CN101215790A - Dyeing and finishing method for cotton/milk protein blended spinning Raschel fabric - Google Patents
Dyeing and finishing method for cotton/milk protein blended spinning Raschel fabric Download PDFInfo
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- CN101215790A CN101215790A CNA2008100590944A CN200810059094A CN101215790A CN 101215790 A CN101215790 A CN 101215790A CN A2008100590944 A CNA2008100590944 A CN A2008100590944A CN 200810059094 A CN200810059094 A CN 200810059094A CN 101215790 A CN101215790 A CN 101215790A
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Abstract
The invention relates to a dyeing and finishing method of cotton/milk egg albumen blending raschel fabric, and the method comprises first, processing fabric before dyeing, second, drying, steaming, washing and drying keffekilite, third, dyeing and printing the fabric, fourth, dyeing or steaming, washing, flexibly handing, stentering or drying print cloth. The invention chooses CN-type reactive dyes and micro-molecular high-performance scouring assistants, and a set of new technological method. The invention solves technical incompatibility of two fibers which are cotton and bovine albumin. The invention has the advantages of low production cost, little pollution, bright color and even dyeing, and excellent performance of bovine albumin fiber can keep invariant.
Description
Technical field
What the present invention relates to is a kind of method of fabrics printing and dyeing technical field, specifically, is a kind of dyeing and finishing method of cotton/milk protein blended spinning Raschel fabric.
Background technology
At present, domestic bed necessaries lining accounts for absolute main flow with 100% cotton, and cotton and goods thereof are good with sucting wet air permeability, being difficult for damaging by worms becomes the first-selected product of people's clothing over the past thousands of years, and its disadvantage is wrinkling easily, and repeatedly the influence of washing back is attractive in appearance.Wool and fleece fabrics are soft, warmth retention property good, but easily damage by worms, and price is higher.
Milk protein fiber (Milk Casein Fiber) is the big molecule graft copolymerization of milk protein and acrylonitrile, form in the structure and contain the macromolecular linear macromolecule of milk protein amino acid, make the albumen spinning solution that is fit to wet spinning technology, after operations such as spinning, drawing-off, oven dry are made novel milk protein fiber.Milk protein fiber has many good characteristics; Milk protein fiber does not use formaldehyde azo analog assistant or raw material, and the fiber content of formaldehyde is zero; Milk fibre has characteristics such as feel is satiny, soft, skin-friendly is good, ventilative, good hygroscopicity, has a general gloss, the texture of goat cashmere sample, high-strength, wear-resisting, corrosion resistant, drapability are good, be rich in 18 seed amino acids to the human body beneficial, human body skin there are special maintenance action and good skin-friendly, simultaneously the milk protein fiber goods have the natural bacteriostatic function, to the broad-spectrum antibacterial rates of staphylococcus aureus, Candida albicans, fungi, mould etc. reach more than 80%, antibiotic rate reaches more than 99%.But because the cohesive force of plain chocolate fiber is relatively poor, cost is higher, so milk protein fiber and other fiber blend are the trend that develops at present.
Milk fibre and cotton fiber blended spinning Raschel fabric have the fiber fluffy jewelry, expensive clothing and other valuables, outward appearance gracefulness, soft-touch, comfortable; The microcellular structure of its three-dimensional multigap and vertically surperficial groove structure have determined its distinctive characteristic cool in summer and warm in winter, particularly the fabric after the blending carries out the bed necessaries that the napping processing is made, has the feel as the cashmere, natural gloss as the real silk and very good flexibility, skin-friendly.But because the not anti-highly basic of milk protein fiber, meet the alkali mutability and make milk protein fiber lose its premium properties, color and luster becomes to wither and tarnishes simultaneously.And need to remove contained pectin, cured matter and the expansion cotton seed hulls of cotton fiber dye-uptake and color and luster uniformity when improving follow-up dyeing in the general COTTON FABRIC dyeing and finishing technology with alkaline solution; Simultaneously also may use the alkaline agent fixation when fixation, therefore dyeing after cotton and the milk protein fiber blending or stamp are owing to the incompatibility of technology becomes very difficult.Application number is that 20061002680.3 Chinese patent discloses a kind of milk protein fiber blended color spinning yarn and production method thereof, this method be earlier with milk protein fiber and other fiber by the processing of dyeing separately of characteristics separately, color ratio is on demand mixed then, the processing method of spinning production by look is produced blended color spinning yarn again, and at the semi-finished product strip complementary color of mixing colours again.This method be owing to need carry out 2-3 time dyeing processing, prolongs technological process, increases production cost, increases the weight of the pressure of sewage disposal, has the homochromatism problem of two kinds of fibers simultaneously and can't carry out the defective that stamp is processed.
