CN106136290A - The application in stem or reconstituted tobacco of a kind of Radix Adenophorae extract - Google Patents
The application in stem or reconstituted tobacco of a kind of Radix Adenophorae extract Download PDFInfo
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- CN106136290A CN106136290A CN201610518557.3A CN201610518557A CN106136290A CN 106136290 A CN106136290 A CN 106136290A CN 201610518557 A CN201610518557 A CN 201610518557A CN 106136290 A CN106136290 A CN 106136290A
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- stem
- radix adenophorae
- reconstituted tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The application in stem or reconstituted tobacco of a kind of Radix Adenophorae extract, it is characterized in that: Radix Adenophorae extract is added in stalk filaments of tobacco stalks or reconstituted tobacco, can substantially reduce xylon gas's (miscellaneous QI) and the zest of stem or reconstituted tobacco, improve stem or reconstituted tobacco mixture proportion in medium-to-high grade cigarette composition, reduce cigarette smoke tar content, reduce production of cigarettes cost, and do not affect the flue gas quality of Medicated cigarette, described Radix Adenophorae extract is with Radix Adenophorae as raw material, by solvent soaking, extract, refine, concentration technology, be prepared from.The outstanding feature of the present invention is: develops the new application of a kind of Radix Adenophorae with conventional solvent and common extracting method, is proposed a kind of new natural tobacco correctives.
Description
Technical field
The present invention relates to tobacco additive agent field, a kind of Radix Adenophorae extract answering in stem or reconstituted tobacco
With, this extract is applied in stalk filaments of tobacco stalks or reconstituted tobacco, can significantly reduce stem or the xylon gas of reconstituted tobacco and thorn
Swash property, improve stem or reconstituted tobacco mixture proportion in cigarette composition, and do not affect the flue gas quality of Medicated cigarette, and can be one
Determine the situation that in degree, after reduction smoking cigarette, respiratory tract is uncomfortable.
Background technology
The main lobe arteries and veins of cabo, i.e. Nicotiana tabacum L., accounts for the 25%～30% of Nicotiana tabacum L. weight.China is tobacco leaf production big country, the most about produces
Raw few hundred thousand tonnes of cabo.The main component of cabo is cell wall substance, accounts for more than 40%, including cellulose, hemicellulose, really
Glue and lignin etc..During cabo burning, this kind of pyrolytic cracking can produce more low-grade aldehydes, catechol, alkyl catechol
With the strong and stimulating material composition such as methanol, these composition xylon gas weight, inhale taste choke cough, puckery mouth, perfume quantity is few, has a strong impact on Medicated cigarette
Smoking quality.Therefore, cabo application percentage in cigarette composition is extremely low, and this has resulted in a large amount of cabo and has discarded, and both wastes
Natural resources, pollutes again environment, increases the production cost of Medicated cigarette the most accordingly simultaneously.But the tar content that cabo burning produces is relatively
Low, for improving cabo application percentage in cigarette composition, domestic and international tobacco has carried out numerous studies to the utilization of cabo.Mesh
The technology that front cigarette industry uses mainly has: (1) expanded cut stem technology.Under relatively high pressure, stem is dipped in certain liquid
In inflating medium, after stem cell is full of liquid swelling medium, reduce rapidly the pressure of system, the intracellular liquid of stem
Inflating medium transient evaporation, makes stem cell volume expand.After stem expands, its flammability significantly improves, and total sugar and nicotine contain
Amount reduces, and the content of cell wall substance is basically unchanged, and its zest substantially reduces, but its xylon gas is the heaviest, to mixing volume
The suction taste harmful effect of cigarette is the most more serious.Therefore, relatively low (general 5% left side of expanded cut stem adding proportion in cigarette composition
Right), in order to avoid its xylon gas brings bigger harmful effect to cigarette odor-absorbing.(2) reconstituted tobacco technology.Medicated cigarette is raw the most both at home and abroad
