CN101768023A - Organosilicon fertilizer and preparation method thereof - Google Patents
Organosilicon fertilizer and preparation method thereof Download PDFInfo
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- CN101768023A CN101768023A CN200810187441A CN200810187441A CN101768023A CN 101768023 A CN101768023 A CN 101768023A CN 200810187441 A CN200810187441 A CN 200810187441A CN 200810187441 A CN200810187441 A CN 200810187441A CN 101768023 A CN101768023 A CN 101768023A
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Abstract
The invention discloses an organosilicon fertilizer; the prepared organic farming fertilizer is composed of the following ingredients by weight percentage: 60-70 percent of oil shale powder, 10-15 percent of calcium superphosphate, 10-15 percent of potassium sulfate and 5-10 percent of magnesium sulfate; the sum of the raw materials is 100 percent; by adopting the organosilicon fertilizer, the using amount of the pesticide is reduced, the agricultural output is improved, the agricultural product quality is improved, hardening and pollution of chemical fertilizer and pesticide to the soil are eliminated, the plant growth is beneficial to environment, soil fertility of the soil is improved and the agricultural high yield and high quality are realized.
Description
Technical field: the present invention relates to a kind of fertilizer and preparation thereof, specifically utilize natural oil shale to be basic raw material, adopt modern biotechnology technology and scientific formula to be refined into a kind of organosilicon fertilizer and preparation method thereof.
Background technology: in recent years along with the development of agriculture production, the peasant utilizes chemical fertilizer to obtain the grain high yield, and the harm that brings of the disease and pest that utilizes highly toxic pesticide control farm crop, but, above-mentioned chemical fertilizer and highly toxic pesticide have also brought potential hazard also for agricultural, the development that spreads along with this harm has directly endangered human beings'health.As the agricultural-food (grain, fruit, vegetables) that use highly toxic pesticide to produce all can inevitably carry the pesticide residue material; The life-time service chemical fertilizer can cause soil compaction in the arable soil of rural area; destroyed soil aggregate; influenced the soil microorganisms eubiosis; make soil fertility fall sharply; bring the hidden danger of the underproduction for later agriculture production, also can cause the agricultural product quality quality of production seriously to descend, the national Ministry of Agriculture had recognized this point in these several years; require soil to use organic fertilizer to improve this state, preserve the ecological environment and human body health.
At present existing many fertiliser production producer is at the fertilizer of development of new, domestic employing resinous shale is made fertilizer also seldom by biological degradation, even the commercial product of minority is arranged, its output is few, can not satisfy the demands far away, can't meet the quality requirement, and promote the use of very difficult.Therefore developing new nuisanceless fertilizer also is the focus that the insider pays close attention to.
Summary of the invention: at the defective or the deficiency of above-mentioned prior art existence, the objective of the invention is to, a kind of organosilicon fertilizer and preparation method thereof is provided, this organosilicon fertilizer is a raw material with natural oil shale, utilize microbial strains to decompose the resinous shale raw material, add nitrogen, phosphorus, potassium element then, be refined into high reactivity with modern vanguard technology, the green organic manure multi-functional, nontoxic, nuisanceless, easy to use, that fertilizer efficiency period is long.
Realize above-mentioned purpose, the technical scheme that the present invention takes is:
A kind of organosilicon fertilizer, the material composition and the weight percent thereof that it is characterized in that this organic agricultural fertilizer of making are: the resinous shale powder raw material: 60%～70%, and calcium superphosphate: 10%～15%, vitriolate of tartar: 10%～15%, sal epsom: 5%～10%, the summation of above-mentioned raw materials is 100%;
The composition of described resinous shale powder raw material and weight percent thereof are: resinous shale: 70%, and straw powder 14%, medical stone powder 10%, wheat bran: 5%, yeast: 0.6%, urea: 0.4%, the summation of raw material is 100%;
The preparation method of above-mentioned organosilicon fertilizer is characterized in that, comprises the following steps:
Step 1 at first prepares the resinous shale powder raw material:
It is oven dry 24 hours under 100 ℃～150 ℃ the condition that resinous shale is placed on temperature, is crushed to 100～200 orders then, sieves, and obtains the resinous shale powder;
In the back resinous shale powder that sieves, add enzymatic microorganism then by prescription, after evenly stirring, the straw powder, medical stone powder, wheat bran, the urea that add in the prescription mix, mixed composite powder carries out spontaneous fermentation between 50 ℃～70 ℃ degree of temperature, by after the fermentation in 7～8 days composite powder being placed the cylinder dryer, temperature remains between 70 ℃～100 ℃, promptly makes the resinous shale powder raw material after the oven dry.
