CN107912801A - One kind heats the reconstituted tobacoo and preparation method thereof that do not burn - Google Patents
One kind heats the reconstituted tobacoo and preparation method thereof that do not burn Download PDFInfo
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- CN107912801A CN107912801A CN201711180874.XA CN201711180874A CN107912801A CN 107912801 A CN107912801 A CN 107912801A CN 201711180874 A CN201711180874 A CN 201711180874A CN 107912801 A CN107912801 A CN 107912801A
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- tobacco
- biological treatment
- reconstituted tobacoo
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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Abstract
The present invention provides one kind to heat the reconstituted tobacoo and preparation method thereof that do not burn.Preparation method provided by the invention includes：A) tobacco leaf is subjected to biological treatment under microbial action, obtains a biological treatment tobacco leaf；Microorganism includes bacillus and/or saccharomycete；B) a biological treatment tobacco leaf is mixed with rhodiola root, obtains mixture；C) after mixture progress water being carried and concentrated, add complex enzyme formulation and carry out biological treatment, obtain secondary biological treatment concentrate；Complex enzyme formulation includes two or more in cellulase, pectase, protease and glucolase；D) secondary biological treatment concentrate is mixed with modifying agent and carries out Maillard reaction, obtain coating medium；E) coating medium is coated on tobacco sheet primary surface and drying, obtains heating the reconstituted tobacoo that do not burn.Above-mentioned preparation method can improve the tensile strength and bulk of reconstituted tobacoo, and be not easy adhesion, while essentially eliminate the bad breaths such as the miscellaneous gas of wood, have rhodiola root fragrance.
Description
Technical field
It is more particularly to a kind of to heat the reconstituted tobacoo and preparation method thereof that do not burn the present invention relates to technical field of tobacco.
Background technology
Reconstituted tobacoo is also known as reconstituted tobacco, is the low-grade cigarette of offal, offal and part that will be discarded during production of cigarettes
The Discarded Tobacco such as leaf material is approached by working process formation shape or the product better than natural tobacco, and then reapplies in cigarette
Production, it can effectively reduce production of cigarettes cost, cigarette production waste is retrieved utilization, reach consumption reduction synergy
Effect.Therefore, reconstituted tobacoo has become the necessary raw material of cigarette composition, and since reconstituted tobacoo has these important actual meanings
Justice, its production development are very fast.
Conventional tobacco products have had centuries history as a kind of preference, however, as people are to health and environment
Growing interest, research and development can effectively reduce the novel tobacco product of tobacco harmful components burst size and be increasingly becoming countries in the world
The development priority of tobacco business.At present, more representative is to heat not burning type tobacco product (also known as low temperature cigarette),
It is to heat (less than 500 DEG C even lower) to cigarette core by special heating source, nicotine and fragrance during heating in pipe tobacco
Material meets the needs of smoker by volatilizing generation flue gas；It is different from traditional cigarette, heating not burning type tobacco product
Pipe tobacco is in heating rather than combustion state, so as to reduce the harmful components that the cracking of traditional tobacco high-temp combustion produces, reduces master
Stream flue gas endangers component；Meanwhile it can also overcome electronic cigarette not have the shortcomings that real smoke taste.Therefore, not burning tobacco is heated
Product is increasingly welcome be subject to consumer.
Heating the mode of heating of not burning type tobacco product mainly includes electric heating type, carbon hot type etc., such as adds for electricity
Heat type, it needs cigarette in-core insertion heater element such as heating bar to cigarette, fever blade etc., by the fever of heater element come
Pipe tobacco is heated, after suction, extracts cigarette.However, existing low-temperature heat is not burnt in cigarette, generally use cigarette
The dry method thin slice that end is formed with binding agent is used as pipe tobacco, and wooden miscellaneous smell is heavier during heating, and taste is relatively simple, and irritation is bright
It is aobvious；Moreover, the tensile strength of dry method thin slice is relatively low, bulk is not good enough, the easy adhesion of pipe tobacco, easy adhesion cutter in process
Piece, and after making cigarette, cannot smoothly be extracted after suction, also easy adhesion pipe tobacco on heating element, cleaning is difficult.Cause
This, the heating that exploitation suction quality is high and mechanical property is good is not burnt cigarette the problem of having become urgent need to resolve in the industry.
The content of the invention
In view of this, the present invention provides one kind to heat the reconstituted tobacoo and preparation method thereof that do not burn.It is provided by the invention
Reconstituted tobacoo has good tensile strength and bulk, and is not easy adhesion, meanwhile, it eliminates the bad breaths such as the miscellaneous gas of wood,
It is fragrant with rhodiola root, and substantially nonirritant and burning sensation, cigarette perfume are enriched soft.
A kind of preparation method for heating the reconstituted tobacoo that do not burn, it is characterised in that comprise the following steps：
A) tobacco leaf is subjected to biological treatment under microbial action, obtains a biological treatment tobacco leaf；
The microorganism includes bacillus and/or saccharomycete；
B) a biological treatment tobacco leaf is mixed with rhodiola root, obtains mixture；
C) after mixture progress water being carried and concentrated, add complex enzyme formulation and carry out biological treatment, it is secondary to obtain two
Thing handles concentrate；
The complex enzyme formulation includes two or more in cellulase, pectase, protease and glucolase；
D) the secondary biological treatment concentrate is mixed with modifying agent and carries out Maillard reaction, obtain coating medium；
E) coating medium is coated on tobacco sheet primary surface and drying, obtains heating the reconstituted tobacoo that do not burn.
Preferably, in the step a), biological treatment carries out under the conditions of constant temperature and humidity, and temperature is 37~45 DEG C, humidity
For 70%~80%；The time of biological treatment is 6~8h.
Preferably, the mass ratio of the tobacco leaf in step a) and the rhodiola root in step b) is 99: 1~90: 10；
In the step c), the quality of the complex enzyme formulation is the 0.2%~0.5% of concentration gained condensed cream.
Preferably, in the step d), modifying agent includes one kind in natural extract, carbohydrate, amino acid and vitamin C
It is or several.