What product enterprise was commonly used is papermaking-method reconstituted tobaccos.Papermaking-method reconstituted tobaccos is exactly with cabo, waste tobacco leaf (fragment, offal)
Make raw material with wood pulp etc., use reconstituted tobacoo prepared by paper process.Cabo is the primary raw material of papermaking-method reconstituted tobaccos, its ratio
Account for the 50%～80% of total amount.In the production process of papermaking-method reconstituted tobaccos, the raw material such as cabo through leaching, pull an oar, sizing mixing, handsheet
With the technical process such as coating, cabo mainly provides the sheet base material that fiber and part are coated with, cabo in ordinary sheet coating medium
Extract consumption is 40%～50%.In reconstituted tobacco, although be that the physical aspect of cabo changes a lot, but it is main
The molecular structure of component cells wall material substantially changes not quite.Therefore, blending proportion is not the most in cigarette composition for reconstituted tobacco
High.(3) additive treating technology.Presently used additive mainly has 2 kinds: chemical reagent and biological preparation.At chemical reagent
Reason is through, with the process of relevant chemical reagent, removing or decompose in cabo or reconstituted tobacco certain or some harmful components, with
Improve the suction taste of cabo or reconstituted tobacco.Chemical addition agent used is more, as the eighties in 20th century abroad processes with regard to useful urea
Improve the patent of cabo smoking quality, and be used in cigarette product；Cigarette is removed by extracting with acid solution or ammonium oxalate solution
Pectin in stalk, improves the smoking quality of cabo；In stalk slurry, add potassium hydroxide contain to reduce the protein in stalk slurry
Amount, or with urea and alkali, cabo pretreatment is improved the quality of papermaking-method reconstituted tobaccos during Terrier Storage；Pass through diammonium phosphate
Salt treatment improves the content of deoxy fructosazine in cabo, and during burning, deoxy fructosazine can decompose and discharges little molecule fragrance component,
Thus the smoking quality of cabo can be improved；Processed the interior quality improving stalk filaments of tobacco stalks by solvent, current industrial mainly adopt
By " washing " technique, although this technique improves the smoking quality of stem to a certain extent, but still can not carry by a relatively large margin
The mixture proportion of high stem.It is exactly to add enzyme or microorganism in cabo that biological preparation processes, and improves stem by fermentative degradation
Smoking quality.Enzyme used has pectase, amylase, lignoenzyme, saccharifying enzyme and cellulase etc., and microorganism used has
Aspergillus niger, and by the bacterial strain etc. separated on Nicotiana tabacum L., improve the property of stem extracting solution with enzyme, microorganism and Maillard reaction
Matter, improves the utilization rate of reconstituted tobacco.
Radix Adenophorae, another name adenophora tetraphylla, Radix Adenophorae (Radix Glehniae), bubble ginseng, bubble Radix Adenophorae (Radix Glehniae), for campanulaceae Lady bell herbaceos perennial.Its
Be born in hill Schattenseite thick grass more, border or roadside, be distributed widely in northeast and Hebei, Shandong, Shanxi, Jiangsu, the peace of China
The ground such as emblem, Zhejiang, Jiangxi, Guangdong, Guizhou, Yunnan.It is used as medicine with root.Autumn, plane was adopted, and removed aerial parts and fibrous root, scraped off thick
Skin, dries immediately.Its sweet in the mouth, hardship, cold nature, have clearing away heat and nourishing YIN, nourishing the lung to arrest cough, the effects such as QI invigorating is reduced phlegm, reinforcing stomach reg fluid, main
Control tracheitis, pertussis, cough due to lung-heat, cough up phlegm yellow thick.Modern study shows, Radix Adenophorae contains polysaccharide, reducing sugar, triterpene, phenolic acid
And the composition such as glycoside, sterols, phospholipid, glucosides, aminoacid and trace element, have enhancing immunity, remove free radical,
Relieving cough and expelling phlegm, expand blood vessel, improve microcirculation, antibacterial, protection hepatocyte, strengthen the effect such as hemopoietic function.At present, Nansha is related to
The application in Medicated cigarette of the Chinese herbal medicine formula of ginseng has been reported [CN201110304512.3；CN200510033644.1], but,
About Radix Adenophorae extract application in cabo or reconstituted tobacco, there is not been reported.