Step 2, with vitriolate of tartar, calcium superphosphate in the resinous shale powder raw material made and the prescription, sal epsom fully mixes, and it is that the granulating disc of 16r/min～20r/min carries out granulation that the mixture that obtains is sent into rotating speed, promptly gets fertiliser granulates;
Step 3, the fertiliser granulates that causes type is inserted drying machine with conveying belt dry, the drying machine rotating speed is 5r/min～6r/min, and bake out temperature remains on 60 ℃～80 ℃, the fertiliser granulates that comes out from drying machine is by the separating screen sorting, packs, checks, seals and get product.
The present invention passes through high temperature detoxification ball milling powdering with resinous shale, contain organic matter behind the biological fermentation, effective silicon, add the required calcium of plant, phosphorus, magnesium, potassic fertilizer, by strict production technique program, make the organic matter of resinous shale and effectively silicon increase, strengthened the fertilizer product biological activity, can directly be absorbed by plant, the toxic chemical substance that can also decompose synthetic, the nutritions such as phosphorus potassium of having degraded and being cured in Chemical Composition such as fertilizer and pesticide and the dissolving soil, increase available nutrient of soil content, organic content improves the crumb structure and the microbial ecological balance of soil, strengthen permeability and protect fertile water retention capacity, impel plant-growth, decompose remains of pesticide, solved in the soil disease problem crop.
Adopt organosilicon fertilizer of the present invention can reduce the usage quantity of agricultural chemicals, improved agricultural output, improved quality of agricultural product, eliminated fertilizer and pesticide and soil is formed harden and pollute, cause plant-growth enabling environment finally to reach the culture fertility of improving the soil, realize the agricultural year high-quality.
Embodiment: the present invention is described in further detail for embodiment that provides below in conjunction with the contriver and laboratory report thereof.
Embodiment 1:
Resinous shale is a kind of high crude substance that contains organic humic acids, and utilizing it to make the green fertilizer product is best basic material, and the resinous shale powder raw material is pressed following formulation:
Resinous shale (100-200 order) 700kg
Straw powder 140kg
Medical stone powder 100kg
Yeast 6kg
Wheat bran 50kg
Urea 4kg
The present invention is at first with the condition detoxification of resinous shale at 100 ℃～150 ℃, add yeast, after evenly stirring, the straw powder, medical stone powder, wheat bran, the urea that add in the prescription mix, mixed composite powder carries out spontaneous fermentation between 50 ℃～70 ℃ degree of temperature, by after the fermentation in 7～8 days composite powder being placed the cylinder dryer, temperature remains between 70 ℃～100 ℃, promptly makes the resinous shale powder raw material after the oven dry.
Prepare organosilicon fertilizer with the resinous shale powder raw material then, its prescription is as follows:
Resinous shale powder raw material 60%
Calcium superphosphate 15%
Sal epsom 10%
Vitriolate of tartar 15%
Its preparation method is:
With vitriolate of tartar, calcium superphosphate in the resinous shale powder raw material made and the prescription, sal epsom fully mixes, and it is that the granulating disc of 16r/min～20r/min carries out granulation that the mixture that obtains is sent into rotating speed, promptly gets fertiliser granulates;
The fertiliser granulates that causes type is inserted drying machine with conveying belt dries, the drying machine rotating speed is 5r/min～6r/min, bake out temperature remains on 60 ℃～80 ℃, and the fertiliser granulates that comes out from drying machine is by the separating screen sorting, packs, checks, seals and get product.
The fertilizer product that present embodiment obtains, wherein organic content is being about 20%, available silicon content is 30%, effectively potassium is between 10%, and contains calcium, magnesium and other nutritive element, through the field systematic testing, the fertilizer function is complete, nutrient is concentrated, and fertilizer efficiency period is long, can make wheat increase yield 15%, corn yield increasing 25%, gourd, fruit and vegetable volume increase 35%, volume increase such as apple mandarin orange straw 25%, cotton increasing production of rice about 20%.
