CN106235375A - A kind of method of the suncured tabacco reconstituted tobacco manufacturing applicable flue-cured tobacco local flavor - Google Patents
A kind of method of the suncured tabacco reconstituted tobacco manufacturing applicable flue-cured tobacco local flavor Download PDFInfo
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- CN106235375A CN106235375A CN201610763252.9A CN201610763252A CN106235375A CN 106235375 A CN106235375 A CN 106235375A CN 201610763252 A CN201610763252 A CN 201610763252A CN 106235375 A CN106235375 A CN 106235375A
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- Prior art keywords
- tobacco
- suncured tabacco
- flue
- cured
- cured tobacco
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Links
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 134
- 241000208125 Nicotiana Species 0.000 title claims abstract description 126
- 238000000034 method Methods 0.000 title claims abstract description 45
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 14
- 235000019634 flavors Nutrition 0.000 title claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- 238000002360 preparation method Methods 0.000 claims abstract description 30
- 102000004190 Enzymes Human genes 0.000 claims abstract description 23
- 108090000790 Enzymes Proteins 0.000 claims abstract description 23
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 20
- 238000000605 extraction Methods 0.000 claims abstract description 19
- 150000001875 compounds Chemical class 0.000 claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 15
- 239000011248 coating agent Substances 0.000 claims abstract description 11
- 238000000576 coating method Methods 0.000 claims abstract description 11
- 239000012530 fluid Substances 0.000 claims abstract description 7
- 238000004537 pulping Methods 0.000 claims abstract description 3
- 239000000463 material Substances 0.000 claims description 49
- 239000007788 liquid Substances 0.000 claims description 23
- 229940088598 enzyme Drugs 0.000 claims description 22
- 235000019504 cigarettes Nutrition 0.000 claims description 16
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 14
- 238000000926 separation method Methods 0.000 claims description 13
- 239000007787 solid Substances 0.000 claims description 13
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 12
- 244000061176 Nicotiana tabacum Species 0.000 claims description 11
- 229940024606 amino acid Drugs 0.000 claims description 10
- 235000001014 amino acid Nutrition 0.000 claims description 10
- 150000001413 amino acids Chemical class 0.000 claims description 10
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 7
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 claims description 6
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims description 6
- 239000012634 fragment Substances 0.000 claims description 6
- 239000004310 lactic acid Substances 0.000 claims description 6
- 235000014655 lactic acid Nutrition 0.000 claims description 6
- 239000002002 slurry Substances 0.000 claims description 6
- 239000000758 substrate Substances 0.000 claims description 6
- 238000010009 beating Methods 0.000 claims description 5
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 4
- 108010059892 Cellulase Proteins 0.000 claims description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 3
- 239000004471 Glycine Substances 0.000 claims description 3
- ONIBWKKTOPOVIA-BYPYZUCNSA-N L-Proline Chemical compound OC(=O)[C@@H]1CCCN1 ONIBWKKTOPOVIA-BYPYZUCNSA-N 0.000 claims description 3
- DCXYFEDJOCDNAF-REOHCLBHSA-N L-asparagine Chemical compound OC(=O)[C@@H](N)CC(N)=O DCXYFEDJOCDNAF-REOHCLBHSA-N 0.000 claims description 3
- OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 claims description 3
- ONIBWKKTOPOVIA-UHFFFAOYSA-N Proline Natural products OC(=O)C1CCCN1 ONIBWKKTOPOVIA-UHFFFAOYSA-N 0.000 claims description 3
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 claims description 3
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 claims description 3
- 229940106157 cellulase Drugs 0.000 claims description 3
- 239000008103 glucose Substances 0.000 claims description 3
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 claims description 3
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 2
- AGPKZVBTJJNPAG-WHFBIAKZSA-N L-isoleucine Chemical compound CC[C@H](C)[C@H](N)C(O)=O AGPKZVBTJJNPAG-WHFBIAKZSA-N 0.000 claims description 2
- 239000001110 calcium chloride Substances 0.000 claims description 2
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 2
- 235000021466 carotenoid Nutrition 0.000 claims description 2
- 150000001747 carotenoids Chemical class 0.000 claims description 2
- 230000007062 hydrolysis Effects 0.000 claims description 2