Summary of the invention
A kind of Radix Adenophorae extract that the purpose of the present invention is developed for the problem that presently, there are just is at stem or again
Make the application in Nicotiana tabacum L., Radix Adenophorae extract is applied in stalk filaments of tobacco stalks or reconstituted tobacco, stem or again can be significantly reduced
Make xylon gas and the zest of Nicotiana tabacum L., improve stem or reconstituted tobacco mixture proportion in cigarette composition, and do not affect Medicated cigarette
Flue gas quality.
It is an object of the invention to be achieved through the following technical solutions: a kind of Radix Adenophorae extract at stem or reproduces cigarette
Application in leaf, adds Radix Adenophorae extract in stalk filaments of tobacco stalks or reconstituted tobacco, can significantly reduce stem or reconstituted tobacco
Xylon gas and zest, improve stem or reconstituted tobacco mixture proportion in medium-to-high grade cigarette composition, and do not affect Medicated cigarette
Flue gas quality.Wherein said Radix Adenophorae extract is with Radix Adenophorae as raw material, by solvent soaking, extracts, refines, concentrates work
Skill, is prepared from.Concrete preparation process is: a. solvent soaking, extraction prepare Radix Adenophorae extracting solution；B. extracting solution is at room temperature
Be centrifuged successively, microfiltration and Ultra filtration membrane；C. the ultrafiltration permeate obtained by membrance separation concentrates and i.e. obtains Radix Adenophorae extraction
Thing.
Described Radix Adenophorae is the Radix Adenophorae powder after dry Chinese crude drug Radix Adenophorae root section or pulverizing.
Described Extraction solvent is mixed by the solvent of following mass percent and forms: water 50% ~ 100%, ethanol 0% ~ 50%, the third two
Alcohol 0% ~ 10%.
Described extraction process is left at room temperature immersion, mechanical oscillation, ultrasound-assisted extraction, heating and refluxing extraction, micro-
Ripple auxiliary extraction, preferably left at room temperature soak and heating and refluxing extraction combines.
Described process for refining be extracting solution centrifugal after carry out microfiltration and ultra-filtration and separation, the membrane aperture that micro-filtration membrane separates is 50 ~
200 nm, collect microfiltration permeate, further Ultra filtration membrane, and ultrafilter membrane aperture is 5 ~ 30 kD, preferably 5 ~ 10 kD, receive
Collection ultrafiltration permeate.
Described concentration technology is distillation and concentration or decompression distillation and concentration under normal pressure, and preferably reduce pressure distillation and concentration, is concentrated into
Soluble solid content is about 20%.
The consumption of Radix Adenophorae extract is stem or the 0.1% ~ 1.0% of reconstituted tobacco quality, preferably 0.3% ~ 0.8%, make
In used time use water, ethanol, propylene glycol any one or two or more by a certain percentage mixed solvent dilution after as cabo
Stem adds feed liquid or reconstituted tobacco coating fluid uses.After balance, technique and tobacco shred blending make Medicated cigarette routinely.
The outstanding feature of the present invention is: develop the new of a kind of Radix Adenophorae with conventional solvent and common extracting method
Purposes, is proposed a kind of new natural tobacco correctives Radix Adenophorae extract, wherein rich in saccharide, Polyphenols, glucosides class
Deng Multiple components, carbohydrate content is to promoting stem and aroma quality time reconstituted tobacco burns and sucks, rich and comfortableness etc. have bigger
Effect；Miscellaneous QI when phenolic acid can significantly reduce stem and reconstituted tobacco burns and sucks and zest, make fragrance richness and
Total tune increases；Glycosides class material can increase fragrance as flavor precursor when burning and sucking.The preparation of the present invention
Technique is extracted these effective ingredient in Radix Adenophorae pointedly, and effectively eliminates the egg in crude extract by membrane separation technique
White matter, starch etc. have the macromolecular substances of side effect to Medicated cigarette sense organ, are enriched effective ingredient further simultaneously.Radix Adenophorae extracts
Thing is together with feed liquid or is applied individually to any in stem or reconstituted tobacco, can reduce stalk filaments of tobacco stalks or reconstituted tobacco xylon gas and
Zest, improves stem or reconstituted tobacco blending proportion in cigarette composition tobacco shred, reduces cigarette smoke tar content, reduces volume
Cigarette production cost, without bringing harmful effect to cigarette odor-absorbing.The present invention does not change the original performance of Medicated cigarette and processing technique.Raw
The abundant raw material producing Radix Adenophorae extract is easy to get, and production technology is simple to operation, and production cost is relatively low, has the valency of actual application
Value.
