CN101048223A - 溶剂组合物 - Google Patents
溶剂组合物 Download PDFInfo
- Publication number
- CN101048223A CN101048223A CNA2005800373275A CN200580037327A CN101048223A CN 101048223 A CN101048223 A CN 101048223A CN A2005800373275 A CNA2005800373275 A CN A2005800373275A CN 200580037327 A CN200580037327 A CN 200580037327A CN 101048223 A CN101048223 A CN 101048223A
- Authority
- CN
- China
- Prior art keywords
- methyl
- pigment
- solvent
- solvent compositions
- resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002904 solvent Substances 0.000 title claims abstract description 57
- 239000000203 mixture Substances 0.000 title claims abstract description 48
- -1 1,2-propylene group Chemical group 0.000 claims abstract description 37
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 15
- 229920000570 polyether Polymers 0.000 claims abstract description 15
- CZZYITDELCSZES-UHFFFAOYSA-N diphenylmethane Chemical class C=1C=CC=CC=1CC1=CC=CC=C1 CZZYITDELCSZES-UHFFFAOYSA-N 0.000 claims abstract description 14
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 9
- 150000001875 compounds Chemical class 0.000 claims description 18
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 12
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 11
- 125000000217 alkyl group Chemical group 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 10
- QWUWMCYKGHVNAV-UHFFFAOYSA-N 1,2-dihydrostilbene Chemical compound C=1C=CC=CC=1CCC1=CC=CC=C1 QWUWMCYKGHVNAV-UHFFFAOYSA-N 0.000 claims description 2
- 239000011368 organic material Substances 0.000 abstract description 4
- 239000000758 substrate Substances 0.000 abstract description 2
- 125000000008 (C1-C10) alkyl group Chemical group 0.000 abstract 2
- 239000000049 pigment Substances 0.000 description 33
- 239000000463 material Substances 0.000 description 25
- 239000011248 coating agent Substances 0.000 description 21
- 238000000576 coating method Methods 0.000 description 21
- 239000000976 ink Substances 0.000 description 19
- 238000005406 washing Methods 0.000 description 16
- 229920005989 resin Polymers 0.000 description 15
- 239000011347 resin Substances 0.000 description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 230000000052 comparative effect Effects 0.000 description 11
- 239000007767 bonding agent Substances 0.000 description 10
- 238000007639 printing Methods 0.000 description 9
- 239000000126 substance Substances 0.000 description 9
- 239000002585 base Substances 0.000 description 8
- 239000003795 chemical substances by application Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- 239000004094 surface-active agent Substances 0.000 description 8