Preferably, the natural extract includes chicory extract；
The carbohydrate includes xylose；
The amino acid includes glycine and/or alanine.
Preferably, in the step d), the temperature of Maillard reaction is 80~120 DEG C, and the time is 1~1.5h.
Preferably, in the step e), the tobacco chip base obtains in the following manner：
S1 the mixture of tobacco material and rhodiola root) is subjected to enzymatic treatment under compound enzyme effect, obtains enzymatic treatment thing；
The tobacco material includes the one or more in offal, offal, tobacco leaf and pipe tobacco；
S2) handled the enzymatic treatment thing slurrying and by paper process, obtain tobacco chip base.
Preferably, the step e) includes：
E1) coating medium is coated in tobacco chip base and dried, obtains reconstituted tobacoo matrix；
E2 spray coating liquor and drying) are coated with to the reconstituted tobacoo matrix surface, obtains heating the reconstituted tobacoo that do not burn；
The spray coating liquor includes cigarette perfume material, adhesive, high molecular material and solvent.
Preferably, the adhesive includes the one or more in expanded graphite micro mist, graphene and mesoporous carbon spheres；
The high molecular material includes sodium alginate and/or cationic starch；
Champignon material of the cigarette perfume material obtained by destructive distillation offal；
The solvent includes propane diols and/or glycerine.
Present invention also offers one kind to heat the reconstituted tobacoo that do not burn, as the preparation method system described in above-mentioned technical proposal
.
The present invention provides a kind of preparation method for heating the reconstituted tobacoo that do not burn, comprise the following steps：A) tobacco leaf is existed
Biological treatment is carried out under microbial action, obtains a biological treatment tobacco leaf；The microorganism includes bacillus and/or yeast
Bacterium；B) a biological treatment tobacco leaf is mixed with rhodiola root, obtains mixture；C) to the mixture carry out water carry with it is dense
After contracting, add complex enzyme formulation and carry out biological treatment, obtain secondary biological treatment concentrate；The complex enzyme formulation includes fiber
Two or more in plain enzyme, pectase, protease and glucolase；D) by the secondary biological treatment concentrate with changing
Property agent mixing carry out Maillard reaction, obtain coating medium；E) coating medium is coated on tobacco sheet primary surface and drying, obtained
Heat the reconstituted tobacoo that do not burn.The processing of preparation method combination multi-biological and specific processing procedure and processing provided by the invention
Means, with heat it is non-ignitable dryout method thin slice compared with, preparation method of the invention can improve heating and not burn the anti-of reconstituted tobacoo
Zhang Qiangdu and bulk, and the problem of overcome reconstituted tobacoo adhesion；Meanwhile the bad breaths such as the miscellaneous gas of wood are also essentially eliminated,
Fragrant with certain rhodiola root, cigarette perfume is enriched, and effectively improves the suction quality for heating the reconstituted tobacoo that do not burn.Experimental result table
Bright, the obtained tensile strength for heating the reconstituted tobacoo that do not burn of preparation method according to the invention is in 0.40KNm-1More than, phase
Than not burning reconstituted tobacoo (its tensile strength≤0.15KNm in the heating of commercially available dry process-1), tensile strength carries significantly
Height, has higher bulk, and is not easy adhesion, also substantially eliminates the bad breaths such as the miscellaneous gas of wood, has certain rhodiola root
Perfume (or spice), and substantially nonirritant and burning sensation, cigarette perfume are enriched soft.In addition, the preparation method of the present invention is given birth in traditional papermaking thin slice
On the basis of producing equipment, it can be achieved by simply increasing lance driving device, it is simple and practicable, easy to large-scale production.
Embodiment
The present invention provides a kind of preparation method for heating the reconstituted tobacoo that do not burn, comprise the following steps：
A) tobacco leaf is subjected to biological treatment under microbial action, obtains a biological treatment tobacco leaf；
The microorganism includes bacillus and/or saccharomycete；
B) a biological treatment tobacco leaf is mixed with rhodiola root, obtains mixture；
C) after mixture progress water being carried and concentrated, add complex enzyme formulation and carry out biological treatment, it is secondary to obtain two
Thing handles concentrate；
The complex enzyme formulation includes two or more in cellulase, pectase, protease and glucolase；
D) the secondary biological treatment concentrate is mixed with modifying agent and carries out Maillard reaction, obtain coating medium；
E) coating medium is coated on tobacco sheet primary surface and drying, obtains heating the reconstituted tobacoo that do not burn.
Preparation method combination multi-biological processing provided by the invention and specific processing procedure and processing means, Neng Gouti
Height heating is not burnt the tensile strength and bulk of reconstituted tobacoo, and is overcome heating and do not burnt that reconstituted tobacoo adhesion is serious to ask
Topic；Meanwhile the bad breaths such as the miscellaneous gas of wood are also essentially eliminated, there is certain rhodiola root fragrance, cigarette perfume is enriched, effectively improved
Heat the suction quality for the reconstituted tobacoo that do not burn.
According to the present invention, tobacco leaf is first subjected to biological treatment under microbial action, obtains a biological treatment tobacco leaf.
Wherein, the microorganism includes bacillus and/or saccharomycete.In some embodiments of the invention, it is described micro-
Biology is bacillus；In further embodiments, microorganism is saccharomycete；In further embodiments, microorganism is gemma
Bacillus and the complex microorganism of saccharomycete.The microorganism for bacillus and saccharomycete complex microorganism when, bacillus
Mass ratio with saccharomycete is preferably (1~3): 1.In the present invention, the species of the bacillus is not particularly limited, for routine
Type, is preferably the one or more in Bacillus cercus, bacillus amyloliquefaciens and bacillus megaterium.Through application
People, which studies, to be found, tobacco leaf is carried out biological treatment under mentioned microorganism effect, it is possible to increase tobacco leaf fragrance, and Optimizing Tobacco knot
Structure, acts synergistically with subsequent treatment, obtains the coating fluid of excellent performance, helps to improve the mechanical property and suction product of tobacco
Matter.
