CN101564201B - Method for improving quality of tobacco leaves by enzyme treatment in tobacco shred making processing technology - Google Patents
Method for improving quality of tobacco leaves by enzyme treatment in tobacco shred making processing technology Download PDFInfo
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- CN101564201B CN101564201B CN 200810047409 CN200810047409A CN101564201B CN 101564201 B CN101564201 B CN 101564201B CN 200810047409 CN200810047409 CN 200810047409 CN 200810047409 A CN200810047409 A CN 200810047409A CN 101564201 B CN101564201 B CN 101564201B
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Abstract
The invention discloses a method for improving the quality of tobacco leaves by enzyme treatment in a tobacco shred making processing technology, belonging to the technical field of tobacco shred making processing. The method comprises the following steps: after a feeding procedure, an enzyme solution is uniformly sprayed on formula tobaccos so that the water content of the tobacco leaves with added enzyme reaches 20 percent+/-1.00 percent; then the tobacco leaves with the added enzyme are placed into a leaf storage cabinet to start a leaf storage procedure, and the tobacco leaves are catalyzed and aged by the added enzyme, wherein the added enzyme loses activity under the short-time temperature in a tobacco shred baking procedure. The method can be directly applied in the tobacco shred making processing process, thereby increasing the production technology content and enhancing the quality of the tobacco leaves so as to obtain finished tobacco shreds with improved smoke gas quality; in addition, the method sufficiently utilizes the storage period time of the leaf storage cabinet and has simple technology, simple and convenient operation, reduced capital overstock and low production cost.
Description
Technical field
The present invention relates to the tobacco cutting processing technique field, specifically a kind of enzyme that carries out in the tobacco cutting processing technology is processed the method for improving quality of tobacco.
Background technology
In tobacco product, the fragrance of tobacco and suction flavor are vital.In prior art, adopt the method that tobacco fermentation is processed to improve the quality of tobacco leaf, but all adopt natural storage to process, the time, generally for the several years, this method wasted time and energy, and also will take a large amount of places.It is in fact at a certain temperature and humidity conditions that tobacco fermentation is processed, and impels tobacco leaf physicochemical property generation profound change, and the process that tabacco fragrance and smoking quality obviously improve claims again ageing.Can eliminate after sleep junior tobacco leaf with cyan, make tobacco leaf color turn dark and uniformity, blue foreign smell, excitant and peculiar smell reduce, fragrance appears, and fragrance matter and fragrance quantitative change are good, inhales flavor pure and mild, pleasant impression is pure comfortable, and viscosity and hygroscopicity reduce, and elasticity and flammability are enhanced.Therefore, sleep is significant to improving quality of tobacco and improving tobacco leaf usability.At present, sleep mainly contains nature ageing (also claiming alcoholization or fermentation) and artificial aging (claiming again heating fermentation) dual mode.The former is mainly during tobacco storage, by the variation of natural climate, impels various chemical change accelerations in tobacco leaf, and then reaches the purpose of improving quality of tobacco and physicochemical character.Latter is under the condition of manual control humiture, and the tobacco leaf physical and chemical properties change that is stacked in the ageing storehouse is accelerated, and improves the method for quality of tobacco within a short period of time.The defective of nature ageing tobacco leaf is storage period long (generally needing 1~3 year), take the warehouse large, let funds lie idle many, production cost is high, but due to natural ageing has that the tobacco leaf color and luster is vivid, fragrance is graceful, a little less than excitant, the advantage such as technique is simple, easy and simple to handle, and the successful that improves fragrance and smoking quality is better than the artificial aging tobacco leaf, so developed country generally adopts the method for nature ageing.And the artificial aging cycle short (being generally 12~20 days), it is few that fund overstocks, and production cost is low.But quality of tobacco is good not as good as natural ageing.China is because being subjected to the restriction of economic condition, domestic middle-size and small-size cigar mill is still take artificial aging as main, even large-scale cigar mill faces too when improving the quality of products, and the problem that reduces production costs, increases economic efficiency, so, can not be completely free of the artificial aging of tobacco leaf.Therefore, further study and improve the tobacco fermentation technology, enterprise improves the cigarette flavor quality to Chinese tobacco, improves the production of cigarettes economic benefit and has realistic meaning widely.
Summary of the invention
Above-mentioned deficiency for prior art, the technical problem to be solved in the present invention is to provide a kind of enzyme that carries out and processes the method for improving quality of tobacco in the tobacco cutting processing technology, it utilizes depositing the turnaround time of leaf storing cabinet in the tobacco cutting processing technology, selected tobacco leaf is processed and had several enzymes of special effect and suitable condition, at short notice tobacco leaf being carried out enzyme processes, reach the effect that promotes quality of tobacco, and then provide strong support for the improvement of cigarette product quality.