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical class CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- LZCLXQDLBQLTDK-UHFFFAOYSA-N ethyl 2-hydroxypropanoate Chemical compound CCOC(=O)C(C)O LZCLXQDLBQLTDK-UHFFFAOYSA-N 0.000 description 6
- 239000002202 Polyethylene glycol Substances 0.000 description 5
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 230000003287 optical effect Effects 0.000 description 5
- 229920001223 polyethylene glycol Polymers 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- AJDIZQLSFPQPEY-UHFFFAOYSA-N 1,1,2-Trichlorotrifluoroethane Chemical compound FC(F)(Cl)C(F)(Cl)Cl AJDIZQLSFPQPEY-UHFFFAOYSA-N 0.000 description 4
- SVONRAPFKPVNKG-UHFFFAOYSA-N 2-ethoxyethyl acetate Chemical compound CCOCCOC(C)=O SVONRAPFKPVNKG-UHFFFAOYSA-N 0.000 description 4
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 4
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 4
- RWGFKTVRMDUZSP-UHFFFAOYSA-N cumene Chemical compound CC(C)C1=CC=CC=C1 RWGFKTVRMDUZSP-UHFFFAOYSA-N 0.000 description 4
- 150000002576 ketones Chemical class 0.000 description 4
- 125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 4
- 150000002894 organic compounds Chemical class 0.000 description 4
- FKRCODPIKNYEAC-UHFFFAOYSA-N propionic acid ethyl ester Natural products CCOC(=O)CC FKRCODPIKNYEAC-UHFFFAOYSA-N 0.000 description 4
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- 239000004925 Acrylic resin Substances 0.000 description 3
- 229920000178 Acrylic resin Polymers 0.000 description 3
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- 239000004698 Polyethylene Substances 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- RDOXTESZEPMUJZ-UHFFFAOYSA-N anisole Chemical class COC1=CC=CC=C1 RDOXTESZEPMUJZ-UHFFFAOYSA-N 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- 150000002170 ethers Chemical class 0.000 description 3
- 229940116333 ethyl lactate Drugs 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 239000000178 monomer Substances 0.000 description 3
- 230000001590 oxidative effect Effects 0.000 description 3
- 239000012188 paraffin wax Substances 0.000 description 3
- 239000004014 plasticizer Substances 0.000 description 3
- 239000004065 semiconductor Substances 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical group C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 description 3
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 2
- ZORQXIQZAOLNGE-UHFFFAOYSA-N 1,1-difluorocyclohexane Chemical compound FC1(F)CCCCC1 ZORQXIQZAOLNGE-UHFFFAOYSA-N 0.000 description 2
- KVNYFPKFSJIPBJ-UHFFFAOYSA-N 1,2-diethylbenzene Chemical compound CCC1=CC=CC=C1CC KVNYFPKFSJIPBJ-UHFFFAOYSA-N 0.000 description 2
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 2
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 2