In the present invention, tobacco leaf and the mode of microorganism immixture are not particularly limited, preferably spray microorganism formulation
Spill in tobacco leaf surface, so that tobacco leaf carries out biological treatment under microbial action.The source of the microorganism formulation is without spy
Different limitation, for general commercially available product or is that training method well known to those skilled in the art obtains, such as by microorganism in routine
Cultivate and obtain in nutrient solution.In the present invention, the mass ratio of microorganism formulation and tobacco leaf is preferably 0.1%~0.3%；In some tools
In body embodiment, concretely 0.1%, 0.2% or 0.3%.In the present invention, content of microorganisms is not special in microorganism formulation
Limitation, is this area conventional formulation specification, is preferably 106~108CFU/mL。
In the present invention, the biological treatment carries out preferably under the conditions of constant temperature and humidity.Wherein, temperature is preferably 37~45
℃；Humidity is preferably 70%~80%.In the present invention, the time of the biological treatment is preferably 6~8h.In the biological treatment
Afterwards, a biological treatment tobacco leaf is obtained.
According to the present invention, after a biological treatment tobacco leaf is obtained, a biological treatment tobacco leaf is mixed with rhodiola root
Close, obtain mixture.
In the present invention, the mass ratio of the additive amount and rhodiola root in the step of tobacco leaf is preferably in an above-mentioned biological treatment
99: 1~90: 10.In the present invention, after adding rhodiola root, rhodiola root is uniformly mixed with a biological treatment tobacco leaf, the present invention is right
The mode of the mixing is not particularly limited, and can be uniformly mixed the two, such as can be uniform by mechanical mixture, mixing
After uniformly, mixture is obtained.
According to the present invention, after mixture is obtained, water is carried out to the mixture and carries and concentrates, adds complex enzyme system afterwards
Agent carries out biological treatment, obtains secondary biological treatment concentrate.
In the present invention, the solid-liquid mass ratio that the water carries is preferably 1: (8~12).The temperature that the water carries is preferably 60~
80℃.After the water carries, the extracting solution that water is carried to gained is concentrated.The present invention does not have special limit to the mode of the concentration
System, is condensing mode well known to those skilled in the art, and such as evaporation and concentration, circumfluence distillation concentration, freeze concentration, film steam
Evaporate concentration etc..In the present invention, the mass concentration for being preferably concentrated into condensed cream is 36%~38%.
In the present invention, after condensed cream is concentrated to give, adds complex enzyme formulation and carry out biological treatment.It is described in the present invention
Complex enzyme formulation includes two or more in cellulase, pectase, protease and glucolase.In some embodiments
In, complex enzyme formulation is cellulase and pectase；In certain embodiments, complex enzyme formulation for cellulase, pectase and
Protease；In certain embodiments, complex enzyme formulation is cellulase, pectase, protease and glucolase；In other realities
Apply in example, complex enzyme formulation is other combinations selected from above-mentioned enzyme.In the present invention, the additive amount of complex enzyme formulation is preferably dense
The 0.2%~0.5% of contracting gained condensed cream quality.In the present invention, the temperature for adding complex enzyme formulation progress biological treatment is preferred
For 50~55 DEG C；The time of biological treatment is preferably 1~1.5h.After the biological treatment, secondary biological treatment concentration is obtained
Liquid.
According to the present invention, after secondary biological treatment concentrate is obtained, by the secondary biological treatment concentrate and modification
Agent mixing carries out Maillard reaction, obtains coating medium.
In the present invention, the modifying agent is preferably included in natural extract, carbohydrate, amino acid and vitamin C (i.e. Vc)
It is one or more of.The natural extract preferably includes chicory extract.The carbohydrate preferably includes xylose.The amino acid is excellent
Choosing includes glycine and/or alanine, more preferably including glycine and alanine.In preferred embodiments, the modifying agent
Including chicory extract, xylose, glycine, alanine and Vc.In some preferred embodiments, chicory extract in modifying agent,
Xylose, glycine, the mass ratio of alanine and Vc are (0.2~0.8)：(0.2~0.8)：(0.2~0.4)：0.2：0.1.This hair
In bright, the mass ratio of the modifying agent and secondary biological treatment concentrate is preferably 1.0%~2.0%.In the present invention, modifying agent
The temperature that Maillard reaction is carried out with secondary biological treatment concentrate is preferably 80~120 DEG C；The time of Maillard reaction is preferred
For 1~1.5h.After the Maillard reaction, coating medium is obtained.
According to the present invention, after coating medium is obtained, the coating medium is coated on tobacco sheet primary surface and drying, is added
The hot reconstituted tobacoo that do not burn.
In the present invention, the tobacco chip base preferably obtains in the following manner：
S1 the mixture of tobacco material and rhodiola root) is subjected to enzymatic treatment under compound enzyme effect, obtains enzymatic treatment thing；
The tobacco material includes the one or more in offal, offal, tobacco leaf and pipe tobacco；
S2) handled the enzymatic treatment thing slurrying and by paper process, obtain tobacco chip base.
In the present invention, the step S1) in, the tobacco material is preferably the tobacco waste during tobacco leaf production,
Preferably include the one or more in offal, offal, tobacco leaf and pipe tobacco.In the present invention, the matter of the tobacco material and rhodiola root
Amount is than being preferably 99: 1~90: 10.In the present invention, the mixture of the tobacco material and rhodiola root is preferably mixed after water carries
Compound, i.e., first carry the mixture of tobacco material and rhodiola root progress water.Wherein, the solid-to-liquid ratio that the water carries is preferably 1: (8~
12)；The temperature that the water carries is preferably 60~80 DEG C；The time that the water carries is preferably 1~1.5h.After water carries, consolidate
Liquid separates, and obtained solid mixture is carried out enzymatic treatment under compound enzyme effect.In the present invention, the complex enzyme preferably includes fibre
Tie up two or more in plain enzyme, pectase and protease.In certain embodiments, the complex enzyme for cellulase and
Pectase；In certain embodiments, the complex enzyme is cellulase, pectase and protease；In further embodiments, institute
It is other combinations selected from above-mentioned enzyme to state complex enzyme.In the present invention, the dosage of the complex enzyme be preferably tobacco material with it is red
The 0.1%~0.3% of red-spotted stonecrop gross mass.In the present invention, the temperature of the enzymatic treatment, which is preferably less than, is equal to 50 DEG C；At the enzyme
The time of reason is preferably 0.5~1h.After the enzymatic treatment, enzymatic treatment thing is obtained.It is excellent when adding complex enzyme in the present invention
Complex enzyme is first uniformly dispersed and obtains enzyme dispersion liquid by choosing with water, then is mixed into the form of enzyme dispersion liquid with above-mentioned solid mixture
Row enzymatic treatment reacts；After enzymatic treatment, enzymatic treatment slurry is first obtained, gained slurry is preferably subjected to separation of solid and liquid, it is separating obtained
Solids is enzymatic treatment thing, then the enzymatic treatment thing is carried out to follow-up chip base working process.