Embodiment 2:
Different is for present embodiment and embodiment 1, and the prescription for preparing organosilicon fertilizer with the resinous shale powder raw material is adjusted to some extent, can reach the purpose of embodiment 1 equally, and its prescription is:
Resinous shale powder raw material 70%
Calcium superphosphate 10%
Sal epsom 5%
Vitriolate of tartar 15%
Its preparation method is with embodiment 1.
Embodiment 3:
Different is for present embodiment and embodiment 1, and the prescription for preparing organosilicon fertilizer with the resinous shale powder raw material is adjusted to some extent, can reach the purpose of embodiment 1 equally, and its prescription is:
Resinous shale powder raw material 65%
Calcium superphosphate 10%
Sal epsom 10%
Vitriolate of tartar 15%
Its preparation method is with embodiment 1.
Embodiment 4:
Different is for present embodiment and embodiment 1, and the prescription for preparing organosilicon fertilizer with the resinous shale powder raw material is adjusted to some extent, can reach the purpose of embodiment 1 equally, and its prescription is:
Resinous shale powder raw material 70%
Calcium superphosphate 13%
Sal epsom 7%
Vitriolate of tartar 10%
Its preparation method is with embodiment 1.
Embodiment 5:
Different is for present embodiment and embodiment 2, substitutes vitriolate of tartar with Repone K, and its preparation method can reach the purpose of embodiment 2 equally with embodiment 1.
Need to prove that the foregoing description is the preferable example of the present invention, the invention is not restricted to the foregoing description.
Below be organosilicon fertilizer the field test report on apple of contriver according to the foregoing description preparation:
The present invention prepares the key technical indexes of organosilicon fertilizer: organic 〉=20%, effective silicon 〉=30%, effective magnesium 〉=5%, potassium oxide 〉=8%, according to economizing the experimental technique rules that the clay fertilizer station requires, carried out field test in 2007 on apple, test-results is reported as follows:
1, test objective
The organosilicon fertilizer that checking the present invention produces compares with effect and effect of increasing production that local fertilizer of the same type commonly used is grown apple development, for the large scale application of Baishui County apple orchard provides scientific basis in Shaanxi Province.
2, test period and place
Test and be arranged in Hou Wa village, Baishui County wine town, Shaanxi Province 4～October in 2007 and implement.
3, overview experimental field
Test orchard height above sea level 858m, physical features is smooth, and soil type is a loessal soil, quality: loam class, 2 grades of soil fertility grades.8 mu of areas, kind: the Fuji apple, the age of tree 15 years, fruit tree is neat, and level of management are higher.Gather the 0-40cm soil sample before test is handled, it is as follows that chemical examination records the basic nutrient situation of soil:
For the basic nutrient situation of examination orchard soil
| Project | Organic (%) | Alkali-hydrolyzable nitrogen (ppm) | Rapid available phosphorus (ppm) | Available potassium (ppm) | PH value |
| Content | ??1.6 | ??75.6 | ??20.5 | ??146.4 | ??7.3 |
4, test design and processing
4.1 test design:
Three processing are established in test, adopt random alignment, three repetitions, and each handles 5 trees.
4.2 test is handled:
1. use 100 kilograms/mu of organosilicon fertilizers (being the present invention);
2. use 100 kilograms/mu in fertilizer of the same type;
3. (CK) do not apply fertilizer;
5, test is implemented and field management
5.1 test is implemented:
The test organosilicon fertilizer, the ring-type trench digging once applies before March in this year fruit tree bud.
5.2 field management:
Test is sprayed the medicine prevention and elimination of disease and pests 6 times in orchard 4-8 month, intertill and clean tillage 4 times, and pour water 2 early stage.
6, the current year, climatic characteristic and apple development were grown
6.1 precipitation: 2007 at apple development phase co-falling water 562.8mm, the many 193.2mm of 369.6mm of the same period over the years, January～June rainfall amount few, precipitation was on the high side in 7,8,9 three months.