- 238000006460 hydrolysis reaction Methods 0.000 claims description 2
- 229960000310 isoleucine Drugs 0.000 claims description 2
- AGPKZVBTJJNPAG-UHFFFAOYSA-N isoleucine Natural products CCC(C)C(N)C(O)=O AGPKZVBTJJNPAG-UHFFFAOYSA-N 0.000 claims description 2
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 2
- 238000007654 immersion Methods 0.000 claims 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 6
- 239000003546 flue gas Substances 0.000 abstract description 6
- 229920002472 Starch Polymers 0.000 abstract description 4
- 238000002156 mixing Methods 0.000 abstract description 4
- 239000001814 pectin Substances 0.000 abstract description 4
- 235000010987 pectin Nutrition 0.000 abstract description 4
- 229920001277 pectin Polymers 0.000 abstract description 4
- 235000018102 proteins Nutrition 0.000 abstract description 4
- 102000004169 proteins and genes Human genes 0.000 abstract description 4
- 108090000623 proteins and genes Proteins 0.000 abstract description 4
- 235000019698 starch Nutrition 0.000 abstract description 4
- 239000008107 starch Substances 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 4
- 229920002521 macromolecule Polymers 0.000 abstract description 3
- 239000002243 precursor Substances 0.000 abstract description 3
- 239000012141 concentrate Substances 0.000 abstract description 2
- 150000003384 small molecules Chemical class 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract 2
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 abstract 1
- 239000000284 extract Substances 0.000 description 13
- 239000003205 fragrance Substances 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000013068 control sample Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 102000005593 Endopeptidases Human genes 0.000 description 4
- 108010059378 Endopeptidases Proteins 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000011269 tar Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 2
- 102000018389 Exopeptidases Human genes 0.000 description 2
- 108010091443 Exopeptidases Proteins 0.000 description 2
- 238000007705 chemical test Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 238000003359 percent control normalization Methods 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229940089401 xylon Drugs 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 102000004400 Aminopeptidases Human genes 0.000 description 1
- 108090000915 Aminopeptidases Proteins 0.000 description 1
- 102000057297 Pepsin A Human genes 0.000 description 1
- 108090000284 Pepsin A Proteins 0.000 description 1
- 102000001253 Protein Kinase Human genes 0.000 description 1
- 102000004142 Trypsin Human genes 0.000 description 1
- 108090000631 Trypsin Proteins 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- 235000019506 cigar Nutrition 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 230000008094 contradictory effect Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000003760 hair shine Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 229920005610 lignin Polymers 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 229940111202 pepsin Drugs 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 108060006633 protein kinase Proteins 0.000 description 1
- 238000001303 quality assessment method Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 239000012588 trypsin Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
Abstract
The present invention provides a kind of method of suncured tabacco reconstituted tobacco manufacturing applicable flue-cured tobacco local flavor.Described suncured tabacco reconstituted tobacco is that the extracting solution mixing concentration that the suncured tabacco extracting solution that carries of tobacco water and flue-cured tobacco cabo water carry is made coating fluid, paper process is used to laminate, then by coating solution on thin slice after being mixed by the filtering residue that the filtering residue that suncured tabacco tobacco water carries carries with flue-cured tobacco cabo water water lift；And water carries, concentrates and be separately added into special compound enzymic preparation and auxiliary agent in pulping process.The present invention utilizes the macromolecular substances such as protein, pectin and starch too much in special enzyme group degraded suncured tabacco raw material, produces a large amount of small-molecule substance and flavor precursors thing, improves extraction efficiency simultaneously, the miscellaneous QI produced after reducing reconstituted tobacco burning and zest；In concentration process more fragrant by all kinds of products, flavouring reacts, and promotes reconstituted tobacco flavouring essence quality, increases flue gas gratification and harmony.