In the present invention, the step S2) in, the mode of enzymatic treatment thing slurrying is not particularly limited, such as by machinery
Grind slurrying etc., in certain embodiments, the slurrying by way of high-energy ball milling.In the present invention, after slurrying, gained slurry is led to
Paper process working process is crossed, obtains tobacco chip base.The present invention is not particularly limited the paper process, according to conventional in this area
Paper process manufacture paper with pulp tobacco chip base working process process carry out.After the working process, tobacco chip base is obtained.The present invention
The thickness equal-specification of gained tobacco chip base is not particularly limited, is this area conventional tobacco chip base specification.
After the present invention obtains coating medium and tobacco chip base, coating medium is coated on tobacco sheet primary surface and drying, obtains cigarette
Careless thin slice.
Wherein, the mode of the coating is not particularly limited, and is coating method conventional in the art, such as by
Coating machine is sprayed.In the present invention, the tobacco sheet primary surface can be any side surface of tobacco sheet base, or cigarette
The both side surface of blade base, is preferably the both side surface of tobacco chip base.By coating solution after tobacco sheet primary surface, done
It is dry.The present invention is not particularly limited the mode of the drying, can with naturally dry or mechanical drying, for improve production efficiency and
Drying effect, preferably mechanical drying, such as by oven for drying, the oven groups that specifically thin slice continuous rolling can be passed through production line
Drying.The temperature of the drying is not particularly limited, and is dried according to conventional tobacco thin slice drying temperature, such as can be at 120 DEG C
Dry left and right.After drying, reconstituted tobacoo is obtained.
Above-mentioned preparation method provided by the invention can improve the tensile strength and bulk for heating the reconstituted tobacoo that do not burn,
And overcome and heat the problem of not burning reconstituted tobacoo adhesion；Meanwhile the bad breaths such as the miscellaneous gas of wood are also essentially eliminated, have one
Fixed rhodiola root fragrance, cigarette perfume are enriched, and effectively improve the suction quality for heating the reconstituted tobacoo that do not burn.In addition, the present invention
Preparation method can be achieved on the basis of traditional papermaking thin slice production equipment by simply increasing lance driving device, simple and practicable,
Easy to large-scale production.
In the present invention, in tobacco sheet primary surface applied coating solution and after being dried to obtain reconstituted tobacoo, preferably with gained tobacco
Thin slice is coated with spray coating liquor and drying, so as to obtain reconstituted tobacoo as reconstituted tobacoo matrix to the reconstituted tobacoo matrix surface.
Wherein, the spray coating liquor preferably includes cigarette perfume material, adhesive, high molecular material and solvent.The present invention is right
The cigarette perfume material is not particularly limited, and is this area routine cigarette perfume material, is preferably obtained by low-temperature bake cigarette
Champignon material；It is furthermore preferred that the cigarette perfume material is the cigarette perfume material at 250~300 DEG C obtained by destructive distillation offal.It is described
In spray coating liquor, the content of sootiness Studies of The Aromatic Substances is preferably 0.1wt%~1.0wt%.In the present invention, the adhesive preferably includes
One or more in expanded graphite micro mist, graphene and mesoporous carbon spheres.In the spray coating liquor, the content of adhesive is preferably
0.01wt%~0.1wt%.In the present invention, the high molecular material preferably includes sodium alginate and/or cationic starch.It is described
In spray coating liquor, the content of the high molecular material is preferably 0.01wt%~0.05wt%.In the present invention, the high score material is excellent
Choosing is introduced in the form of micro- aqueous solution, i.e., high molecular material is first dissolved in after disperseing to form high concentration Polymer Solution in a small amount of water
Reuse；The mass concentration of the high concentration Polymer Solution is preferably 15%~30%.In the present invention, the solvent serves as mist
Agent, it preferably includes propane diols and/or glycerine, more preferably propane diols and glycerine.When the solvent is propane diols and glycerine,
The mass ratio of propane diols and glycerine is preferably 3:7~5:5.In the present invention, the content of solvent preferably complements in spray coating liquor
100%.
The present invention is preferably to be sprayed using spray gun to the coating method that spray coating liquor is coated on to reconstituted tobacoo matrix surface
Apply.The reconstituted tobacoo matrix surface can be any side surface of reconstituted tobacoo matrix, or reconstituted tobacoo matrix
Both side surface, is preferably the both side surface of reconstituted tobacoo matrix.In the present invention, after being coated with spray coating liquor, preferably also it is dried.This
Invention is not particularly limited the mode of the drying, can be with naturally dry or mechanical drying, to improve production efficiency and drying
Effect, preferably mechanical drying, such as by oven for drying, specifically can be dried thin slice continuous rolling by the oven groups of production line
It is dry.The temperature of the drying is preferably 50~80 DEG C, after the drying, sprayed on material is formed in the reconstituted tobacoo matrix surface
Layer, obtains reconstituted tobacoo.The present invention is further coated with above-mentioned spray coating liquor after reconstituted tobacoo matrix is obtained, and obtains containing spraying material
The reconstituted tobacoo of the bed of material, can preferably overcome heating do not burn reconstituted tobacoo easy adhesion the defects of, solve that adhesion is serious to ask
Topic.
