CN101759161B - 一种高光学质量硒化锌的制备方法 - Google Patents
一种高光学质量硒化锌的制备方法 Download PDFInfo
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- CN101759161B CN101759161B CN2008102465436A CN200810246543A CN101759161B CN 101759161 B CN101759161 B CN 101759161B CN 2008102465436 A CN2008102465436 A CN 2008102465436A CN 200810246543 A CN200810246543 A CN 200810246543A CN 101759161 B CN101759161 B CN 101759161B
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- zinc
- gas
- zinc selenide
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- PFNQVRZLDWYSCW-UHFFFAOYSA-N (fluoren-9-ylideneamino) n-naphthalen-1-ylcarbamate Chemical compound C12=CC=CC=C2C2=CC=CC=C2C1=NOC(=O)NC1=CC=CC2=CC=CC=C12 PFNQVRZLDWYSCW-UHFFFAOYSA-N 0.000 title claims abstract description 24
- 230000003287 optical effect Effects 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000007789 gas Substances 0.000 claims abstract description 38
- 239000011701 zinc Substances 0.000 claims abstract description 30
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract description 24
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 22
- 238000000151 deposition Methods 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 17
- 238000006243 chemical reaction Methods 0.000 claims abstract description 16
- 230000008021 deposition Effects 0.000 claims abstract description 15
- 229910052786 argon Inorganic materials 0.000 claims abstract description 12
- 238000005229 chemical vapour deposition Methods 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000013049 sediment Substances 0.000 claims description 21
- 238000010792 warming Methods 0.000 claims description 8
- 238000001514 detection method Methods 0.000 claims description 4
- 230000008020 evaporation Effects 0.000 claims description 4
- 238000001704 evaporation Methods 0.000 claims description 4
- 238000009413 insulation Methods 0.000 claims description 4
- 238000005086 pumping Methods 0.000 claims description 4
- 238000010257 thawing Methods 0.000 claims description 4
- 239000000463 material Substances 0.000 abstract description 10
- 239000000843 powder Substances 0.000 abstract description 5
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 238000002834 transmittance Methods 0.000 abstract 1
- SBIBMFFZSBJNJF-UHFFFAOYSA-N selenium;zinc Chemical compound [Se]=[Zn] SBIBMFFZSBJNJF-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 238000012544 monitoring process Methods 0.000 description 3
- 239000000376 reactant Substances 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005137 deposition process Methods 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- SPVXKVOXSXTJOY-UHFFFAOYSA-N selane Chemical compound [SeH2] SPVXKVOXSXTJOY-UHFFFAOYSA-N 0.000 description 1
- 229910000058 selane Inorganic materials 0.000 description 1
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- Chemical Vapour Deposition (AREA)
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CN2008102465436A CN101759161B (zh) | 2008-12-25 | 2008-12-25 | 一种高光学质量硒化锌的制备方法 |
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CN2008102465436A CN101759161B (zh) | 2008-12-25 | 2008-12-25 | 一种高光学质量硒化锌的制备方法 |
Publications (2)
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CN101759161A CN101759161A (zh) | 2010-06-30 |
CN101759161B true CN101759161B (zh) | 2012-06-20 |
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CN2008102465436A Active CN101759161B (zh) | 2008-12-25 | 2008-12-25 | 一种高光学质量硒化锌的制备方法 |
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Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104477859B (zh) * | 2014-12-26 | 2016-09-14 | 浙江理工大学 | 一种纳米结构鱼刺状硒化锌及其制备方法和装置 |
CN109250749A (zh) * | 2017-07-14 | 2019-01-22 | 清远先导材料有限公司 | 硫化锌的生产方法 |
CN109943884A (zh) * | 2019-03-28 | 2019-06-28 | 北京中材人工晶体研究院有限公司 | 一种硒化锌原料高温提纯方法 |
KR102239584B1 (ko) * | 2019-11-18 | 2021-04-13 | 송병호 | 셀렌화아연의 재생방법 |
CN112095150B (zh) * | 2020-09-28 | 2022-02-22 | 安徽中飞科技有限公司 | 硒化锌的生长方法 |
CN113416074A (zh) * | 2021-08-10 | 2021-09-21 | 广东先导稀材股份有限公司 | 一种碲化锌粉末及其靶材的制备方法 |
CN115961350A (zh) * | 2022-12-29 | 2023-04-14 | 安徽光智科技有限公司 | 一种高均匀性多晶硒化锌红外材料的生长方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1796286A (zh) * | 2004-12-24 | 2006-07-05 | 北京有色金属研究总院 | 制备大尺寸高均匀CVD ZnS材料的设备及其工艺 |
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2008
- 2008-12-25 CN CN2008102465436A patent/CN101759161B/zh active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1796286A (zh) * | 2004-12-24 | 2006-07-05 | 北京有色金属研究总院 | 制备大尺寸高均匀CVD ZnS材料的设备及其工艺 |
Non-Patent Citations (3)
Title |
---|
杨海等.红外用CVD ZnS多晶材料的研制.《应用光学》.2008,第29卷(第1期),57-61. * |
魏乃光等.化学气相沉积ZnSe生长过程中粉末的控制.《中国有色金属学报》.2005,第15卷264-267. * |
鲁泥藕等.大功率激光窗口ZnSe的制备原理及方法.《功能材料》.2004,第35卷246-248. * |
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CN101759161A (zh) | 2010-06-30 |
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Address after: 065201 Langfang city of Hebei province Sanhe Yanjiao Hing Village South Patentee after: GRINM GUOJING ADVANCED MATERIALS CO., LTD. Address before: Langfang City, Hebei Province, Sanhe Yanjiao 065201 Star Village South Patentee before: GRINM GUOJING ADVANCED MATERIALS CO., LTD. |
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Effective date of registration: 20220506 Address after: 065001 No. 4, Baihe Road, economic and Technological Development Zone, Langfang City, Hebei Province Patentee after: GRINM GUOJING ADVANCED MATERIALS Co.,Ltd. Patentee after: Shandong Youyan guojinghui New Material Co., Ltd Address before: 065201 south of Xingdu village, Yanjiao, Sanhe City, Langfang City, Hebei Province Patentee before: GRINM GUOJING ADVANCED MATERIALS Co.,Ltd. |