Description
Technical field
The present invention relates to the production method of the papermaking-method reconstituted tobaccos of tobacco industry, produced especially by reconstituted tobacco
Journey is added enzyme decompose the macromole in suncured tabacco (mainly Dark sun-cured) raw material and promote coating fluid flavouring, improve suncured tabacco
Reconstituted tobacco quality, promotes its suitability in Virginian-type cigarette product.
Background technology
The Nicotiana tabacum L. of suncured tabacco utilizes sunlight to modulate, and mainly has Dark sun-cured and Sun cured tobacco.General Sun cured tobacco external appearance characteristic and contained
Chemical composition is close with flue-cured tobacco, and Dark sun-cured is then bigger with flue-cured tobacco difference.The blade of Dark sun-cured is the most less, and mesophyll is thicker, point
Secondary gather or once gather, many in dark brown or puce after dry in the sun, best with top leaf quality；The general sugar content of Nicotiana tabacum L. is relatively
Low, protein and nicotine content are higher, and smoke is dense, and strength is big.Suncured tabacco is pipe tobacco, shredded tobacco for water pipes, Medicated cigarette in this world, is also as cigar
Core leaf, Shu Ye and Folium Nicotianae preparatum, the raw material of chewing tobacco, additionally, some suncured tabacco can also be processed into insecticide.
The major country producing suncured tabacco in the world is the nations of China and India.There is suncured tabacco plantation each province of China, but is distributed scattered,
Have Sichuan, Guizhou, Hubei, Guangdong, Hunan, Yunnan, Jilin, Shandong, the Shaanxi etc. relatively concentrated save.Suncured tabacco, especially shines red
Cigarette, tobacco leaf ingredient and flue gas style differ bigger with flue-cured tobacco, it is impossible to the tobacco leaf formulation directly as Virginian-type cigarette uses, even if
It is prepared as reconstituted tobacco, it is also difficult to the requirement in gratification official face.At present, most research topics concentrate on utilize physical method and
Technological transformation, a small amount of suncured tabacco is mixed flue-cured tobacco fragment, unqualified and cabo, is prepared as reconstituted tobacco.This kind of technology pattern reduces suncured tabacco
Breath effect is limited, and the loss of reconstituted tobacco cigarette perfume (or spice) can be caused serious.
State Tobacco Monopoly Bureau requires that each Cigarette Industrial Enterprise constantly promotes low-coke tar cigarette and develops, but Medicated cigarette " low tar,
Less harmful " there is certain contradictory relation with " high fragrance ", reduce tar content in cigarette, it will usually make suction taste weaken, fragrance not
Foot.Dark sun-cured fragrance is dense, and strength is big, develops a kind of papermaking-method reconstituted tobaccos product with Dark sun-cured style and features, is playing
Improve fragrance level while lowering harm and decreasing coking effect and flue gas is rich.By reconstituted tobacco, on the one hand realize Medicated cigarette low tar,
The design requirement of high fragrance, on the other hand widens reconstituted tobacco raw material range, solves the product cigarette based on Virginian-type cigarette
Raw material sources problem in grass company.
Summary of the invention
Present invention aims to suncured tabacco and become, with cured tobacco leaf, the difference being grouped into, utilize compound enzyme (enzyme alive 2～10
Ten thousand U) etc. biotechnology combine the reaction of natural product perfume (or spice), it is provided that a kind of a kind of manufacture with suncured tabacco as primary raw material is suitable for flue-cured tobacco local flavor
Suncured tabacco reconstituted tobacco preparation method.The present invention on the premise of not increase equipment, integrated use biological and chemical technology, promote
The production suitability of suncured tabacco raw material, promotes reconstituted tobacco quality and functional use value, and it is several latent to reduce main flume
Content in harmful components.