Technical scheme of the present invention is that a kind of enzyme that carries out in the tobacco cutting processing technology is processed the method for improving quality of tobacco, the throwing processing technology contains charging process, storage leaf operation, Qie Yesi operation, baking cut tobacco operation, perfuming operation successively, and the improvements of described technique are:
(1) after described charging process, carry out following operation:
Or the aqueous solution of enzyme evenly is sprayed onto on the formula tobacco leaf, make enzyme-added rear moisture content in leaves reach 20% ± 1.00%;
Or complete with the device of flavoring and casing of the prior art, before enzyme-added, reduce the carbohydrate moisture when feeding in raw material, be reduced to 1.75%-2.25% from 3.5%-3.75%, with blade flow 5400 ± 80Kg/h, drum speed: 500 ± 25rpm, shower nozzle steam pressure 0.2-0.4Mpa, under the condition that temperature is 28 ± 5 ℃, enzyme liquid evenly is sprayed onto on the formula tobacco leaf, after enzyme-added liquid, moisture content in leaves reaches 20% ± 1.00%;
Described enzyme is single enzyme among solid powdery neutral proteinase, AMS, carbohydrase, cellulase, pectase or the combination enzyme of 2~5 kinds among them;
Ratio in the combination enzyme between each component is 0.5~2: 0.5~2; Mass ratio between enzyme and formula tobacco leaf is 0.075%~0.08%;
(2) in described storage leaf operation, enzyme-added tobacco leaf in above-mentioned (1) is put into leaf storing cabinet enter storage leaf operation, enzyme is processed tobacco leaf in storage leaf operation;
Temperature in storage leaf operation is that 28~32 ℃, humidity are 65~70%; The time that enzyme is processed is 4~6 hours;
(3) in described baking cut tobacco operation, enzyme is lost activity in the of short duration high temperature of baking cut tobacco operation; Described of short duration high temperature refers to 1~2 minute high temperature of 100 ℃~200 ℃.
The concentration of aqueous solution of enzyme is 4%~5%.
Mass ratio between the aqueous solution of enzyme and formula tobacco leaf is 1.5%~2%.
The inventive method can directly be used in the throwing process, and the technology content of production is improved, promote quality of tobacco, obtain the finished cut tobacco that flue gas matter is improved, take full advantage of depositing the turnaround time of leaf storing cabinet, technique is simple, easy and simple to handle, fund is overstock few, and production cost is low.
The specific embodiment
Below in conjunction with embodiment, the specific embodiment of the present invention is described in further detail.In prior art, the throwing processing technology of cigarette industry contain successively charging process, storage leaf operation, Qie Yesi operation,, the master operations such as baking cut tobacco operation, perfuming operation.
In the throwing process, be subject to the industrial production Restricted requirement, produce cigarette product consuming time often within a few hours, the depositing the most nearly 48 hours turnaround time of leaf storing cabinet, 6-9 month in summer mostly is 36 hours most, utilizing this section to deposit the turnaround time adopts enzymatic to process tobacco leaf, can not only improve quality of tobacco, improve the fragrance matter of finished cigarettes and inhale flavor, and technique be simple, easy and simple to handle, fund is overstock few, production cost is low.
The applicant has efficient catalytic and height selectivity from enzyme known in the state of the art, recognizes suitable enzyme and the suitable condition selected, and it is possible being used for the tobacco processing, can shorten the processing time and promote the tobacco leaf Disposal quality.Protein in tobacco leaf is larger on the quality of tobacco impact, produce a kind of rotten-egg odour when burning, and the protein in neutral protein endonuclease capable hydrolysis tobacco leaf improves quality of tobacco; Starch, cellulose, pectin all belong to the polysaccharide in tobacco leaf, and is water insoluble, without reducing power, can be hydrolyzed into monose under acid condition He under the enzyme effect, improves inherent quality of tobacco leaf; And amylase, cellulase, pectase, carbohydrase all can make the reduced sugar of tobacco leaf increase, and improve quality of tobacco.