Summary of the invention
Technical problem to be solved by this invention provides a kind of dyeing and finishing method of cotton/milk protein blended spinning Raschel fabric, this dyeing and finishing method has been selected hydrogen peroxide bleaching process at high proportion in pre-treatment process, and add the influence that a kind of scintilla high-efficiency refining agent is eliminated the yellow juice that produces when the pectin in the cotton fiber, cured matter and cotton commensal cotton seed hulls expand, omit the white silk that needs highly basic, boiled technology and color fixing process; Select the neutral REACTIVE DYES of CN type in the dyeing, solve that milk protein fiber is met the alkali mutability and the key issue that loses its premium properties; The long ring of suspension type decatize technology can prevent because the contact between the cloth cover causes staining of the expanded yellow juice of cotton seed hulls simultaneously.
The present invention realizes that the technical scheme of above-mentioned purpose is: a kind of dyeing and finishing method of cotton/milk protein blended spinning Raschel fabric may further comprise the steps;
1. textile dyeing pre-treatment; Bleach with hydrogen peroxide bleaching agent before dyeing, the pH value of bleaching liquid is 9.5-10.5, the bleaching liquid prescription; 100%H
2O
2The 10-20 grams per liter, hydrogen peroxide stabilizer 3-7 grams per liter, scintilla high-efficiency refining agent 6-12 grams per liter, concise brightening agent 2-4 grams per liter; With every premium on currency is benchmark, adds described bleaching agent of prescription and bleaching assistant composition bleaching liquid in 60-70 ℃ of water.
2. oven dry, decatize, washing, oven dry bleach cloth; Described decatize is the long ring of a suspension type decatize technology.
3. textile dyeing or stamp; Neutral REACTIVE DYES dyes, and the pH value of dye liquor is 7-7.5, the dye liquor prescription; CN type REACTIVE DYES 0.1-50 grams per liter, Buffer Ac 0.5-2 grams per liter, calgon 1-1.5 grams per liter, reservehao S 5-15 grams per liter, levelling agent 0.1-0.5 grams per liter is a benchmark with every premium on currency, adds described stain of prescription and dyeing assistant composition dye liquor in 60-70 ℃ of water.
4. dyeing or calico decatize, washing, soft treatment, tentering oven dry; Described decatize is the long ring of a suspension type decatize technology, and described soft treatment is to add hydrophilic softener.
Step 1. textile dyeing pre-treatment process is; Two soak one rolls, and pads bleaching liquid, padding machine pressure 0.1Mpa, pick-up 85%, speed of a motor vehicle 10m/min, 100 ℃ of temperature, time 25min.
Step is textile dyeing 3.; Dyeing technique is on the REACTIVE DYES; Two soak one rolls, padding machine pressure 0.5Mpa, pick-up 100%, 100 ℃ of steam temperatures, steaming time 20min, speed of a motor vehicle 15m/min.
Step is textile printing 3., the stamp prescription; CN type REACTIVE DYES 0.1-50 grams per liter, Buffer Ac0.5-2 grams per liter, calgon, 1-1.5 grams per liter, reservehao S 5-15 grams per liter, the former paste of sodium alginate 300-500 grams per liter.Add described dyestuff of prescription and dyeing assistant composition printing paste in 60-70 ℃ of water, printing technology is the flat screen printing machine stamp.
The dyeing or the step of stamp 3. in added CN type REACTIVE DYES be a kind of triazine type REACTIVE DYES with quaternary amine type pyridine carboxylic acid radical reaction base.
The dyeing or the step of stamp 3. in added CN type REACTIVE DYES be reactive red, reactive yellow, reactive blue.
Compared with prior art, the invention has the advantages that: behind the cotton/milk protein fiber weaving, adopt single bath process dyeing and finishing technology to dye or stamp, nothing is boiled, practices technology, do not have color fixing process after dyeing in pre-treatment, shortened technological process, production cost is low, pollute fewly, have lovely luster, even dyeing, and characteristics that the premium properties of milk protein fiber is remained unchanged simultaneously.
Specific embodiments
Below in conjunction with embodiment the present invention is described in further detail.
