CN100369564C - Perfume for tobacco and its preparing method - Google Patents
Perfume for tobacco and its preparing method Download PDFInfo
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- CN100369564C CN100369564C CNB2006100110115A CN200610011011A CN100369564C CN 100369564 C CN100369564 C CN 100369564C CN B2006100110115 A CNB2006100110115 A CN B2006100110115A CN 200610011011 A CN200610011011 A CN 200610011011A CN 100369564 C CN100369564 C CN 100369564C
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Abstract
The present invention is a kind of tobacco perfume and its preparation process. The tobacco perfume is prepared through the following steps: 1. crushing the materials including balloon flower root 150-250 weight portions, fritillary bulb 30-80 weight portions, root of straight lady bell 150-250 weight portions, licorice 30-80 weight portions, tuckahoe 150-250 weight portions and Dangshen 70-130 weight portions, adding water and inoculating microbe strain to ferment to obtain fermented product; and 2. extracting the fermented product with water soluble solvent, concentrating the extracted liquid to obtain tobacco perfume paste. Compared with available technology, the present invention has the advantages of the microbial fermentation process, mallow flavor and obvious cigarette modifying effect of the tobacco perfume.
Description
Technical field
The present invention relates to the preparation method of tobacco aromatics using, especially a kind ofly utilize microorganism at the Chinese herbal medicine material or contain the preparation method of tobacco aromatics using of the matrix top fermentation preparation of Chinese herbal medicine material.
Background technology
In tobacco product, fragrance of tobacco and suction flavor are vital, and providing the cigarette products of some fragrance and the satisfaction of suction flavor to the consumer is the target that the tobacco business product designer is pursued.The spices that uses in the cigarette industry has chemically composite perfume and natural perfume material.Current, along with progress of science and technology, the harm problem that people more and more pay close attention to smoking and brought, the smoker is more and more higher to the quality requirement of cigarette, and the cigarette that production toxicity is low, fragrance good, quality is high is imperative.Is the focus of tobacco industry research in recent years with the Chinese herbal medicine for the development of raw materials tobacco aromatics using; add extracts of Chinese herbal medicine in the cigarette; can make cigarette smoke exquisiteness, pleasant impression clean; can alleviate smoking to cardiovascular and murder by poisoning microcirculqtory system; and can antibechic, relieving asthma, improve immunologic function; harmfulness of smoking can be obviously alleviated, and health of smokers can be protected.Currently used cigarette mostly is the direct extract of Chinese herbal medicine with Chinese herbal medicine spices, and is that raw material adopts biofermentation technique to produce tobacco aromatics using not appear in the newspapers in the prior art with the Chinese herbal medicine.
Summary of the invention
The purpose of this invention is to provide a kind of improved preparation method who utilizes the tobacco aromatics using of Chinese herbal medicine production.The spices of producing with this method is big to perfume (or spice), the smoking quality improvement effect of cigarette, can alleviate harmfulness of smoking, and can protect health of smokers.
The present invention is achieved by the following technical solutions: tobacco aromatics using be prepare by the following method and:
Balloonflower root 150～250, the bulb of fritillary 30～80, the root of straight ladybell 150～250, Radix Glycyrrhizae 30～80, Poria cocos 150～250, Radix Codonopsis 70～130 with weight portion are raw material, directly add the water sterilization after the pulverizing, insert fermented bacterium,, form karusen 20～60 ℃ of temperature bottom fermentations 2 hours～30 days;
1. use water-soluble solvent extractive fermentation wine with dregs, extract is concentrated promptly get paste tobacco aromatics using finished product then;
2. use water-soluble solvent extractive fermentation wine with dregs, then extract is concentrated back alcohol precipitation, remove sediment, the pure paste tobacco aromatics using finished product that gets is reclaimed in evaporation;
Among the preparation method of the present invention, extracting used water-soluble solvent is the double solvents of water, alcohols or water and alcohols; Wherein said pure kind of extractants is ethanol, propane diols, and the double solvents of water and alcohols is the double solvents of water and ethanol or propane diols.