6.2 illumination: in April, 2007～October, lighting delay number was 1138 hours, than 1270.3 hours of the same period over the years reducing 132 hours.In a word, this year, apple rainfall amount breeding time was on the high side, and temperature is moderate, and illumination is suitable, and weather helps growing of apple and tests the performance of effect of fertilizer.
7, test result analysis
7.1 influence to output
From table 1: the contrast per mu yield is 2415.3 kilograms, and using organosilicon fertilizer per mu yield of the present invention is 2855.0 kilograms, and the contrast volume increase 18.2%; Using fertilizer per mu yield of the same type is 2626.6 kilograms, and the contrast volume increase 8.7%.From variance analysis, different treatment all has effect of increasing production, especially with organosilicon fertilizer effect of increasing production the best.
7.2 influence to the fruit quality
From table 5,6: after apple was used organosilicon fertilizer, single fruit weight contrast increased by 40.7 grams, and degree of staining contrast improves 21.8%, and sugar degree contrast increases by 1.6%.
7.3 influence to the fruit tree biology proterties
From table 7: after apple was used organosilicon fertilizer, blinds fresh weight contrast increased by 13.5 grams, and the leaf area ratio contrast increases 4.39cm
2, bud forms number and contrasts 14 of increases.
8, conclusions and recommendations
8.1 conclusion: after apple is used organosilicon fertilizer, the tree vigo(u)r robust growth, blade is dark green, and early defoliation disease does not take place in drought resisting, strong stress resistance, and physiology nutritional deficiency disease is not taken place, and the fruit face is bright and clean, painted good, and sugar degree improves.Can improve the visual appearance and the interior quality of apple, obvious effect of increasing production.
8.2 suggestion: this product test effect on apple proves, obvious effect of increasing production, and can enlarge demonstration and large scale application next year in the apple orchard in county.
Table 1: each handles the yield result table
Table 2: analysis of variance table
| Source of variation | Sum of squares | Degree of freedom | Square root of the variance | ??F | ??5％ | ??1％ |
| Between processing | ??290104.66 | ??2 | ??145052.33 | ??338.38 ** | ??6.94 | ??18.00 |
| Between repetition | ??3960.66 | ??2 | ??1980.33 | ??4.62 | ||
| Error | ??1714.66 | ??4 | ??428.66 | |||
| Total variation | ??295780.00 | ??8 |
Table 3: the minimum significantly extreme difference table of multiple range test
| ??P | ??2 | ??3 |
| ??SSR0.05 | ??3.93 | ??4.01 |
| ??LSR0.05 | ??46.96 | ??47.91 |
| ??SSR0.01 | ??6.51 | ??6.80 |
| ??LSR0.01 | ??77.79 | ??81.26 |
Table 4: volume variance table
Table 5: apple quality questionnaire
Table 6: apple single fruit weight questionnaire
Table 7: fruit tree growth changes questionnaire
The organosilicon fertilizer of the present invention's preparation, its prescription can also be made corresponding adjustment, all available useful effect according to the demand of place soil regime and crop classification.
Claims (4)
1. organosilicon fertilizer, the material composition and the weight percent thereof that it is characterized in that this organic fertilizer of making are: the resinous shale powder raw material: 60%～70%, and calcium superphosphate: 10%～15%, vitriolate of tartar: 10%～15%, sal epsom: 5%～10%, the summation of above-mentioned raw materials is 100%;
The composition of described resinous shale powder raw material and weight percent thereof are: resinous shale: 70%, and straw powder 14%, medical stone powder 10%, wheat bran: 5%, yeast: 0.6%, urea: 0.4%, the summation of raw material is 100%.
2. the described organosilicon fertilizer of claim 1 is characterized in that, described vitriolate of tartar is substituted by Repone K.
3. the preparation method of the described organosilicon fertilizer of claim 1 is characterized in that, comprises the following steps:
Step 1 at first prepares the resinous shale powder raw material:
It is oven dry 24 hours under 100 ℃～150 ℃ the condition that resinous shale is placed on temperature, is crushed to 100～200 orders then, sieves, and obtains the resinous shale powder;
In the back resinous shale powder that sieves, add yeast then by prescription, after evenly stirring, the straw powder, medical stone powder, wheat bran, the urea that add in the prescription mix, mixed composite powder carries out spontaneous fermentation between 50 ℃～70 ℃ degree of temperature, by after the fermentation in 7～8 days composite powder being placed the cylinder dryer, temperature remains between 70 ℃～100 ℃, promptly makes the resinous shale powder raw material after the oven dry.