- ARXJGSRGQADJSQ-UHFFFAOYSA-N 1-methoxypropan-2-ol Chemical compound COCC(C)O ARXJGSRGQADJSQ-UHFFFAOYSA-N 0.000 description 2
- QPUYECUOLPXSFR-UHFFFAOYSA-N 1-methylnaphthalene Chemical compound C1=CC=C2C(C)=CC=CC2=C1 QPUYECUOLPXSFR-UHFFFAOYSA-N 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 2
- YBYIRNPNPLQARY-UHFFFAOYSA-N 1H-indene Chemical compound C1=CC=C2CC=CC2=C1 YBYIRNPNPLQARY-UHFFFAOYSA-N 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- 229920002799 BoPET Polymers 0.000 description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 2
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 description 2
- 239000005041 Mylar™ Substances 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 2
- 239000004952 Polyamide Substances 0.000 description 2
- 239000004743 Polypropylene Substances 0.000 description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 description 2
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 2
- IYFATESGLOUGBX-YVNJGZBMSA-N Sorbitan monopalmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O IYFATESGLOUGBX-YVNJGZBMSA-N 0.000 description 2
- HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 description 2
- 239000004147 Sorbitan trioleate Substances 0.000 description 2
- PRXRUNOAOLTIEF-ADSICKODSA-N Sorbitan trioleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](OC(=O)CCCCCCC\C=C/CCCCCCCC)[C@H]1OC[C@H](O)[C@H]1OC(=O)CCCCCCC\C=C/CCCCCCCC PRXRUNOAOLTIEF-ADSICKODSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical class ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 2
- 229920001807 Urea-formaldehyde Polymers 0.000 description 2
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 2
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 2
- IJCWFDPJFXGQBN-RYNSOKOISA-N [(2R)-2-[(2R,3R,4S)-4-hydroxy-3-octadecanoyloxyoxolan-2-yl]-2-octadecanoyloxyethyl] octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](OC(=O)CCCCCCCCCCCCCCCCC)[C@H]1OC[C@H](O)[C@H]1OC(=O)CCCCCCCCCCCCCCCCC IJCWFDPJFXGQBN-RYNSOKOISA-N 0.000 description 2
- LWZFANDGMFTDAV-BURFUSLBSA-N [(2r)-2-[(2r,3r,4s)-3,4-dihydroxyoxolan-2-yl]-2-hydroxyethyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O LWZFANDGMFTDAV-BURFUSLBSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 229920000180 alkyd Polymers 0.000 description 2
- 150000001450 anions Chemical class 0.000 description 2
- RJGDLRCDCYRQOQ-UHFFFAOYSA-N anthrone Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3CC2=C1 RJGDLRCDCYRQOQ-UHFFFAOYSA-N 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 239000013556 antirust agent Substances 0.000 description 2
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- OCKPCBLVNKHBMX-UHFFFAOYSA-N butylbenzene Chemical compound CCCCC1=CC=CC=C1 OCKPCBLVNKHBMX-UHFFFAOYSA-N 0.000 description 2