Embodiment 1:
Coloration of textile materials
1. textile dyeing pre-treatment; Grey cloth is bleached with hydrogen peroxide bleaching agent before dyeing, and it is 10 that bleaching liquid is regulated the pH value with NaOH, the bleaching liquid prescription; 100%H
2O
210 grams per liters, hydrogen peroxide stabilizer 3 grams per liters, scintilla high-efficiency refining agent 12 grams per liters, concise brightening agent 2 grams per liters; Above-mentioned weight is to be benchmark with every premium on currency.Process conditions are two to soak one and roll, and pad bleaching liquid, padding machine pressure 0.1Mpa, and pick-up 85%, technological parameter are speed of a motor vehicle 10m/min, 100 ℃ of steam temperatures, steaming time 25min.The pH value of bleaching liquid is adjusted to 10 with NaOH, is alkalescent.Select hydrogen peroxide bleaching process at high proportion for use and add the influence that the scintilla high-efficiency refining agent is the yellow juice that produces in order to eliminate the part pectin of cotton fiber, cured matter and divide the commensal cotton seed hulls of loose wool to expand under the weak base condition, therefore omit the boiling of cotton fiber, practiced technology, avoided the highly basic in the boiling that milk protein fiber is damaged.Low selecting for use of pick-up makes the cloth cover liquid content few, the yellow juice diffusion limited system of cotton seed hulls; The macula lutea that reduces the bleaching washing produces, and keeps cloth cover whiteness unanimity.
2. oven dry, decatize, washing, oven dry bleach cloth; Described decatize is the long ring of a suspension type decatize technology.The contact that can prevent between the cloth cover of selecting for use of long ring decatize technology causes staining of the expanded yellow juice of cotton seed hulls.
3. textile dyeing; Neutral REACTIVE DYES is dyed on carrying out, and the pH value of dye liquor is 7.5, the dye liquor prescription; CN type REACTIVE DYES reactive yellow 10 grams per liters, reactive red 5 grams per liters, reactive blue 0.3 grams per liter, Buffer Ac 2 grams per liters, calgon 1 grams per liter, reservehao S 10 grams per liters, levelling agent 0.5 grams per liter, above-mentioned weight is to be benchmark with every premium on currency, adds described dyestuff of prescription and dyeing assistant in 70 ℃ of water.Last dyeing technique is: two soak one rolls, padding machine pressure 0.5Mpa, pick-up 100%, 100 ℃ of steam temperatures, steaming time 20min, speed of a motor vehicle 15m/min.CN type REACTIVE DYES is a kind of triazine type REACTIVE DYES with quaternary amine type pyridine carboxylic acid radical reaction base, can be under neutral high temperature (100-130 ℃) or weak basic condition, with the reaction of cellulose fibre or azelon, irregular or spot can effectively be covered and have the grey cloth whiteness and also can be reached bright-coloured color and luster when not high to the color and luster of cloth cover simultaneously.CN type REACTIVE DYES has positive pyrazinyl gets close to easily with negative cellulose key and adheres to, and along with the compatibility of temperature rising dyestuff and fiber is bigger, fixation promptly begins in dyeing, so does not need the highly basic fixation, has avoided the infringement to milk protein.The dyeing of various colors or stamp are formed by proportioning by reactive red, reactive yellow, the reactive blue three primary colours of CN type REACTIVE DYES.
4. stained clot-h decatize, washing, soft treatment, tentering oven dry; Described decatize is the long ring of a suspension type decatize technology, and described soft treatment is to add hydrophilic softener.The contact that can prevent between the cloth cover of selecting for use of long ring decatize technology causes staining of the expanded yellow juice of cotton seed hulls.
Dye process finishes.
Embodiment 2:
The white ground stamp of fabric
1. textile printing pre-treatment; Grey cloth is bleached with hydrogen peroxide bleaching agent before stamp, and it is 9.5 that bleaching liquid is regulated the pH value with NaOH, the bleaching liquid prescription; 100%H
2O
220 grams per liters, hydrogen peroxide stabilizer 4 grams per liters, scintilla high-efficiency refining agent 6 grams per liters, concise brightening agent 4 grams per liters; Above-mentioned weight is to be benchmark with every premium on currency.Process conditions are two to soak one and roll, and pad bleaching liquid, padding machine pressure 0.1Mpa, and pick-up 85%, technological parameter are speed of a motor vehicle 10m/min, 100 ℃ of temperature, time 25min.
2. oven dry, decatize, washing, oven dry bleach cloth; Described decatize is the long ring of a suspension type decatize
3. textile printing; Neutral REACTIVE DYES is carried out stamp, and the pH value of mill base is 7, the stamp prescription; CN type REACTIVE DYES reactive yellow 6 grams per liters, reactive red 0.2 grams per liter,, reactive blue 0.1 grams per liter, Buffer Ac 2 grams per liters, calgon, 1 grams per liter, reservehao S 10 grams per liters, former paste 400 grams per liters of sodium alginate.Above-mentioned weight is to be benchmark with every premium on currency, is mixed with printing paste, the flat screen printing machine stamp.