the present invention has the following advantages compared with the prior art: the present invention adopts in during Primary Processing, evenly spraying enzyme liquid after charging process (is the aqueous solution of enzyme, as follows) to tobacco leaf, (this device can adopt in prior art the device of flavoring and casing to complete also can to increase the operation that a kind of special device-enzyme-added cylinder carries out enzyme-added liquid, its critical piece and function are close, before using enzyme-added cylinder, reduce the carbohydrate moisture when feeding in raw material, be reduced to 1.75%-2.25% from 3.5%-3.75%, with blade flow 5400 ± 80Kg/h, drum speed: 500 ± 25rpm, shower nozzle steam pressure 0.2-0.4Mpa, under the condition that temperature is 28 ± 5 ℃, enzyme liquid evenly is sprayed onto on the formula tobacco leaf, after enzyme-added liquid, moisture content in leaves reaches 20% ± 1.00%, ).Tobacco leaf after enzyme-added enters leaf storing cabinet, and then the design temperature in leaf storing cabinet, humidity and deposit and carry out enzyme in the turnaround time to the catalysis ageing of tobacco leaf carry out follow-up throwing common process, namely the Qie Yesi operation,, baking cut tobacco operation, perfuming operation etc.Method of the present invention consuming time short, the technique simple operations is easy, is convenient to be applied in industrial production; The enzyme that the present invention adopts, consumption is few, wide material sources, with low cost; Finished cut tobacco quality through the inventive method processing obviously makes moderate progress, and increases with the quality of the cigarette product of this finished cut tobacco production, fund is overstock lack, and has reduced production cost.
It is neutral proteinase that the applicant has in 8 embodiment: embodiment 1 what use altogether.What use in embodiment 2 is AMS.What use in embodiment 3 is pectase.What use in embodiment 4 is cellulase.What use in embodiment 5 is carbohydrase.What use in embodiment 6 is the combination enzyme of neutral proteinase, AMS, carbohydrase; Wherein, neutral proteinase: AMS: carbohydrase=0.5: 1: 1.What use in embodiment 7 is the combination enzyme of neutral proteinase, cellulase, pectase; Wherein, neutral proteinase: cellulase: pectase=1: 2: 1.Embodiment 8 is the combination enzyme of neutral proteinase, AMS, carbohydrase, cellulase, pectase, wherein, and neutral proteinase: AMS: carbohydrase: cellulase: pectase=2: 1: 1: 1.5: 1.
Enzyme liquid (the aqueous solution of preparation, as follows) be: enzyme (single enzyme or complex enzyme) is added water is mixed with 4~5%, the enzyme liquid of pH value 4~8, the mass ratio of enzyme liquid and tobacco leaf is 1.5%~2%, and wherein the mass ratio of enzyme and tobacco leaf is 0.075%~0.08%.
The applicant has carried out the mensuration of enzymatic activity to the pipe tobacco before and after transformation throwing processing technology, after the baking silk.
The alphalise starch activity determination adopts the iodine-starch development process, is defined as: 37 ℃, the amylase energy complete hydrolysis starch 10mg in pH7.0,30min in 100ml enzyme liquid is called a diastatic activity unit of force.
Neutral protein activity determination: adopt folin's methods, be defined as: 40 ℃, pH7.2, it is an enzyme activity unit that caseinhydrolysate per minute produces 1ug tyrosine.
Pectin activity determination: adopt hypoiodous acid sodium method, be defined as: 50 ℃, pH3.5, it is an enzyme activity unit that catalysis hydrolyzed pectin per minute generates the 1ug galacturonic acid.
Cellulose activity determination: adopt the DNS development process, be defined as: 50 ℃, under pH4.8, catalyzing hydrolysis generation half an hour 1mg glucose is an enzyme activity unit.
Saccharification activity determination: adopt hypoiodous acid sodium method, be defined as: 40 ℃, it is an enzyme activity unit that pH4.5 hydrolysis in lower 1 hour generates 1mg glucose.
Testing result shows, the enzyme activity in the pipe tobacco after the baking silk is zero, illustrate that in baking silk process, deactivation under 1~2 minute high temperature of 150 ℃ ± 10 ℃ in enzyme process drying process stops the reaction of enzymatic ageing tobacco leaf.
Pipe tobacco and prior art that the applicant produces the inventive method compare, and have carried out sensory evaluating smoking's experiment.Contrast experiment's pipe tobacco adopts red certain two class cigarette of gold dragon that Wuhan tobacco Group Co.,Ltd produces to cut filler, and is smoked panel test to organize by the expert by pertinent regulations of the prior art and carries out the sensory evaluating smoking, the results are shown in following table 1.
Table 1, the contrast of cigarette sensory evaluating smoking result
By upper table 1 sensory evaluating smoking presentation of results, the cigarette that the pipe tobacco that this method is produced is made, due to tobacco leaf process enzymatic ageing in raw silk production process, the effect that improves significantly flue gas matter, the quality of cigarette product increases.
The applicant has carried out the chemical composition detection to the finished cut tobacco of the inventive method, and the chemical composition of being undertaken by the pipe tobacco after the enzymatic ageing detects and comprises the protein of measuring finished cut tobacco, starch, reduced sugar etc.Choose 3 parallel sample detects at every turn.And compare checking with testing result and sensory evaluating smoking's result.Sample detection the results are shown in following table 2~4.