The technical scheme that the present invention provides is: a kind of method of suncured tabacco reconstituted tobacco manufacturing applicable flue-cured tobacco local flavor, it is special
Levy and be to specifically comprise the following steps that
(1), suncured tabacco tobacco is added in raw material extraction pot in temperature 45-according to the ratio of solid-liquid ratio 1:4-7 with water
Under conditions of 65 DEG C, water carries 25-45 minute；And during extracting, in head tank, add compound enzymic preparation and auxiliary agent, described multiple
In synthase preparation, to account for the percentage ratio of suncured tabacco tobacco quality as follows for every kind of enzyme:
(2), flue-cured tobacco stalk material is added in another raw material extraction pot according to the ratio of solid-liquid ratio 1:2-4, in temperature with water
Under conditions of 55-75 DEG C, water carries 25-45 minute；And during extracting, in head tank, add compound enzymic preparation and auxiliary agent, institute
Stating in compound enzymic preparation every kind of enzyme, to account for the percentage ratio of flue-cured tobacco stalk material quality as follows:
Cellulase 0～0.10%
Pectase 0.05%～0.15%
Saccharifying enzyme 0.05%～0.15%
(3), by solid-liquid separation after the extracting solution obtained of solid-liquid separation after hydrolysis in step (1) and water body in step (2)
The extracting solution that obtains merges, and carries out concentrating under reduced pressure and prepare coating fluid, the process of its concentrating under reduced pressure and existing thin slice coating fluid
Preparation method is identical, adds propylene glycol, reducing sugar and aminoacid, also added mix preparation further during concentrating under reduced pressure
With acidity Control agent, it is as follows that the concrete material added accounts for the percentage ratio of suncured tabacco tobacco gross weight in step (1):
(4), solid-liquid after the solid matter obtained of solid-liquid separation after water body in step (1) and water body in step (2) is divided
Merging making beating from the solid matter obtained, it is identical that methods of beating prepares methods of beating with existing thin slice, and pulping process is to tobacco pulp
Middle addition reducing sugar and aminoacid, it is as follows that the concrete material added accounts for the percentage ratio of suncured tabacco tobacco gross weight in step (1):
(5), papermaking-method reconstituted tobaccos normal procedure is used to carry out manufacturing paper with pulp by the slurry in step (4) and obtain reconstituted tobacco base
Sheet, then by the coating solution of concentration in step (3) to reconstituted tobacco substrate, is dried and makes reconstituted tobacco；Described
The process manufactured paper with pulp and be coated with is all identical with existing preparation of sections process.
The present invention preferably technical scheme: the auxiliary agent added in step (1) accounts for the percentage of suncured tabacco tobacco quality such as
Under:
Lactic acid 0～0.5%
Sodium carbonate 0～0.5%
Magnesium chloride or calcium chloride 0～0.2%
The percentage ratio that the auxiliary agent added in step (2) accounts for flue-cured tobacco stalk material quality is as follows:
Lactic acid 0～0.5%
Sodium carbonate 0～0.5%
Auxiliary agent in described step (1) and step (2) plays regulation pH value and the effect of kinase, it is generally the case that cigarette
Grass extracting solution is weak acid partial neutral, can be added without regulating the auxiliary agent of acidity.
Heretofore described endopeptidase includes the existing endopeptidase such as microorganism endopeptidase, pepsin, trypsin all
Of course, exopeptidase includes that all of amino peptidase, endopeptidase and amino exopeptidase all can use the product directly bought in market
Product.
The present invention preferably technical scheme: described suncured tabacco tobacco is carrying out before water carries, and adds its weight 2-2.5 times
Water soak 5-10 minute under conditions of 65-75 DEG C.
The present invention preferably technical scheme: described suncured tabacco tobacco material include Dark sun-cured Nicotiana tabacum L., Dark sun-cured tobacco leaf fragment,
A kind of or the most several in Dark sun-cured offal, Sun cured tobacco Nicotiana tabacum L., Sun cured tobacco tobacco leaf fragment, Sun cured tobacco offal.