Radix Adenophorae is that inventor passes through a large amount of different Chinese medicine extract one by one as correctives application on cabo
Interpolation in stem and reconstituted tobacco smokes panel test what test found, is in the repeatedly different extraction of Chinese herbal medicine, examinations of adding and smoke panel test
Draw on the basis of testing.
Specific embodiments
The present invention is described in further detail below with reference to example, but is not limiting as the present invention.
Embodiment 1:
Take the Radix Adenophorae root powder that 400 g are dried, add 4000 mL water, under room temperature, soak 2 h, use ultrasonic and circulated extraction machine
Extraction, ultrasonic frequency 45 kHz, power 750 W, to extract total time 40 min, ultrasonic time and interval time are 2 s/1 s,
Mixing speed 1300 r/min.Extraction is filtered after terminating, and filtering residue repeats to extract 2 times with commensurability water under similarity condition, merges 3
Secondary extracting solution, centrifugal 20 min under 4000 r/min, supernatant after the micro-filtrate membrane filtration of membrane aperture 200 nm again with retaining
Molecular weight is the ultrafiltration membrance filter of 10 kD, and it is 20% i.e. to obtain sky that permeate is concentrated into soluble solid content in evaporated under reduced pressure
So cigarette correctives I.
Correctives I is diluted, according to reconstituted tobacco quality with the mixed solvent of suitable quantity of water, propylene glycol (9:1, mass ratio)
Correctives I is added in reconstituted tobacco coating fluid by the use ratio of 0.8%, is applied in reconstituted tobacco chip base after mix homogeneously,
Papermaking-method reconstituted tobaccos finished product is obtained after drying.To mix roasting by the ratio uniform ground of 5% (mass fraction) after reconstituted tobacco shredding
During tobacco type of cigarette cuts filler, compare and join for interpolation 5% Virginian-type cigarette of the same race without correctives process reconstituted tobacco silk of the same race
Side's tobacco shred.Medicated cigarette is rolled into by conventional method.Medicated cigarette balances 48 in temperature (22 ± 1) DEG C and relative humidity (60 ± 2) % environment
H, takes out, and by Medicated cigarette, the group of smokeing panel test smokes panel test.Result (table 1) shows, with the Medicated cigarette added without correctives process reconstituted tobacco silk
Comparing, the cigarette smoke xylon gas (miscellaneous QI) adding the reconstituted tobacco silk that correctives I processes substantially alleviates, and zest substantially drops
Low, aroma quality and perfume quantity all have a certain degree of improvement.
The aesthetic quality of table 1, comparison Medicated cigarette and test Medicated cigarette contrasts smoking result
| Cigarette sample | Gloss (5) | Fragrance (32) | Harmony (6) | Miscellaneous QI (12) | Zest (20) | Pleasant impression (25) | Add up to |
| Comparison Medicated cigarette | 5.00 | 27.35 | 5.00 | 10.20 | 16.35 | 21.25 | 85.15 |
| Test Medicated cigarette | 5.00 | 27.80 | 5.00 | 10.50 | 16.75 | 21.50 | 86.55 |
Embodiment 2
Take the Radix Adenophorae root section that 50 g are dried, add 500 mL 30% ethanol, soak 2 h under room temperature, be heated to reflux 0.5 h,
Filtering, filtering residue repeats to extract 2 times with 30% commensurability ethanol under similarity condition, merges 3 extracting solution, under 4000 r/min
Centrifugal 20 min, supernatant after the micro-filtrate membrane filtration of membrane aperture 50 nm again with the ultrafiltration membrance filter that molecular cut off is 5 kD,
Permeate distillation and concentration to soluble solid content under normal pressure is 20% i.e. to obtain natural tobacco correctives II.