Present invention also offers one kind to heat the reconstituted tobacoo that do not burn, as the preparation method system described in above-mentioned technical proposal
.Gained, which heats the reconstituted tobacoo that do not burn, has high-tensile and higher bulk, and is not easy adhesion, meanwhile, disappear substantially
Except bad breaths such as the miscellaneous gas of wood, but with rhodiola root perfume, and substantially nonirritant and burning sensation, cigarette perfume are enriched soft.
For a further understanding of the present invention, the preferred embodiment of the invention is described with reference to embodiment, still
It should be appreciated that these descriptions are simply further explanation the features and advantages of the present invention, rather than to the claims in the present invention
Limitation.In following embodiments, the water of tobacco material is carried to be operated according to the tobacco material abstract methods described in above-mentioned technical proposal；
Scent material of the cigarette perfume material obtained by destructive distillation offal in spray coating liquor used, high molecular material are added in the form of micro- aqueous solution
Add.
Embodiment 1
1.1 heat the preparation for the reconstituted tobacoo that do not burn：
To the Bacillus cercus preparation (10 of raw tobacco material surface sprinkling 0.1%8CFU/mL), it is subsequently placed in 37 DEG C of temperature
With biological treatment 8h in the thermo-humidistat cabinet of humidity 70%, a biological treatment tobacco leaf is obtained；With raw tobacco material:Rhodiola root is
99:1 mass ratio adds rhodiola root into biological treatment tobacco leaf of gained and mechanical mixture is uniform, obtains mixture；By institute
Mixture soaks water and puies forward (solid-to-liquid ratio 1:8) after, extracting solution is concentrated into 36%~38%, obtains condensed cream, then to
0.2% complex enzyme formulation (cellulase is added in gained condensed cream：The mass ratio of pectase is 1:1) it is, biological at 50 DEG C
1h is handled, obtains secondary biological treatment concentrate.It is subsequently added into 1.0% modifying agent (chicory extract：Xylose：Glycine：Third
Propylhomoserin：Mass ratio=0.2 of Vc:0.2:0.3:0.2:0.1) Maillard reaction 1h, is carried out at 90 DEG C, obtains coating fluid.
The solid mixture of tobacco material (offal and offal) after Xiang Shuiti and rhodiola root be (tobacco material and rhodiola root
Mass ratio is 99:1) 0.10% complex enzyme (cellulase is added in：The mass ratio of pectase is 0.5:0.5), in 50 DEG C of lifes
Thing handles 1h, obtains enzymatic treatment thing.Gained enzymatic treatment thing is copied through high-energy ball milling slurrying, gained slurry by paper process technique
Make, squeeze and dry, obtain tobacco chip base.
Gained coating fluid is sprayed into tobacco sheet primary surface using coating machine, through oven for drying, obtains reconstituted tobacoo matrix.
By 0.01% cigarette perfume material, 0.1% expanded graphite micro mist, the third the two of 0.01% sodium alginate and surplus
(propane diols is 3 with qualities of glycerin ratio to alcohol with Glycerol solvents:7) it is mixed and stirred for uniformly, obtaining spray coating liquor.It will be sprayed using spray gun
Liquid sprays to reconstituted tobacoo matrix surface, then is placed in 80 DEG C of baking ovens and dries, and obtains heating the reconstituted tobacoo that do not burn.
1.2 measure of merit：
The reconstituted tobacoo that do not burn to gained heating carries out Mechanics Performance Testing and adhesive test, the results show that gained adds
The tensile strength of the hot reconstituted tobacoo that do not burn is 0.44KNm-1, bulk 2.04cm3·g-1(according to national standard GB/T 453-
2002 tests)；Do not burn reconstituted tobacoo adhesion cutting blade, after suction, the fever of adhesion heat source are heated in process
Element, cigarette are easily extracted.
The reconstituted tobacoo that do not burn to gained heating carries out suction quality test, according to GB5606.4-2005《Cigarette sense organ skill
Art requirement》Corresponding index Evaluation Method evaluates aromatic style feature etc., altogether to " fragrance " " miscellaneous gas " " the miscellaneous gas of wood "
" irritation " " burning sensation " and " pleasant impression " 6 projects have carried out marking evaluation, and the score range of each project is 0~5 point, test
As a result referring to table 1, wherein, each project score is that (score value is higher, represents corresponding project for the average value of 100 sample datas
Effect of testing and assessing is better, as fragrance score value is higher, represents that aroma effect is better, and miscellaneous gas and xylon gas' score value are higher, represent miscellaneous gas and
The bad breath such as xylon gas is fewer, and irritation and burning sensation score value are higher, represents irritation and burning sensation is lower, the person's of smokeing panel test impression
Better).Test result shows aspiration procedure almost without the miscellaneous gas of wood, and has certain rhodiola root perfume, and substantially non-stimulated
Property and burning sensation, cigarette perfume are enriched soft, and suction quality is preferable.
1 the present embodiment suction quality test result of table
| Sample | Fragrance | Miscellaneous gas | Xylon gas | Irritation | Burning sensation | Pleasant impression | It is total |
| Embodiment 1 | 3.18 | 3.13 | 3.13 | 3.11 | 3.09 | 3.11 | 18.75 |
Embodiment 2
1.1 heat the preparation for the reconstituted tobacoo that do not burn：
Bacillus megaterium and yeast bacteria preparation (10 to raw tobacco material surface sprinkling 0.3%6CFU/mL；Huge gemma
Bacillus：The mass ratio of saccharomycete is 1:1) biological treatment 8h in the thermo-humidistat cabinet of 37 DEG C of temperature and humidity 70%, is subsequently placed in,
Obtain a biological treatment tobacco leaf；With raw tobacco material:Rhodiola root is 90:10 mass ratio is into biological treatment tobacco leaf of gained
Add rhodiola root and mechanical mixture is uniform, obtain mixture；Gained mixture is soaked into water and puies forward (solid-to-liquid ratio 1:8) after,
Extracting solution is concentrated into 36%~38%, obtains condensed cream, then 0.5% complex enzyme formulation (fibre is added into gained condensed cream
The plain enzyme of dimension：Pectase：Protease：The mass ratio of glucolase is 2:1:1:1), the biological treatment 1.5h at 50 DEG C, obtains secondary
Biological treatment tobacco leaf.It is subsequently added into 2.0% modifying agent (chicory extract：Xylose：Glycine：Alanine：The mass ratio of Vc=
0.8:0.5:0.4:0.2:0.1) Maillard reaction 1h, is carried out at 120 DEG C, obtains coating fluid.