As the method that the preparation method of reconstituted tobacco of the present invention prepares reconstituted tobacoo with existing paper process, successively
Including extraction, solid-liquid separation, pull an oar, manufacture paper with pulp, be coated with and drying process, in the present invention extraction be by suncured tabacco Nicotiana tabacum L. and end material with bake
Cigarette cabo material is respectively adopted extractor and extracts, and is separately added into different compound enzymic preparations and auxiliary agent (bag in extraction process
Include lactic acid, citric acid, catalyst) join in tobacco soak, under controlled heat environment, enzyme is to the albumen in tobacco
The macromole such as matter, pectin, lignin, starch carry out enzymolysis, meanwhile, under the effect of catalyst, part macromole and enzymolysis are produced
Thing be changed into flavouring produce perfume reaction precursor, and carry out flavouring produce perfume reaction (include Maillard reaction, organic acid acidifying, ammonia
Change reaction etc.).
The inventive method also can operate with any one routine reconstituted tobacco manufacture (mainly include roll-in method, thick paste method,
Paper process etc.) in production process, but for papermaking-method reconstituted tobaccos best results.
This technology utilizes enzyme preparation to reduce the macromolecular substances such as starch in suncured tabacco, pectin, protein targetedly, in conjunction with raw
Thing chemical reaction, flavouring upgrading, can fundamentally improve suncured tabacco flue gas unfavorable breath many to Virginian-type cigarette.This technical side
The reconstituted tobacco that method produces compared with traditional product, have xylon gas cover thoroughly, fragrance compared with enough, the advantage such as zest is little, more
Add the low evil of low Jiao.
The technical scheme is that and utilize in special enzyme group degraded suncured tabacco raw material materials such as () Nicotiana tabacum L., offal, fragments
The macromolecular substances such as too much protein, pectin and starch, produce a large amount of small-molecule substance and flavor precursors thing, carry simultaneously
High extraction efficiency, the miscellaneous QI produced after reducing reconstituted tobacco burning and zest；In concentration process more fragrant by all kinds of products,
Flavouring reacts, and promotes reconstituted tobacco flavouring essence quality, increases flue gas gratification and harmony, promotes suncured tabacco reconstituted tobacco and joins at flue-cured tobacco
The suitability in side and usage ratio.
Specific implementation method
Below in conjunction with embodiment, the specific embodiment of the invention is described in further detail.
Embodiment one: use the method in the present invention respectively Dark sun-cured end material and flue-cured tobacco stalk material to be extracted, and with not
The suncured tabacco offal material extracting solution and the flue-cured tobacco stalk material extracting solution that add compound enzymic preparation contrast, specific as follows:
(1) extraction of Dark sun-cured offal material: Dark sun-cured offal material is added raw material with water according to the ratio of solid-liquid ratio 1:4.5
In extraction pot, and putting into compound enzymic preparation and auxiliary agent in whipping process, under conditions of temperature 45-65 DEG C, water carries 25-45 and divides
Clock, then solid-liquid separation obtains extract and Dark sun-cured offal material solids, the compound enzymic preparation of input of Dark sun-cured offal material
With auxiliary agent shared by Dark sun-cured offal material percentage by weight as shown in table 1 below:
The enzyme preparation adding proportion table of table 1 Dark sun-cured offal material case study on implementation
The extraction of comparison Dark sun-cured offal material: Dark sun-cured offal material is added former with water according to the ratio of solid-liquid ratio 1:4.5
In material extraction pot, after under conditions of temperature 45-65 DEG C, water carries 25-45 minute, solid-liquid separation obtains compareing Dark sun-cured offal material
Extract.