Table 2, the contrast of finished cut tobacco protein content testing result
The embodiment that exemplifies in table 2 is for using the embodiment of neutral proteinase, can find out, the inventive method is after carrying out the enzymatic ageing to tobacco leaf on production line, the complex enzyme that uses single enzyme of neutral proteinase or contain neutral proteinase all can reduce protein content, promote the inherent quality of tobacco leaf, in table 1, sensory evaluating smoking's result illustrates that also above-described embodiment can promote cigarette smoke matter.
Table 3, the contrast of finished cut tobacco content of starch testing result
In table 3, embodiment contains AMS, the inventive method is carried out the enzymatic ageing to tobacco leaf on production line, the complex enzyme that uses single enzyme of AMS or contain AMS all can reduce content of starch, promote the inherent quality of tobacco leaf, table 1 sensory evaluating smoking result illustrates that also above-described embodiment can promote cigarette smoke matter.
Table 4, the contrast of finished cut tobacco content of reducing sugar testing result
The embodiment that table 4 shows is the sample that contains reduced sugar, the syntax of the present invention are carried out the enzymatic ageing to tobacco leaf on production line, use single enzyme of cellulase, pectase, carbohydrase or contain these three kinds of enzymes one of two or three complex enzyme all can increase content of reducing sugar, promote the inherent quality of tobacco leaf, table 1 sensory evaluating smoking result illustrates that also above-described embodiment sample can promote cigarette smoke matter.
Claims (3)
1. one kind is carried out the method that the enzyme processing improves quality of tobacco in the tobacco cutting processing technology, the throwing processing technology contains charging process, storage leaf operation, Qie Yesi operation, baking cut tobacco operation, perfuming operation successively, it is characterized in that the improvements of described technique are:
(1) after described charging process, carry out following operation:
Or the aqueous solution of enzyme evenly is sprayed onto on the formula tobacco leaf, make enzyme-added rear moisture content in leaves reach 20% ± 1.00%;
Or complete with the device of flavoring and casing of the prior art, before enzyme-added, reduce the carbohydrate moisture when feeding in raw material, be reduced to 1.75%-2.25% from 3.5%-3.75%, with blade flow 5400 ± 80Kg/h, drum speed: 500 ± 25rpm, shower nozzle steam pressure 0.2-0.4Mpa, under the condition that temperature is 28 ± 5 ℃, enzyme liquid evenly is sprayed onto on the formula tobacco leaf, after enzyme-added liquid, moisture content in leaves reaches 20% ± 1.00%;
Described enzyme is single enzyme among solid powdery neutral proteinase, AMS, carbohydrase, cellulase, pectase or the combination enzyme of 2~5 kinds among them;
Ratio in the combination enzyme between each component is 0.5~2: 0.5~2; Mass ratio between enzyme and formula tobacco leaf is 0.075%~0.08%;
(2) in described storage leaf operation, enzyme-added tobacco leaf in above-mentioned (1) is put into leaf storing cabinet enter storage leaf operation, enzyme is processed tobacco leaf in storage leaf operation;
Temperature in storage leaf operation is that 28~32 ℃, humidity are 65~70%; The time that enzyme is processed is 4~6 hours;
(3) in described baking cut tobacco operation, enzyme is lost activity in the of short duration high temperature of baking cut tobacco operation; Described of short duration high temperature refers to 1~2 minute high temperature of 100 ℃~200 ℃.
2. the enzyme that carries out in the tobacco cutting processing technology according to claim 1 is processed the method for improving quality of tobacco, and it is characterized in that: the concentration of aqueous solution of enzyme is 4%~5%.
3. the enzyme that carries out in the tobacco cutting processing technology according to claim 1 is processed the method for improving quality of tobacco, it is characterized in that: the mass ratio between the aqueous solution of enzyme and formula tobacco leaf is 1.5%~2%.
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CN102178344B (en) * | 2011-05-13 | 2012-10-03 | 川渝中烟工业有限责任公司 | Method for reducing protein of cigar core leaves |
CN103355740A (en) * | 2012-03-26 | 2013-10-23 | 李森会 | Microbial invertase composition for improving cigarette quality and preparation method thereof |
CN102894472B (en) * | 2012-09-29 | 2014-12-24 | 福建中烟工业有限责任公司 | Method for improving sensory quality of tobacco leaves by using compound enzymic preparation |
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CN111990684B (en) * | 2020-09-17 | 2022-07-05 | 内蒙古昆明卷烟有限责任公司 | Method for treating tobacco leaves by biological enzyme, and prepared tobacco leaves and cigarettes |
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CN101040723A (en) * | 2006-03-22 | 2007-09-26 | 夏炳乐 | Tobacco slice high-activity bio-enzyme regulator and method for improving the quality of the tobacco slice |
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