The solid mixture of tobacco material (offal and offal) after Xiang Shuiti and rhodiola root be (tobacco material and rhodiola root
Mass ratio is 90:10) 0.30% complex enzyme (cellulase is added in：Pectase：The mass ratio of protease is 1:1:1), exist
50 DEG C of biological treatment 0.5h, obtain enzymatic treatment thing.Gained enzymatic treatment thing is passed through into paper process through high-energy ball milling slurrying, gained slurry
Technique is manufactured paper with pulp, squeezes and dried, and obtains tobacco chip base.
Gained coating fluid is sprayed into tobacco sheet primary surface using coating machine, through oven for drying, obtains reconstituted tobacoo matrix.
By 0.01% cigarette perfume material, 0.01% graphene, 0.05% cationic starch and the propane diols of surplus
(propane diols is 5 with qualities of glycerin ratio with Glycerol solvents:5) it is mixed and stirred for uniformly, obtaining spray coating liquor.Using spray gun by spray coating liquor
Reconstituted tobacoo matrix surface is sprayed to, then is placed in 60 DEG C of baking ovens and dries, obtains heating the reconstituted tobacoo that do not burn.
1.2 measure of merit：
According to embodiment 1 test mode to gained heating do not burn reconstituted tobacoo carry out mechanical property, adhesion performance and
Suction quality is tested, the results show that gained heating is not burnt, the tensile strength of reconstituted tobacoo is 0.43KNm-1, bulk is
2.05cm3·g-1；Do not burn reconstituted tobacoo adhesion cutting blade, after suction, the hair of adhesion heat source are heated in process
Thermal element, cigarette are easily extracted.For suction quality test result referring to table 2, the results show aspiration procedure does not produce the miscellaneous gas of wood substantially
Etc. bad breath, but it is fragrant with certain rhodiola root, and substantially nonirritant and burning sensation, cigarette perfume are enriched soft.
2 the present embodiment suction quality test result of table
| Sample | Fragrance | Miscellaneous gas | Xylon gas | Irritation | Burning sensation | Pleasant impression | It is total |
| Embodiment 2 | 3.21 | 3.14 | 3.15 | 3.12 | 3.11 | 3.10 | 18.83 |
Embodiment 3
1.1 heat the preparation for the reconstituted tobacoo that do not burn：
To the bacillus preparation (10 of raw tobacco material surface sprinkling 0.2%7CFU/mL；Bacillus cercus：Solve starch bud
The mass ratio of spore bacillus is 1:1) biological treatment 8h in the thermo-humidistat cabinet of 37 DEG C of temperature and humidity 70%, is subsequently placed in, is obtained
Biological treatment tobacco leaf；With raw tobacco material:Rhodiola root is 95:5 mass ratio is added into biological treatment tobacco leaf of gained
Simultaneously mechanical mixture is uniform for rhodiola root, obtains mixture；Gained mixture is soaked into water and puies forward (solid-to-liquid ratio 1:8) after, will carry
Take liquid to be concentrated into 36%~38%, obtain condensed cream, then 0.30% complex enzyme formulation (cellulose is added into gained condensed cream
Enzyme：Pectase：The mass ratio of protease is 1:1:1), the biological treatment 1.5h at 50 DEG C, obtains secondary biological treatment tobacco leaf.Connect
The modifying agent (chicory extract of addition 1.5%：Xylose：Glycine：Alanine：Mass ratio=0.4 of Vc:0.6:0.2:
0.2:0.1) Maillard reaction 1h, is carried out at 120 DEG C, obtains coating fluid.
The solid mixture of tobacco material (offal and offal) after Xiang Shuiti and rhodiola root be (tobacco material and rhodiola root
Mass ratio is 95:5) 0.20% complex enzyme (cellulase is added in：Pectase：The mass ratio of protease is 1:0.5:0.5),
In 50 DEG C of biological treatment 0.5h, enzymatic treatment thing is obtained.Gained enzymatic treatment thing is passed through into papermaking through high-energy ball milling slurrying, gained slurry
Method technique is manufactured paper with pulp, squeezes and dried, and obtains tobacco chip base.
Gained coating fluid is sprayed into tobacco sheet primary surface using coating machine, through oven for drying, obtains reconstituted tobacoo matrix.
By 0.01% cigarette perfume material, 0.01% graphene, 0.01% cationic starch and the propane diols of surplus
(propane diols is 5 with qualities of glycerin ratio with Glycerol solvents:5) it is mixed and stirred for uniformly, obtaining spray coating liquor.Using spray gun by spray coating liquor
Reconstituted tobacoo matrix surface is sprayed to, then is placed in 50 DEG C of baking ovens and dries, obtains heating the reconstituted tobacoo that do not burn.
1.2 measure of merit：
According to embodiment 1 test mode to gained heating do not burn reconstituted tobacoo carry out mechanical property, adhesion performance and
Suction quality is tested, the results show that gained heating is not burnt, the tensile strength of reconstituted tobacoo is 0.45KNm-1, bulk is
2.06cm3·g-1；Do not burn reconstituted tobacoo adhesion cutting blade, after suction, the hair of adhesion heat source are heated in process
Thermal element, cigarette are easily extracted.For suction quality test result referring to table 3, the results show aspiration procedure does not produce the miscellaneous gas of wood substantially
Etc. bad breath, but it is fragrant with certain rhodiola root, and substantially nonirritant and burning sensation, cigarette perfume are enriched soft.