Respectively the Dark sun-cured end in above-mentioned five embodiments is expected solid content (the papermaking-method reconstituted tobaccos production row of extract
Industry detection the total component content of extract a kind of Testing index) and Baume degrees (B precision reaches 0.1) be measured, and with
Control sample extract without enzyme compares, and see table 2:
Table 2 end material extract Physico-chemical tests index
| Baume degrees value added | Solid content raising value | |
| Example 1 | 1.5 Baume | 11.6% |
| Example 2 | 1.6 Baume | 12.0% |
| Example 3 | 1.5 Baume | 11.6% |
| Example 4 | 1.7 Baume | 12.4% |
| Example 5 | 1.6 Baume | 12.0% |
| Control sample | 1.2 Baume | 10.3% |
By table 2 it can be seen that Dark sun-cured end is expected after enzymolysis processing, extract solid content all has carrying in various degree
Height, enzymolysis process improves extraction efficiency.
(2) extraction of flue-cured tobacco stalk material: flue-cured tobacco stalk material is added another raw material with water according to the ratio of solid-liquid ratio 1:2.5 and carries
Taking in tank, and put into compound enzymic preparation and auxiliary agent in whipping process, under conditions of temperature 55-75 DEG C, water carries 25-45 minute；
Then solid-liquid separation obtains extract and the solids of flue-cured tobacco stalk material of flue-cured tobacco stalk material, shared by the compound enzymic preparation of input and auxiliary agent
Flue-cured tobacco stalk material percentage by weight is as shown in table 3 below:
The enzyme preparation adding proportion table of table 3 cabo material case study on implementation
| Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | |
| Cellulase | 0.10% | 0.05% | 0.10% | 0.05% | 0.10% |
| Pectase | 0.15% | 0.05% | 0.05% | 0.10% | 0.10% |
| Saccharifying enzyme | 0.15% | 0.15% | 0.10% | 0.05% | 0.10% |
| Lactic acid | 0.4% | 0.1% | 0.1% | 0.2% | 0.3% |
| Sodium carbonate | 0.3% | 0.1% | 0.1% | 0.2% | 0.2% |
The extraction of comparison flue-cured tobacco stalk material: flue-cured tobacco stalk material is added another raw material with water according to the ratio of solid-liquid ratio 1:2.5
In extraction pot, under conditions of temperature 55-75 DEG C, water carries 25-45 minute；Then solid-liquid separation obtains compareing the extraction of flue-cured tobacco stalk material
Take liquid.
Respectively the flue-cured tobacco in above-mentioned five embodiments is obstructed solid content (the papermaking-method reconstituted tobaccos production industry of material extract
Detection the total component content of extract a kind of Testing index) and Baume degrees (B precision reaches 0.1) be measured, and with not
The control sample extract adding enzyme compares, and see table 4:
Table 4 stalk material extract Physico-chemical tests index
| Baume degrees value added | Solid content raising value | |
| Example 1 | 1.6 Baume | 11.9% |
| Example 2 | 1.5 Baume | 11.4% |
| Example 3 | 1.4 Baume | 11.2% |
| Example 4 | 1.6 Baume | 11.9% |
| Example 5 | 1.5 Baume | 11.5% |
| Control sample | 1.2 Baume | 10.7% |
By table 4 it can be seen that utilize these three enzyme that stalk material is carried out in extraction process enzymolysis, effect of extracting is had one
Fixed positive effect.