4. calico decatize, washing, soft treatment, tentering oven dry; Described decatize is the long ring of a suspension type decatize technology, and described soft treatment is to add hydrophilic softener.
The printing technology process finishes.
Embodiment 3:
The look ground stamp of fabric
1. textile dyeing pre-treatment; Bleach with hydrogen peroxide bleaching agent before dying on dyestuff, the pH value of bleaching liquid is 10.5, the bleaching liquid prescription; 100%H
2O
215 grams per liters, hydrogen peroxide stabilizer 7 grams per liters, scintilla high-efficiency refining agent 6 grams per liters, concise brightening agent 2 grams per liters; With every premium on currency is benchmark, adds described bleaching agent of prescription and bleaching assistant composition bleaching liquid in 60-70 ℃ of water.Process conditions are two to soak one and roll, and pad bleaching liquid, padding machine pressure 0.1Mpa, and pick-up 85%, technological parameter are speed of a motor vehicle 10m/min, 100 ℃ of temperature, time 25min.
2. oven dry, decatize, washing, oven dry bleach cloth; Described decatize is the long ring of a suspension type decatize technology.The contact that can prevent between the cloth cover of selecting for use of long ring decatize technology causes staining of the expanded yellow juice of cotton seed hulls.
3. textile dyeing; Neutral REACTIVE DYES is dyed on carrying out, and the pH value of dye liquor is 7.5, the dye liquor prescription; CN type REACTIVE DYES reactive red 2.2 grams per liters, reactive blue 1.5 grams per liters, Buffer Ac 0.5 grams per liter, hexa metaphosphoric acid 1.5 grams per liters, reservehao S 5 grams per liters, levelling agent 0.5 grams per liter, above-mentioned weight is to be benchmark with every premium on currency, adds the described dyestuff of prescription and dyeing assistant is formed dye liquor in 70 ℃ of water.Last dyeing technique is; Two soak one rolls, padding machine pressure 0.5Mpa, pick-up 100%, 100 ℃ of steam temperatures, steaming time 20min, speed of a motor vehicle 15m/min.Dyeing technique is on the REACTIVE DYES; Two soak one rolls, padding machine pressure 0.5Mpa, pick-up 100%, 100 ℃ of steam temperatures, steaming time 20min, speed of a motor vehicle 15m/min.
4. stained clot-h decatize, washing, soft treatment, tentering oven dry; Described decatize is the long ring of a suspension type decatize technology, and described soft treatment is to add hydrophilic softener.The contact that can prevent between the cloth cover of selecting for use of long ring decatize technology causes staining of the expanded yellow juice of cotton seed hulls.
(5) textile printing; Neutral REACTIVE DYES is carried out stamp, and the pH value of mill base is 7, the stamp prescription; CN type REACTIVE DYES Reactive Red 35 grams per liter, reactive yellow 6 grams per liters, reactive blue 0.5 grams per liter, Buffer Ac 2 grams per liters, calgon 1 grams per liter, reservehao S 15 grams per liters, former paste 400 grams per liters of sodium alginate.Above-mentioned weight is to be benchmark with every premium on currency, is mixed with printing paste, the flat screen printing machine stamp.
(6) calico decatize, washing, soft treatment, tentering oven dry; Described decatize is the long ring of a suspension type decatize technology, and described soft treatment is to add hydrophilic softener.
The printing technology process finishes.
The present invention has selected CN type REACTIVE DYES and the efficient scouring assistant of scintilla for use in the dyeing and finishing method of cotton/milk protein blended spinning Raschel fabric, and the new process of a cover, solves the technology incompatibility of two kinds of fibers.It is low to have production cost, pollutes fewly, has lovely luster, even dyeing, and characteristics that the premium properties of milk protein fiber is remained unchanged simultaneously.
Claims (6)
1. the dyeing and finishing method of a cotton/milk protein blended spinning Raschel fabric is characterized in that comprising the steps;
1. textile dyeing pre-treatment; Bleach with hydrogen peroxide bleaching agent before dyeing, the pH value of bleaching liquid is 9.5-10.5,
The bleaching liquid prescription; 100%H
2O
2The 10-20 grams per liter
Hydrogen peroxide stabilizer 3-7 grams per liter
Scintilla high-efficiency refining agent 6-12 grams per liter
Concise brightening agent 2-4 grams per liter
With every premium on currency is benchmark, adds described bleaching agent of prescription and bleaching assistant composition bleaching liquid in 60-70 ℃ of water.