3 the present embodiment suction quality test result of table
| Sample | Fragrance | Miscellaneous gas | Xylon gas | Irritation | Burning sensation | Pleasant impression | It is total |
| Embodiment 3 | 3.19 | 3.14 | 3.14 | 3.11 | 3.11 | 3.12 | 18.81 |
Embodiment 4
1.1 heat the preparation for the reconstituted tobacoo that do not burn：
To the complex microorganism preparations (10 of raw tobacco material surface sprinkling 0.2%7CFU/mL；Bacillus cercus：Huge bud
Spore bacillus：The mass ratio of saccharomycete is 1:0.5:1), it is subsequently placed in biology in the thermo-humidistat cabinet of 43 DEG C of temperature and humidity 70%
8h is handled, obtains a biological treatment tobacco leaf；With raw tobacco material:Rhodiola root is 97:3 mass ratio is to biological treatment of gained
Rhodiola root is added in tobacco leaf and mechanical mixture is uniform, obtains mixture；Gained mixture is soaked into water and puies forward (solid-to-liquid ratio 1:
8) after, extracting solution is concentrated into 36%~38%, obtains condensed cream, then 0.35% complex enzyme system is added into gained condensed cream
Agent (cellulase：Pectase：The mass ratio of protease is 2:1:1.5), the biological treatment 1.5h at 50 DEG C, obtains two secondary pollutants
Handle tobacco leaf.It is subsequently added into 1.8% modifying agent (chicory extract：Xylose：Glycine：Alanine：Mass ratio=0.3 of Vc:
0.8:0.4:0.2:0.1) Maillard reaction 1h, is carried out at 90 DEG C, obtains coating fluid.
The solid mixture of tobacco material (offal and offal) after Xiang Shuiti and rhodiola root be (tobacco material and rhodiola root
Mass ratio is 97:3) 0.25% complex enzyme (cellulase is added in：The mass ratio of pectase is 1:1.5), in 50 DEG C of biologies
1h is handled, obtains enzymatic treatment thing.By gained enzymatic treatment thing through high-energy ball milling slurrying, gained slurry manufactured paper with pulp by paper process technique,
Squeezing and drying, obtain tobacco chip base.
Gained coating fluid is sprayed into tobacco sheet primary surface using coating machine, through oven for drying, obtains reconstituted tobacoo matrix.
By 0.01% sootiness Studies of The Aromatic Substances, 0.03% expanded graphite micro mist, 0.02% sodium alginate and the third of surplus
(propane diols is 4 with qualities of glycerin ratio to glycol with Glycerol solvents:6) it is mixed and stirred for uniformly, obtaining spray coating liquor.It will be sprayed using spray gun
Masking liquid sprays to reconstituted tobacoo matrix surface, then is placed in 70 DEG C of baking ovens and dries, and obtains reconstituted tobacoo.
1.2 measure of merit：
According to embodiment 1 test mode to gained heating do not burn reconstituted tobacoo carry out mechanical property, adhesion performance and
Suction quality is tested, the results show that gained heating is not burnt, the tensile strength of reconstituted tobacoo is 0.43KNm-1, bulk is
2.08cm3·g-1；Do not burn reconstituted tobacoo adhesion cutting blade, after suction, the hair of adhesion heat source are heated in process
Thermal element, cigarette are easily extracted.For suction quality test result referring to table 4, the results show aspiration procedure essentially eliminates the miscellaneous gas of wood
Etc. bad breath, but it is fragrant with certain rhodiola root, and substantially nonirritant and burning sensation, cigarette perfume are enriched soft.
4 the present embodiment suction quality test result of table
| Sample | Fragrance | Miscellaneous gas | Xylon gas | Irritation | Burning sensation | Pleasant impression | It is total |
| Embodiment 4 | 3.21 | 3.15 | 3.15 | 3.12 | 3.11 | 3.12 | 18.94 |
Embodiment 5
1.1 heat the preparation for the reconstituted tobacoo that do not burn：
To the complex microorganism preparations (10 of raw tobacco material surface sprinkling 0.25%7CFU/mL；Bacillus cercus：Xie Dian
The mass ratio of afnyloliquefaciens is 1:1.5), it is subsequently placed in biological treatment in the thermo-humidistat cabinet of 40 DEG C of temperature and humidity 70%
8h, obtains a biological treatment tobacco leaf；With raw tobacco material:Rhodiola root is 96:4 mass ratio is to biological treatment tobacco leaf of gained
Simultaneously mechanical mixture is uniform for middle addition rhodiola root, obtains mixture；Gained mixture is soaked into water and puies forward (solid-to-liquid ratio 1:8)
Afterwards, extracting solution is concentrated into 36%~38%, obtains condensed cream, then 0.2% complex enzyme formulation is added into gained condensed cream
(cellulase：The mass ratio of pectase is 1:1), the biological treatment 1.5h at 50 DEG C, obtains secondary biological treatment tobacco leaf.Then
Add 1.7% modifying agent (chicory extract：Xylose：Glycine：Alanine：Mass ratio=0.5 of Vc:0.7:0.2:0.2:
0.1) Maillard reaction 1h, is carried out at 110 DEG C, obtains coating fluid.
The solid mixture of tobacco material (offal and offal) after Xiang Shuiti and rhodiola root be (tobacco material and rhodiola root
Mass ratio is 96:4) 0.25% complex enzyme (cellulase is added in：Pectase：The mass ratio of protease is 1:1:0.5), exist
50 DEG C of biological treatment 0.5h, obtain enzymatic treatment thing.Gained enzymatic treatment thing is passed through into paper process through high-energy ball milling slurrying, gained slurry
Technique is manufactured paper with pulp, squeezes and dried, and obtains tobacco chip base.
Gained coating fluid is sprayed into tobacco sheet primary surface using coating machine, through oven for drying, obtains reconstituted tobacoo matrix.
By 0.01% sootiness Studies of The Aromatic Substances, 0.02% mesoporous carbon spheres, the third the two of 0.01% cationic starch and surplus
(propane diols is 5 with qualities of glycerin ratio to alcohol with Glycerol solvents:5) it is mixed and stirred for uniformly, obtaining spray coating liquor.It will be sprayed using spray gun
Liquid sprays to reconstituted tobacoo matrix surface, then is placed in 65 DEG C of baking ovens and dries, and obtains heating the reconstituted tobacoo that do not burn.