Embodiment two: the preparation method of the Dark sun-cured reconstituted tobacco of a kind of applicable flue-cured tobacco local flavor, it is characterised in that specifically walk
Rapid as follows:
(1) Dark sun-cured end material extracting solution in each embodiment and Dark sun-cured stalk material extracting solution are merged, and it is dense to carry out reducing pressure
Residual enzyme, for coating fluid, is inactivated in concentration technology and reconstituted tobacco stoving process by contraction.Meanwhile, concentration tank adds
Aminoacid etc. produce fragrant catalysts, add in concentration tank the auxiliary agents such as sugar material, aminoacid to and account for Dark sun-cured end and expect the hundred of gross weight
Proportion by subtraction is as follows:
Table 5 concentration tank throws in the schedule of proportion of the auxiliary agents such as aminoacid
| Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | |
| Propylene glycol | 0.20% | 0.20% | 0.40% | 0.40% | 0.50% |
| Xylose | 0 | 0.2% | 0.1% | 0.1% | 0.2% |
| Glucose | 0.5% | 2.0% | 2.0% | 1.0% | 1.0% |
| Glycine | 0.15% | 0.20% | 0.15% | 0.20% | 0.10% |
| Isoleucine | 0.05% | 0.10% | 0.05% | 0.10% | 0.15% |
| Proline | 0.05% | 0.10% | 0.05% | 0.05% | 0.10% |
| Tyrosine | 0 | 0.05% | 0.05% | 0.05% | 0.10% |
| Agedoite | 0.10% | 0.10% | 0.05% | 0.05% | 0 |
| Carotenoid | 0.10% | 0.10% | 0.20% | 0.10% | 0.20% |
| Sodium carbonate | 0.30% | 0.30% | 0.40% | 0.40% | 0.50% |
The Dark sun-cured end the obtained material solid matter of solid-liquid separation in each embodiment is merged with flue-cured tobacco stalk material solids
Making beating uses paper process to prepare Nicotiana tabacum L. substrate, in reconstituted tobacco stoving process inactivates residual enzyme.Meanwhile, add at slurry mixing tank
Enter aminoacid etc. and produce fragrant catalysts, add the auxiliary agent such as sugar material, aminoacid of slurry mixing tank to and account for Dark sun-cured end and expect gross weight
Percentage ratio is as follows:
Table 6 slurry mixing tank throws in the schedule of proportion of the auxiliary agents such as aminoacid
(3) carry out manufacturing paper with pulp by the slurry in step (2) according to paper process and obtain reconstituted tobacco substrate, then by step (1)
The coating solution of middle concentration, on reconstituted tobacco substrate, is dried and makes reconstituted tobacco.
The characteristic Dark sun-cured papermaking-method reconstituted tobaccos of preparation and control sample are according to reconstituted tobacco industry sensory quality assessment side
Method is evaluated, 5 provincial product suction persons carry out product suction, all in all, all thinks that what above-mentioned 5 case study on implementation produced reproduces
Nicotiana tabacum L. has the following characteristics that wooden breath substantially reduces, and fragrance level substantially increases, and miscellaneous QI weakens, and zest reduces, and entirety changes
Enter effectiveness comparison obvious.But example 5 reconstituted tobacco has sense of significantly fermenting, and flue gas is slightly discord, and strength is big.Marking is by up to
Low order is: example 3 > example 2 > example 4 > example 1 > example 5 > comparison.
The papermaking-method reconstituted tobaccos prepared is from comparing with control sample in appearance, it can be seen that processed by the method
The reconstituted tobacco crossed, closer to Nicotiana tabacum L. on color and luster.
Inventor is through productive experiment certification repeatedly, through the Dark sun-cured paper process that above biochemistry complex art processed
Reconstituted tobacco product xylon gas, miscellaneous QI significantly reduce, and zest reduces, and fragrance increased；Physical property is almost without negatively
Impact, color and luster optimization, closer to Nicotiana tabacum L..