In the method for preparing tobacco aromatics using of the present invention, the fermentation strain that fermentation procedure inserts is Angel Yeast, Bacillus acidi lactici, bacillus, aspergillus oryzae, wine yeast, and bacterial classification can be bacterium song or bacterium liquid form.
Composition of raw materials of the present invention can be made up of Chinese herbal medicine fully, also can add some grain raw materials and other compound in right amount.Used grain raw material has ground rice, bean powder, potato powder, corn flour, wheat flour, and compound has inorganic salts such as starch, yeast extract, peptone, glucose, amino acid, potassium dihydrogen phosphate.
Tobacco aromatics using of the present invention and existing tobacco aromatics using are relatively, owing to adopted this biotransformation of microbial fermentation, the tobacco aromatics using of gained is more general, and with the Chinese herbal medicine to be that tobacco aromatics using that raw material is produced is modified the cigarette flavor effect obvious, have the cigarette of making aromatic and, pleasant impression is clean, reduces the effect that stimulates.
The specific embodiment
Embodiment 1:
Get balloonflower root 200g, bulb of fritillary 50g, the root of straight ladybell 200g, Radix Glycyrrhizae 50g, Poria cocos 200g, Radix Codonopsis 100g, ground rice 20g adds water 2000ml, and in 108 ℃, 0.04MP sterilized 30 minutes, and the cooling back adds Angel Yeast 50g, and 30 ℃ of fermentations got karusen in 5 days; Karusen is solvent hot reflux extracting twice with water, adds water 5000ml at every turn, 2 hours extraction times; Filter extract, concentrated extract with 3000ml 95% ethanol Hui Rong, removes by filter insoluble matter, and decompression concentrates recovery ethanol and gets fragrance product.
Embodiment 2:
Balloonflower root 150g, bulb of fritillary 30g, the root of straight ladybell 150g, Radix Glycyrrhizae 30g, Poria cocos 150g, Radix Codonopsis 70g, bean powder 10g, potato powder 10g, add water 1000ml, in 108 ℃, 0.04MP sterilize 30 minutes, the cooling back added Bacillus acidi lactici bacterium liquid 200ml, mixes, 30 ℃ of fermentations got karusen in 7 days, karusen is a solvent hot reflux extracting twice with 75% ethanol, adds ethanol 3000ml at every turn, 2 hours extraction times.Filter extract and remove insoluble matter, decompression concentrates the recovery solvent and gets fragrance product.
Embodiment 3:
Get balloonflower root 250g, bulb of fritillary 80g, the root of straight ladybell 250g, Radix Glycyrrhizae 80g, Poria cocos 250g, Radix Codonopsis 130g raw material pulverizing, with yeast extract 10g, potassium dihydrogen phosphate 2g, glucose 10g, add water 1500ml, in 108 ℃, 0.04MP sterilization 30 minutes, the cooling back adds bacillus bacterium liquid 200ml, mix, 30 ℃ of fermentations got karusen in 7 days, and karusen extracts 2 times with propane diols and water mixed liquid hot reflux, adds water 3000ml at every turn, propane diols 100g, 2 hours extraction time.Filter extract and remove insoluble matter, decompression concentrates the recovery solvent and gets fragrance product.
Embodiment 4:
Get balloonflower root 180g, bulb of fritillary 40g, the root of straight ladybell 180g, Radix Glycyrrhizae 40g, Poria cocos 180g, Radix Codonopsis 90g raw material pulverizing, wheat flour 10g, use potassium dihydrogen phosphate 1.5g, sodium hydrogen phosphate 0.3g, magnesium sulfate 0.3g, glucose 10g, amino acid 5g adds water 2000ml, in 108 ℃, 0.04MP sterilize 30 minutes, the cooling back added aspergillus oryzae bacterial classification 20g, mixes, 30～32 ℃ of fermentations got karusen in 10 days, karusen water hot reflux extraction 2 times adds water 3000ml, 2 hours extraction time at every turn, collect extract, remove by filter insoluble matter, decompression concentrates removes moisture, with 3000ml 95% ethanol Hui Rong, cross and filter out insoluble matter, decompression concentrates recovery ethanol and gets fragrance product.