2. oven dry, decatize, washing, oven dry bleach cloth; Described decatize is the long ring of a suspension type decatize technology,
3. textile dyeing or stamp; Neutral REACTIVE DYES dyes, and the pH value of dye liquor is 7-7.5, the dye liquor prescription;
CN type REACTIVE DYES 0.1-50 grams per liter
Buffer Ac 0.5-2 grams per liter
Calgon 1-1.5 grams per liter
Reservehao S 5-15 grams per liter
Levelling agent 0.1-0.5 grams per liter
With every premium on currency is benchmark, adds described dyestuff of prescription and dyeing assistant composition dye liquor in 60-70 ℃ of water.
4. stained clot-h decatize, washing, soft treatment, tentering oven dry; Described decatize is the long ring of a suspension type decatize technology, and described soft treatment is to add hydrophilic softener.
2. the dyeing and finishing method of a kind of cotton/milk protein blended spinning Raschel fabric according to claim 1 is characterized in that: step 1. textile dyeing pre-treatment process is; Two soak one rolls, and pads bleaching liquid, padding machine pressure 0.1Mpa, pick-up 85%, speed of a motor vehicle 10m/min, 100 ℃ of temperature, time 25min.
3. the dyeing and finishing method of a kind of cotton/milk protein blended spinning Raschel fabric according to claim 1 is characterized in that: step is textile dyeing 3.; Dyeing technique is on the REACTIVE DYES; Two soak one rolls, padding machine pressure 0.5Mpa, pick-up 100%, 100 ℃ of steam temperatures, steaming time 20min, speed of a motor vehicle 15m/min.
4. the dyeing and finishing method of a kind of cotton/milk protein blended spinning Raschel fabric according to claim 1 is characterized in that: step is textile printing 3.,
The stamp prescription;
CN type REACTIVE DYES 0.1-50 grams per liter
Buffer Ac 0.5-2 grams per liter
Calgon 1-1.5 grams per liter
Reservehao S 5-15 grams per liter
The former paste of sodium alginate 300-500 grams per liter
Add described dyestuff of prescription and dyeing assistant composition printing paste in 60-70 ℃ of water, printing technology is the flat screen printing machine stamp.
5. according to the dyeing and finishing method of claim 1 or 4 described a kind of cotton/milk protein blended spinning Raschel fabrics, it is characterized in that: the dyeing or the step of stamp 3. in added CN type REACTIVE DYES be a kind of triazine type REACTIVE DYES with quaternary amine type pyridine carboxylic acid radical reaction base.
6. according to the dyeing and finishing method of claim 1 or 4 or 5 described a kind of cotton/milk protein blended spinning Raschel fabrics, it is characterized in that: the dyeing or the step of stamp 3. in added CN type REACTIVE DYES be reactive red, reactive yellow, reactive blue.
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| CN2008100590944A CN101215790B (en) | 2008-01-09 | 2008-01-09 | Dyeing and finishing method for cotton/milk protein blended spinning Raschel fabric |
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| CN102220706A (en) * | 2011-06-02 | 2011-10-19 | 浙江华隆丝绸有限公司 | Georgette dyeing process |
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| CN103015225A (en) * | 2012-11-30 | 2013-04-03 | 吴江市超维纺织有限公司 | Method for dyeing milk fiber and cotton blended fabric |
| CN103498272A (en) * | 2013-09-17 | 2014-01-08 | 上海婉静纺织科技有限公司 | Fabric blended by milk protein fibers and cotton fibers |
| CN103643563A (en) * | 2013-11-30 | 2014-03-19 | 江苏金泰针织有限责任公司 | Dyeing and finishing process for protein fiber-containing blended knitted fabric |
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| CN102785495B (en) * | 2012-07-26 | 2015-06-17 | 浙江亿得化工有限公司 | Multi-color roller gravure printing production method of textile dye |
| CN103015225A (en) * | 2012-11-30 | 2013-04-03 | 吴江市超维纺织有限公司 | Method for dyeing milk fiber and cotton blended fabric |
| CN103498272A (en) * | 2013-09-17 | 2014-01-08 | 上海婉静纺织科技有限公司 | Fabric blended by milk protein fibers and cotton fibers |
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| CN108411649A (en) * | 2018-02-07 | 2018-08-17 | 嘉兴市桑田新材料科技有限公司 | N/R Roman cloth black dyeing and finishing technologies |
| CN108411649B (en) * | 2018-02-07 | 2020-11-20 | 嘉兴市桑田新材料科技有限公司 | N/R Roman cloth black dyeing and finishing process |
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