Claims (6)
1. the method manufacturing the suncured tabacco reconstituted tobacco being suitable for flue-cured tobacco local flavor, it is characterised in that specifically comprise the following steps that
(1), suncured tabacco tobacco is added in raw material extraction pot in temperature 45-65 DEG C according to the ratio of solid-liquid ratio 1:4-7 with water
Under conditions of water carry 25-45 minute；And during extracting, in head tank, add compound enzymic preparation and auxiliary agent, described compound enzyme
In preparation, to account for the percentage ratio of suncured tabacco tobacco quality as follows for every kind of enzyme:
(2), flue-cured tobacco stalk material is added in another raw material extraction pot according to the ratio of solid-liquid ratio 1:2-4, in temperature 55-75 with water
Under conditions of DEG C, water carries 25-45 minute；And during extracting, in head tank, add compound enzymic preparation and auxiliary agent, described compound
In enzyme preparation, to account for the percentage ratio of flue-cured tobacco stalk material quality as follows for every kind of enzyme:
Cellulase 0～0.10%
Pectase 0.05%～0.15%
Saccharifying enzyme 0.05%～0.15%
(3), solid-liquid separation after the extracting solution obtained of solid-liquid separation after hydrolysis in step (1) and water body in step (2) is obtained
Extracting solution merge, and carry out concentrating under reduced pressure and prepare coating fluid, during concentrating under reduced pressure, add propylene glycol, reducing sugar and amino
Acid, it is as follows that the concrete material added accounts for the percentage ratio of suncured tabacco tobacco gross weight in step (1): propylene glycol 0.1～0.5%,
Xylose 0～0.2%, glucose 0.5～2.0%, glycine 0.10～0.20%, isoleucine 0.05～0.20%, proline
0.05～0.10%, agedoite 0～0.10%, tyrosine 0～0.10%；
(4), solid-liquid separation after the solid matter obtained of solid-liquid separation after water body in step (1) and water body in step (2) is obtained
The solid matter arrived merges making beating, and pulping process adds reducing sugar and aminoacid in tobacco pulp, and the concrete material added accounts for step
Suddenly the percentage ratio of suncured tabacco tobacco gross weight is as follows in (1): xylose 0～0.10%, glucose 0.2～1.0%, glycine
0.05～0.10%, agedoite 0～0.10%, proline 0～0.10%, tyrosine 0～0.05%；
(5), paper process is used to carry out manufacturing paper with pulp by the slurry in step (4) and obtain reconstituted tobacco substrate, then by dense in step (3)
The coating solution of contracting, on reconstituted tobacco substrate, is dried and makes reconstituted tobacco.
Kind the most according to claim 1 is suitable for the preparation method of the suncured tabacco reconstituted tobacco of flue-cured tobacco local flavor, it is characterised in that
The percentage ratio that the auxiliary agent that step (1) is added accounts for suncured tabacco tobacco quality is as follows:
Lactic acid 0～0.5%
Sodium carbonate 0～0.5%
Magnesium chloride or calcium chloride 0～0.2%.
Kind the most according to claim 1 is suitable for the preparation method of the suncured tabacco reconstituted tobacco of flue-cured tobacco local flavor, it is characterised in that
The percentage ratio that the auxiliary agent added in step (2) accounts for flue-cured tobacco stalk material quality is as follows:
Lactic acid 0～0.5%
Sodium carbonate 0～0.5%.
Kind the most according to claim 1 is suitable for the preparation method of the suncured tabacco reconstituted tobacco of flue-cured tobacco local flavor, it is characterised in that
Carrying out in step (3) being additionally added following material during concentrating under reduced pressure prepares coating fluid, its addition accounts for suncured tabacco in step (1)
Tobacco mass percent is as follows:
Carotenoid 0～0.6%
Sodium carbonate 0～0.8%.
5. according to a kind of applicable flue-cured tobacco local flavor described in claim 1 or 2 or 3 or 4 suncured tabacco reconstituted tobacco preparation method, its
It is characterised by: described suncured tabacco tobacco is carrying out before water carries, adds the condition that the water of its weight 2-2.5 times is at 65-75 DEG C
Lower immersion 5-10 minute.
6. according to a kind of applicable flue-cured tobacco local flavor described in claim 1 or 2 or 3 or 4 suncured tabacco reconstituted tobacco preparation method, its
It is characterised by: described suncured tabacco tobacco material includes Dark sun-cured Nicotiana tabacum L., Dark sun-cured tobacco leaf fragment, Dark sun-cured offal, Sun cured tobacco cigarette
A kind of or the most several in leaf, Sun cured tobacco tobacco leaf fragment, Sun cured tobacco offal.
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