- 239000004359 castor oil Substances 0.000 description 2
- 235000019438 castor oil Nutrition 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000007859 condensation product Substances 0.000 description 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 2
- LJOODBDWMQKMFB-UHFFFAOYSA-N cyclohexylacetic acid Chemical compound OC(=O)CC1CCCCC1 LJOODBDWMQKMFB-UHFFFAOYSA-N 0.000 description 2
- HHNHBFLGXIUXCM-GFCCVEGCSA-N cyclohexylbenzene Chemical compound [CH]1CCCC[C@@H]1C1=CC=CC=C1 HHNHBFLGXIUXCM-GFCCVEGCSA-N 0.000 description 2
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
- 239000013530 defoamer Substances 0.000 description 2
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 2
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 229920001971 elastomer Polymers 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000003822 epoxy resin Substances 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
- XLLIQLLCWZCATF-UHFFFAOYSA-N ethylene glycol monomethyl ether acetate Natural products COCCOC(C)=O XLLIQLLCWZCATF-UHFFFAOYSA-N 0.000 description 2
- 230000005669 field effect Effects 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 229910052731 fluorine Inorganic materials 0.000 description 2
- 239000011737 fluorine Substances 0.000 description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 2
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 229910052736 halogen Inorganic materials 0.000 description 2
- 150000002367 halogens Chemical class 0.000 description 2
- 125000003187 heptyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 2
- 125000001972 isopentyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])C([H])([H])* 0.000 description 2
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 description 2
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
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- 125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
- 150000002790 naphthalenes Chemical class 0.000 description 2
- ZWRUINPWMLAQRD-UHFFFAOYSA-N nonan-1-ol Chemical compound CCCCCCCCCO ZWRUINPWMLAQRD-UHFFFAOYSA-N 0.000 description 2
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 150000004880 oxines Chemical class 0.000 description 2
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 2
- 125000002080 perylenyl group Chemical group C1(=CC=C2C=CC=C3C4=CC=CC5=CC=CC(C1=C23)=C45)* 0.000 description 2
- 229920006287 phenoxy resin Polymers 0.000 description 2
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- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
- IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 description 2
- 229920000058 polyacrylate Polymers 0.000 description 2