Embodiment 5:
Get balloonflower root 220g, bulb of fritillary 70g, the root of straight ladybell 220g, Radix Glycyrrhizae 70g, Poria cocos 220g, Radix Codonopsis 120g raw material pulverizing, corn flour 20g, with dipotassium hydrogen phosphate 0.5g, sodium sulphate 0.5g, water 1500ml, in 108 ℃, 0.04MP sterilize 30 minutes, the cooling back adds wine yeast bacterial classification 20g, mix, 30～33 ℃ fermented 4 days, got karusen, karusen extracts 3 times with 95% alcohol heat reflux, add ethanol 3000ml at every turn, 2 hours extraction time, collect extract, remove by filter insoluble matter, decompression concentrates recovery ethanol and gets fragrance product.
Claims (4)
1. the preparation method of a tobacco aromatics using is characterized in that carrying out according to the following steps:
1) be raw material with weight portion balloonflower root 150～250, the bulb of fritillary 30～80, the root of straight ladybell 150～250, Radix Glycyrrhizae 30～80, Poria cocos 150～250, Radix Codonopsis 70～130, pulverize or directly add water and sterilize, insert fermented bacterium,, form karusen 20～60 ℃ of temperature bottom fermentations 2 hours～30 days;
2), extract is concentrated promptly get paste tobacco aromatics using finished product then with water-soluble solvent extractive fermentation wine with dregs; Or, then extract is concentrated back alcohol precipitation with water-soluble solvent extractive fermentation wine with dregs, and remove sediment, the pure paste tobacco aromatics using finished product that gets is reclaimed in evaporation.
2. the preparation method of tobacco aromatics using according to claim 1 is characterized in that extracting used water-soluble solvent and is the double solvents of water or water and ethanol, propane diols.
3. the preparation method of tobacco aromatics using according to claim 1 is characterized in that described bacterial strain is: the single culture of Angel Yeast, Bacillus acidi lactici, bacillus, aspergillus oryzae, wine yeast.
4. the preparation method of tobacco aromatics using according to claim 1 is characterized in that can adding some grain raw materials and compound in right amount in the raw material; Grain raw material has ground rice, bean powder, potato powder, corn flour, wheat flour, and compound has starch, yeast extract, peptone, glucose, amino acid, potassium dihydrogen phosphate inorganic salts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CNB2006100110115A CN100369564C (en) | 2006-07-04 | 2006-07-04 | Perfume for tobacco and its preparing method |
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| CNB2006100110115A CN100369564C (en) | 2006-07-04 | 2006-07-04 | Perfume for tobacco and its preparing method |
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| CN1899140A CN1899140A (en) | 2007-01-24 |
| CN100369564C true CN100369564C (en) | 2008-02-20 |
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| CNB2006100110115A Expired - Fee Related CN100369564C (en) | 2006-07-04 | 2006-07-04 | Perfume for tobacco and its preparing method |
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| CN101423785B (en) * | 2007-10-30 | 2011-02-23 | 武汉烟草(集团)有限公司 | Method for preparing perfume for red jujube fermentation type wine flavor cigarette |
| CN101449854B (en) * | 2008-12-30 | 2011-12-21 | 无锡华馨香精香料有限公司 | Fermentation optimization method of tobacco essence |
| CN101518358B (en) * | 2009-04-01 | 2012-01-25 | 红云红河烟草(集团)有限责任公司 | Cigarette perfume solvent and preparation method thereof |
| CN101619271B (en) * | 2009-07-02 | 2011-09-21 | 华顺香料(上海)有限公司 | Traditional Chinese medicine combination spice for cigarette as well as preparation method and application thereof |