Take natural tobacco correctives II 3 g, with 10 g 30% ethanol dilutions, diluent is sprayed equably that to be added in 1 kg swollen
In swollen stem, process stem and seal, place 6 h at room temperature, mix fire-cured tobacco type volume by the ratio uniform ground of 5% (mass fraction)
During cigarette cuts filler, compare and cut filler for the Virginian-type cigarette of the same race adding 5% untreated expanded cut stem of the same race.Use routine side
Method rolls into Medicated cigarette.Medicated cigarette balances 48 h in temperature (22 ± 1) DEG C and relative humidity (60 ± 2) % environment, takes out, by Medicated cigarette
The group of smokeing panel test smokes panel test.Result (table 2) shows, compared with the Medicated cigarette adding untreated expanded cut stem, adds correctives II and processes swollen
The cigarette smoke xylon gas (miscellaneous QI) of swollen stem substantially alleviates, and zest substantially reduces, fragrance level and note is rich
Determine the improvement of degree.
The aesthetic quality of table 2, comparison Medicated cigarette and test Medicated cigarette contrasts smoking result
| Cigarette sample | Gloss (5) | Fragrance (32) | Harmony (6) | Miscellaneous QI (12) | Zest (20) | Pleasant impression (25) | Add up to |
| Comparison Medicated cigarette | 5.00 | 27.60 | 5.00 | 10.40 | 16.50 | 21.35 | 85.85 |
| Test Medicated cigarette | 5.00 | 28.05 | 5.00 | 10.65 | 17.00 | 21.60 | 87.30 |
Embodiment 3
Take the Radix Adenophorae root powder that 400 g are dried, add 4000 mL water, ethanol and the mixed solvent of 1,2-PD, water, second
The mass percent of alcohol and 1,2-PD is respectively under 50%, 45% and 5%, room temperature soaks 2 h, ultrasound-assisted extraction 1 h,
Ultrasonic frequency 45 kHz, power 750 W, ultrasonic time and interval time are 2 s/1 s, mixing speed 1400 r/min.Cross
Filter, filtering residue repeats to extract under similarity condition 2 times with the combination water of ratio, ethanol and 1,2-PD mixed solution with commensurability, closes
And 3 extracting solution, centrifugal 20 min under 4000 r/min, supernatant is used after the micro-filtrate membrane filtration of membrane aperture 100 nm again and is cut
The ultrafiltration membrance filter staying molecular weight to be 8 kD, permeate is concentrated into soluble solid content in evaporated under reduced pressure and is 20% and get final product
Natural tobacco correctives III.
(1) according to the use ratio of reconstituted tobacco quality 0.5%, correctives I is added in reconstituted tobacco coating fluid, mixing
It is applied to after Jun Yun in reconstituted tobacco chip base, after drying, obtains papermaking-method reconstituted tobaccos finished product.(2) natural tobacco correctives III is taken
5 g, with the mixed solvent dilution of 10 g 50% ethanol and propylene glycol (9:1, mass ratio), diluent sprays that to be added in 1 kg swollen equably
In swollen stem, process stem and seal, place 6 h at room temperature.By the reconstituted tobacco silk obtained in (1) and (2) and stem respectively by
The ratio uniform ground of 3% (mass fraction) mixes during Virginian-type cigarette cuts filler, compare into add 3% of the same race without correctives at
The Virginian-type cigarette of the same race of reason reconstituted tobacco silk and stem cuts filler.Medicated cigarette is rolled into by conventional method.Medicated cigarette is in temperature (22
± 1) DEG C and balancing 48 h in relative humidity (60 ± 2) % environment, take out, by Medicated cigarette, the group of smokeing panel test smokes panel test.Result (table 3) shows,
Compared with adding the Medicated cigarette processing reconstituted tobacco silk and stem without correctives, add reconstituted tobacco silk that correctives III processes and
The cigarette smoke xylon gas (miscellaneous QI) of stem substantially alleviates, and zest substantially reduces, and aroma quality and perfume quantity all have to a certain degree
Improvement.