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- 229920000647 polyepoxide Polymers 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 229920001155 polypropylene Polymers 0.000 description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
- 235000011067 sorbitan monolaureate Nutrition 0.000 description 2
- 239000001593 sorbitan monooleate Substances 0.000 description 2
- 235000011069 sorbitan monooleate Nutrition 0.000 description 2
- 229940035049 sorbitan monooleate Drugs 0.000 description 2
- 239000001570 sorbitan monopalmitate Substances 0.000 description 2
- 235000011071 sorbitan monopalmitate Nutrition 0.000 description 2
- 229940031953 sorbitan monopalmitate Drugs 0.000 description 2
- 239000001587 sorbitan monostearate Substances 0.000 description 2
- 235000011076 sorbitan monostearate Nutrition 0.000 description 2
- 229940035048 sorbitan monostearate Drugs 0.000 description 2
- 235000019337 sorbitan trioleate Nutrition 0.000 description 2
- 229960000391 sorbitan trioleate Drugs 0.000 description 2
- 239000001589 sorbitan tristearate Substances 0.000 description 2
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/18—Hydrocarbons
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
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Abstract
本发明的溶剂组合物含有(a)由下述通式(I)表示的二苯基甲烷化合物和(b)由下述通式(II)表示的聚醚化合物，并且安全性优异，几乎没有臭味，各种有机材料的溶解性优异，对各种基材的亲和性也优异。上述通式(I)中，n表示1或2，x和y分别独立地表示0、1、2或3，R1和R2分别独立地表示碳原子数为1－10的烷基，R1和R2分别存在多个时，它们也可以不同；上述通式(II)中，m表示1－10，p表示0、1、2或3，Prop表示1，2－亚丙基，R3和R4分别独立地表示碳原子数为1－10的烷基，其中，以Prop表示的1，2－亚丙基在m为2以上时，甲基取代位置可以是任意的。
Description
技术领域
本发明涉及溶剂组合物，详细地讲，涉及将特定的二苯基甲烷化合物和特定的聚醚化合物组合而得到的安全性优异、臭味小，并且各种有机材料的溶解性优异，对各种基材的亲和性也优异的溶剂组合物。
背景技术
在涂料、粘接剂、印刷油墨等领域中，溶剂发挥着重要的作用。对于溶剂，当然要求其具有较大的溶质溶解性。另外，在这些领域中，溶剂对涂敷面的润湿性、干燥性等性能施以较大的影响。
以往，作为与涂料、粘接剂、印刷油墨等领域中常用的纤维素树脂、环氧树脂、丙烯酸树脂、醋酸乙烯酯树脂、氯乙烯树脂、醇酸树脂、聚酯树脂等并用的溶剂，乙二醇醚系的溶纤剂类、特别是醋酸溶纤剂由于其优异的性能而备受偏爱使用。但是，最近由于公害问题等，对化学物质的安全性的要求变得非常强烈，醋酸溶纤剂也因为毒性问题而被增加了使用限制，正在根据劳动安全卫生法设定操作环境管理浓度标准。
因此，正在踊跃开发具有可以代替醋酸溶纤剂的溶解性、且无需担心安全性的替代溶剂。例如，研究了乳酸乙酯、丙二醇单甲基醚乙酸酯、甲氧基丙醇、β-环氧丙酸乙酯等作为最有希望的的备选的替代溶剂，但在溶解力、安全性、臭味、操作性等方面不一定可以满足要求。而且，这些之中，从安全性的观点出发，即使作为食品添加剂也被允许的乳酸乙酯被认为是最优选的溶剂，但在高分子化合物和各种添加剂的溶解性的方面很难说是能够充分满足的。
另外，从溶解性的观点考虑，一般认为β-甲氧基丙酸甲酯和β-乙氧基丙酸乙酯等β-烷氧基丙酸烷基酯类最优选，但是这些溶剂的高分子化物和各种添加剂的溶解性也不能满足要求，另外，在涂敷后的挥发性方面也不能满足要求。
此外，溶剂除了如上所述的用途以外，还可以用于作为切削油、加工油、冲压油、防锈油、润滑油、润滑脂或者沥青等使用的油类的洗涤用、或者助焊剂、油墨、液晶等洗涤用等。作为这些洗涤用的溶剂，广泛使用以氟利昂113(1，1，2-三氯-1，2，2-三氯乙烷)、甲基氯仿(1，1，1-三氯乙烷)和三氯乙烯等卤素类溶剂为主体的溶剂。尤其氟利昂(フロン)113是不燃性，且毒性也低，安全性优异，而且由于具有在不侵害金属、塑料、弹性体等的情况下可以选择性地溶解各种污物的性质，所以被广泛应用。但是，由于氟利昂113和甲基氯仿破坏平流层的臭氧层，甚至成为引起皮肤癌产生的原因，正在迅速限制其使用。另外，三氯乙烯具有怀疑致癌性等问题，其从安全性方面考虑也正被限制使用。
因此，正在踊跃开发具有可以代替氟利昂113等、且无需担心破坏臭氧层的替代氟利昂系洗涤剂，例如，在专利文献1中，公开了以1，2-二氟乙烷为主成分的溶剂，在专利文献2中，公开了1，1-二氯-2，2，2-三氟乙烷和二甲氧基苯的混合物，在专利文献3中，公开了以六氟苯为主成分的溶剂，但是这些溶剂除了在性能方面不及氟利昂113外，从环境问题和安全性问题方面考虑，这些卤素系溶剂将来也会向全面限制使用的方向发展。
专利文献1：特开平1-132694号公报
专利文献2：特开平2-178396号公报
专利文献3：特开平3-167298号公报