| CN102352283A (en) * | 2011-07-19 | 2012-02-15 | 湖北中烟工业有限责任公司 | Acid flavor type tobacco Chimonanthus Praecox flavor and its preparation method |
| CN102488317B (en) * | 2011-12-23 | 2014-04-09 | 华宝食用香精香料（上海）有限公司 | Biological spice for tobacco and preparation method and use thereof |
| CN103099303A (en) * | 2013-02-04 | 2013-05-15 | 红云红河烟草(集团)有限责任公司 | Application of leavening japonica rice in improving quality of cigarette flavor |
| CN104099179B (en) * | 2014-07-23 | 2016-03-09 | 湖北中烟工业有限责任公司 | A kind of method utilizing solid phase Maillard reaction to prepare cigarette filter rod perfumed beads |
| CN104223352B (en) * | 2014-08-19 | 2016-02-24 | 云南中烟工业有限责任公司 | A kind of Radix Glycyrrhizae fermentation gained tobacco aromatics using and application thereof |
| CN104789362A (en) * | 2015-04-22 | 2015-07-22 | 湖北中烟工业有限责任公司 | Preparation method of fermentation-type buchu leaf essential oil for cigarettes |
| CN105255591A (en) * | 2015-10-09 | 2016-01-20 | 云南中烟工业有限责任公司 | Brewed spice for cigarettes and application of spice to cigarette smoking quality improvement |
| CN106136290A (en) * | 2016-07-05 | 2016-11-23 | 中国烟草总公司郑州烟草研究院 | The application in stem or reconstituted tobacco of a kind of Radix Adenophorae extract |
| CN106753790A (en) * | 2016-12-05 | 2017-05-31 | 湖北中烟工业有限责任公司 | Uniform, stable tobacco aromaticss of fragrance and preparation method thereof |
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| CN108685166A (en) * | 2018-05-25 | 2018-10-23 | 颐中（青岛）实业有限公司 | A kind of fermentation of Chinese herbal medicine filter-tip |
| CN108685160A (en) * | 2018-05-30 | 2018-10-23 | 重庆中烟工业有限责任公司 | A kind of pure tobacco oil, preparation method and electronics tobacco tar |
| CN110144260A (en) * | 2019-04-11 | 2019-08-20 | 杨伟祖 | A method of fragrance is produced using papermaking-method reconstituted tobaccos waste residue |
| CN113940443A (en) * | 2021-10-22 | 2022-01-18 | 深圳市真味生物科技有限公司 | Production method of electronic atomized liquid |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1086106A (en) * | 1992-10-23 | 1994-05-04 | 吴越东 | A kind of method for making non-toxic cigarette |
| CN1102558A (en) * | 1993-10-09 | 1995-05-17 | 珠海天元保健添加剂有限公司 | Cigarette toxicity reducing additive |
| CN1029724C (en) * | 1991-03-18 | 1995-09-13 | 杨一兵 | Making method of tobacco extract |
| CN1128637A (en) * | 1995-02-12 | 1996-08-14 | 宋书林 | Purifying agent for cigarette and mfg. method thereof |
| CN1233484A (en) * | 1998-04-30 | 1999-11-03 | 王志群 | Series health-care food for detoxication for smoking persons |
| CN1332985A (en) * | 2001-05-08 | 2002-01-30 | 李瑛� | Health care cigarette and production method thereof |
-
2006
- 2006-07-04 CN CNB2006100110115A patent/CN100369564C/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1029724C (en) * | 1991-03-18 | 1995-09-13 | 杨一兵 | Making method of tobacco extract |
| CN1086106A (en) * | 1992-10-23 | 1994-05-04 | 吴越东 | A kind of method for making non-toxic cigarette |
| CN1102558A (en) * | 1993-10-09 | 1995-05-17 | 珠海天元保健添加剂有限公司 | Cigarette toxicity reducing additive |
| CN1128637A (en) * | 1995-02-12 | 1996-08-14 | 宋书林 | Purifying agent for cigarette and mfg. method thereof |
| CN1233484A (en) * | 1998-04-30 | 1999-11-03 | 王志群 | Series health-care food for detoxication for smoking persons |
| CN1332985A (en) * | 2001-05-08 | 2002-01-30 | 李瑛� | Health care cigarette and production method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 含中草药成分造纸法再造烟叶的制备. 郑勤安等.烟草科技，第6期. 2004 * |
| 微生物技术在烟草生产上应用研究进展. 王津军等.耕作与栽培，第6期. 2004 * |
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| CN1899140A (en) | 2007-01-24 |
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