The aesthetic quality of table 3, comparison Medicated cigarette and test Medicated cigarette contrasts smoking result
| Cigarette sample | Gloss (5) | Fragrance (32) | Harmony (6) | Miscellaneous QI (12) | Zest (20) | Pleasant impression (25) | Add up to |
| Comparison Medicated cigarette | 5.00 | 27.72 | 5.00 | 10.45 | 16.60 | 21.50 | 86.27 |
| Test Medicated cigarette | 5.00 | 28.10 | 5.00 | 10.65 | 17.05 | 21.80 | 87.60 |
Claims (10)
1. the Radix Adenophorae extract application in stem or reconstituted tobacco, it is characterised in that: Radix Adenophorae extract is added
In stalk filaments of tobacco stalks or reconstituted tobacco, stem or the xylon gas of reconstituted tobacco and zest can be significantly reduced, improve stem or again
Make Nicotiana tabacum L. mixture proportion in medium-to-high grade cigarette composition, reduce cigarette smoke tar content, reduction production of cigarettes cost, and not shadow
Ringing the flue gas quality of Medicated cigarette, described Radix Adenophorae extract is with Radix Adenophorae as raw material, by solvent soaking, extracts, refines, concentrates
Technique, is prepared from.
The Radix Adenophorae extract the most according to claim 1 application in stem or reconstituted tobacco, it is characterised in that: described
Radix Adenophorae is the Radix Adenophorae powder after dry Chinese crude drug Radix Adenophorae root section or pulverizing.
The Radix Adenophorae extract the most according to claim 1 application in stem or reconstituted tobacco, it is characterised in that: described
Extraction solvent is mixed by the solvent of following mass percent and forms: water 50% ~ 100%, ethanol 0% ~ 50%, propylene glycol 0% ~ 10%.
The Radix Adenophorae extract the most according to claim 1 application in stem or reconstituted tobacco, it is characterised in that: described
Extraction process is left at room temperature immersion, mechanical oscillation, ultrasound-assisted extraction, be heated to reflux, microwave auxiliary extraction.
5. according to the application in stem or reconstituted tobacco of the Radix Adenophorae extract described in claim 1 or 4, it is characterised in that:
Described extraction process is that left at room temperature soaks and is heated to reflux extraction combination.
The Radix Adenophorae extract the most according to claim 1 application in stem or reconstituted tobacco, it is characterised in that: described
Process for refining is centrifugal, microfiltration and combining ultrafiltration.
The Radix Adenophorae extract the most according to claim 1 application in stem or reconstituted tobacco, it is characterised in that: described
Concentration technology is distillation and concentration or decompression distillation and concentration under normal pressure, is concentrated into soluble solid content and is about 20%.
8. according to the application in stem or reconstituted tobacco of the Radix Adenophorae extract described in claim 1 or 7, it is characterised in that:
Described concentration technology is decompression distillation and concentration.
The Radix Adenophorae extract the most according to claim 1 application in stem or reconstituted tobacco, it is characterised in that: Nansha
The consumption of conopsea extraction is stem or the 0.1% ~ 1% of reconstituted tobacco quality, any one in use water, ethanol, propylene glycol during use
It is applied to stalk filaments of tobacco stalks or reconstituted tobacco after kind or the dilution of two or more mixed solvents.
The Radix Adenophorae extract the most according to claim 9 application in stem or reconstituted tobacco, it is characterised in that: south
The consumption of Radix Adenophorae (Radix Glehniae) extract is stem or the 0.3% ~ 0.8% of reconstituted tobacco quality.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610518557.3A CN106136290A (en) | 2016-07-05 | 2016-07-05 | The application in stem or reconstituted tobacco of a kind of Radix Adenophorae extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610518557.3A CN106136290A (en) | 2016-07-05 | 2016-07-05 | The application in stem or reconstituted tobacco of a kind of Radix Adenophorae extract |
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| CN106136290A true CN106136290A (en) | 2016-11-23 |
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| CN201610518557.3A Pending CN106136290A (en) | 2016-07-05 | 2016-07-05 | The application in stem or reconstituted tobacco of a kind of Radix Adenophorae extract |
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| CN1899140A (en) * | 2006-07-04 | 2007-01-24 | 云南瑞升烟草技术（集团）有限公司 | Perfume for tobacco and its preparing method |
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Application publication date: 20161123 |