发明内容
因此，本发明的目的在于鉴于这种现状，提供安全性优异，臭味小，且各种有机材料的溶解性优异，对各种基材的亲和性也优异的溶剂组合物。
本发明者等经过反复潜心研究，结果发现将特定的二苯基甲烷化合物和聚醚化合物组合而得到的溶剂组合物可以解决上述课题，从而完成了本发明。
即，本发明提供一种溶剂组合物，其含有(a)由下述通式(I)表示的二苯基甲烷化合物和(b)由下述通式(II)表示的聚醚化合物。
(式中，n表示1或2，x和y分别独立地表示0、1、2或3，R1和R2分别独立地表示碳原子数为1-10的烷基。R1和R2分别存在多个时，它们也可以不同。)
(式中，m表示1-10，p表示0、1、2或3，Prop表示1，2-亚丙基，R3和R4分别独立地表示碳原子数为1-10的烷基。其中，以Prop表示的1，2-亚丙基在m为2以上时，甲基取代位置可以是任意的。)
具体实施方式
下面，对本发明的溶剂组合物进行详细的说明。
在表示作为(a)成分的二苯基甲烷化合物的上述通式(I)中，作为由R1和R2表示的碳原子数为1-10的烷基，可列举例如甲基、乙基、丙基、异丙基、丁基、异丁基、仲丁基、叔丁基、戊基、异戊基、叔戊基、己基、庚基、辛基、异辛基、2-乙基己基、壬基、异壬基、癸基、异癸基等基团。其中，R1优选碳原子数为1-4的烷基，R2也优选碳原子数为1-4的烷基。
作为本发明中使用的作为(a)成分的二苯基甲烷化合物的具体例子，可列举下述的化合物。而且，这些二苯基甲烷化合物可以单独使用，也可以将二种以上组合使用。
[化学式3]
[化学式4]
这些二苯基甲烷化合物中，由于苄基甲苯(上述[化学式3]中所示的BoT、BmT和BpT)由于溶解性特别优异，所以优选。
在表示作为(b)成分的聚醚化合物的上述通式(II)中，作为R3和R4表示的碳原子数为1-10的烷基，可列举例如甲基、乙基、丙基、异丙基、丁基、异丁基、仲丁基、叔丁基、戊基、异戊基、叔戊基、己基、庚基、辛基、异辛基、2-乙基己基、壬基、异壬基、癸基、异癸基等基团。其中，R3优选碳原子数为1-4的烷基，R4也优选碳原子数为1-4的烷基。
作为本发明中使用的作为(b)成分的聚醚化合物的具体例子，可列举下述的化合物。而且，这些聚醚化合物可以单独使用，也可以将二种以上组合使用。
[化学式5]
[化学式6]
这些聚醚化合物中，优选使用选自[(2-甲氧基-1，2-丙氧基)甲基]苯(上述[化学式5]中所示的M1PMB和M2PMB)以及[(2-甲氧基-1，2-丙氧基)甲基]甲苯(上述[化学式5]中所示的M1PMoT和M2PMoT)中的一种以上，因为它们可以进一步提高对涂敷面的润湿性，特别优选使用[(2-甲氧基-1，2-甲基乙氧基)甲基]苯(上述[化学式5]中所示的M1PMB)。
本发明的溶剂组合物含有作为(a)成分的二苯基甲烷化合物和作为(b)成分的聚醚化合物，各自的使用量是：(a)成分优选为0.1-99.9质量％，特别优选为5-95质量％，(b)成分优选为0.1-99.9质量％，特别优选为5-95质量％。(a)成分小于0.1质量％时，溶解性容易变得不充分，而(b)成分小于0.1质量％时，润湿性容易变得不充分。
本发明的溶剂组合物可以与水或其它的有机溶剂混合使用。
作为其它的有机溶剂，可列举甲醇、乙醇、丙醇、异丙醇、丁醇、3-甲基丁醇、甲基异丁基甲醇、庚醇、辛醇、2-乙基-1-己醇、3，3，5-三甲基-1-己醇、壬醇、环己醇、苄醇、萘醇、氟代醇等醇类；乙二醇、二乙二醇、三乙二醇、聚乙二醇、丙二醇、二丙二醇、聚丙二醇等二元醇类；3-甲氧基丁醇、3-甲基-3-甲氧基丁醇、乙二醇单甲醚(甲基溶纤剂)、乙二醇单乙醚(溶纤剂)、乙二醇单丁醚(丁基溶纤剂)、二乙二醇单乙醚(卡必醇)、二乙二醇单丁醚(丁基卡必醇)、丙二醇单甲醚等醚醇类；丙酮、甲乙酮、甲基异丁基酮、环己酮、异佛尔酮等酮类；吡咯烷酮、N-甲基吡咯烷酮、四氢呋喃、噁唑、苯并呋喃、二噁烷等杂环式化合物；二甲基甲酰胺、二甲基乙酰胺等酰胺类；二甲基亚砜、环丁砜等砜类；醋酸甲酯、醋酸乙酯、醋酸丁酯、醋酸戊酯、3-甲氧基丁基乙酸酯、30-甲基-3-甲氧基丁基乙酸酯、2-乙基己基乙酸酯、环己基乙酸酯、苄基乙酸酯、乳酸甲酯、乳酸乙酯、乳酸丁酯、3-甲氧基丙酸甲酯、3-乙氧基丙酸乙酯等酯类；二苄醚、苯甲醚等醚类；硝基乙烷、硝基甲烷等硝基化合物；乙腈等腈化合物；γ-丁内酯等内酯类；乙二醇单甲醚乙酸酯、乙二醇单乙醚乙酸酯、丙二醇单甲醚乙酸酯等醚酯类；苯、甲苯、二甲苯、枯烯、异丙基苯、二己基苯、四甲基苯、二乙苯、二丁苯、环己苯、联苯、均三甲苯、环己苯等芳香族烃；萘烷、烷基萘烷、萘满等稠环烃；正己烷、正庚烷、矿油精等脂肪族烃；环己烷、烷基环己烷、烷基环戊烷等脂环式烃等。
本发明的溶剂组合物可以用于各种涂料、各种粘接剂、胶印油墨、平版油墨、凸版油墨、特殊油墨、照相凹版印刷油墨、圆珠笔墨水、喷墨印刷油墨等各种油墨、各种涂敷材料等用途。
将本发明的溶剂组合物用于涂料、粘接剂、油墨、涂敷材料等时，可以并用作为粘合剂的各种高分子材料。作为成为该粘合剂的高分子材料，可列举例如松香、虫胶、硬树脂、达马树脂、硬沥青、玉米蛋白、纤维素等天然树脂及其衍生物；天然橡胶；各种油脂类；丙烯酸树脂(聚丙烯酸酯、聚甲基丙烯酸酯等)、醋酸乙烯酯树脂、氯乙烯树脂、醇酸树脂、聚酯树脂、酚醛清漆树脂、尿素树脂、蜜胺树脂、苯酚树脂、间苯二酚树脂、环氧树脂、聚氨酯、聚乙烯醇、二甲苯树脂、尿素树脂、酮树脂、色满-茚(chroman indene)树脂、石油树脂、萜烯树脂、聚酰胺树脂、氯乙烯-醋酸乙烯酯共聚树脂、聚乙烯醇缩丁醛、氯化聚丙烯、苯乙烯树脂、聚碳酸酯、苯氧基树脂、聚丙烯腈等合成树脂；氯丁橡胶、丁腈、苯乙烯丁二烯橡胶、氯化橡胶、环化橡胶等合成橡胶等。
另外，将本发明的溶剂组合物用于涂料、粘接剂、油墨、涂敷材料等时，可以并用各种填充剂和/或颜料。作为该填充剂和颜料，可列举例如玻璃纤维、碳纤维、纤维素、硅砂、水泥、高岭土、粘土、氢氧化铝、皂土、滑石、硅石、微粉末二氧化硅、二氧化钛、碳黑、石墨、氧化铁、沥青物质、有机颜料等。
另外，将本发明的溶剂组合物用于涂料、粘接剂、油墨、涂敷材料等时，可以与各种表面活性剂组合使用。作为该表面活性剂，阴离子性、非离子性、阳离子性、两离子性、高分子系或反应性表面活性剂都可以使用。