1.2 measure of merit：
According to embodiment 1 test mode to gained heating do not burn reconstituted tobacoo carry out mechanical property, adhesion performance and
Suction quality is tested, the results show that gained heating is not burnt, the tensile strength of reconstituted tobacoo is 0.45KNm-1, bulk is
2.09cm3·g-1；Do not burn reconstituted tobacoo adhesion cutting blade, after suction, the hair of adhesion heat source are heated in process
Thermal element, cigarette are easily extracted.For suction quality test result referring to table 5, the results show aspiration procedure essentially eliminates the miscellaneous gas of wood
Etc. bad breath, but it is fragrant with certain rhodiola root, and substantially nonirritant and burning sensation, cigarette perfume are enriched soft.
5 the present embodiment suction quality test result of table
| Sample | Fragrance | Miscellaneous gas | Xylon gas | Irritation | Burning sensation | Pleasant impression | It is total |
| Embodiment 5 | 3.22 | 3.15 | 3.14 | 3.12 | 3.12 | 3.12 | 18.87 |
The heating produced by the present invention reconstituted tobacoo that do not burn has the excellent anti-tensile strong it can be seen from above test result
Degree, heating with commercially available dry process not combustion shim (tensile strength≤0.15KNm-1) compare, mechanical property carries significantly
Height, bulk are also obviously improved；And also overcome the defects of its adhesion is serious；In addition, it is bad to essentially eliminate the miscellaneous gas of wood etc.
Breath, has certain rhodiola root fragrance, and substantially nonirritant and burning sensation, cigarette perfume are enriched soft.
Specific case used herein is set forth the principle of the present invention and embodiment, and above example is said
It is bright to be only intended to help the method and its core concept for understanding the present invention, including best mode, and also so that this area is appointed
What technical staff can put into practice the present invention, including manufacture and using any device or system, and implement the method for any combination.
It should be pointed out that for those skilled in the art, without departing from the principle of the present invention, can also be right
The present invention carries out some improvement and modification, these are improved and modification is also fallen into the protection domain of the claims in the present invention.This hair
The scope of bright patent protection is defined by the claims, and may include those skilled in the art it is conceivable that other implementation
Example.If these other embodiments, which have, is similar to the structural element of claim character express, or if they include with
Equivalent structural elements of the character express of claim without essence difference, then these other embodiments should also be included in right will
In the range of asking.
Claims (10)
1. a kind of preparation method for heating the reconstituted tobacoo that do not burn, it is characterised in that comprise the following steps：
A) tobacco leaf is subjected to biological treatment under microbial action, obtains a biological treatment tobacco leaf；
The microorganism includes bacillus and/or saccharomycete；
B) a biological treatment tobacco leaf is mixed with rhodiola root, obtains mixture；
C) after mixture progress water being carried and concentrated, add complex enzyme formulation and carry out biological treatment, obtain at two secondary pollutants
Manage concentrate；
The complex enzyme formulation includes two or more in cellulase, pectase, protease and glucolase；
D) the secondary biological treatment concentrate is mixed with modifying agent and carries out Maillard reaction, obtain coating medium；
E) coating medium is coated on tobacco sheet primary surface and drying, obtains heating the reconstituted tobacoo that do not burn.
2. preparation method according to claim 1, it is characterised in that in the step a), biological treatment is in constant temperature and humidity
Under the conditions of carry out, temperature be 37~45 DEG C, humidity be 70%~80%；The time of biological treatment is 6~8h.
3. preparation method according to claim 1, it is characterised in that the tobacco leaf in step a) and the rhodiola root in step b)
Mass ratio be 99: 1~90: 10；
In the step c), the quality of the complex enzyme formulation is the 0.2%~0.5% of concentration gained condensed cream.
4. preparation method according to claim 1, it is characterised in that in the step d), modifying agent includes natural extraction
One or more in thing, carbohydrate, amino acid and vitamin C.
5. preparation method according to claim 4, it is characterised in that the natural extract includes chicory extract；
The carbohydrate includes xylose；
The amino acid includes glycine and/or alanine.
6. the preparation method according to claim 1 or 4, it is characterised in that in the step d), the temperature of Maillard reaction
For 80~120 DEG C, the time is 1~1.5h.
7. preparation method according to claim 1, it is characterised in that in the step e), the tobacco chip base by with
Under type obtains：
S1 the mixture of tobacco material and rhodiola root) is subjected to enzymatic treatment under compound enzyme effect, obtains enzymatic treatment thing；
The tobacco material includes the one or more in offal, offal, tobacco leaf and pipe tobacco；
S2) handled the enzymatic treatment thing slurrying and by paper process, obtain tobacco chip base.
8. preparation method according to claim 1, it is characterised in that the step e) includes：
E1) coating medium is coated in tobacco chip base and dried, obtains reconstituted tobacoo matrix；
E2 spray coating liquor and drying) are coated with to the reconstituted tobacoo matrix surface, obtains heating the reconstituted tobacoo that do not burn；
The spray coating liquor includes cigarette perfume material, adhesive, high molecular material and solvent.
9. preparation method according to claim 8, it is characterised in that the adhesive includes expanded graphite micro mist, stone
One or more in black alkene and mesoporous carbon spheres；
The high molecular material includes sodium alginate and/or cationic starch；
Champignon material of the cigarette perfume material obtained by destructive distillation offal；
The solvent includes propane diols and/or glycerine.
The reconstituted tobacoo 10. one kind heating is not burnt, it is characterised in that by preparation method according to any one of claims 1 to 9
It is made.
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| CN112955030A (en) * | 2018-07-31 | 2021-06-11 | 尼科创业贸易有限公司 | Aerosol generation |
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| CN106235375A (en) * | 2016-08-30 | 2016-12-21 | 湖北中烟工业有限责任公司 | A kind of method of the suncured tabacco reconstituted tobacco manufacturing applicable flue-cured tobacco local flavor |
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| CN102283434A (en) * | 2010-06-18 | 2011-12-21 | 福建中烟工业公司 | Preparation method of morinda officinalis regenerated thin tablet and application of morinda officinalis regenerated thin tablet prepared by the preparation method in tobacco product |
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