless mensal sweetening material: at first, the oligoisomaltose with 6%, knob is sweet joins respectively in the heating container, adds deionized water respectively and mixes; Be warming up to 52～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank of heat tracing; Then, with xylitol, put into after oligoisomaltose and antierythrite are pulverized in the spray-fluidized bed apparatus (heating temperature control and by the positive negative pressure boiling of equipment technology with the boiling that in fluid bed, circulates of sugar alcohol material, mix that fluidisation is anhydrated and fluffy processing, sugar alcohol mixtures material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom, be sprayed onto on the trickle solid material body of boiling), xylitol, the mixed material of oligoisomaltose and antierythrite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, the bed temperature that the sweet spraying of control knob disperses is 35～50 ℃, and the sweet even spraying of knob is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature, at mixing sugar alcohol after fluidisation loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines again, continuous spray drying granulation, the bed temperature of oligoisomaltose mist projection granulating controlled well is 50～80 ℃, and the oligoisomaltose spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain fluffy the shape product that even sugariness is modified.
Embodiment 1:
6 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, knob sweet 0.072 kilogram and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 15 kilograms of xylitols, 59 kilograms of oligoisomaltoses, 19.928 kilograms of antierythrites, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 2:
6 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, knob sweet 0.086 kilogram and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 19.914 kilograms of xylitols, 57 kilograms of oligoisomaltoses, 17 kilograms of antierythrites, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 3:
6 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, knob sweet 0.10 kilogram and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 15 kilograms of xylitols, 55 kilograms of oligoisomaltoses, 23.90 kilograms of antierythrites, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 4:
6 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, knob sweet 0.12 kilogram and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 17 kilograms of xylitols, 56 kilograms of oligoisomaltoses, 20.88 kilograms of antierythrites, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
Embodiment 5:
6 kilograms of oligoisomaltoses and deionized water are dissolved in a stainless steel heating reaction pot for 25 kilograms, knob sweet 0.15 kilogram and deionized water are also dissolved in another stainless steel heating reaction pot for 20 kilograms, material is heated to 62 ℃ by chuck in the pot, start stirring, add 1 kilogram of active carbon respectively, be incubated 30 minutes, filter while hot, filtrate collects in the storage tank of chuck insulation stand-by respectively; 13.85 kilograms of xylitols, 59 kilograms of oligoisomaltoses, 21 kilograms of antierythrites, pulverizing reaches 130 orders through pulverizer, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, control fluidized-bed layer temperature is 35～50 ℃, the multiple spot even spraying is disperseed, after operation is finished, improve bed temperature to 50～80 ℃ again, after the mixing of above-mentioned various sugar alcohol alcohol fluidisations loses surface crystallization water, pump into the above-mentioned oligoisomaltose solution that refines, continuously spray drying granulation, control air quantity and mist flow well, obtain the fluffy granular product that even sugariness is modified.
After testing, the fluffy granular composite low-sugar and low-calorie sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Particle size | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders | 30～60 orders |
| Sugariness (sucrose contrast) | 5 times | 6 times | 7 times | 8 times | 10 times |
| Outward appearance | White particle | White particle | White particle | White particle | White particle |
| Bulk density (g/mm 3) | ??0.60 | ??0.62 | ??0.63 | ??0.66 | ??0.66 |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the dining table sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and stability is very superior.
The sugariness degree of modification of fluffy granular composite sugar-free table sweetener of the present invention, will be according to the sweet adjustment in consumption of knob, usually select the common sucrose sugariness for use 5～10 times, relatively be fit to people's use needs, according to the prescription composition, under same sugariness situation, people are almost nil to the absorption of heat, and this dining table sweetener can not cause blood sugar to raise, not carious tooth, be fit to the diabetes patient, satisfy three high crowds, the healthy people's of pursuit needs.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, do not have color, and is soluble in water, and it is very convenient that this fluffy granule-shaped sugar-free dining table sweetener is used.Granularity, molten speed, mouthfeel, sugariness all are much better than the prior art value, and the technological process of production of science is simple and easy to do, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
Claims (4)
1. Sugarless mensal sweetening material is characterized in that comprising following composition (percentage by weight): xylitol 11～20%, antierythrite 17～26%, oligoisomaltose 55～70%, knob sweet 0.07～0.16%.
2. Sugarless mensal sweetening material according to claim 1 is characterized in that its component has following percentage by weight: xylitol 15%, antierythrite 19.928%, oligoisomaltose 65%, knob sweet 0.072%.
3. the production method of the described Sugarless mensal sweetening material of claim 1 is characterized in that: comprise following processing step---
1. with 6% sweet the joining respectively in the heating container of oligoisomaltose, knob, add deionized water respectively and mix;
2. be warming up to 52～80 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned oligoisomaltose solution and the sweet solution of knob, be incubated 25～30 minutes, filter while hot, filtrate is pooled in the storage tank of heat tracing stand-by respectively;
4. with xylitol, oligoisomaltose and antierythrite are put in the spray-fluidized bed apparatus after pulverizing, xylitol, the mixed material of oligoisomaltose and antierythrite enters the fluidized bed with spraying with malleation from the bottom of fluidized bed with spraying and quickens from bottom to top and flows, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, pump into the above-mentioned oligoisomaltose solution that refines again, spray-drying obtains fluffy granular composite sugar-free table sweetener continuously.
4. the production method of Sugarless mensal sweetening material according to claim 3 is characterized in that: the oligoisomaltose with 6%, knob is sweet joins respectively in the container, adds deionized water respectively and mixes; Be warming up to 60～80 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 30 minutes, filter while hot, filtrate is pooled to respectively in the storage tank that has heat tracing; Xylitol, oligoisomaltose and antierythrite reach 120～180 orders through pulverizing, be sent in the spray-fluidized bed apparatus, the mixed material of above-mentioned various sugar alcohols entered the fluidized bed with spraying and quicken from bottom to top from the bottom of fluidized bed with spraying with malleation flow, the top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling, control fluidized-bed layer temperature is at 35～80 ℃, the multiple spot spray gun of fluid bed sidepiece is sprayed the sweet solution of the above-mentioned knob that refines continuously earlier and is distributed on the fine sugar alcohol body, after the mixing of sugar alcohol fluidisation loses surperficial moisture content, pump into the above-mentioned oligoisomaltose solution that refines again, spray drying granulation obtains fluffy granular composite sugar-free table sweetener continuously.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102550707A (en) * | 2011-12-20 | 2012-07-11 | 苏州工业园区尚融科技有限公司 | Production method of sugarless fermented whey beverage |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1099846C (en) * | 1999-12-09 | 2003-01-29 | 北京恒毅利科贸有限责任公司 | Method for preparing granular flavouring enriched food and its product |
| US20080069938A1 (en) * | 2006-09-18 | 2008-03-20 | ISON Renny | Cohesive non-free flowing sweetener compositions including low-calorie ingredients |
| CN101253968B (en) * | 2008-04-15 | 2011-12-28 | 苏州苏克瑞甜品科技有限公司 | Granular sugar-free sweetening agent and method of preparing the same |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102550707A (en) * | 2011-12-20 | 2012-07-11 | 苏州工业园区尚融科技有限公司 | Production method of sugarless fermented whey beverage |
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