作为上述阴离子性表面活性剂，可列举例如十二烷基硫酸钠、十二烷基硫酸钾、十二烷基硫酸铵等烷基硫酸盐；十二烷基聚乙二醇醚硫酸钠；磺基蓖麻油酸钠；磺化石蜡的碱金属盐、磺化石蜡的铵盐等烷基磺酸盐；月桂酸钠、三乙醇胺油酸盐、松香酸三乙醇胺等脂肪酸盐；苯磺酸钠、烷基苯酚羟基乙烯的碱金属硫酸盐等烷基芳基磺酸盐；高烷基萘磺酸；萘磺酸甲醛缩合物；二烷基磺基琥珀酸盐；聚氧乙烯烷基硫酸盐；聚氧乙烯烷基芳基硫酸盐等。
另外，作为上述非离子性表面活性剂，可列举例如聚氧乙烯聚丙烯共聚物、月桂醚环氧乙烷加成物、十六烷基醚环氧乙烷加成物、硬脂酰基醚环氧乙烷加成物、油烯基醚环氧乙烷加成物、辛基苯基醚环氧乙烷加成物、壬基苯基醚环氧乙烷加成物、双酚A环氧乙烷加成物、山梨糖醇酐单月桂酸酯、山梨糖醇酐单棕榈酸酯、山梨糖醇酐单硬脂酸酯、山梨糖醇酐三硬脂酸酯、山梨糖醇酐单油酸酯、山梨糖醇酐三油酸酯、山梨糖醇酐倍半油酸酯、山梨糖醇酐二硬脂酸酯、山梨糖醇酐单月桂酸酯环氧乙烷加成物、山梨糖醇酐单棕榈酸酯环氧乙烷加成物、山梨糖醇酐单硬脂酸酯环氧乙烷加成物、山梨糖醇酐三硬脂酸酯环氧乙烷加成物、山梨糖醇酐单油酸酯环氧乙烷加成物、山梨糖醇酐三油酸酯环氧乙烷加成物、四油酸聚氧乙烯山梨糖醇、甘油单硬脂酸酯、聚乙二醇单月桂酸酯、聚乙二醇单硬脂酸酯、聚乙二醇二硬脂酸酯、聚乙二醇单油酸酯、聚乙烯烷基胺、蓖麻油环氧乙烷加成物、硬化蓖麻油环氧乙烷加成物或者将它们用聚异氰酸酯化合物缩合而得到的缩合物等。
另外，作为上述阳离子性表面活性剂，可列举例如伯～叔胺盐、吡啶鎓盐、季铵盐等。
此外，作为上述两离子性表面活性剂，可列举甜菜碱型、硫酸酯型、磺酸型等两性表面活性剂。
另外，作为上述高分子系表面活性剂，可列举例如聚乙烯醇；聚(甲基)丙烯酸钠、聚(甲基)丙烯酸钾、聚(甲基)丙烯酸铵、聚羟乙基(甲基)丙烯酸酯、聚羟丙基(甲基)丙烯酸酯；作为这些聚合物的结构单元的聚合性单体的二种以上的共聚物或者与其它单体的共聚物等。另外，冠醚类等称为相转移催化剂的物质也可合适地作为表现出表面活性的物质。
此外，作为上述反应性表面活性剂，只要是在分子内具有可以与不饱和单体共聚的不饱和键的物质即可，无论非离子系、阴离子系或者阳离子系都可以使用。
另外，将本发明的溶剂组合物用于涂料、粘接剂、油墨、涂敷材料等时，可以并用增塑剂。作为该增塑剂，可列举酞酸二丁酯、酞酸二辛酯、己二酸二辛酯、壬二酸二辛酯、柠檬酸三乙酯、乙酰基柠檬酸三丁酯、癸二酸二丁酯、癸二酸二辛酯、环氧化动植物油、环氧化脂肪酸酯、聚酯系增塑剂、氯化石蜡等。
此外，将本发明的溶剂组合物用于涂料、粘接剂、油墨、涂敷材料等时，还可以根据需要混合防锈剂、防腐剂、消泡剂、稳定剂、抗氧化剂、增稠剂等。
另外，使用了本发明的溶剂组合物的涂料、粘接剂、油墨、涂敷材料等可以适当用于各种基材。作为该基材，可列举例如聚醚砜、聚对苯二甲酸乙二酯、聚碳酸酯、聚醚醚酮、聚氟化乙烯、聚丙烯酸酯、聚甲基丙烯酸甲酯、聚酰胺、聚丙烯、聚乙烯、环烯烃聚合物、非晶质聚烯烃、含氟树脂等高分子材料；玻璃、陶瓷等无机材料等。
另外，本发明的溶剂组合物在利用了以往的印刷技术的光学记录材料、有机EL元件、场效应晶体管等电子设备的制造中，也可以有效地用作溶解各种有机化合物的溶剂。
上述光学记录材料由含有光学存储器色素的色素层、PC基盘、反射膜等构成。作为该光存储器色素，可列举例如花青系色素、酞菁系色素、萘酞青(naphthalocyanine)系色素、naphtholactam系色素、甲基吡啶系色素、偶氮系色素、酚噻嗪系色素、吡喃鎓系色素、硫代吡喃鎓系色素、方酸内鎓盐(squarylium)系色素、甘菊环型鎓(azulenium)系色素、靛酚系色素、茚并苯胺(indoaniline)系色素、三苯基甲烷系色素、醌系色素、蒽醌系色素、铵鎓(aminium)系色素、二茚铸(diimmonium)系色素、金属络盐系色素等。
上述有机EL元件由含有发光材料的发光层、基板、ITO阳极、空穴注入层、空穴导电层、电子输送层、AI阴极等构成。作为该发光材料，可列举例如芴系衍生物、对苯撑乙烯衍生物、聚苯撑衍生物、聚乙烯基咔唑、聚噻吩衍生物、二萘嵌苯衍生物、香豆素系色素、若丹明系色素、吡喃系色素、蒽酮系色素、卟啉系色素、喹吖酮系色素、N，N’-二烷基取代喹吖酮系色素、萘酰亚胺系色素、N，N’-二芳基取代吡咯并吡咯系色素等。
上述场效应晶体管由含有有机半导体材料的半导体层、绝缘层、栅电极、源电极、漏电极等构成。作为该有机半导体材料，可列举例如N，N’-二烷基二萘嵌苯-3，4，9-10-四羧酸二酰亚胺等二萘嵌苯系颜料、萘-1，4，5，8-四羧酸二酰亚胺类、各种金属酞菁类、硝基芴酮类、取代芴-丙二腈加成物、卤化蒽酮垛蒽酮类、三(8-羟基喹啉)铝、以及含有它们的低聚物和聚合物等。
另外，本发明的溶剂组合物也可以用作洗涤印刷基板或液晶单元等中使用的松香系助焊剂的洗涤剂；或用作去除电子元件和精密机械、例如精密元件及其组装工序中使用的夹具等电子元件的金属部分、和腐蚀加工元件(例如印刷配线、集成电路、模板(shadow mask))的存在于固体表面的以油等有机物为主体的污物等的洗涤剂。
将本发明的溶剂组合物用作洗涤剂时，可以与表面活性剂组合使用。作为该表面活性剂，阴离子系、阳离子系、两离子系、非离子系都可以使用，但是从对洗涤面的影响的观点考虑，优选非离子系表面活性剂。
另外，作为洗涤剂使用时，也可以根据需要混合柠檬酸、酒石酸、邻苯二甲酸等有机酸；单乙醇胺、二乙醇胺等烷醇胺；防锈剂、防腐剂、消泡剂、稳定剂、抗氧化剂等。
此外，洗涤方法可以适当使用浸渍法、超声波洗涤法、摇动法、喷雾法、蒸汽洗涤法、手洗(hand cleaning)法、水置换干燥法等各种洗涤方法。
实施例
下面，通过示出实施例等更加详细地说明本发明的溶剂组合物，但是本发明受它们的限定。
[实施例1-5]
按照如表1所示的配方分别制作溶剂组合物S1-S5。
[表1]
| 实施例 | ||||||
| 1 | 2 | 3 | 4 | 5 | ||
| 溶剂组合物 | S1 | S2 | S3 | S4 | S5 | |
| 配方(质量份) | BT*1 | 90 | 85 | 80 | ||
| BoT | 85 | |||||
| BpT | 85 | |||||
| M1PMB | 10 | 15 | 20 | 15 | 15 | |
| 外观 | 无色透明 | 无色透明 | 无色透明 | 无色透明 | 无色透明 | |
*1：BoT/BpT混合物(质量比1/1)
[比较例1-5]
按照如表2所示的配方分别制作溶剂组合物HS1-HS5。
[表2]
| 比较例 | ||||||
| 1 | 2 | 3 | 4 | 5 | ||