Step 2, with vitriolate of tartar, calcium superphosphate in the resinous shale powder raw material made and the prescription, sal epsom fully mixes, and it is that the granulating disc of 16r/min～20r/min carries out granulation that the mixture that obtains is sent into rotating speed, promptly gets fertiliser granulates;
Step 3, the fertiliser granulates that causes type is inserted drying machine with conveying belt dry, the drying machine rotating speed is 5r/min～6r/min, and bake out temperature remains on 60 ℃～80 ℃, the fertiliser granulates that comes out from drying machine is by the separating screen sorting, packs, checks, seals and get product.
4. the preparation method of the described organosilicon fertilizer of claim 3 is characterized in that, described vitriolate of tartar is substituted by Repone K.
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| CN200810187441A CN101768023A (en) | 2008-12-29 | 2008-12-29 | Organosilicon fertilizer and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102153385A (en) * | 2010-12-20 | 2011-08-17 | 陕西省土肥新技术研究开发有限公司 | Method for producing biological organic fertilizer by using oil shale as raw material |
| CN104261948A (en) * | 2014-10-11 | 2015-01-07 | 延边遵杰资源开发利用有限公司 | Organic and inorganic compound fertilizer prepared from oil-shale waste residues and preparation method thereof |
| CN104355813A (en) * | 2014-10-29 | 2015-02-18 | 贵州省化工研究院 | Method for producing organic-inorganic compound fertilizer through potassium-bearing shale |
| CN108440109A (en) * | 2018-04-16 | 2018-08-24 | 隋皓为 | A kind of production bio-bacterial manure of oil shale and do bio-bacterial manure additive |
| CN108794254A (en) * | 2018-06-13 | 2018-11-13 | 隋皓为 | A kind of oil shale production composite fertilizer and do additive for compound fertilizer |
| CN108794255A (en) * | 2018-06-13 | 2018-11-13 | 隋皓为 | A kind of oil shale makes compound organic and inorganic fertilizer and does compound organic and inorganic fertilizer additive |
| CN108794156A (en) * | 2018-06-13 | 2018-11-13 | 隋皓为 | A kind of oil shale production Blending Fertilizer and do blending fertilizer additive |
| CN110881295A (en) * | 2019-12-02 | 2020-03-17 | 澄城硅绿农业科技服务有限公司 | Apple tree fertilizing method |
-
2008
- 2008-12-29 CN CN200810187441A patent/CN101768023A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102153385A (en) * | 2010-12-20 | 2011-08-17 | 陕西省土肥新技术研究开发有限公司 | Method for producing biological organic fertilizer by using oil shale as raw material |
| CN104261948A (en) * | 2014-10-11 | 2015-01-07 | 延边遵杰资源开发利用有限公司 | Organic and inorganic compound fertilizer prepared from oil-shale waste residues and preparation method thereof |
| CN104355813A (en) * | 2014-10-29 | 2015-02-18 | 贵州省化工研究院 | Method for producing organic-inorganic compound fertilizer through potassium-bearing shale |
| CN108440109A (en) * | 2018-04-16 | 2018-08-24 | 隋皓为 | A kind of production bio-bacterial manure of oil shale and do bio-bacterial manure additive |
| CN108794254A (en) * | 2018-06-13 | 2018-11-13 | 隋皓为 | A kind of oil shale production composite fertilizer and do additive for compound fertilizer |
| CN108794255A (en) * | 2018-06-13 | 2018-11-13 | 隋皓为 | A kind of oil shale makes compound organic and inorganic fertilizer and does compound organic and inorganic fertilizer additive |
| CN108794156A (en) * | 2018-06-13 | 2018-11-13 | 隋皓为 | A kind of oil shale production Blending Fertilizer and do blending fertilizer additive |
| CN110881295A (en) * | 2019-12-02 | 2020-03-17 | 澄城硅绿农业科技服务有限公司 | Apple tree fertilizing method |
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Open date: 20100707 |