| 溶剂组合物 | HS1 | HS2 | HS3 | HS4 | HS5 | |
| 配方(质量份) | BT | 85 | ||||
| 甲基萘 | 90 | 85 | 80 | 85 | ||
| M1PMB | 15 | |||||
| 乙基溶纤剂 | 10 | 15 | 20 | 15 | ||
| 外观 | 无色透明 | 无色透明 | 无色透明 | 无色透明 | 无色透明 | |
[评价例]
对由上述实施例和比较例得到的溶剂组合物以及其它溶剂(BT和M1PMB)，进行以下的评价和测定。
(臭味评价)
通过10名被试验者完成官能试验，按照以下三个等级进行评价：○：几乎没有臭味、△：有臭味、×：有强烈的臭味。
(溶解性评价)
加入5质量％如[表3]中所示的溶质(有机化合物)，在30℃下搅拌1小时，观察溶解性，按照以下三个等级进行评价：○：完全溶解、△：看到微量不溶物、×：完全或者几乎不溶解。
(接触角测定)
用中性溶剂洗涤后，用超纯水漂洗且干燥之后的玻璃(松浪硝子工业(株)制；MICRO SLIDE GLASS S 1226)上滴加溶剂10μL，使用协和界面科学(株)制CONTACT-ANGLE METER CA-D测定接触角。测定时的气温为22-25℃，湿度为50-70％。接触角是测定6次、且除去了最大值和最小值的值的平均值。
而且，当接触角超过20°时难以涂敷，在15°以下时涂敷特别好。
这些评价结果和测量结果如[表3]所示。
[表3]
| 溶剂 | 臭味 | 溶解性 | 接触角 | |||||
| 溶质1*2 | 溶质2*3 | 溶质3*4 | 溶质4*5 | 溶质5*6 | 溶质6*7 | |||
| S1(实施例1) | ○ | ○ | ○ | ○ | ○ | ○ | ○ | 15 |
| S2(实施例2) | ○ | ○ | ○ | ○ | ○ | ○ | ○ | 14 |
| S3(实施例3) | ○ | ○ | ○ | ○ | ○ | ○ | ○ | 13 |
| S4(实施例4) | ○ | ○ | ○ | ○ | ○ | ○ | ○ | 14 |
| S5(实施例5) | ○ | ○ | ○ | ○ | ○ | ○ | ○ | 14 |
| HS1(比较例1) | × | ○ | ○ | ○ | ○ | ○ | ○ | 18 |
| HS2(比较例2) | × | ○ | ○ | ○ | ○ | ○ | ○ | 17 |
| HS3(比较例3) | × | ○ | ○ | ○ | ○ | ○ | ○ | 16 |
| HS4(比较例4) | △ | ○ | ○ | ○ | ○ | ○ | ○ | 16 |
| HS5(比较例5) | × | ○ | ○ | ○ | ○ | ○ | ○ | 16 |
| BT | ○ | ○ | ○ | ○ | ○ | ○ | △ | 21 |
| M1PMB | ○ | △ | △ | △ | △ | △ | ○ | 11 |
*2：溶质1＝ER·1002(三菱Rayon(株)制；聚酯)
*3：溶质2＝QP×2B(电气化学工业(株)制；聚苯乙烯)
*4：溶质3＝MS-300(新日铁化学(株)制；MMA-苯乙烯共聚物)
*5：溶质4＝Acrydic A-405(大日本油墨工业(株)制；丙烯酸树脂)
*6：溶质5＝PKH-H(UCC社制；苯氧基树脂)
*7：溶质6＝P1800NT11(AMOCO制；聚砜)
由表3显而易见的是，将萘系溶剂和醚系溶剂组合而得到的溶剂组合物对作为粘合剂使用的各种有机化合物的溶解性优异，但是臭味大，另外，接触角大且对基材的润湿性差(比较例1-3)。将萘系溶剂和本发明中使用的特定的聚醚化合物组合的情况也相同(比较例5)。此外，将本发明中使用的特定的二苯基甲烷化合物和乙基溶纤剂等本发明中使用的特定的聚醚化合物以外的醚系溶剂组合时，虽然溶解性优异，但是有臭味，另外，在安全性方面也有问题(比较例4)。而且，单独使用本发明中使用的特定的二苯基甲烷化合物时，润湿性差(BT)，单独使用本发明中使用的特定的聚醚化合物时，溶解性差(M1PMB)。
与此相反，含有特定的二苯基甲烷化合物和特定的聚醚化合物的本发明的溶剂组合物臭味小，各种有机化合物的溶解性优异，对各种基材的湿润性也优异。
本发明的溶剂组合物，安全性优异，几乎没有臭味，各种有机材料的溶解性优异，对各种基材的亲和性也优异，可以在各种涂料、各种粘接剂、各种涂敷材料、各种洗涤剂等各种用途中适当地加以使用。
Claims (3)
1、一种溶剂组合物，其含有(a)由下述通式(I)表示的二苯基甲烷化合物和(b)由下述通式(II)表示的聚醚化合物，
所述通式(I)中，n表示1或2，x和y分别独立地表示0、1、2或3，R1和R2分别独立地表示碳原子数为1-10的烷基，R1和R2分别存在多个时，它们也可以不同；
所述通式(II)中，m表示1-10，p表示0、1、2或3，Prop表示1，2-亚丙基，R3和R4分别独立地表示碳原子数为1-10的烷基，其中，以Prop表示的1，2-亚丙基在m为2以上时，甲基取代位置可以是任意的。
2、根据权利要求1记载的溶剂组合物，其特征在于，(a)二苯基甲烷化合物是苄基甲苯。
3、根据权利要求1或2记载的溶剂组合物，其特征在于，(b)聚醚化合物是[(2-甲氧基-1-甲基乙氧基)甲基]苯。
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| JP5420311B2 (ja) * | 2009-05-15 | 2014-02-19 | 株式会社Ａｄｅｋａ | 溶剤組成物 |
| EP2508572B1 (en) * | 2011-04-08 | 2014-06-25 | Dow Global Technologies LLC | Low/zero voc glycol ether-esters and use as clean-up solvents and paint thinners |
| DE102013007177B4 (de) * | 2013-04-24 | 2016-05-12 | Clariant International Ltd. | Benzylalkoholalkoxylate als Lösevermittler für wässrige Tensidlösungen |
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